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    The document describes techniques for microencapsulation including bulk polymerization, interfacial polymerization, spray drying and congealing, and fluidized bed technology. It discusses mixing an aqueous gum arabic and gelatin mixture with water at 4.5 pH and 40-50°C, adding methyl salicylate and slowly cooling the mixture over 1 hour to form microencapsules, which are then rigidized by cooling further to 10°C. It provides schematics of bulk polymerization and interfacial polymerization processes involving monomers, bioactive materials, initiators, and aqueous solutions to form polymer microspheres. Spray drying involves spraying an aqueous solution into hot air while spray congealing uses

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    The document describes techniques for microencapsulation including bulk polymerization, interfacial polymerization, spray drying and congealing, and fluidized bed technology. It discusses mixing an aqueous gum arabic and gelatin mixture with water at 4.5 pH and 40-50°C, adding methyl salicylate and slowly cooling the mixture over 1 hour to form microencapsules, which are then rigidized by cooling further to 10°C. It provides schematics of bulk polymerization and interfacial polymerization processes involving monomers, bioactive materials, initiators, and aqueous solutions to form polymer microspheres. Spray drying involves spraying an aqueous solution into hot air while spray congealing uses

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    The document describes techniques for microencapsulation including bulk polymerization, interfacial polymerization, spray drying and congealing, and fluidized bed technology. It discusses mixing an aqueous gum arabic and gelatin mixture with water at 4.5 pH and 40-50°C, adding methyl salicylate and slowly cooling the mixture over 1 hour to form microencapsules, which are then rigidized by cooling further to 10°C. It provides schematics of bulk polymerization and interfacial polymerization processes involving monomers, bioactive materials, initiators, and aqueous solutions to form polymer microspheres. Spray drying involves spraying an aqueous solution into hot air while spray congealing uses

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    © All Rights Reserved
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    92 views5 pages

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    The document describes techniques for microencapsulation including bulk polymerization, interfacial polymerization, spray drying and congealing, and fluidized bed technology. It discusses mixing an aqueous gum arabic and gelatin mixture with water at 4.5 pH and 40-50°C, adding methyl salicylate and slowly cooling the mixture over 1 hour to form microencapsules, which are then rigidized by cooling further to 10°C. It provides schematics of bulk polymerization and interfacial polymerization processes involving monomers, bioactive materials, initiators, and aqueous solutions to form polymer microspheres. Spray drying involves spraying an aqueous solution into hot air while spray congealing uses

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    of 5

    Aq. Gum arabic + Aq.

    Gelatin mixture + water


    4.5 pH, 40-50 0C

    polymer interact to causes phase separation


    warm
    mixture + methyl salicylate

    slowly cooled the mixture at 25 0C over 1 hr

    rigidization of coating is done by cooling


    microencapsule at 10 0C

    21
    Polymerization Techniques
    1. Normal polymerization

    Monomer
    Bioactive material
    Initiator

    Polymerization

    Polymer block

    Mould/ mechanical
    fragmentation

    Microspheres

    Fig.-Schematic for Bulk Polymerization


    22
    2. Interfacial Polymerization1,4
    Monomer/ Aq. Solution of NaOH with Initiator,
    Bioactive material Surfactant above CMC Stabilizer

    Dispersion with vigorous


    stirring

    Micellar solution of polymer in aq. medium

    Polymerization

    Microspheres formation

    Separation, Washing, Drying


    Microspheres
    23
    SPRAY DRYING & CONGEALING ( COOLING):

    Spray drying : spray = aqueous solution / Hot air

    Spray congealing : spray = hot melt/cold air


    FLUIDIZED BED TECHNOLOGY:

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