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Setyawan Synthesis + Sembering
Setyawan Synthesis + Sembering
hydrothermal process works well for producing zeolite, specifically zeolite-Y from rice
husk silica (Pangesti et. al. 2021). On the other hand, the present study used the sol-gel
The study of Setyawan et, al (2021) is similar to the current study conducted since
they also synthesize silica but differ in the raw materials used where this study used rice
husk while the present study used lemongrass. This study used XRF to identify the
chemical compositions and purity of silica powders produced from the rice husk, XRD to
determine the pattern of silica powders produce from various concentrarion of KOH, and
SEM or Scanning Electron Microscopy to depict morphology of the nano-silica while the
present study did not used these test. Also, they used varying KOH solution for silica
extraction 7, 10, 13 which is also used in the present study and also the extraction time
90, 120 150 mins were also the same. Meanwhile, the gel drying temperature considered
by this study is 110°C while the present study considered 100°C, 110°C, and 120°C.
The study of Firdaus et al. (2017) is also similar to the current study being
conducted since it also used lemongrass (Cymbopogon citratus) in producing pure silica
whereas the current study also used lemongrass (Cymbopogon citratus) as the raw
materials in producing silica. The results of this study shows that it is really possible to
extract silica from lemongrass and synthesize it to improve the amount of silica that can
be produce. The methods utilized in the study were different to the current study since
the study of Firdaus et al. (2017) used hydrochloric acid leaching and thermal burning
while the current study utilized alkali extraction method and sol-gel method.
The study of Sembiring et al. (2014) is similar to the current study because both
study uses alkali extraction method to extract silica for the sol process of sol-gel method.
The sol-gel method is recognized as the most appealing since it allows for good mixing
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to ensure that the beginning elements are consistent, as a result of which the distribution
of components at the to create monophasic gels at the atomic level. There is a difference
between the two is the raw materials utilized and the laboratory test conducted. Also, the
study of Sembering et. al consider only 110°C as the temperature for oven drying the gel
temperature while the present study considered 100°C, 110°C, and 120°C.
The study of Bera, J. and Nayak, J.P. (2011) and the present study is similar in
terms of the intended output which is to produce a color indicating silica gel. The findings
of this work are applicable to the development of low-cost, high-efficiency silica desiccant
with better safety due to its low cobalt level. One of the differences between this study
and the present study is that this study utilized rice husk ash as its raw materials and
sodium silicate extraction and acid neutralization method for silica extraction and silica
synthesizing while the present study uses lemongrass as its raw material and alkali
extraction method for silica extraction and sol-gel method for synthesizing the extracted
silica from lemongrass. Another is the color indicator for silica gel, the study of Bera and
Nayak utilize cobalt chloride while the present study used methyl violet. Also, this study
used pH 2, 4, 6, 8, and 10 of cobalt chloride while the present study only considered pH
4, 6, and 8 for methyl violet. Moreover, it also indicates that pH 6 gel has the most notable
blue to pink color change behavior in 6 days. Meanwhile the present study considered
impregnation time of 4, 6, and 8 days. They use 150°C as their envirogel drying
temperature while the present study consider 100°C ,110°C, and 120°C. Lastly, the study
of Bera and Nayak do not consider envirogel drying time since they let it dry until the
weight is contant.
For a better understanding of this research, the associated literature cited above
relied on earlier investigations. Although the study shared certain raw materials,
methodologies, and ideas with the previous studies, it cannot be regarded as a duplicate
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because it aims to enhance and determine the optimal method to increase the silica
information in developing the best-suited solution methodology and procedure design for