PHAR 3208 Lab Activities

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PHAR 3208

Cosmetic Product Development


Laboratory Activities
Name/s:
Date:
Activity No.1
Shampoo
Production Formulation:
Ingredients Master Formula Working Formula
Leaf extract of choice 25 ml
Aloe vera gel 25 g
Soft soap 150 ml
Alcohol 250 ml
Lavender oil 5 ml
Rosemary oil 2 ml
Geranium oil 3 ml
Potash solution (5%) 50 ml
Purified water 590 ml

Production size: Order: Prepare 250 ml of Leaf extract-Aloe Shampoo


Reduction factor:

Manufacturing Equipment:
 Wet mixer
 Blender
 Bottle shaker

Procedure:
1. Blend the leaf extract and aloe vera gel.
2. Set aside.
3. Dissolve the soft soap in alcohol in the bottle shaker.
4. Add the volatile oils.
5. Mix the potash solution with half part of water in separate container.
6. Add the potash solution to soft soap-alcoholic solution.
7. Gradually add little by little the leaf extract-aloe vera gel mixture.
8. Add the remaining water to come up with a desired volume.
9. Place in a suitable container.
10. Attach the label.

Production Record:
Product Name

Brand Name

Standard Batch Size Unit Size

Date of Preparation Date of Release

Time of Preparation Time of Release


Prepared by Evaluated by

Guide Questions:
1. What is the etiology of the word “shampoo”?

2. Differentiate soap from shampoo. What main ingredients of shampoo makes it different from soap?

3. What is the chemical name of potash solution?

4. Give the role of each ingredient in the formulation.


PHAR 3208
Cosmetic Product Development
Laboratory Activities
Name/s:
Date:
Activity No.2
Lotion
Production Formulation:
Ingredients Master Formula Working Formula
Jojoba oil 1268 g
Beeswax 600 g
Vitamin E capsule 20 pcs
Lavender/Rose oil 100 ml
Aloe vera gel 400 g
Purified water 900 g 90 g

Production size: Order: Prepare a lotion using 90 g of purified water only.


Reduction factor:

Manufacturing Equipment: Agitator or Blender

Procedure:
1. In a beaker over low heat, melt together the jojoba oil, beeswax, and Vitamin E oil.
Note: Do this slowly.
2. When almost entirely melted, remove from the heat.
3. Place the mixture into large beaker.
4. Add the aloe vera gel and 1/5 parts of water. (Add less water for thicker, more butter-like consistency).
5. Mix using blender until lotion becomes thick.
6. Let it sit for 15-20 minutes. It requires time to thicken and congeal. It does not necessarily need to be
covered or moved to a cool area.

Production Record:
Product Name

Brand Name

Standard Batch Size Unit Size

Date of Preparation Date of Release

Time of Preparation Time of Release

Prepared by Evaluated by

Guide Questions:
1. Write the structural formula of Vitamin E.
2. Wat is the chemical name of natural, bioactive Vitamin E?

3. Give the role of each ingredient.

PHAR 3208
Cosmetic Product Development
Laboratory Activities
Name/s:
Date:
Activity No.3
Lipstick
Production Formulation:
Ingredients Master Formula Working Formula
Fresh flower extract 5g
Paraffin wax 1200 g
White beeswax 750 g
Cocoa butter 150 g
Shea butter 5g
Jojoba oil 1200 ml
Vanillin 1500 g
Colorant (congo red) qs

Production size: Order: Prepare 200 g and repackaged to 4 lipsticks each containing 50 g each of moisturizing
lipstick

Reduction factor:

Manufacturing Equipment:
 Suppository/Lipstick Molder
 Filling Pot

Procedure:
1. Place the paraffin wax and white beeswax in the suppository/lipstick molding and filling pot.
2. Add the cocoa butter, shea butter and jojoba oil.
3. Stir until uniformly mixed.
4. Switch off the machine and add while stirring the vanillin.
5. Add the colorant depending on the shade you desire.
6. Fill into the molds.
7. Allow to solidify.

Production Record:
Product Name

Brand Name

Standard Batch Size Unit Size

Date of Preparation Date of Release

Time of Preparation Time of Release

Prepared by Evaluated by

Guide Questions:
1. Enumerate the factors that contribute to lip darkening/burning.
- sun exposure, tobacco smoking, pregnancy, certain medications, medical condition.

2. List down the different constituents present in the flower extract of your choice according to credible journals and
articles.
- In our lipstick product we use gumamela flower extract as active ingredient because according to the study of Paje
G and Ramirez I., 2021, it shows that the main constituents found in hibiscus flower or gumamela are alkaloids,
cardenolides and bufadienolides, tannins, protein and carbohydrates which helps the skin;s ability to maintain
moisture. It provides the skin to keep hydrated, soft and supple for longer. In addition, for the lips it benefits to
remove layers of dead skin cells to reveal a rosy and toned lips.

3. What is magic lipstick? What is the component that makes it different from the usual-colored lipstick?
- Magic lipstick is a color-changing lipstick. The lipsticks contain dyes that act a bit like litmus paper, the
acidity indicator dyes are colorless, weak acids. But lips have a higher pH than the lipstick, which triggers a
chemical reaction that converts the acids into a strongly colored compound.

4. Give the role of each ingredient.


 Fresh flower extract
- Active ingredient
 Paraffin wax
- Emulsifiers
 White beeswax
- Humectant
 Cocoa butter
- Antioxidant
 Shea butter
- emollient
 Jojoba oil
- Antioxidant
 Vanillin
- Flavoring agent
 Congo red
- Colorant

PHAR 3208
Cosmetic Product Development
Laboratory Activities
Name/s:
Date:
Activity No.4
Mouthwash
Production Formulation:
Ingredients Master Formula Working Formula
Lemon oil 2 ml
Peppermint oil 2 ml
Potassium bicarbonate 20 g
Sodium borate 20 g
Thymol 0.5 g
Eucalyptol 1 ml
Methyl salicylate 0.5 ml
Amaranth solution 14 ml
Alcohol (70%) 50 ml
Glycerin 100 ml
Purified water qs 2000 ml

Production size: Order: Prepare 250 ml of Aromatic Mouthwash


Reduction factor:

Manufacturing Equipment:
 Bottle shaker

Procedure:
1. Dissolve potassium bicarbonate and sodium borate in 1/5 part of purified water then add glycerin.
2. When effervescence or bubbling stopped, add the mixture to 50 ml of purified water.
3. Dissolve the other ingredients in the alcohol, and the solution of salts to the alcoholic solution with
agitation in the bottle shaker.
4. Then add sufficient quantity of purified water to come up with desired volume.
5. Allow the mixture to stand, with occasional shaking during 24 hours.
6. Filter using talc when necessary to produce a clear solution.
7. Transfer to a suitable container.
8. Attach the label.

Production Record:
Product Name

Brand Name

Standard Batch Size Unit Size

Date of Preparation Date of Release

Time of Preparation Time of Release

Prepared by Evaluated by

Guide Questions:
1. Differentiate mouthwash from gargle.
2. What is the chemical name of amaranth?

3. Enumerate the ingredients that constitute to the aromatic sting of the formulation.

4. Give the role of each ingredient in the formulation.

PHAR 3208
Cosmetic Product Development
Laboratory Activities
Name/s:
Date:
Activity No.5
Perfume
Production Formulation:
Ingredients Master Formula Working Formula
Fragrance oil 15 ml
Fixative (liquid) 0.6 ml
Dipropylene Glycol 3 ml
Alcohol 75 ml
Distilled water qs 100 ml

Production size: Order: Prepare 100 ml of Eau de Parfum


Reduction factor:

Manufacturing Equipment:
 Mixer

Procedure:
1. Mix the fragrance oil and fixative.
2. In another container, mix the dipropylene glycol and alcohol.
3. Let it stand for 30 minutes.
4. Add the first mixture to the second mixture.
5. Add sufficient quantity of distilled water to make up 100 ml.

Production Record:
Product Name

Brand Name

Standard Batch Size Unit Size

Date of Preparation Date of Release

Time of Preparation Time of Release

Prepared by Evaluated by

Guide Questions:
1. What are the different types of perfume? Describe each.

2. What are the methods for extraction of fragrance oils? Describe each.
3. Give the role of each ingredient.

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