Date 1-8"2

Expt. No. Page No.

ExXPERIMENI
-AIM: Je anauya theqnen satt and ;ind ot
ait
acidie and Lbaie Laclical
APPARATIUS: Jst thbes
-CHEMICALS USED: Guçen aalt, dil H, S0,Conc H,S0,4
lisme aatin, aoH, Nessl?
iageit
IEST FOR AcIDIC RADICAL :
EXPERIMENT OBSERVATION NEERENCE
PAETMINARY TEST:
Take ainc Bzisk PiLit Cdil)
Lgwen Aat ina etheecena
at tulse an adel co maybicoiatain,
dilu,0, to it

2CoNEIRMATORYEST:
Pass. iksesoted qas Hime ater co-Carbonateion)
etauqh the lime
tiane

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 "REACIION FoR AcIDIC RADICAL
2 Co+ Ha504So + HaQ + Co.
2, Coa + Ca loH)2Caco3t Ha0
(Lime weter) white
B. Cost +HqSot
(white prty
 "REACIION FOR. BASTC RADICAL I
>Nct t NH4OH
1, NH+ NaOH
’NH3 + H2O
2. NH4OH
NH4Clt H*
3. NH4 t HC (cdende ehite fome)A
NaOHHaNHO.HqT
4. (Nesselers NH4 +
2KaHç Iu tReaqent)NaI+ 2Hjo
Qadloich Bronn

PHYSICAL EXAMINATON
L. CoLOUR hite (colourless)
2. TEXTURE Cauystelline
3. OpOUR ’ imnical
4 SoLUBILTTY-’ Wats dslulsle
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.FOR BASIC RADICAL :

4EXPERIMENT IOBSERVATON INFERENCE
PATLTMINARY EST:
Take a hinch af etion aqad
ith sacll tueaet.
nakáctt
,dde
seuitina cMmoniana
andaconc. NaOH to thiu,(Punqtdmell).

ONETRMATORY EST:
Take salt sstro Racldih Bzon NHI i conti
Amed

eagent
RESULT:
Acidie nadical lanieu) > co?
Bauic adical Ciactien) > NHt
qirew salt dAnamaniLAa Canlaate

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 REACTTON For AcTDTc RADICAL:
(27. cHcoOH+ C,oH
9. CH,GO+ Fe

FeCkgA,O0)t 3c
 Dates2024.
Expt. No, Page No.

E XPERIMEN-2
ATM: J Jind he aidand basic nadicaL
in the qinen satt
APPARATUS : Jost tube
CHEMICALS enn dalt,il H6o concH,SO
NabH,ilHCe, KI, K,c0Fecg

PAYSICAL EXAMINATTON:
-FoR. AeTD RAbICAL
EXPERIMENILAOB5ERVAhoNNEERENCE
Take Aalt inmttNo clseualle
tue and adal change abtnt

2.Tak Aaltin a
dec tet tube adgaà ith ine-esLaat ma
add 2- mlig conc. H,so.qn ike dnalle

3.akeaseanti hubu
and dat caucH,Sot
+ Amell
CHSOO Coliaccl.
tehalehel auc
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 "REACITON FOR, BASIc BADICAL :
4). PL2+
pb +2HCL ’ PbcL +2H
whiti ppt.itsA
(27. PbCl, t 2KI ’ PbI,+ 2kce
3).. Pbcl, t Kyyo pbCxotakclA
yellow

PHYSTCAL EXAMINATON:
4. JEXTuRE >Gustallin
o CoLOUR. white
3" ODoUR.
4. Vinge
50LUBILITY’het liku
seba
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Expt. No. Page No.

4.dake dat intut Laddish CH,co0

tale adacldFecd, CeLouL conimad.
LalHeat the eotust

FOR. BASTC KADICAL

EXPERIMENT 1OBSEVATTON LNFERENCE
1.Take salt sel andNa cobaeunle 2e0
add NaÔH.
chamg
2..Tak salt sctn andlAwthite bbt ia
dil H to it. otteineel
aclo ynnntat
3.Eit abnept and
diiiee itto z uhata
LAcc KI 5ol Yellew bpt is
ottaind
pconitnad..
"Add Kk,CuO hight ylew pjst pk conlnicl.
ietteined'

"Addil H,0 hide ppt obtainsd PEconind.

RESULT Audic 9uadicalanion)

BaLsic aclical(Catian)
CH_COO
ph2
Guen alt i ead acttte.
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 - REACTION FOR ACTDIC RADICAL
2
S04 +Bacly Baso, (s) t2ce
te. ppt
 Date
141ol202)
Expt. No. 37 Page No.

ENXPERIMENI
AIM: T <ind the acicl and oaaie adical
nhe qwenAatt.
APPARATUS: Teat tubea, qinen satt
"CHEMICALS : Gúxen salt ,dil H,s0. concH,so,
Fe So Na,s, dil HNO,, NH,OH
PHYSICAL ExAMINATION -
FOR ACTID RADICAL
EXPERIMENT OBSERVATION NEERENCE
A. Take qien salt No obAWalleL
im ta} tubeand
Ladd d H,soto it change alsent

2
2: Tak gwen satt in No ebseunle
tat- tulse and ald albet
chamge

inTae
Taks aiven. salti e Aohite
and add Bacly solutian oecihitat
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 " BEACIIONS FOR BASIC RADICAL

Cu2t + HaS
Blcuck Caqy
3CuScs)+ BHN03 CcL4)3culNos) 4Ho(p t3S )
BlLeishqen
CuCNo),t YNH,0H’ u(NHs)Tt t0
2cuzt K LFe
Deep blue
(NOt
(c)elCulfe t c +
Hao TKOH
checelcte colour
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FOR BASIC RADICAL

-xPERIMENI OBSEVATLON NEERENCE
1-Take quen salt No oAe7walsle
in tiat tuleand alsent.
acldcne. NaOH.
chamqe

2.Take giuen salt No ol80Ualole TSt

and addcil HCL alt
to it chang

3-To balt iolticn Blacko nshite

heant.

4. Risseuse black ppt

in dilHNO, and
diiele
two
delictiea
iato 2hat
A.
ddd NH,oH daelight Jolue ppt Qtconizmed
arhecA and
dissered is
in ecess
NHDH 4ing
deeolee
alitien
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 "PAYSICAL EXAMINATION
A7. TEXTURE - Cystalline
<2 CoLOUR
Coloulea
47. SoLUAILITY- wctu elubte
 Date

Expt. No Page No. 7

Cut2
Chotolati colon ct2
B.Addl CH,COOH o
altwe ole -PptJemecl. Conirmecl
Selutie, the
add hottassuLm.
Jeeryanicle.

BESULT- The qiren salt contoins

Actdlic adical- ScCGulphate îrind)
Baaic adical - Cu|Ccepb
uzCCapk ima)

Teacher's Signature
REACTION FOR ACTD RADICAL :
’BaGo, t 2ce
 Dato_14]]2)
Expt. No. Page No.

ExXPERIMENT
AIM: o nd theL acicl ancl basie adical ine.
glen adalt.
-AreARATUS: Test tube
-CHEMICALS: Gçuen dalt, Na,s NaOH , ilH,Soç
conc. HsOz HNO,, Bacl,,NH
OH, NHcl,KEeCCNDe KeNS
PHYSICAL EXAMINATIoN:
4.TextLe Gystalie
2. CeeL Gueenish yello
3. doUL
Qdubility iaitin soluble
-FoR ACID BADICAL
EXPERIMENI JBSERVATION INERENCE

lake qwen salt in No obAervable lil

test tuleand add abucnt
dil Hso, do t chag
tTake qien sntt in Nlo gbscvelelectinc. qst
t cne. HeSOu toit. chang Teacher's Signature
-REACTION FoR BASIC RADIÇAL :
Fe+ 30H Fe (o),
Fe(oH), t 3HC
(Radclish Byawn)
Fe Chg t 3,0
FeClt K, TFeCcN)l’ KEe LFe Cc;]+ 3ku
Fe Cig
 Date

Expt. No. Page No.

Lakegiuen dalt Lshite precipitate so

conjimad
add Back, sol to it.
-FoR. BASIC RADICAL
XPERIMENI OBSERVATION NEERENCE

1-Taki salt amd add.

LAntand NaD!! to claang alt

2.To abte aonade olbsevableizst

dil HC abicat
chaug
no cerVable
chang alient

To aboe Ael Ldd Reddish brbwn Tairdl galp

NHCI and N,OHppt omecl pacient (uaghe Fe
6.Disolve alsve pht in
alil Hce bciiele it

To ist hat acd set? conied

|Kute (enh4 fomee

To Accond, hant accl| Red ppt -bumscl retfimecl

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 Date
Expt. No. 4
Page No.

RESULT:
cleidie Gadical Canion) Go
Bauic Roudical Ccatio) e+2
iven alt uFesou

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 Date 1lele1
Expt. No, Page No.

ExXPERIMENI
AIM: analyeacicic and oaaie sadical in the
quen aatt.
APFARATUS: attube, bako, dsckpilbt, chanicala
-PEYSICAL FAMINATTON&
GFOR ACID RADICAL
FXPERTMENI OBSERVATTON NEERENCE
ak Almall aMguít No change dil qeip
aat md add
dil H,So to it
a.stako att ad add No chang
Coc, H,s0, to it alient

3.lakc att amd White ppt isota

add ti and
add Batl Conc, HCe

FOR BASTC RADICAL

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 Date

Page No. |2.

Expt.No.

ExPERIMENI OBSERVAILON NEERENE

Jake watt soution hlo chanq. zeD qAoL

Land dcl NaoH alodet
to it.
2abave delettion No change
Ladalil HcL. CLlelent

3 o abtve ieuttna IThd

Nochang
4odo abe selttion nshite qlatinmu
Lada NHeamd
NH,OH
hoeset,mat
be At3

5-isele
5.
alve ppt
amc duice it in
tuoo hatta

ahite glatinausats
escUsis, hem NHcl
Lamdtil

iád Iitan Aclu- |Blue ppt, loccts Afotexent

celutiou

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 Date

Expt.No. Page No. |3

RESULT -

Acidic Radlical -2
Sa

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Expt. No. 02 A Date :13/oa|23
Page No. 5

ExleRLMENT- o2
Aien
T6 prxpaxe M oxal. oc?d Solution
Prinei pal
hicn known Concentraion 's pepaud
Theoxy
Oxafc acid s a psimaxy standbsd 5 oethex
deliauescent hox elloreScent oRa ccid does not
aletampose on expoSuxe to ht
Stoble Solotn.

Caystbl hauing amula CqoH

CoOH
2420
The moleculay mass of oxallc ac s 1n6 & has base
dityas 2 due to presence of tuo yeplocable mo
Rons to pzepare M oxalic acid salohon txel26oof salutn
Oxale aclds to be d'ssolved per
So to pse porse 25o MI M
of oxali
Oxalic ocd saloton 12:6 =3-I5 gm of oxalßc acid

Bs xequred

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 Expt. No. Date:
Page No.: 6

MATENials Reqvico
Appasatus
box
eqinedioatch a5s Chomicol balanse oeiaht
wash battle. , fonnel

Chemicals eqúined :- Oxali'e acid & d'silcd uoater

Paoceduxe
4 Hake awotch ghss d'skled
Clean t psopesly with diskled water
& then
2 the clean doy watch alass Chemical
balance & xeco t's tne noste booh.

3.
3Loe'ah 315 gm Oxalc acd on tae watch Alass ecoxd
Weight Pn the note boo k
Tansfes oxalie acd to a clean bcoakes Caxefully wash
the watch glass wsn os fled watex to ensuse. Ol|

he Caystals Gtcking to tae oatch a6e transfened

the Ovd of dSRLed wates fos tis pus pose Shold not
be more than 5o ML

5 Toanstes ne enfre Soln faom tne baker into meaiuzing

Flask 25om
50 withn toe heln ote tunnel wash the
beakex iHa distled water transfer tae
Unto 4ask

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 Date
Expt. No.
Page No. : +

Jtoash funnel Sevesal Rncl woth oticd twater to trosfer

tne Stickingpatdleeento mmeosoaing lask wle
the fonnels adol water in Small Amts that
OShould not be. mooe than Eo M)

)Anally wash khe funnel Loith dlstled wates

5o tht no oxalic actd Solution to the tunnel
8)Add enaugh disllied toates to the measusing aFlask Covekully
up to AuSt below the etched
Just mask
9)Suwisl tae FniSh fuu Sold oxale Ad a'ssalved
19) The Final addiion o wsts mult be csop w'se the lauoex
leuel ot tne memiscuS touchel the mosk on the measusing
Flask

) Stappe Lne
the Flask & Shake
Shoahe . to make up the
Uilom tsognouk label t as bwo
Oxalic ad saln
lo

Precautions
1weghing of bhe oralic ocid Cystal Shayld be accuxate
2- he of tne
done
3-he lower meniscos Should be on the mark
9lalt few daops of d'sued water Should odded
using a pipete or doppen.
Teacher's Signature: