£>.no.

L\3'l-

ACG ASSOCIATED CAPSULES PVT. LTD.

CERTIFICATE OF ANALYSIS

Format No : FT-QAL-05

Material Code : rmgrgbro2

Qty Received : 5,000.000 kg
Qty. Sampled : 1.001 kg
Sampled By : ppp
Manufacturer: RAMA INDUSTRIES LIMITED
Supplied By : RAMA INDUSTRIES LIMITED

SLNO
1
2
3
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5
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8
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10
11
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13
14
15
16
17
18
19
20
21
22
23

CERTIFICATE OF ANALYSIS

Lot No : 010000839475

24
25
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30
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40
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42
43
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48
49
50
51
52
53
54
55
56
* Values taken based on reduced test monitoring programme.
Disposition : The batch tested conforms to the prescribed release specification. STATUS OF THE MATERIAL : APPROVED r j»L. AN

JfwcUt&fyieA a£mu/ecl
—-------V

WORKS : VILL. CHAUNDHERI,

P.O. DAPPAR, TEH. DERABASSI,

AMBALA-CHANDIGARH HIGHWAY, NEAR LALRU

DISTT. MOHALI-140 506, PUNJAB, INDIA

CIN : U24110MH1987PLC043127

PHONE : 01762-248810-12
Fax : 01762-248761

E-mail : rama.gelatine@ramagroup.co.in

Website : www.ramagelatine.com

Iff Q1 lolCE!

Corporate Office : 51/52, Free Press House, 215, Nariman Point, Mumbai - 400 021, Maharashtra, India
Ph.: 022-2283-3355/2283-4126 Fax : 022-2204-9946 E-mail: rama@ramagroup.co.in
Regd. Office : 812, Raheja Chambers, Nariman Point, Mumbai -400 021, Maharashtra, India

0lrmta Jfnda&foceA <&nu/ed

-—-“ \

WORKS : VILL. CHAUNDHERI,

P.O. DAPPAR, TEH. DERABASSI,

AMBALA-CHANDIGARH HIGHWAY, NEAR LALRU

DISTT. MOHALI-140 506, PUNJAB, INDIA

CIN : U24110MH1987PLC043127

PHONE : 01762-248810-12

Fax : 01762-248761

E-mail : rama.gelatine@ramagroup.co.in

Website : www.ramagelatine.com

Customer
Customer D.O. No.
Quantity
Grade
Report No.

Physical & Chemical Parameters

1
W (? Qu. In l CER

Corporate Office : 51/52, Free Press House, 215, Nariman Point, Mumbai - 400 021, Maharashtra, India
Ph.: 022-2283-3355/2283-4126 Fax:022-2204-9946 E-mail: rama@ramagroup.co.in
Regd. Office : 812, Raheja Chambers, Nariman Point, Mumbai - 400 021, Maharashtra, India
PVT. LTD.

Material Name : GELATIN I.P. (RAMA), 210 BLOOM

Date of Sampling : 21.05.2020
Date of Analysis : 26.05.2020
Date Of Report : 26.05.2020
Reassesment Date : 20.05.2021
GR No: 5012844806 GR Date: 20.05.2020

TEST
DESCRIPTION
SOLUBILITY IN COLD WATER
WATER ABSORPTION & SWELLING
SOLUBILITY-HOT WATER
SOLUBILITY -6N ACETIC ACID*
SOLUBILITY-HOT GLYCERIN&WATER*
SOLUBILITY-ALCOHOL
SOLUBILITY-ETHER
SOLUBILITY-CHLOROFORM
SOLUBILITY-VOLATILE OILS*
IDENTIFICATION CUS04
IDENTIFICATION GELLING PROPERTY
APPEARANCE OF SOLUTION
PH OF 1% W/VSOL.
ARSENIC*
HEAVY METALS(NMT 20 PPM)*
SULPHUR DIOXIDE
ASH
LOSS ON DRYING
ODOR & WATER INSOLUBLE SUBSTANCES*
BLOOM STH OF 6.67% GL.SOL.
BLACK PARTICLES*
VISCOSITY (6.67 % SOLN)

>/o LOSS IN VISCOSITY

FRANSMITTANCE (6.67%SOL M 510NM)
PARTICLE SIZE (ABOVE 4 MESH)*
PARTICLE SIZE (BETWEEN 4 & 22 MESH)*
PARTICLE SIZE (BETWEEN 22&30 MESH)*
PARTICLE SIZE (BELOW 30 MESH)*
 HYDROGEN PEROXIDE
KEEPING QUALITY
ISOELECTRIC PH
CONDUCTIVITY
PHENOLIC PRESERVATIVE*
GREASE CONTENT*
IRON*
CHROMIUM*
ZINC*
MERCURY*
NITRATE*
TOTAL MICROBIAL COUNT
E.COLI
SALMONELLA
S.AUREUS
PSEUDOMONAS
SHIGELLA
GELLIQUIFYING ORGANISMS
THERMOPHILIC SPORES*
ANAEROBIC BACTERIA
TOTAL YEAST & MOLD COUNT
ENTEROBACTERIACEAE
COLIFORMS
CLOSTRIDIUM
BILE TOLERANT GRAM NEGATIVE BACTERIA
LEAD*
CADMIUM*
rogramme.
o the prescribed release specification. STATUS OF THE MATERIAL : APPROVED r j»L. ANALYSED BY . CHECKED BY rffiT' „ , APPROVED BY of1
 QualityAssurance (Department
Certificate ofjZnaCysis ( QeCatin ID)
Customer
Customer D.0. No.
Quantity
Grade
Report No.
Physical & Chemical Parameters
S. No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16

19 TAT IT1
20''
C 11 • 1

e, 215, Nariman Point, Mumbai - 400 021, Maharashtra, India

204-9946 E-mail: rama@ramagroup.co.in
man Point, Mumbai -400 021, Maharashtra, India
QuaCity Assurance (Department
Certificate of flnaCysis (QeCatin IP)
M/s ACG Associated Capsules Pvt. Ltd., Shirwai.
RIM/HO/107 dt 16.05.2020
100x 50 kg = 5.000 M.T.
210 + Bloom
3622

S.No.
22
23
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27
28
29
Microb
1
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5
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 13
UJTY riFIEMna _/S7

e, 215, Nariman Point, Mumbai - 400 021, Maharashtra, India

4-9946 E-mail: rama@ramagroup.co.in
man Point, Mumbai - 400 021, Maharashtra, India
Batch No : 1120114400 Vendor Batch : B-2551
Mfg. Date : 01.05.2020
Exp. Date : 30.04.2025
AR NO.: 010000839475
Specific No.: SP-QAL-^IP+USP+PH^UR+BS+ACG)
COA of Supplier: Yes / No

METHOD SPECIFICATIONS
SOPQAL03 Lt amber/ ft yellow granules,charac odor
Insoluble in cold H20 but swells &soften
Should absorb 5-10 times its weight
v
Soluble in hot water
Soluble in 6N acetic acid
Soluble in hot mixture of glycerin & H20
Insoluble in alcohol
Insoluble in ether
Insoluble in chloroform
Insoluble in volatile oils
Violet colour is produced
Contents will not immediately flow out
Soln compares with std OS4 & YS4
5.00-6.00
NMT O.IOppm
NMT 0.5 ppm
NMT 40.00ppm
NMT 2.00% w/w
9.00% w/w -12.50% w/w
Free from foul/disagreeable odor
197.OOg - 230.OOg
NMT 20.00NO.
40.00MilliPoise -50.00MilliPoise

NMT 18.00%
NLT 82.00%
NMT 0.50% w/w
NLT 95.00% w/w
NMT 5.00% w/w
NMT 1.00% w/w
 NMT 10.00ppm
No turbidity, foul, fishy odor & liquefy
4.70-5.20
NMT 1.00mSiemen/cm
Not detected/g
NMT 0.15% w/w
NMT 30.00ppm
NMT 2.00ppm
NMT 30.00ppm
NMT O.IOppm
NMT 100.00ppm
NMT 50.00cfu
Absent in 1g
Absent in 10g
Absent in 1 g
Absent in 1g
Absent in 10g
NMT 50.00cfu
NMT O.OOcfu
NMT O.OOcfu
NMT 50.00cfu
Absent in 10g
Absent in 10g
Absent in 1g
Absent in 1 g
NMT 0.5 ppm
Maximum 0.5 ppm

ROVED r j»L. ANALYSED BY . CHECKED BY rffiT' „ , APPROVED BY of1 ^ ^ Name: Designation: c Date: c
 m/s ACG Associated Capsules Pvt. Ltd., Shirwal.
RIM/HO/107 dt 16.05.2020
100x 50 kg = 5.000 M.T.
210 + Bloom
3622

Parameters
Description
Solubility
Identification
Appearance of Solution
pH of 1% solution at 25°C
Arsenic
Lead
Sulphur Di-Oxide(Titration)
Residue on ignition
Loss on drying at105°C
Odor & water insoluble substances
Bloom strength (6.67%) w/v solution.
Black Particles
Viscosity of 6.67% w/v solution! at 60°C)
Viscosity Drop
Transmittance at 510 nm
Particle Size BSS (-4+22)
Hydrogen Peroxide
\r\[
Keeping quality at 37°C /
Isa eletric pH at 25°C
Conductivity 1% Solution at mwo°c
Date 16.05.2020
Batch No. B-2551
Mfg. Date May - 2020
Exp. Date Apr - 2025
Page 2 of 2

Parameters
Phenolic Preservatives
Grease Content
Iron
Chromium
Zinc
Mercury
Nitrate
Cadmium
iological Parameters
Total bacterial counts
Presence of E.coli
Salmonella
Pseudomonas
Staphylococcus aurous
Geiatin Liquefying Organisms
Thermophilic bacteria
Coliform organisms
Total yeast & Mould
Fntern
)acteriaceae
 )acteriaceae
Anaerc bic Bacteria
Clostri ium
Shigel
Pr jj Sst(Q.C)
RESULTS
GRANULE, LT AMBER TO FT.YELLOW.CHAR ODOR
INSOLUBLE IN COLD H20 BUT SWELLS &SOFTEN
ABSORBS 5-10TIMES ITS WEIGHT
SOLUBLE
SOLUBLE
SOLUBLE
INSOLUBLE
INSOLUBLE
INSOLUBLE
INSOLUBLE
VIOLET COLOUR
CONTENT DO NOT IMMEDIATELY FLOW OUT
COMPLIES
5.49
NMT 0.10 ppm
COMPLIES
22.04 ppm
0.50 % w/w
10.96 % w/w
FREE FROM FOUL/DISAGREEABLE ODOR
215.29 g
NMT 20.00 No.
43.06 MilliPoise

16.17 %
92.44 %
NMT 0.50 % w/w
NLT 95.00 % w/w
NMT 5.00 % w/w
NMT 1.00% w/w
 NMT 10.00 ppm
NOTURBIDITY,FOUL/FISHYO DOR.LIQUEFACTN
4.94
0.14 mSiemen/cm
ABSENT
NMT 0.15% w/w
NMT 30.00 ppm
NMT 2.00 ppm
NMT 30.00 ppm
NMT 0.10 ppm
NMT 100.00 ppm
NMT 50.00 cfu
ABSENT IN 1 GM
ABSENT IN 10 GMS
ABSENT IN 1 GM
ABSENT IN 1 GM
ABSENT IN 10 GMS
10.00 cfu
NMT 0.00 cfu
NMT 0.00 cfu
NMT 10.00 cfu
ABSENT IN 10 GMS
ABSENT IN 10 GMS
ABSENT IN 1 GM
ABSENT IN 1 GM
COMPLIES
Complies

on: c Date: c
es Pvt. Ltd., Shirwal. Date
Batch No.
Mfg. Date
Exp. Date
Page

Units Standard Methods Specification

- IP Passes
- IP Passes
- IP Passes
- IP Passes
- IP 5.0 to 6.0
ppm IP 0.1(Max.)
ppm IP 0.5(Max.)
ppm IHS 40(Max.)
% IP 1.0 (Max.)
% IP 9.0 to 12.5
- IHS No foreign particle & disagrreable odor
gms IP 205-230 (Corrected to 11.50% moisture)
- IHS 20(Max.)/100g
mps IHS 43 to 47 (Corrected to 11,50%moisture)
% IHS 18(Max.)
% IHS 82 (Min.)
% IHS 90%
ppm IHS 10 (Max.)
- IHS No. foul odor after 72 hrs.
- IHS 4.7 to 5.2
mS/cm IHS 1(Max.)
Units Standard Methods Specification Actual Findings
- IHS Absent Passes
% BS 757-1975 0.1500 %W/W 0.0623
ppm IHS 30 (Max.) 03
ppm IHS 2 (Max.) Passes
ppm IHS 30 (Max.) Passes
ppm IHS 0.1(Max.) Passes
ppm IHS 100( Max.) Passes
ppm IHS 0.5 (Max.) Passes

1gm IP 50 CFU/gm(Max.) 10
1gm IP Absent Passes
10gms IP Absent Passes
1gm IP Absent Passes
1gm IP Absent Passes
Igm IHS 50 CFU/gm(Max.) Passes
1gm IHS Passes Passes
10gms IHS Absent Passes
1gm Ph.Eur 50 CFU/gm(Max.) Passes

1 gm IHS Absent Passes

1 gm IHS Absent Passes
10gms IHS Absent Passes
1gm IP Absent Passes
10gms IP
Manager(Q.C) 'elite
Absent
Wi
Passes\
F Manager(Q.A)
 16.05.2020
B-2551
May - 2020
Apr-2025
1 of 2

Actual Findings
Passes
Passes
Passes
Passes
5.51
Passes
Passes
9.6
0.38
10.64
Passes
210
Passes
45.72
15.98
96.3
Passes
Absent
Passes
4.95
0.389
F Manager(Q.A)