3 Former McGills Service Station BSA Report

Brownfields Site Assessment
Former McGills Service Station

Kings Mountain, North Carolina
Isothermal Planning and
Development Commission
May 5, 2011
Prepared for
Isothermal Planning and Development Commission
111 West Court Street
Rutherfordton, North Carolina 28139
Prepared by
Altamont Environmental, Inc.
231 Haywood Street
Asheville, NC 28801
(828) 281-3350
Brownfields Site Assessment Report, Former McGills Service Station May 5, 2011
Isothermal Planning and Development Commission Page ii
Table of Contents
1.0 Executive Summary .......................................................................................................... 1
2.0 General Information ......................................................................................................... 3

2.1 Site Information .............................................................................................................. 3
2.2 Contacts .......................................................................................................................... 3
2.3 Professional Certification ................................................................................................ 4
3.0 Site History and Characterization .................................................................................... 5

3.1 Background ..................................................................................................................... 5
3.2 Site Characteristics ......................................................................................................... 6
4.0 Site Investigation.............................................................................................................. 7

4.1 Health and Safety Information ....................................................................................... 7
4.2 Ground-Penetrating Radar and UST Survey ................................................................... 7
4.3 Soil Sampling .................................................................................................................. 7
4.4 Monitoring Well Installation ............................................................................................ 8
4.4.1 Monitoring Well Soil Boring Sampling ............................................................... 9
4.4.2 Monitoring Well Development............................................................................ 9
4.4.3 Monitoring Well Surveying and Water Level Gauging ..................................... 10
4.5 Monitoring Well Sampling ............................................................................................. 10
4.6 Quality Control Measures ............................................................................................. 10
5.0 Data Evaluation ............................................................................................................. 12

5.1 Soil Sampling ................................................................................................................ 12
5.1.1 Fill Port Soil Sampling Results ......................................................................... 12
5.1.2 UST Soil Sampling Results ............................................................................... 12
5.1.3 Product Line Soil Sampling Results ................................................................. 12
5.1.4 Monitoring Well Soil Boring Sampling Results ................................................ 12
5.2 Monitoring Well Sampling ............................................................................................. 13
5.2.1 Potentiometric Surface Elevations .................................................................. 13
5.2.2 Laboratory Analytical Results........................................................................... 13
5.3 Initial Response and Reporting .................................................................................... 13
5.4 Receptor Survey ............................................................................................................ 13
5.5 Investigative Derived Waste Management .................................................................. 14
6.0 Conclusions and Recommendations ............................................................................ 15
P:\Isothermal PDC\Former McGills Service Station\Brownfield Site Assessment\Reports\BSA Report\BSA Report - FINAL.docx
Isothermal Planning and Development Commission Page iii
7.0 References .................................................................................................................... 16
Figures
1. Site Location Map
2. Site Plan Map
3. UST Soil Sample Locations
4. Groundwater Contour Map
Tables
1. UST Information
2. Monitoring Well Construction Details
3. UST Assessment Soil Sample Analytical Results Summary
4. Soil Boring MW-2 Analytical Results
5. Groundwater Analytical Results
Appendices
A. Laboratory Analytical Reports and Chain-of-Custody Documentation Forms
B. Boring Log for Monitoring Well MW-2
C. Monitoring Well Construction Logs for MW-1, MW-2, and MW-3
D. Equipment Calibration Logs
E. Well Development and Low-Flow Sampling Logs
F. Form UST-61
Isothermal Planning and Development Commission Page 1
1.0 Executive Summary

The Isothermal Planning and Development Commission (IPDC) contracted Altamont Environmental, Inc.
(Altamont) to perform a Brownfield Site Assessment for the Former McGills Service Station in Kings
Mountain, Cleveland County, North Carolina (Figure 1). The Former McGills Service Station is referred to as
the “site” in the remainder of this report. This report is designed to present the methods used and results
found during the Brownfields Site Assessment (BSA), which was performed under an Environmental
Protection Agency (EPA) community-wide brownfields assessment grant held by IPDC.
Altamont prepared a Phase I Environmental Site Assessment (Phase I ESA) dated July 23, 2010, for the
subject property (Altamont 2010c). The subject property is currently vacant but was used as a tire service
center for approximately the last 10 years and was a filling station between the 1940s and 1980s. The
Phase I ESA identified two Recognized Environmental Conditions (RECs) on the subject property as follows:
• Five underground storage tanks (USTs) were identified by the North Carolina Department of
Environment and Natural Resources (DENR)
• Fill ports and vent pipes were observed during the site reconnaissance
Other items of potential concern were identified:
• Three aboveground storage tanks (ASTs) were observed during the Phase I ESA site reconnaissance
• The interior of the building and the storage trailer on the subject property were not accessible during
the Phase I ESA site reconnaissance
As of December 9, 2010, no ASTs remained on-site. The storage trailer was no longer located at the site.
Portions of the interior of the building were inspected during the field investigation conducted March 22
through March 24, 2011. Abundant oil staining was observed on the concrete floor of the two-bay garage.
One bay of the garage contained a recessed work area for accessing the bottoms of vehicles. Water and a
thin layer of oil were observed in the bottom of the recessed work area.
No closure documents or soil sample analytical results associated with the USTs could be located during the
Phase I ESA. A Ground-Penetrating Radar (GPR) survey was performed as part of this assessment to
evaluate the location and approximate size of underground tanks and utilities. The GPR survey indicated the
presence of a total of eight USTs, rather than five as determined by the Phase I ESA. The tanks identified by
GPR were designated UST-1 through UST-8. Maps indicating the approximate location of the USTs are
included as Figure 2 and Figure 3. A summary table for the subject property USTs is included as Table 1.
The purpose of the BSA project was to determine if the soil and/or groundwater quality at the site has been
impacted by any releases associated with the eight USTs located on-site. The BSA results are summarized
as follows:
• Approximately 57 soil samples were collected, three monitoring wells were installed (Table 2), and
seven groundwater samples were collected during BSA field activities in March 2011 at the Former
McGills Service Station site.
• Soil analytical results for samples collected from UST fill ports indicate that overfilling likely occurred
in UST-1, UST-2, UST-3, UST-7, and UST-8 (Figure 3, Table 3, Appendix A). Overfilling that occurred in
UST-7 and UST-8 may not have affected surrounding soils or groundwater, as the fill ports for these
USTs are surrounded by concrete manholes. However, as noted below, contamination was detected
in soil samples collected from the sides of UST-7 and UST-8 adjacent to their fill port areas.
• Concentrations of Total Petroleum Hydrocarbons (TPH) Gasoline Range Organics (GRO) and TPH
Diesel Range Organics (DRO) that exceeded the DENR UST Action Level of 10 mg/kg in soil samples
collected from the sides of the USTs indicate that petroleum constituents have impacted soil near
the south side of UST-3, the west side of UST-6, the north side of UST-7, and the east side of UST-8
(Figure 3, Table 3, Appendix A) suggesting that these tanks may have leaked.
• None of the analytical results from soil samples collected from below product lines contained
concentrations of TPH-GRO or TPH-DRO above UST Action Levels (10 mg/kg) (Figure 3, Table 3,
Appendix A).
• No volatile organic compounds (VOCs), semivolatile organic compounds (SVOCs), extractable
petroleum hydrocarbons (EPH), or volatile petroleum hydrocarbons (VPH) hydrocarbon fractions
exceeded Soil-to-Groundwater (GW) Maximum Soil Contaminant Concentrations (MSCCs) in the soil
samples collected at 10-foot intervals during the installation of the “source area” monitoring well
MW-2 (Figure 2, Table 4, Appendix A).
• Apparent groundwater flow direction is to the southwest (Figure 4). However, only three monitoring
wells were used to measure potentiometric surface elevations, which can be locally variable.
Therefore, the estimated groundwater flow direction is not necessarily representative of the entire
site. Based upon surface topography and features, groundwater had been expected to flow toward
the southeast.
• No constituents were detected above the North Carolina Ground Water Quality Standards (NC GWQS)
in groundwater samples collected from monitoring wells MW-2 and MW-3. Four VOCs were detected
above NC GWQS in monitoring well MW-1, including 1,2-dichloroethane, 1,2-dichloropropane,
benzene, and diisopropyl ether (Figure 2, Table 5, Appendix A). These constituents are not
commonly associated with USTs and may have originated from the site’s septic tank or the recessed
work areas in the garage, which are located upgradient of monitoring well MW-1.
Based on the constituent concentrations detected in soil and groundwater, a receptor survey will be
conducted by Altamont and submitted under a separate cover. The results of the receptor survey and the
site groundwater and soil analytical data will be used by DENR to determine the risk level of the site and
whether additional site activities will be required by DENR in the future.
2.0 General Information

2.1 Site Information
1. Date of Report: May 5, 2011
2. Property Owner / Underground Storage Tank (UST) Owner:
Wallace Properties, Inc.
P.O. Box 470407
Charlotte, North Carolina 28247
3. Site Coordinates:
Latitude (decimal degrees): 35 degrees, 14 minutes, 26.32 seconds north
Longitude (decimal degrees): 81 degrees, 20 minutes, 31.68 seconds west
Location method: Determined from Google Earth software program
4. Incident Number: 28935
2.2 Contacts
1. Name, address, telephone number, and job title of primary contact person:
Mr. Steve Wallace
Property Owner
Wallace Properties, Inc.
P.O. Box 470407
Charlotte, North Carolina 28247
(704) 541-1133
2. Name, address, and telephone number of brownfields grant contact:
Mr. Josh King
Isothermal Planning and Development Commission
111 West Court Street
Rutherfordton, North Carolina 28139
(828) 387-2281, ext. 264
3. Name, address, and telephone number of primary consultant:
Ms. Lisa Manning, P.E.
Altamont Environmental, Inc.
231 Haywood Street
Asheville, North Carolina 28801
(828) 281-3350
4. Name, address, telephone number, and state certification number of laboratory:
Ms. Lorri Patton
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, North Carolina 28804
(828) 254-7176
North Carolina Certification Number: 37706
3.0 Site History and Characterization

3.1 Background
The Isothermal Planning and Development Commission (IPDC) contracted Altamont Environmental, Inc.
(Altamont) to perform a Brownfield Site Assessment (BSA) for the Former McGills Service Station in
Cleveland County, North Carolina (Figure 1). The Former McGills Service Station is referred to as the “site” in
the remainder of this report. This report is designed to support the Brownfields Site Assessment, which was
performed under a United States Environmental Protection Agency (EPA) community-wide brownfields
assessment grant. The methodologies described in this document are in general accordance with EPA’s
Environmental Investigation Standard Operating Procedures and Quality Assurance Manual (EISOPQAM,
EPA 2001) and North Carolina Department of Environment and Natural Resources’ (DENR’s) Guidelines for
Assessment and Corrective Action for UST Releases (DENR 2008a). The underground storage tank (UST)
assessment activities adhered to the guidelines presented in the DENR’s Guidelines for Site Checks, Tank
Closure, and Initial Response and Abatement for UST Releases (DENR 2008b).
Altamont prepared a Phase I Environmental Site Assessment (Phase I ESA) dated July 23, 2010, for the
subject property (Altamont 2010c). The subject property is currently vacant, but was used as a tire service
center for approximately the last 10 years and was a filling station between the 1940s and 1980s. The
Phase I ESA identified two Recognized Environmental Conditions (RECs) on the subject property as follows:
• Five underground storage tanks (USTs) were identified by the DENR
• Fill ports and vent pipes were observed during the site reconnaissance
Other items of potential concern were identified:
• Three aboveground storage tanks (ASTs) were observed during the Phase I ESA site reconnaissance
• The interior of the building and the storage trailer on the subject property were not accessible during
the Phase I ESA site reconnaissance
As of December 9, 2010, no ASTs remained on-site. The storage trailer was no longer located at the site.
Portions of the interior of the building were inspected during the field investigation conducted March 22
through March 24, 2011, and are described in this report. Abundant oil staining was observed on the
concrete floor of the two-bay garage. One bay of the garage contained a recessed work area for accessing
the bottoms of vehicles. Water and a thin layer of oil were observed in the bottom of the recessed work
area.
No closure documents or soil sample analytical results associated with the USTs could be located during the
Phase I ESA. A ground-penetrating radar (GPR) survey was performed as part of this assessment. The GPR
survey indicated the presence of a total of eight USTs. Maps indicating the approximate location of the USTs
are included as Figure 2 and Figure 3. A summary table for the subject property USTs is included as Table 1.
Altamont developed multiple planning documents for the Brownfields Site Assessment: Site-Specific Quality
Assurance Project Plan (QAPP), a Work Plan, and a Health and Safety Plan (HASP). They are available under
separate covers (Altamont 2011a, 2011b, and 2010b, respectively). The Site-Specific QAPP is considered to
be Addendum 2 of the IPDC Generic QAPP (Altamont 2010a). These documents were designed to
complement each other in the implementation of the assessment.
The purpose of the BSA was to determine if the soil and/or groundwater quality at the site have been
impacted by any releases associated with the USTs described above and in Table 1. This assessment is
designed to provide enough information for the development of a Phase I Limited Site Assessment (LSA) and
a Regulated In-Place Closure of USTs Assessment in accordance with DENR (2008a) and (DENR 2008b),
respectively.
3.2 Site Characteristics

The IPDC Former McGills Service Station site is located at 100 East King Street in Kings Mountain, North
Carolina. Figure 1 illustrates the general location of the property. The site includes one building with a two-
bay garage and is located on approximately 0.25 acres. The remainder of the site is asphalt, and there is a
small grassed area in the southern portion of the property. A site plan map is included as Figure 2.
The center of the site is located at the approximate latitudinal and longitudinal coordinates of 35 degrees,
14 minutes, 27.2 seconds and 81 degrees, 20 minutes, 31.9 seconds, respectively. According to the USGS
topographic map, included as Figure 1, the elevation of the site is approximately 1,018 feet above mean sea
level (MSL). Drainage across the surface of the site flows in a southeasterly direction.
The Former McGills Service Station is currently unused. Until the summer of 2010, it was used as a tire
resale store. It was formerly operated as a service station. The site is located in an area that is
characterized primarily by light commercial and residential uses. It is bounded by Kings Street to the north,
residential homes to the east, a business to the south, and Piedmont Avenue to the west. King’s Mountain
Development, LLC has plans to either redevelop the site for light commercial purposes or sell the property to
others.
According to DENR’s Geologic Map of North Carolina (DENR 1985), the site is located in the inner Kings
Mountain Belt Physiographic Province, which is a major shear zone. The three prominent formations are the
Cherryville Granite, the Blacksburg Formation, and a Mica Schist. Locally, the bedrock in this area is sericite
schist with graphite, phyllite with sericite quartzite, banded marble, amphibolites, and minor calc-silicate
rock.
According to Cleveland County Soil Survey data accessed on October 14, 2010,
(http://websoilsurvey.nrcs.usda.gov/app/WebSoilSurvey.aspx), a majority of the surface soils on the site are
Uwharrie-Urban land (UxB) well-drained silty clay loams derived from weathered metavolcanics and/or
argillite bedrock.
4.0 Site Investigation

4.1 Health and Safety Information
Prior to conducting any intrusive work, Altamont notified the North Carolina One-Call Center to mark the
utilities in the area. A GPR Survey was also conducted to locate the USTs as well as any other potential
utilities on-site. Altamont and sub-contractor staff participated in an initial thorough discussion of Altamont’s
Health and Safety Plan for McGills Service Station (Altamont 2010b) prior to beginning work at the site. In
addition, health and safety “tailgate” meetings were held at the beginning of each fieldwork day. All
personnel wore the following safety gear, at a minimum:
• Long pants and steel-toed boots (at all times)
• Hardhats, safety glasses, cut-resistant gloves, and nitrile gloves (as appropriate for specific activities)
No accidents or injuries occurred during fieldwork activities.
4.2 Ground-Penetrating Radar and UST Survey

On March 14, 2011, an Altamont representative conducted a UST assessment and supervised a GPR survey
in order to confirm the number and locations of USTs at the subject property. Reed Tech, Inc. from
Columbia, South Carolina, performed the GPR survey. A total of eight USTs and three product lines were
identified during the GPR survey conducted at the site. Each UST location was confirmed by the presence of
a fill port and designated as UST-1 through UST-8. The tank locations, product lines, and additional utilities
were marked on the pavement with spray paint. Approximate tank locations are shown on Figure 2.
The manhole covers for all eight identified UST fill ports were located and removed. The USTs were then
gauged using an oil-water interface probe for the presence of free product or water. Based on the odor and
appearance of observed free product (if any), the type of free product was assessed and recorded. One to
three inches of product were measured in most of the USTs. The USTs labeled UST-1 and UST-7 on Figure 2
contained no free product. The depth to the bottom of the tanks was also measured and recorded. A
summary table for the site USTs is included as Table 1.
According to DENR, five steel USTs are located on the property associated with the former McGills Exxon
Service Center and owned by Patterson Oil Company of Kings Mountain (Facility ID# 0-012740). Therefore,
three of the tanks observed on-site are unregistered. The UST information provided by the DENR is as
follows:
• Three gasoline USTs installed on January 1, 1966. Two of the USTs are 4,000 gallons in capacity,
and the other one is 6,000 gallons.
• One 1,000-gallon diesel UST installed on February 26, 1980.
• One 130-gallon used-oil UST installed on March 3, 1956.
No closure documents or soil-sample analytical results associated with the USTs could be located during the
Phase I ESA (Altamont 2010c).
4.3 Soil Sampling

Altamont performed a UST soil assessment at the site on March 22 and 23, 2011. EarthCon, Inc.
(EarthCon), a well driller certified in North Carolina and located in Greenville, South Carolina, performed the
intrusive activities at the site under the supervision of an Altamont representative. Discrete subsurface soil
samples were collected from dedicated Macro-Core® sleeves advanced with a Geoprobe® 7720DT direct-
push machine, or using a decontaminated stainless steel hand auger. Disposable nitrile gloves were also
used during sampling activities and were changed in between sample locations to prevent sample cross-
contamination.
Soil samples were collected in accordance with the Guidelines for Site Checks, Tank Closure, and Initial
Response and Abatement for UST Releases (DENR 2008b). Soil samples were collected from borings
located around the perimeter of a single UST or around the perimeter of a set of closely spaced USTs. These
samples were collected within three feet of the USTs at the depth of the tank bottom, or no deeper than two
feet into native soil below the depth of the tank bottom. Soil samples from locations near USTs were
collected from seven to ten feet below ground surface (ft-bgs), depending on the depth of the tank. Soil
samples are designated with an “SB-X” nomenclature, with the “X” designating the boring number. One soil
sample was collected for every ten feet of UST, on each side of a UST. However, soil samples could not be
collected from the south side of UST-7, the east side of UST-3, or the west sides of UST-1 and UST-2, due to
the proximity of the site building, the two-bay garage, and a sewer line, respectively.
Subsurface soil samples were also collected adjacent to and beneath identified product lines. Product line
samples were collected at a depth of 2-3 ft-bgs and are designated with a “SB-PL-X” nomenclature, with the
“X” designating the boring number.
In addition, one surface soil sample was collected at each of the fill ports identified at the subject property to
evaluate the potential of past overfills. These samples were designated with a “SB-FP-X” nomenclature, with
the “X” designating the UST from which the sample was collected. Fill port samples from UST-1 through
UST-6 were collected with a decontaminated hand auger from a depth of about two ft-bgs. Fill port samples
from UST-7 and UST-8 were collected from the surface, as the manholes surrounding these fill ports were
cemented in place.
All soil samples were submitted to Pace Analytical Services (Pace), an analytical laboratory certified in North
Carolina and located in Asheville, North Carolina, for analysis. Samples were submitted for Gasoline Range
Organic Total Petroleum Hydrocarbons (TPH-GRO) analysis by EPA Method 8015B, if the former contents of
the associated UST were gasoline-related. For USTs that contained diesel or kerosene, the soil samples
were analyzed for TPH-GRO and TPH-Diesel Range Organics (DRO) by EPA Method 8015B. According to
observations made of the free product and review of DENR records, UST-1, UST-2, and UST-4 contained
gasoline. Therefore, soil sample collected from the fill ports and the border of these USTs were analyzed for
only TPH-GRO.
UST soil sample locations are displayed on Figure 3. A summary of soil sample depths, associated USTs,
and analytical results are included as Table 3.
4.4 Monitoring Well Installation

During field activities conducted on March 23-24, 2011, Altamont oversaw the installation of three
permanent monitoring wells (MW-01, MW-02, and MW-03). Monitoring well MW-2 was installed at the
eastern edge of UST-1 and UST-2, adjacent to the fill ports of these USTs. This location was considered a
“source area” due to the elevated petroleum odor detected in the soil samples collected from the fill ports of
UST-1 and UST-2 (designated as SB-FP-1, SB-FP-2, respectively). MW-1 was installed in a presumed
downgradient location, based upon local topography, to the south of the two-bay garage. MW-3 was
installed in a presumed upgradient location, in a position to facilitate the measurement of groundwater flow
direction and measure background conditions at the subject property.
Monitoring well borings were advanced by EarthCon using hollow stem augers (HSAs) powered by a
Geoprobe® 7720DT. The standard methods for the design and installation of monitoring wells, as provided
in Section 6 of the EISOPQAM (EPA 2001), were followed. A boring log for MW-2 and monitoring well
construction logs for MW-1, MW-2, and MW-3 were prepared and are included in Appendix B and Appendix
C, respectively. The DENR Guidelines (DENR 2008a) did not require soil lithology to be described for the
MW-1 and MW-3 borings (the “non-source area” well borings).
All equipment, well materials, and tools that entered the borehole were steam-cleaned with a high
temperature pressure washer, prior to installation. The monitoring wells were composed of two-inch nominal
inside-diameter (ID) Schedule 40 PVC. The 0.010-inch machine-slotted well screens used for the monitoring
wells were ten feet in length for MW-2 and MW-3, and 15 feet in length for MW-1. A clean, washed, well-
rounded silica sand was installed to two feet above the top of the well screen to function as a filter-pack
between the well screen and the formation. A two-foot bentonite seal was installed on top of the sand pack
and hydrated, followed by cement grout mixture installed to ground surface.
Each monitoring well was designed so that the well screen would bracket the water table. The depth to the
well bottom for MW-1, MW-2, and MW-3 was 58, 53, and 53 ft-bgs, respectively. Monitoring well
construction details are included in Table 2 and Appendix C.
4.4.1 Monitoring Well Soil Boring Sampling
Consistent with the Guidelines for Assessment and Corrective Action for UST Releases (DENR 2008a),
Altamont collected soil samples from the monitoring well installed in the “source area” (MW-2), at ten-foot
intervals. Specifically, soil samples were collected at 8-10 ft-bgs, 18-20 ft-bgs, 28-30 ft-bgs, 38-40 ft-bgs,
and a sample collected just above the water table at 43-45 ft-bgs. The DENR Guidelines did not require soil
samples to be collected from the MW-1 and MW-3 soil borings (the “non-source area” well borings).
The organic vapor analyzer (OVA) with photo-ionization detector (PID) used on-site stopped working on March
22, 2011, due to an expired bulb. A functioning PID had to be shipped to the site the next day. Therefore,
the soil samples collected from the boring for MW-2 were placed in plastic Ziploc® bags and stored on ice
overnight. The following day, March 23, 2011, each soil sample was split, and one of the split samples was
allowed to volatilize in a warm environment for at least 10 minutes. The volatized samples were then
screened with the PID using proper headspace screening techniques (EPA 2001), as described in the BSA
Work Plan (Altamont 2011b) to help Altamont personnel preliminarily identify whether the soils were
potentially contaminated. The headspace screening results are recorded on the boring log for monitoring
well MW-2 (Appendix B).
The iced samples that were the counterparts to the volatilized samples were submitted to Pace for analysis
of volatile organic compounds (VOCs) by EPA Method 8260B, semivolatile organic compounds (SVOCs) EPA
Method 8270D, Massachusetts Department of Environmental Protection (MADEP) volatile petroleum
hydrocarbons (VPH), and MADEP extractable petroleum hydrocarbons (EPH), in accordance with DENR
guidance (2008a).
4.4.2 Monitoring Well Development
After installation of the monitoring wells and a minimum 24-hour period for grout curing, each monitoring
well was developed using a Mini-Monsoon submersible pump. To enhance the removal of sediment, the
pump was intermittently agitated by rapid short upward strokes from the bottom of the well. During
development, the field parameters of pH, temperature, dissolved oxygen (DO), specific conductivity (SC), and
oxidation-reduction potential (ORP) were measured approximately every five minutes with a calibrated YSI
multi-parameter water quality meter. Turbidity was also measured every five minutes with a calibrated
Lamotte 2020 turbidity meter. Equipment calibration information is included in Appendix D. The monitoring
wells were pumped until these parameters stabilized. Parameters were considered stabilized if, after three
consecutive readings:
• pH ± 0.1 unit
• SC ± 3%
• Temperature, DO, and turbidity ± 10%

• ORP ± 10 mV
• Turbidity was below 20 nephelometric turbidity units (NTUs)
Due to the very low recharge rate for monitoring well MW-2, field parameters did not stabilize during
development of this well. Approximately eight well volumes (eight gallons) were removed from MW-2 before
development activities were terminated. A total of twelve well volumes (26 gallons) and thirteen well
volumes (16 gallons) were removed from MW-1 and MW-3, respectively, during development activities. Well
Development Logs are included in Appendix E.
4.4.3 Monitoring Well Surveying and Water Level Gauging
Monitoring well top-of-casing (TOC) elevations were measured by Altamont personal using laser level
surveying equipment. Altamont personnel are not North Carolina licensed surveyors. Therefore, monitoring
well elevation data are considered to be approximate and not meant to substitute for a survey.
All of the monitoring wells were gauged using a decontaminated Solinst water level meter prior to well
development on March 23, 2011, and prior to groundwater sampling on March 24, 2011. Monitoring well
elevation data and water level gauging data are included on Table 2.
4.5 Monitoring Well Sampling

Groundwater samples were collected by an Altamont representative from monitoring wells MW-1, MW-2, and
MW-3 on March 24, 2011. The collection of groundwater samples was performed in general accordance
with the guidance from Section 7 of the EISOPQAM (EPA 2001).
Before beginning the sampling process, the water levels of all the monitoring wells were measured and
recorded. Monitoring wells were purged using a low-flow bladder pump with dedicated polyethylene tubing.
The field parameters of pH, temperature, DO, SC, ORP and turbidity were measured with a calibrated flow-
through cell water quality meter and a turbidity meter. The monitoring wells were considered sufficiently
purged when the pH, temperature, DO, SC, and ORP of the groundwater had stabilized to within 10 percent
between two readings. Despite purging multiple well volumes, the turbidity in the monitoring wells remained
elevated at 215, 275, and 28 nephelometric turbidity units (NTUs) for MW-1, MW-2, and MW-3, respectively.
See Appendix E for the monitoring well low-flow sampling logs.
Groundwater samples from each of the monitoring wells were immediately placed in a cooler with ice. The
samples were delivered to Pace for analysis of VOCs by EPA Method 602, SVOCs by EPA Method 625,
MADEP VPH, MADEP EPH, and lead by EPA Method 3030C.
4.6 Quality Control Measures

QC samples made up approximately 10% of the samples collected, in accordance with the Site-Specific
QAPP (Altamont 2011a). Specifically, five duplicate samples, two matrix spike/matrix spike duplicate
(MS/MSD) samples, and two equipment rinsate (EQR) samples were collected during the UST and
monitoring well installation soil sampling activities. One duplicate sample and one field blank sample were
collected during the monitoring well groundwater sampling. Additionally, a total of two trip blanks were
submitted for analysis, one in each cooler containing VOC samples. QC data are included in the lab report
(Appendix A). Altamont reviewed the QC data from the laboratory. Sample SB-36 (240 milligrams per
kilogram (mg/kg) TPH-DRO) and its duplicate SB-36-R (115 mg/kg TPH-DRO) did not demonstrate a high
level of reproducibility in the lab data. However, the soil samples were collected as grab samples rather
than composite samples. Therefore, the discrepancy between the values of the sample and its duplicate is
more representative of the wide variability in the concentration of constituents in a saprolitic soil than in a
lack of precision in the laboratory instruments. Altamont did not detect any quality control problems with the
laboratory analysis. In accordance with the Site-Specific QAPP, a field audit was conducted by Stuart Ryman,
P.G. of Altamont on March 23, 2011. The field audit was conducted to ensure that the proper protocols
were being followed during field work. No deficiencies were noted.
5.0 Data Evaluation

Laboratory analytical data was tabulated and compared against applicable action levels provided in the
DENR UST guidance, UST Action Levels for TPH-GRO and TPH-DRO, Soil-to-Groundwater Maximum Soil
Contaminant Concentration (MSCC) levels for soil, and North Carolina Groundwater Quality Standards (NC
GWQS) and Gross Contaminant Levels (GCLs) for Groundwater (DENR 2008a). Water level gauging data and
elevation data were used to calculate the groundwater elevations in the site’s monitoring wells and
groundwater flow direction at the site. A map showing the locations of the monitoring wells and soil samples
is included as Figure 3. A groundwater contour map is included as Figure 4. Tabulated analytical results for
UST assessment soil samples, soil samples collected from the “source area” well boring for MW-2, and
groundwater samples are included as Tables 3, 4, and 5, respectively. The laboratory analytical report is
included in Appendix A.
5.1 Soil Sampling

5.1.1 Fill Port Soil Sampling Results
Concentrations of TPH-GRO exceeding the UST Action Level of 10 mg/kg were detected in soil samples
collected from the UST fill ports of UST-1, UST-2, and UST-7. Concentrations of TPH-DRO exceeding the UST
Action Level of 10 mg/kg were detected in soil samples collected from the fill ports of UST-3, UST-7, and
UST-8. The most elevated concentration of TPH-GRO detected in a fill port sample was detected in sample
SB-FP-1 (1,960 mg/kg). The most elevated concentration of TPH-DRO detected in a fill-port sample was
detected in sample SB-FP-8 (41,300 mg/kg). These results suggest that overfilling likely occurred at UST-1,
UST-2, UST-3, UST-7, and UST-8 in the past. Analytical results are included in Table 3.
5.1.2 UST Soil Sampling Results
Soil sample analytical results collected from the sides of the USTs at just below the tank bottom displayed
concentrations of TPH-GRO above the UST Action Level of 10 mg/kg near only UST-6. Concentrations of
TPH-DRO were detected above the UST Action Level of 10 mg/kg near UST-3, UST-6, UST-7, and UST-8. The
most elevated concentration of TPH-GRO collected from the sides of the USTs was detected in SB-14 (2,930
mg/kg), which was collected from the west side of UST-6. The most elevated concentration of TPH-DRO
collected from the sides of the USTs was detected in SB-31 (2,360 mg/kg), which was collected from the
east side of UST-8. These data indicate that petroleum constituents have impacted soil near the south side
of UST-3, near the west side of UST-6, the north side of UST-7, and the east side of UST-8. Sample locations
are displayed on Figure 3, and analytical results are included in Table 3.
5.1.3 Product Line Soil Sampling Results
None of the analytical results from soil samples collected from below product lines contained concentrations
of TPH-GRO or TPH-DRO above UST Action Levels. Sample locations are displayed on Figure 3, and
analytical results are included in Table 3.
5.1.4 Monitoring Well Soil Boring Sampling Results
No VOCs, SVOCs, or VPH hydrocarbon fractions were detected in excess of the Soil-to-GW MSCCs from the
soil samples collected at 10-foot intervals during the installation of monitoring well MW-2. Analytical results
are included in Table 4.
5.2 Monitoring Well Sampling

5.2.1 Potentiometric Surface Elevations
Site-wide gauging of monitoring wells occurred just before well development on March 23, 2011, and just
before monitoring well sampling on March 24, 2011. The depth-to-groundwater data from these two events
were within 0.02 ft of respective measurements for each monitoring well. The depth-to-water btoc in
monitoring wells MW-1, MW-2, and MW-3 was measured at 45.76 ft, 46.61 ft, and 45.97 ft, respectively.
Relative groundwater elevations for monitoring wells MW-1, MW-2, and MW-3 were calculated to be 7.43 ft,
7.96 ft, and 9.50 ft, respectively (Table 2). These elevations were plotted on site map and used to calculate
groundwater flow direction (Figure 4). Apparent groundwater flow direction is to the southwest.
5.2.2 Laboratory Analytical Results
Analytical results from groundwater samples collected from monitoring wells MW-2 and MW-3 did not
contain any SVOCs or VOCs in exceedance of DENR NC GWQS. Analytical results from the sample collected
from monitoring well MW-1 contained no SVOCs, but did contain multiple VOCs at concentrations above the
NC GWQS. Specifically, 1,2-dichloroethane was detected at a concentration of 17.7 micrograms per liter
(µg/L), above the NC GWQS (0.38 µg/L). 1,2-dichloropropane was detected at a concentration of 1.5 µg/L,
above the NC GWQS (0.51 µg/L). Benzene was detected at a concentration of 2.3 µg/L, above the NC
GWQS (1 µg/L). Diisopropyl ether was detected at a concentration of 195 µg/L, above the NC GWQS (70
µg/L). These concentrations were also compared against the Gross Contaminant Level (GCL) for GW and
were found to be below those action levels. Analytical results are summarized in Table 5.
5.3 Initial Response and Reporting

In accordance with DENR’s Guidelines for Site Checks, Tank Closure, and Initial Response and Abatement
for UST Releases a 24-hour Release and Leaking UST Form (Form UST-61) was prepared for the site (DENR
2008b). Form UST-61 was submitted via email on May 3, 2011, to Ms. Diane Eskenasy with UST Section of
the Asheville Regional DENR office and is included in Appendix F. Ms. Eskenasy issued incident number
28935 for this site.
5.4 Receptor Survey

Soil and groundwater samples collected at the site contain contaminant concentrations in excess of DENR
UST Section Action Levels, MSCCs (for soils), and/or NC GWQS (for groundwater). Therefore, in accordance
with the Site-Specific QAPP for the project (Altamont 2011a), Altamont will complete a receptor survey for
the property. The receptor survey will include the following tasks:
• Identify all water supply wells and the properties served by these supplies within 1,500 feet of the
site.
• Determine availability of public water supply to all properties within 1,500 feet of the site.
• Identify designated wellhead protection areas and surface waters within 1,500 feet of the site.
• Determine the land use, including zoning if applicable, within 1,500 feet of the site.
• Locate all subsurface structures present on and adjacent to the site.
• Determine whether vapors from the discharge or release pose a threat of explosion due to the
accumulation of vapors in a confined space or pose any other serious threat to public health, public
safety, or the environment.
All receptor survey results will be documented on the DENR Receptor Survey form and will be displayed on a
Receptor Survey map, as appropriate. The Receptor Survey package will be submitted to IPDC and DENR
under a separate cover.
5.5 Investigative Derived Waste Management

All soil and groundwater investigative derived waste (IDW) was placed in Department of Transportation (DOT)
approved 55-gallon drums with lids until analytical data for the soil and groundwater could be reviewed.
Disposable acetate sleeves used during the Macro-Core® activities were disposed of by EarthCon.
The soil IDW will be spread on-site in accordance with DENR guidance (DENR 2008a) and with verbal
approval from Ms. Diane Eskenasy on April 27, 2011.
Groundwater analytical data indicated that the groundwater IDW contained non-petroleum constituents.
Analytical data was compared against the toxicity characteristic constituents and regulatory levels (TCLP) for
Resource Conservation and Recovery Act (RCRA) characteristic hazardous waste. Concentrations of
constituents detected in monitoring well MW-1 were well below the TCLP levels. Altamont contacted Mr.
Bruce Parris with the Inactive Hazardous Sites Branch in the DENR Mooresville Regional office on April 28,
2011, regarding the appropriate management of the groundwater IDW. Mr. Parris indicated that it would be
permissible to discharge the groundwater on the site, as long as the discharged IDW will be in accordance
with the IHSB guidance document’s IDW policy (DENR 2010). Therefore, groundwater IDW will be spread
near monitoring well MW-1 because the concentrations of the constituents in groundwater in the area were
greater than or equal to that of the groundwater IDW, and the IDW will not increase the spread of
contamination, in accordance with DENR guidance (DENR 2010).
6.0 Conclusions and Recommendations

The purpose of the BSA project was to determine if the soil and/or groundwater quality at the site has been
impacted by any releases associated with the USTs located on-site. The results of a GPR survey conducted
as part of this assessment indicated the presence of eight USTs located on-site (Figures 2 and 3, Table 1).
The BSA results are summarized as follows:
• Approximately 57 soil samples were collected, three monitoring wells were installed (Table 2), and
seven groundwater samples were collected during BSA field activities in March 2011 at the Former
McGills Service Station Site.
• Soil analytical results for samples collected from UST fill ports indicate that overfilling likely occurred
in UST-1, UST-2, UST-3, UST-7, and UST-8 (Figure 3, Table 3, Appendix A). Overfilling that occurred in
UST-7 and UST-8 may not have affected surrounding soils or groundwater, as the fill ports for these
USTs are surrounded by concrete manholes. However, as noted below, contamination was detected
in soil samples collected from the sides of UST-7 and UST-8 adjacent to their fill port areas.
• Concentrations of TPH-GRO and TPH-DRO that exceeded the DENR UST Action Level of 10 mg/kg in
soil samples collected from the sides of the USTs indicate that petroleum constituents have
impacted soil near the south side of UST-3, the west side of UST-6, the north side of UST-7, and the
east side of UST-8 (Figure 3, Table 3, Appendix A) suggesting that these tanks may have leaked.
• None of the analytical results from soil samples collected from below product lines contained
concentrations of TPH-GRO or TPH-DRO above UST Action Levels (10 mg/kg) (Figure 3, Table 3,
Appendix A).
• No VOCs, SVOCs, or VPH hydrocarbon fractions were detected in excess of Soil-to-GW MSCCs from
the soil samples collected at 10-ft intervals during the installation of monitoring well MW-2 (Figure
2, Table 4, Appendix A).
• Apparent groundwater flow direction is to the southwest (Figure 4). However, only three monitoring
wells were used to measure potentiometric surface elevations, which can be locally variable.
Therefore, the calculated groundwater flow direction is not necessarily representative of the entire
site. Based on surface topography and features, groundwater would have been expected to flow
toward the southeast.
• No constituents were detected above NC GWQS in groundwater samples collected from monitoring
wells MW-2 and MW-3. However, four VOCs were detected above NC GWQS in monitoring well MW-
1, including 1,2-dichloroethane, 1,2-dichloropropane, benzene, and diisopropyl ether (Figure 2,
Table 5, Appendix A). These constituents may have originated from the former septic tank or the
recessed work areas in the garage, which are located upgradient of monitoring well MW-1.
Based on the constituent concentrations detected in soil and groundwater, a receptor survey will be
conducted by Altamont and submitted under a separate cover. The results of the receptor survey and the
site groundwater and soil analytical data will be used by DENR to determine the risk level of the site and
whether additional site activities will be required by DENR in the future.
7.0 References
Altamont Environmental, Inc. 2010a. Generic Quality Assurance Project Plan, Revision 1, Isothermal
Planning and Development Commission.
Altamont Environmental, Inc. 2010b. Health and Safety Plan, Brownfields Site Assessment, Former McGills
Service Station.
Altamont Environmental, Inc. 2010c. Phase I Environmental Site Assessment, Former McGills Service
Station.
Altamont Environmental, Inc. 2011a. Site-Specific Quality Assurance Project Plan, Former McGills Service
Station, Revision 1, Addendum 2, Isothermal Planning and Development Commission.
Altamont Environmental, Inc. 2011b. Work Plan, Brownfields Site Assessment, Former McGills Service
Station.
Environmental Protection Agency (EPA). 2001. Environmental Investigation Standard Operating Procedures
and Quality Assurance Manual (EISOPQAM).
North Carolina Department of Environment and Natural Resources (DENR). 1985. Geologic Map of North
Carolina.
North Carolina Department of Environment and Natural Resources (DENR). 2008a. Guidelines for
Assessment and Corrective Action for UST Releases.
North Carolina Department of Environment and Natural Resources (DENR). 2008b. Guidelines for Site
Checks, Tank Closure, and Initial Response and Abatement.
North Carolina Department of Environment and Natural Resources (DENR), Division of Waste Management,
Inactive Hazardous Sites Branch. 2010. Inactive Hazardous Sites Program, Guidelines for
Assessment and Cleanup.
FIGURES
TABLES
Table 1
UST Information

Current/ Last Capacity Date Tank Approximate Last Did a Release

UST ID Number Use Status of UST
Contents* (gallons)** Installed Date Used Occur?
Yes (fill port area

1 Gasoline ~6,000 Unknown Unknown Filling Station In Place
only)
Yes (fill port area
2 Gasoline ~6,000 Unknown Unknown Filling Station In Place
only)
3 Heating Oil ~1,000 Unknown Unknown Filling Station In Place Yes
4 Gasoline ~6,000 Unknown Unknown Filling Station In Place No
5 Unknown ~4,000 Unknown Unknown Filling Station In Place No
6 Unknown ~4,000 Unknown Unknown Filling Station In Place Yes
7 Unknown ~1,000 Unknown Unknown Filling Station In Place Yes
8 Oil ~1,000 Unknown Unknown Filling Station In Place Yes
Notes:
* The DENR UST Section has record of five USTs being at the site. The UST information provided by DENR is included in
Section 4.2 of the BSA Report.
** UST capacity was estimated based on the size of the UST footprint obtained from the GPR survey.
~ Approximately
P:\Isothermal PDC\Former McGills Service Station\Brownfield Site Assessment\Reports\BSA Report\Tables\Table 1 - UST Information Table.xls Page 1 of 1
Table 2
Monitoring Well Construction Details

Top of Casing Depth to Groundwater Depth to Length of
Monitoring Well Well Diameter
Installation Date Elevation* Water Elevation* Bottom Screen Completion
Identification
(ft) (ft-btoc) (ft) (ft-bgs) (ft) (in)
MW-1 3/22/2011 53.19 45.76 7.43 58 15 2 flush-mount
MW-2 3/22/2011 54.57 46.61 7.96 53 10 2 flush-mount
MW-3 3/22/2011 55.47 45.97 9.50 53 10 2 flush-mount
Notes:
* Elevations are reported relative to an arbitrary survey station elevation of 60 feet. The manhole cover at the northwest property boundary has an
elevation of 54.96 feet. Elevations were not collected by North Carolina licensed surveyors and are considered approximate.
ft feet
ft-btoc feet below top of casing
ft-bgs feet below ground surface
in inches
P:\Isothermal PDC\Former McGills Service Station\Brownfield Site Assessment\Reports\BSA Report\Tables\Tables 2-5.xlsx Page 1 of 1
Table 3
UST Assessment Soil Sample Analytical Results Summary

TPH-Gasoline Range TPH-Diesel Range
Sample Depth
Sample Identification Collection Date Organics Organics
(ft-bgs) (mg/kg) (mg/kg)
Action Levels: 10 10
UST-1, UST-2, UST-4
SB-1 3/22/2011 9-10 ND NA
SB-2 3/22/2011 9-10 ND NA
SB-3 3/22/2011 9-10 ND NA
SB-4 3/22/2011 9-10 ND NA
SB-5 3/22/2011 9-10 ND NA
SB-5-R 3/22/2011 9-10 ND NA
SB-6 3/22/2011 9-10 ND NA
SB-7 3/22/2011 9-10 ND NA
SB-8 3/22/2011 9-10 ND NA
SB-9 3/22/2011 9-10 ND NA
SB-10 3/22/2011 9-10 ND NA
SB-11 3/23/2011 9-10 ND ND
SB-12 3/23/2011 9-10 ND ND
SB-FP-1 3/22/2011 2-3 1960 NA
SB-FP-2 3/22/2011 2-3 42.5 NA
SB-FP-4 3/22/2011 2-3 ND NA
UST-3
SB-33 3/23/2011 7-8 ND ND
SB-34 3/23/2011 7-8 ND ND
SB-35 3/23/2011 7-8 ND 68.8
SB-36 3/23/2011 7-8 ND 240
SB-36-R 3/23/2011 7-8 ND 115
SB-FP-3 3/22/2011 2-3 ND 48.0
UST-5, UST-6
SB-13 3/23/2011 8-9 ND ND
SB-14 3/23/2011 8-9 2930 918
SB-15 3/23/2011 8-9 ND 9.7
SB-16 3/23/2011 8-9 ND ND
SB-17 3/23/2011 8-9 ND ND
SB-17-R 3/23/2011 8-9 ND ND
SB-18 3/23/2011 8-9 ND ND
SB-FP-5 3/22/2011 2-3 ND 6.4
SB-FP-6 3/22/2011 2-3 ND 7.6
SB-PL-13 3/23/2011 2-3 ND ND
SB-PL-19 3/23/2011 2-3 ND ND
SB-PL-20 3/23/2011 2-3 ND ND
SB-PL-21 3/23/2011 2-3 8.3 ND
Notes appear on Final Page.
Table 3
UST Assessment Soil Sample Analytical Results Summary

TPH-Gasoline Range TPH-Diesel Range
Sample Depth
Sample Identification Collection Date Organics Organics
(ft-bgs) (mg/kg) (mg/kg)
Action Levels: 10 10
UST-5, UST-6
SB-PL-22 3/23/2011 2-3 ND ND
SB-PL-23 3/23/2011 2-3 ND ND
UST-7, UST-8
SB-26 3/23/2011 7-8 ND ND
SB-27 3/23/2011 7-8 ND ND
SB-28 3/23/2011 7-8 ND ND
SB-29 3/23/2011 7-8 ND ND
SB-29-R 3/23/2011 7-8 ND ND
SB-30 3/23/2011 7-8 ND ND
SB-30-EQR* 3/23/2011 - ND ND
SB-31 3/23/2011 7-8 ND 2360
SB-32 3/23/2011 7-8 ND 35.2
SB-FP-7 3/22/2011 0-1 247 605
SB-FP-8 3/22/2011 0-1 ND 41300
SB-PL-24 3/23/2011 2-3 ND ND
SB-PL-25 3/23/2011 2-3 ND ND
Notes:
ft-bgs feet below ground surface.
TPH Total Petroleum Hydrocarbons.
mg/kg milligrams per killogram.
PQL Practical Quantitation Limit. PQL ranged from 5.1 to 8.4 mg/kg for ND analytical results.
6.4 Indicates a detection above Laboratory PQL.
Action Levels TPH-GRO and TPH-DRO UST Action Levels are from North Carolina UST Section Guidelines
for Assessment and Corrective Action for UST Releases dated July 15, 2008, and
updated December 1, 2008.
247 Indicates a detection above Action Levels.
ND Constituent was not detected at a concentration greater than associated PQL.
NA Sample was not analyzed for constituent.
SB-FP-1 Designates soil sample collected from fill port of Tank 1.
SB-PL-13 Designates soil sample collected from product line location.
SB-5-R Designates duplicate soil sample of SB-5.
SB-30-EQR Designates rinsate sample collected from macro-core sleeve used to collect SB-30.
SB-30-EQR* Rinsate sample is reported in milligrams per liter.
Table 4
Soil Boring MW-2 Analytical Results

McGills Service Station
Sample ID: MW-2-SB-10 MW-2-SB-20 MW-2-SB-30 MW-2-SB-40 MW-2-SB-45 MW-2-SB-45-R
Sample Depth (ft bgs): 8-10 18-20 28-30 38-40 43-45 43-45
Constituent Date Collected: 3/23/2011 3/23/2011 3/23/2011 3/23/2011 3/23/2011 3/23/2011
Volatile Organics (µg/kg) Soil to GW

(Method 8260) MSCCs
1,1,1,2-Tetrachloroethane NL ND ND ND ND ND ND
1,1,1-Trichloroethane 1,600 ND ND ND ND ND ND
1,1,2,2-Tetrachloroethane 1 ND ND ND ND ND ND
1,1,2-Trichloroethane NL ND ND ND ND ND ND
1,1-Dichloroethane 380 ND ND ND ND ND ND
1,1-Dichloroethene 45 ND ND ND ND ND ND
1,1-Dichloropropene NL ND ND ND ND ND ND
1,2,3-Trichlorobenzene NL ND ND ND ND ND ND
1,2,3-Trichloropropane NL ND ND ND ND ND ND
1,2,4-Trichlorobenzene 2,600 ND ND ND ND ND ND
1,2,4-Trimethylbenzene 7,500 ND ND ND ND ND ND
1,2-Dibromo-3-chloropropane NL ND ND ND ND ND ND
1,2-Dibromoethane (EDB) 0.002 ND ND ND ND ND ND
1,2-Dichlorobenzene 280 ND ND ND ND ND ND
1,2-Dichloroethane 1.8 ND ND ND ND ND ND
1,2-Dichloropropane 2.6 ND ND ND ND ND ND
1,3,5-Trimethylbenzene 7,300 ND ND ND ND ND ND
1,3-Dichlorobenzene 6,500 ND ND ND ND ND ND
1,3-Dichloropropane NL ND ND ND ND ND ND
1,4-Dichlorobenzene 23 ND ND ND ND ND ND
2,2-Dichloropropane NL ND ND ND ND ND ND
2-Butanone (MEK) 17,000 ND ND ND ND ND ND
2-Chlorotoluene NL ND ND ND ND ND ND
2-Hexanone 1,900 ND ND ND ND ND ND
4-Chlorotoluene NL ND ND ND ND ND ND
4-Methyl-2-pentanone (MIBK) NL ND ND ND ND ND ND
Acetone 2,800 ND ND ND ND ND ND
Benzene 5.6 ND ND ND ND ND ND
Bromobenzene NL ND ND ND ND ND ND
Bromochloromethane NL ND ND ND ND ND ND
Bromodichloromethane NL ND ND ND ND ND ND
Bromoform 28 ND ND ND ND ND ND
Bromomethane NL ND ND ND ND ND ND
Carbon tetrachloride NL ND ND ND ND ND ND
Chlorobenzene 440 ND ND ND ND ND ND
Chloroethane NL ND ND ND ND ND ND
Chloroform 370 ND ND ND ND ND ND
Chloromethane 20 ND ND ND ND ND ND
Dibromochloromethane 2.2 ND ND ND ND ND ND
Dibromomethane NL ND ND ND ND ND ND
Dichlorodifluoromethane 306,000 ND ND ND ND ND ND
Diisopropyl ether 370 ND ND ND ND ND ND
Ethylbenzene 4,600 ND ND ND ND ND ND
Hexachloro-1,3-butadiene NL ND ND ND ND ND ND
Isopropylbenzene (Cumene) 1,700 ND ND ND ND ND ND
Methyl-tert-butyl ether 920 ND ND ND ND ND ND
Methylene Chloride 20 ND ND ND ND ND ND
Naphthalene NL ND ND ND ND ND ND
Styrene 2,200 ND ND ND ND ND ND
Tetrachloroethene 7.4 ND ND ND ND ND ND
Notes appear on final page.
Table 4

Volatile Organics (µg/kg) Soil to GW

(Method 8260) MSCCs
Toluene 7,300 ND ND ND ND ND ND
Trichloroethene 18 ND ND ND ND ND ND
Trichlorofluoromethane 31,000 ND ND ND ND ND ND
Vinyl acetate NL ND ND ND ND ND ND
Vinyl chloride 0.094 ND ND ND ND ND ND
cis-1,2-Dichloroethene 350 ND ND ND ND ND ND
cis-1,3-Dichloropropene NL ND ND ND ND ND ND
m&p-Xylene 5,000 ND ND ND ND ND ND
n-Butylbenzene 4,300 ND ND ND ND ND ND
n-Propylbenzene NL ND ND ND ND ND ND
o-Xylene 5,000 ND ND ND ND ND ND
p-Isopropyltoluene NL ND ND ND ND ND ND
sec-Butylbenzene 3,300 ND ND ND ND ND ND
tert-Butylbenzene 3,400 ND ND ND ND ND ND
trans-1,2-Dichloroethene 540 ND ND ND ND ND ND
trans-1,3-Dichloropropene 1 ND ND ND ND ND ND
Semi-Volatile Organics (µg/kg)
(Method 8270)
1,2,4-Trichlorobenzene NL ND ND ND ND ND ND
1,2-Dichlorobenzene NL ND ND ND ND ND ND
1-Methylnaphthalene NL ND ND ND ND ND ND
2,4,5-Trichlorophenol NL ND ND ND ND ND ND
2,4,6-Trichlorophenol NL ND ND ND ND ND ND
2,4-Dichlorophenol NL ND ND ND ND ND ND
2,4-Dimethylphenol 900 ND ND ND ND ND ND
2,4-Dinitrophenol NL ND ND ND ND ND ND
2,4-Dinitrotoluene NL ND ND ND ND ND ND
2,6-Dinitrotoluene NL ND ND ND ND ND ND
2-Chloronaphthalene NL ND ND ND ND ND ND
2-Chlorophenol NL ND ND ND ND ND ND
2-Methylnaphthalene 1,700 ND ND ND ND ND ND
2-Methylphenol(o-Cresol) NL ND ND ND ND ND ND
2-Nitroaniline NL ND ND ND ND ND ND
2-Nitrophenol NL ND ND ND ND ND ND
3&4-Methylphenol(m&p Cresol) NL ND ND ND ND ND ND
3,3'-Dichlorobenzidine NL ND ND ND ND ND ND
4,6-Dinitro-2-methylphenol NL ND ND ND ND ND ND
4-Bromophenylphenyl ether NL ND ND ND ND ND ND
4-Chloro-3-methylphenol NL ND ND ND ND ND ND
4-Chloroaniline NL ND ND ND ND ND ND
4-Chlorophenylphenyl ether NL ND ND ND ND ND ND
4-Nitrophenol NL ND ND ND ND ND ND
Acenaphthene 8,200 ND ND ND ND ND ND
Acenaphthylene 11,000 ND ND ND ND ND ND
Anthracene 1,000,000 ND ND ND ND ND ND
Table 4

Semi-Volatile Organics (µg/kg) Soil to GW

(Method 8270) MSCCs
Benzo(a)anthracene 340 ND ND ND ND ND ND
Benzo(a)pyrene 91 ND ND ND ND ND ND
Benzo(b)fluoranthene 1,200 ND ND ND ND ND ND
Benzo(g,h,i)perylene 6,700,000 ND ND ND ND ND ND
Benzo(k)fluoranthene 12,000 ND ND ND ND ND ND
Benzoic Acid 110,000 ND ND ND ND ND ND
Benzyl alcohol NL ND ND ND ND ND ND
Butylbenzylphthalate NL ND ND ND ND ND ND
Chrysene 38,000 ND ND ND ND ND ND
Di-n-butylphthalate NL ND ND ND ND ND ND
Di-n-octylphthalate NL ND ND ND ND ND ND
Dibenz(a,h)anthracene 170 ND ND ND ND ND ND
Dibenzofuran 4,700 ND ND ND ND ND ND
Diethylphthalate NL ND ND ND ND ND ND
Dimethylphthalate NL ND ND ND ND ND ND
Fluoranthene 280,000 ND ND ND ND ND ND
Fluorene 44,000 ND ND ND ND ND ND
Hexachloro-1,3-butadiene 260 ND ND ND ND ND ND
Hexachlorobenzene NL ND ND ND ND ND ND
Hexachlorocyclopentadiene NL ND ND ND ND ND ND
Hexachloroethane NL ND ND ND ND ND ND
Indeno(1,2,3-cd)pyrene 3,300 ND ND ND ND ND ND
Isophorone NL ND ND ND ND ND ND
N-Nitroso-di-n-propylamine NL ND ND ND ND ND ND
N-Nitrosodimethylamine NL ND ND ND ND ND ND
N-Nitrosodiphenylamine NL ND ND ND ND ND ND
Naphthalene 580 ND ND ND ND ND ND
Nitrobenzene NL ND ND ND ND ND ND
Pentachlorophenol 6.3 ND ND ND ND ND ND
Phenanthrene 60,000 ND ND ND ND ND ND
Phenol 1700 ND ND ND ND ND ND
Pyrene 290,000 ND ND ND ND ND ND
bis(2-Chloroethoxy)methane NL ND ND ND ND ND ND
bis(2-Chloroethyl) ether 0.2 ND ND ND ND ND ND
bis(2-Chloroisopropyl) ether NL ND ND ND ND ND ND
bis(2-Ethylhexyl)phthalate 5,600 ND ND ND ND ND ND
Table 4

Hydrocarbon Fractions (mg/kg) Soil to GW

(MADEP EPH) MSCCs
Aliphatic (C09-C18) 3,300 ND ND ND ND ND ND

Aliphatic (C19-C36) NL ND ND ND ND ND ND
Aromatic (C11-C22) 34 ND ND ND ND ND ND
Hydrocarbon Fractions (mg/kg)
(MADEP VPH)
Aliphatic (C05-C08) 72 ND ND ND ND ND ND
Aliphatic (C09-C12) 3,300 10.9 ND 12.6 15.3 10.3 ND
Aromatic (C09-C10) 34 2.6 ND 3.5 3.6 2.9 ND
Final VPH (mg/kg)
(Calculated)
Aliphatic (C09-C18) 3,300 8.3 ND 9.1 11.7 7.4 ND
Aromatic (C09-C22) 34 2.6 ND 3.5 3.6 2.9 ND
Notes:
ND Not detected at a concentration greater than associated method detection limit (MDL). For specific detection limits see the analyt
reports (Appendix A).
ft bgs feet below ground surface.
µg/kg micrograms per kilogram.
mg/kg milligrams per kilogram.
Soil to GW MSCCs Soil-to-Groundwater Maximum Soil Contaminant Concentrations (MSCCs) levels are from Guidelines for Assessment and Correctiv
Action for UST Releases (DENR 2008).
MADEP VPH Massachusetts Department of Environmental Protection Volatile Petroleum Hydrocarbons.
10.9 Indicates constituent was detected above the MDL.
NL Not Listed in Guidelines for Assessment and Corrective Action for UST Releases (DENR 2008).
MW-2-SB-45-R Designates duplicate sample collected simultaneousely with MW-2-SB-45
Final VPH Final VPH concentrations calculated based on Table 10, Guidelines for Assessment and Corrective Actions for UST Releases
(DENR 2008).
Table 5
Groundwater Analytical Results

Sample ID: MW-1 MW-2 MW-3 MW-3-Dup Field Blank

Constituent Date Collected: 3/25/2011 3/25/2011 3/25/2011 3/25/2011 3/25/2011
Volatile Organics (µg/L) NC GWQS GCL for GW
(Method 6200B)
1,1,1,2-Tetrachloroethane NL NL ND ND ND ND ND
1,1,1-Trichloroethane 200 200,000 ND ND ND ND ND
1,1,2,2-Tetrachloroethane 0.17 170 ND ND ND ND ND
1,1,2-Trichloroethane NL NL 1.3 ND ND ND ND
1,1-Dichloroethane 70 70,000 ND ND ND ND ND
1,1-Dichloroethene 7 7,000 ND ND ND ND ND
1,1-Dichloropropene NL NL ND ND ND ND ND
1,2,3-Trichlorobenzene NL NL ND ND ND ND ND
1,2,3-Trichloropropane NL NL ND ND ND ND ND
1,2,4-Trichlorobenzene 70 9,500 ND ND ND ND ND
1,2,4-Trimethylbenzene 350 28,500 0.50 ND ND ND ND
1,2-Dibromo-3-chloropropane NL NL ND ND ND ND ND
1,2-Dibromoethane (EDB) 0.0004 50 ND ND ND ND ND
1,2-Dichlorobenzene 24 24,000 ND ND ND ND ND
1,2-Dichloroethane 0.38 380 17.7 ND ND ND ND
1,2-Dichloropropane 0.51 510 1.5 ND ND ND ND
1,3,5-Trimethylbenzene 350 25,000 ND ND ND ND ND
1,3-Dichlorobenzene 170 61,500 ND ND ND ND ND
1,3-Dichloropropane NL NL ND ND ND ND ND
1,4-Dichlorobenzene 1.4 39,500 ND ND ND ND ND
2,2-Dichloropropane NL NL ND ND ND ND ND
2-Chlorotoluene NL NL ND ND ND ND ND
4-Chlorotoluene NL NL ND ND ND ND ND
Benzene 1 5,000 2.3 ND ND ND ND
Bromobenzene NL NL ND ND ND ND ND
Bromochloromethane NL NL ND ND ND ND ND
Bromodichloromethane NL NL ND ND ND ND ND
Bromoform 0.19 190 ND ND ND ND ND
Bromomethane NL NL ND ND ND ND ND
Carbon tetrachloride NL NL ND ND ND ND ND
Chlorobenzene 50 5,000 ND ND ND ND ND
Chloroethane NL NL ND ND ND ND ND
Chloroform 70 70,000 ND 1.6 1.5 1.5 ND
Chloromethane 2.6 2,600 ND ND ND ND ND
Dibromochloromethane 0.41 410 ND ND ND ND ND
Dibromomethane NL NL ND ND ND ND ND
Dichlorodifluoromethane 1,400 140,000 ND ND ND ND ND
Diisopropyl ether 70 70,000 195 ND ND ND ND
Ethanol NL NL ND ND ND ND ND
Ethylbenzene 550 84,500 1.8 ND ND ND ND
Hexachloro-1,3-butadiene NL NL ND ND ND ND ND
Isopropylbenzene (Cumene) 70 25,000 ND ND ND ND ND
Methyl-tert-butyl ether 200 200,000 1.3 ND ND ND ND
Methylene Chloride 4.6 4600 ND ND ND ND ND
Naphthalene 21 15,500 3.9 ND ND ND ND
Table 5


Volatile Organics (µg/L) NC GWQS GCL for GW
(Method 6200B)
Styrene 100 100,000 ND ND ND ND ND
Tetrachloroethene 0.7 700 ND ND ND ND ND
Toluene 1000 257,500 ND ND ND ND ND
Trichloroethene 2.8 2,800 ND ND ND ND ND
Trichlorofluoromethane 2,100 2,100,000 ND ND ND ND ND
Vinyl chloride 0.015 15 ND ND ND ND ND
cis-1,2-Dichloroethene 70 70,000 ND ND ND ND ND
cis-1,3-Dichloropropene 0.19 190 ND ND ND ND ND
m&p-Xylene 530 87,500 ND ND ND ND ND
n-Butylbenzene 70 6,900 ND ND ND ND ND
n-Propylbenzene 70 30,000 ND ND ND ND ND
o-Xylene 530 87,500 0.71 ND ND ND ND
sec-Butylbenzene 70 8,500 ND ND ND ND ND
tert-Butylbenzene 70 15,000 ND ND ND ND ND
trans-1,2-Dichloroethene 100 100,000 ND ND ND ND ND
trans-1,3-Dichloropropene 0.19 190 ND ND ND ND ND
Semi-Volatile Organics (µg/L)
(Method 625)
1,2,4-Trichlorobenzene NL NL ND ND ND ND ND
2,4,6-Trichlorophenol NL NL ND ND ND ND ND
2,4-Dichlorophenol NL NL ND ND ND ND ND
2,4-Dimethylphenol 140 140,000 ND ND ND ND ND
2,4-Dinitrophenol NL NL ND ND ND ND ND
2,4-Dinitrotoluene NL NL ND ND ND ND ND
2,6-Dinitrotoluene NL NL ND ND ND ND ND
2-Chloronaphthalene NL NL ND ND ND ND ND
2-Chlorophenol NL NL ND ND ND ND ND
2-Nitrophenol NL NL ND ND ND ND ND
3,3'-Dichlorobenzidine NL NL ND ND ND ND ND
4,6-Dinitro-2-methylphenol NL NL ND ND ND ND ND
4-Bromophenylphenyl ether NL NL ND ND ND ND ND
4-Chloro-3-methylphenol NL NL ND ND ND ND ND
4-Chlorophenylphenyl ether NL NL ND ND ND ND ND
4-Nitrophenol NL NL ND ND ND ND ND
Acenaphthene 80 2,120 ND ND ND ND ND
Acenaphthylene 210 1,965 ND ND ND ND ND
Anthracene 2,100 2,100 ND ND ND ND ND
Benzo(a)anthracene 0.0479 22 ND ND ND ND ND
Benzo(a)pyrene 0.00479 1.5 ND ND ND ND ND
Benzo(b)fluoranthene 0.0479 0.4 ND ND ND ND ND
Benzo(g,h,i)perylene 210 210 ND ND ND ND ND
Benzo(k)fluoranthene 0.479 0.6 ND ND ND ND ND
Butylbenzylphthalate NL NL ND ND ND ND ND
Chrysene 4.79 4.79 ND ND ND ND ND
Di-n-butylphthalate NL NL ND ND ND ND ND
Di-n-octylphthalate NL NL ND ND ND ND ND
Table 5


Semi-Volatile Organics (µg/L) NC GWQS GCL for GW
(Method 625)
Dibenz(a,h)anthracene 0.0047 0.25 ND ND ND ND ND
Diethylphthalate NL NL ND ND ND ND ND
Dimethylphthalate NL NL ND ND ND ND ND
Fluoranthene 280 280 ND ND ND ND ND
Fluorene 280 950 ND ND ND ND ND
Hexachloro-1,3-butadiene 0.44 440 ND ND ND ND ND
Hexachlorobenzene NL NL ND ND ND ND ND
Hexachlorocyclopentadiene NL NL ND ND ND ND ND
Hexachloroethane NL NL ND ND ND ND ND
Indeno(1,2,3-cd)pyrene 0.047 31 ND ND ND ND ND
Isophorone NL NL ND ND ND ND ND
N-Nitroso-di-n-propylamine NL NL ND ND ND ND ND
N-Nitrosodimethylamine NL NL ND ND ND ND ND
N-Nitrosodiphenylamine NL NL ND ND ND ND ND
Naphthalene 21 15,500 ND ND ND ND ND
Nitrobenzene NL NL ND ND ND ND ND
Pentachlorophenol 0.29 290 ND ND ND ND ND
Phenanthrene 210 410 ND ND ND ND ND
Phenol 300 300,000 ND ND ND ND ND
Pyrene 210 210 ND ND ND ND ND
bis(2-Chloroethoxy)methane NL NL ND ND ND ND ND
bis(2-Chloroethyl) ether 0.0031 31 ND ND ND ND ND
bis(2-Chloroisopropyl) ether NL NL ND ND ND ND ND
bis(2-Ethylhexyl)phthalate 2.5 2,500 ND ND ND ND ND
Table 5


Lead (µg/L) NC GWQS GCL for GW
(Method 200.7)
Lead 15 15000 ND ND ND ND ND
Hydrocarbon Fractions (µg/L)
(MADEP EPH)
Aliphatic (C09-C18) 4,200 NL ND ND ND ND ND
Aliphatic (C19-C36) 42,000 NL ND ND ND ND ND
Aromatic (C11-C22) 210 NL ND ND ND ND ND
Hydrocarbon Fractions (µg/L)
(MADEP VPH)
Aliphatic (C05-C08) 420 NL ND 260 ND ND ND
Aliphatic (C09-C12) 4,200 NL ND 737 ND ND ND
Aromatic (C09-C10) 210 NL ND 153 ND ND ND
Final VPH (µg/L)
(Calculated)
Aliphatic (C09-C18) 4,200 NL ND 584 ND ND ND
Aromatic (C09-C22) 210 NL ND 153 ND ND ND
Notes:
ND Not detected at a concentration greater than associated method detection limit (MDL). For specific detection limits see
the analytical reports (Appendix A).
µg/L micrograms per liter.
NC GWQS North Carolina Groundwater Quaility Standards (NC GWQS) levels are from Guidelines for Assessment and Corrective
GCL for GW Gross Contaminant Levels (GCLs) for Groundwater (are from Guidelines for Assessment and Corrective
MADEP VPH Massachusetts Department of Environmental Protection Volatile Petroleum Hydrocarbons.
260 Indicates constituent was detected above the associated MDL.
195 Indicates constituent was detected above the associated NC GWQS.
NL Not Listed in Guidelines for Assessment and Corrective Action for UST Releases (DENR 2008).
MW-3-Dup Designates duplicate sample collected from monitoring well MW-3.
Final VPH Final VPH Concentrations calculated based on Table 10, Guidelines for Assessment and Corrective Actions for UST
Releases (DENR 2008).
APPENDICES
APPENDIX A
Laboratory Analytical Reports and Chain-of-Custody

Documentation Forms
Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
(336)623-8921 (828)254-7176 (704)875-9092
LIMS USE: FR - LISA MANNING

LIMS OBJECT ID: 9290652
April 07, 2011
Ms. Lisa Manning

Altamont Environmental
231 Haywood St.
Asheville, NC 28801
RE: Project: McGill Kings Mountain 03/24

Pace Project No.: 9290652
Dear Ms. Manning:

Enclosed are the analytical results for sample(s) received by the laboratory on March 24, 2011. The
results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lorri Patton
lorri.patton@pacelabs.com
Project Manager
Enclosures
cc: Mr. Adam Tripp, Altamont Environmental
REPORT OF LABORATORY ANALYSIS Page 1 of 133
This report shall not be reproduced, except in full,

without the written consent of Pace Analytical Services, Inc..
(336)623-8921 (828)254-7176 (704)875-9092
CERTIFICATIONS
Project: McGill Kings Mountain 03/24

Charlotte Certification IDs

9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Drinking Water Cert. #: 99006003
Louisiana/LELAP Certification #: 04034 Virginia Certification #: 00213
New Jersey Certification #: NC012 Connecticut Certification #: PH-0104
North Carolina Drinking Water Certification #: 37706 Florida/NELAP Certification #: E87627
North Carolina Field Services Certification #: 5342 Kentucky UST Certification #: 84
North Carolina Wastewater Certification #: 12 Louisiana DHH Drinking Water # LA 100031
Pennsylvania Certification #: 68-00784 West Virginia Certification #: 357
South Carolina Certification #: 99006001

(336)623-8921 (828)254-7176 (704)875-9092
SAMPLE ANALYTE COUNT

Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
9290652001 SB-1 EPA 8015 Modified AW 2 PASI-C

ASTM D2974-87 KDF 1 PASI-C
9290652010 SB-5R EPA 8015 Modified AW 2 PASI-C
9290652012 SB-11 EPA 8015 Modified CAH 2 PASI-C
EPA 8015 Modified AW 2 PASI-C
9290652014 SB-FP-1 EPA 8015 Modified AW 2 PASI-C

(336)623-8921 (828)254-7176 (704)875-9092

Analytes

9290652021 SB-36-R EPA 8015 Modified CAH 2 PASI-C
9290652023 SB-FP-3 EPA 8015 Modified CAH 2 PASI-C

(336)623-8921 (828)254-7176 (704)875-9092

Analytes

9290652033 SB-PL-13 EPA 8015 Modified CAH 2 PASI-C

(336)623-8921 (828)254-7176 (704)875-9092

Analytes

9290652045 SB-30-EQR EPA 8015 Modified CAH 2 PASI-C
EPA 5030/8015 Mod. AW 2 PASI-C
9290652052 MW-02-SB-10 MADEP EPH RES 5 PASI-C
MADEP VPH AW 5 PASI-C
EPA 8270 BPJ 73 PASI-C
EPA 8260 DLK 70 PASI-C

(336)623-8921 (828)254-7176 (704)875-9092

Analytes

9290652058 MW-02-SB-BQR MADEP EPH RES 5 PASI-C
EPA 8260 MCK 63 PASI-C
9290652059 MW-02-SB-45-R MADEP EPH RES 5 PASI-C
9290652060 TRIP BLANK EPA 8260 MCK 63 PASI-C

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

Sample: SB-1 Lab ID: 9290652001 Collected: 03/22/11 11:20 Received: 03/24/11 17:15 Matrix: Solid
Results reported on a "dry-weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Gasoline Range Organics Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics ND mg/kg 5.5 1 03/29/11 14:51 03/29/11 20:24 8006-61-9
4-Bromofluorobenzene (S) 137 % 70-167 1 03/29/11 14:51 03/29/11 20:24 460-00-4
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 16.9 % 0.10 1 03/28/11 14:15
Date: 04/07/2011 04:17 PM REPORT OF LABORATORY ANALYSIS Page 8 of 133

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

Sample: SB-5R Lab ID: 9290652010 Collected: 03/22/11 13:36 Received: 03/24/11 17:15 Matrix: Solid

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

4-Bromofluorobenzene (S) 168 % 70-167 1 03/29/11 14:51 03/30/11 00:31 460-00-4 S3

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

8015 GCS THC-Diesel Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components ND mg/kg 5.9 1 03/30/11 11:15 03/31/11 18:44 68334-30-5

n-Pentacosane (S) 85 % 41-119 1 03/30/11 11:15 03/31/11 18:44 629-99-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


n-Pentacosane (S) 91 % 41-119 1 03/30/11 11:15 03/31/11 19:18 629-99-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

Sample: SB-FP-1 Lab ID: 9290652014 Collected: 03/22/11 12:30 Received: 03/24/11 17:15 Matrix: Solid
Gasoline Range Organics 1960 mg/kg 58.7 10 03/29/11 14:51 03/30/11 01:46 8006-61-9

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

Gasoline Range Organics 42.5 mg/kg 5.2 1 03/29/11 14:51 03/30/11 03:00 8006-61-9

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


n-Pentacosane (S) 88 % 41-119 1 03/30/11 11:15 03/31/11 19:18 629-99-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


n-Pentacosane (S) 85 % 41-119 1 03/30/11 11:15 03/31/11 19:53 629-99-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

Diesel Components 68.8 mg/kg 6.1 1 03/30/11 11:15 03/31/11 20:27 68334-30-5
n-Pentacosane (S) 108 % 41-119 1 03/30/11 11:15 03/31/11 20:27 629-99-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

Sample: SB-36-R Lab ID: 9290652021 Collected: 03/23/11 18:17 Received: 03/24/11 17:15 Matrix: Solid
Diesel Components 115 mg/kg 6.1 1 03/30/11 11:15 04/01/11 16:20 68334-30-5
n-Pentacosane (S) 96 % 41-119 1 03/30/11 11:15 04/01/11 16:20 629-99-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

n-Pentacosane (S) 90 % 41-119 1 03/30/11 11:15 03/31/11 21:01 629-99-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

n-Pentacosane (S) 109 % 41-119 1 03/30/11 11:15 04/01/11 16:55 629-99-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


n-Pentacosane (S) 85 % 41-119 1 03/30/11 14:45 04/01/11 02:10 629-99-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

n-Pentacosane (S) 0 % 41-119 10 03/30/11 14:45 04/01/11 18:38 629-99-2 S4

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

n-Pentacosane (S) 100 % 41-119 1 03/30/11 14:45 04/01/11 19:13 629-99-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


n-Pentacosane (S) 89 % 41-119 1 03/30/11 14:45 04/01/11 02:45 629-99-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


n-Pentacosane (S) 77 % 41-119 1 03/30/11 14:45 04/01/11 03:19 629-99-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


n-Pentacosane (S) 91 % 41-119 1 03/30/11 14:45 04/01/11 03:19 629-99-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


n-Pentacosane (S) 95 % 41-119 1 03/30/11 14:45 04/01/11 03:53 629-99-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

n-Pentacosane (S) 84 % 41-119 1 03/30/11 14:45 04/01/11 03:53 629-99-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

n-Pentacosane (S) 93 % 41-119 1 03/30/11 14:45 04/01/11 19:47 629-99-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

Sample: SB-PL-13 Lab ID: 9290652033 Collected: 03/23/11 14:58 Received: 03/24/11 17:15 Matrix: Solid

n-Pentacosane (S) 87 % 41-119 1 03/30/11 14:45 04/01/11 04:27 629-99-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


n-Pentacosane (S) 74 % 41-119 1 03/30/11 14:45 04/01/11 05:02 629-99-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


n-Pentacosane (S) 72 % 41-119 1 03/30/11 14:45 04/01/11 05:02 629-99-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


n-Pentacosane (S) 83 % 41-119 1 03/30/11 14:45 04/01/11 05:36 629-99-2
Gasoline Range Organics 8.3 mg/kg 6.4 1 03/31/11 15:37 04/01/11 02:27 8006-61-9

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


n-Pentacosane (S) 78 % 41-119 1 03/30/11 14:45 04/01/11 05:36 629-99-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


n-Pentacosane (S) 86 % 41-119 1 03/30/11 14:45 04/01/11 06:10 629-99-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


n-Pentacosane (S) 99 % 41-119 1 03/30/11 14:45 04/01/11 06:44 629-99-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


n-Pentacosane (S) 86 % 41-119 1 03/30/11 14:45 04/01/11 07:18 629-99-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


n-Pentacosane (S) 74 % 41-119 1 03/30/11 14:45 04/01/11 07:18 629-99-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


n-Pentacosane (S) 77 % 41-119 1 03/30/11 14:45 04/01/11 07:53 629-99-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


n-Pentacosane (S) 79 % 41-119 1 03/30/11 14:45 04/01/11 07:53 629-99-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


n-Pentacosane (S) 67 % 41-119 1 04/01/11 11:15 04/03/11 16:07 629-99-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

Sample: SB-30-EQR Lab ID: 9290652045 Collected: 03/23/11 17:30 Received: 03/24/11 17:15 Matrix: Water
8015 GCS THC-Diesel for SP Analytical Method: EPA 8015 Modified Preparation Method: EPA 3535
Diesel Components ND mg/L 0.62 1 03/30/11 15:30 04/01/11 14:03 68334-30-5

n-Pentacosane (S) 91 % 48-110 1 03/30/11 15:30 04/01/11 14:03 629-99-2
Gasoline Range Organics Analytical Method: EPA 5030/8015 Mod.
Gasoline Range Organics ND mg/L 0.080 1 03/29/11 00:39 8006-61-9

4-Bromofluorobenzene (S) 142 % 70-145 1 03/29/11 00:39 460-00-4

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

n-Pentacosane (S) 0 % 41-119 10 04/01/11 11:15 04/04/11 11:00 629-99-2 S4

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

n-Pentacosane (S) 69 % 41-119 1 04/01/11 11:15 04/03/11 16:41 629-99-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

Diesel Components 605 mg/kg 31.7 1 04/01/11 11:15 04/03/11 16:41 68334-30-5 P3
n-Pentacosane (S) 0 % 41-119 1 04/01/11 11:15 04/03/11 16:41 629-99-2 S4

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

Diesel Components 41300 mg/kg 1480 20 04/01/11 11:15 04/04/11 14:45 68334-30-5 P3
n-Pentacosane (S) 0 % 41-119 20 04/01/11 11:15 04/04/11 14:45 629-99-2 S4

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


n-Pentacosane (S) 80 % 41-119 1 04/01/11 11:15 04/03/11 17:15 629-99-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


n-Pentacosane (S) 79 % 41-119 1 04/01/11 11:15 04/03/11 17:50 629-99-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

Sample: MW-02-SB-10 Lab ID: 9290652052 Collected: 03/23/11 11:30 Received: 03/24/11 17:15 Matrix: Solid
MADEP EPH NC Soil Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18) ND mg/kg 12.7 1 03/29/11 13:30 03/30/11 20:51 N2

Aromatic (C11-C22) ND mg/kg 12.7 1 03/29/11 13:30 03/30/11 20:51 N2
Nonatriacontane (S) 85 % 40-140 1 03/29/11 13:30 03/30/11 20:51 7194-86-7
o-Terphenyl (S) 92 % 40-140 1 03/29/11 13:30 03/30/11 20:51 84-15-1
VPH NC Soil Analytical Method: MADEP VPH Preparation Method: MADEP VPH

Aliphatic (C09-C12) 10.9 mg/kg 1.7 1 04/05/11 17:47 04/05/11 19:22 N2
Aromatic (C09-C10) 2.6 mg/kg 1.7 1 04/05/11 17:47 04/05/11 19:22 N2
2,5-Dibromotoluene (PID)(S) 160 % 70-130 1 04/05/11 17:47 04/05/11 19:22 1g
2,5-Dibromotoluene (FID)(S) 149 % 70-130 1 04/05/11 17:47 04/05/11 19:22 1g
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 83-32-9

Acenaphthylene ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 208-96-8
Anthracene ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 120-12-7
Benzo(a)anthracene ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 56-55-3
Benzo(a)pyrene ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 50-32-8
Benzo(b)fluoranthene ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 205-99-2
Benzo(g,h,i)perylene ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 191-24-2
Benzo(k)fluoranthene ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 207-08-9
Benzoic Acid ND ug/kg 2070 1 03/29/11 11:30 03/29/11 18:27 65-85-0
Benzyl alcohol ND ug/kg 828 1 03/29/11 11:30 03/29/11 18:27 100-51-6
4-Bromophenylphenyl ether ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 101-55-3
Butylbenzylphthalate ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 85-68-7
4-Chloro-3-methylphenol ND ug/kg 828 1 03/29/11 11:30 03/29/11 18:27 59-50-7
4-Chloroaniline ND ug/kg 2070 1 03/29/11 11:30 03/29/11 18:27 106-47-8
bis(2-Chloroethoxy)methane ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 111-91-1
bis(2-Chloroethyl) ether ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 111-44-4
bis(2-Chloroisopropyl) ether ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 108-60-1
2-Chloronaphthalene ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 91-58-7
2-Chlorophenol ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 95-57-8
4-Chlorophenylphenyl ether ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 7005-72-3
Chrysene ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 218-01-9
Dibenz(a,h)anthracene ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 53-70-3
Dibenzofuran ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 132-64-9
1,2-Dichlorobenzene ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 95-50-1
3,3'-Dichlorobenzidine ND ug/kg 2070 1 03/29/11 11:30 03/29/11 18:27 91-94-1
2,4-Dichlorophenol ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 120-83-2
Diethylphthalate ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 84-66-2
2,4-Dimethylphenol ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 105-67-9
Dimethylphthalate ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 131-11-3

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

Di-n-butylphthalate ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 84-74-2

4,6-Dinitro-2-methylphenol ND ug/kg 828 1 03/29/11 11:30 03/29/11 18:27 534-52-1
2,4-Dinitrophenol ND ug/kg 2070 1 03/29/11 11:30 03/29/11 18:27 51-28-5
2,4-Dinitrotoluene ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 121-14-2
Di-n-octylphthalate ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 117-84-0
bis(2-Ethylhexyl)phthalate ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 117-81-7
Fluoranthene ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 206-44-0
Fluorene ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 86-73-7
Hexachloro-1,3-butadiene ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 87-68-3
Hexachlorobenzene ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 118-74-1
Hexachlorocyclopentadiene ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 77-47-4
Hexachloroethane ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 67-72-1
Indeno(1,2,3-cd)pyrene ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 193-39-5
Isophorone ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 78-59-1
1-Methylnaphthalene ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 90-12-0
2-Methylphenol(o-Cresol) ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 95-48-7
3&4-Methylphenol(m&p Cresol) ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27
Naphthalene ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 91-20-3
2-Nitroaniline ND ug/kg 2070 1 03/29/11 11:30 03/29/11 18:27 88-74-4
Nitrobenzene ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 98-95-3
2-Nitrophenol ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 88-75-5
N-Nitrosodimethylamine ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 62-75-9
N-Nitroso-di-n-propylamine ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 621-64-7
N-Nitrosodiphenylamine ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 86-30-6
Pentachlorophenol ND ug/kg 2070 1 03/29/11 11:30 03/29/11 18:27 87-86-5
Phenanthrene ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 85-01-8
Phenol ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 108-95-2
Pyrene ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 129-00-0
1,2,4-Trichlorobenzene ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 120-82-1
2,4,5-Trichlorophenol ND ug/kg 414 1 03/29/11 11:30 03/29/11 18:27 95-95-4
Nitrobenzene-d5 (S) 68 % 23-110 1 03/29/11 11:30 03/29/11 18:27 4165-60-0
2-Fluorobiphenyl (S) 66 % 30-110 1 03/29/11 11:30 03/29/11 18:27 321-60-8
Terphenyl-d14 (S) 82 % 28-110 1 03/29/11 11:30 03/29/11 18:27 1718-51-0
Phenol-d6 (S) 60 % 22-110 1 03/29/11 11:30 03/29/11 18:27 13127-88-3
2-Fluorophenol (S) 58 % 13-110 1 03/29/11 11:30 03/29/11 18:27 367-12-4
2,4,6-Tribromophenol (S) 57 % 27-110 1 03/29/11 11:30 03/29/11 18:27 118-79-6
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 104 1 03/29/11 08:53 67-64-1

Benzene ND ug/kg 5.2 1 03/29/11 08:53 71-43-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

Bromobenzene ND ug/kg 5.2 1 03/29/11 08:53 108-86-1

Bromochloromethane ND ug/kg 5.2 1 03/29/11 08:53 74-97-5
Bromodichloromethane ND ug/kg 5.2 1 03/29/11 08:53 75-27-4
Bromoform ND ug/kg 5.2 1 03/29/11 08:53 75-25-2
Bromomethane ND ug/kg 10.4 1 03/29/11 08:53 74-83-9
2-Butanone (MEK) ND ug/kg 104 1 03/29/11 08:53 78-93-3
n-Butylbenzene ND ug/kg 5.2 1 03/29/11 08:53 104-51-8
sec-Butylbenzene ND ug/kg 5.2 1 03/29/11 08:53 135-98-8
tert-Butylbenzene ND ug/kg 5.2 1 03/29/11 08:53 98-06-6
Carbon tetrachloride ND ug/kg 5.2 1 03/29/11 08:53 56-23-5
Chlorobenzene ND ug/kg 5.2 1 03/29/11 08:53 108-90-7
Chloroethane ND ug/kg 10.4 1 03/29/11 08:53 75-00-3
Chloroform ND ug/kg 5.2 1 03/29/11 08:53 67-66-3
Chloromethane ND ug/kg 10.4 1 03/29/11 08:53 74-87-3
2-Chlorotoluene ND ug/kg 5.2 1 03/29/11 08:53 95-49-8
1,2-Dibromo-3-chloropropane ND ug/kg 5.2 1 03/29/11 08:53 96-12-8
Dibromochloromethane ND ug/kg 5.2 1 03/29/11 08:53 124-48-1
1,2-Dibromoethane (EDB) ND ug/kg 5.2 1 03/29/11 08:53 106-93-4
Dibromomethane ND ug/kg 5.2 1 03/29/11 08:53 74-95-3
1,2-Dichlorobenzene ND ug/kg 5.2 1 03/29/11 08:53 95-50-1
Dichlorodifluoromethane ND ug/kg 10.4 1 03/29/11 08:53 75-71-8
1,1-Dichloroethane ND ug/kg 5.2 1 03/29/11 08:53 75-34-3
1,1-Dichloroethene ND ug/kg 5.2 1 03/29/11 08:53 75-35-4
cis-1,2-Dichloroethene ND ug/kg 5.2 1 03/29/11 08:53 156-59-2
trans-1,2-Dichloroethene ND ug/kg 5.2 1 03/29/11 08:53 156-60-5
1,2-Dichloropropane ND ug/kg 5.2 1 03/29/11 08:53 78-87-5
1,1-Dichloropropene ND ug/kg 5.2 1 03/29/11 08:53 563-58-6
cis-1,3-Dichloropropene ND ug/kg 5.2 1 03/29/11 08:53 10061-01-5
trans-1,3-Dichloropropene ND ug/kg 5.2 1 03/29/11 08:53 10061-02-6
Diisopropyl ether ND ug/kg 5.2 1 03/29/11 08:53 108-20-3
Ethylbenzene ND ug/kg 5.2 1 03/29/11 08:53 100-41-4
Hexachloro-1,3-butadiene ND ug/kg 5.2 1 03/29/11 08:53 87-68-3
2-Hexanone ND ug/kg 52.1 1 03/29/11 08:53 591-78-6
Isopropylbenzene (Cumene) ND ug/kg 5.2 1 03/29/11 08:53 98-82-8
p-Isopropyltoluene ND ug/kg 5.2 1 03/29/11 08:53 99-87-6
Methylene Chloride ND ug/kg 20.8 1 03/29/11 08:53 75-09-2
4-Methyl-2-pentanone (MIBK) ND ug/kg 52.1 1 03/29/11 08:53 108-10-1
Methyl-tert-butyl ether ND ug/kg 5.2 1 03/29/11 08:53 1634-04-4
Naphthalene ND ug/kg 5.2 1 03/29/11 08:53 91-20-3
n-Propylbenzene ND ug/kg 5.2 1 03/29/11 08:53 103-65-1

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

Styrene ND ug/kg 5.2 1 03/29/11 08:53 100-42-5

1,1,1,2-Tetrachloroethane ND ug/kg 5.2 1 03/29/11 08:53 630-20-6
Tetrachloroethene ND ug/kg 5.2 1 03/29/11 08:53 127-18-4
Toluene ND ug/kg 5.2 1 03/29/11 08:53 108-88-3
1,2,3-Trichlorobenzene ND ug/kg 5.2 1 03/29/11 08:53 87-61-6
1,1,1-Trichloroethane ND ug/kg 5.2 1 03/29/11 08:53 71-55-6
Trichloroethene ND ug/kg 5.2 1 03/29/11 08:53 79-01-6
Trichlorofluoromethane ND ug/kg 5.2 1 03/29/11 08:53 75-69-4
1,2,3-Trichloropropane ND ug/kg 5.2 1 03/29/11 08:53 96-18-4
1,2,4-Trimethylbenzene ND ug/kg 5.2 1 03/29/11 08:53 95-63-6
Vinyl acetate ND ug/kg 52.1 1 03/29/11 08:53 108-05-4
Vinyl chloride ND ug/kg 10.4 1 03/29/11 08:53 75-01-4
m&p-Xylene ND ug/kg 10.4 1 03/29/11 08:53 179601-23-1
o-Xylene ND ug/kg 5.2 1 03/29/11 08:53 95-47-6
Dibromofluoromethane (S) 98 % 70-130 1 03/29/11 08:53 1868-53-7
Toluene-d8 (S) 99 % 70-130 1 03/29/11 08:53 2037-26-5
1,2-Dichloroethane-d4 (S) 90 % 70-132 1 03/29/11 08:53 17060-07-0

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


o-Terphenyl (S) 81 % 40-140 1 03/29/11 13:30 03/30/11 21:27 84-15-1

2,5-Dibromotoluene (PID)(S) 131 % 70-130 1 04/05/11 17:47 04/05/11 19:47 1g
2,5-Dibromotoluene (FID)(S) 129 % 70-130 1 04/05/11 17:47 04/05/11 19:47

Chrysene ND ug/kg 383 1 03/29/11 11:30 03/29/11 18:55 218-01-9

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


Fluorene ND ug/kg 383 1 03/29/11 11:30 03/29/11 18:55 86-73-7
Phenol ND ug/kg 383 1 03/29/11 11:30 03/29/11 18:55 108-95-2
Pyrene ND ug/kg 383 1 03/29/11 11:30 03/29/11 18:55 129-00-0
Nitrobenzene-d5 (S) 54 % 23-110 1 03/29/11 11:30 03/29/11 18:55 4165-60-0
Terphenyl-d14 (S) 76 % 28-110 1 03/29/11 11:30 03/29/11 18:55 1718-51-0
Phenol-d6 (S) 51 % 22-110 1 03/29/11 11:30 03/29/11 18:55 13127-88-3
2-Fluorophenol (S) 52 % 13-110 1 03/29/11 11:30 03/29/11 18:55 367-12-4
Acetone ND ug/kg 117 1 03/30/11 17:16 67-64-1

Benzene ND ug/kg 5.9 1 03/30/11 17:16 71-43-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


2-Hexanone ND ug/kg 58.7 1 03/30/11 17:16 591-78-6

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

Styrene ND ug/kg 5.9 1 03/30/11 17:16 100-42-5

Toluene ND ug/kg 5.9 1 03/30/11 17:16 108-88-3
m&p-Xylene ND ug/kg 11.7 1 03/30/11 17:16 179601-23-1
o-Xylene ND ug/kg 5.9 1 03/30/11 17:16 95-47-6
Toluene-d8 (S) 103 % 70-130 1 03/30/11 17:16 2037-26-5

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


o-Terphenyl (S) 89 % 40-140 1 03/29/11 13:30 03/31/11 17:37 84-15-1
2-Bromonaphthalene (S) 124 % 40-140 1 03/29/11 13:30 03/31/11 17:37 580-13-2

2,5-Dibromotoluene (PID)(S) 127 % 70-130 1 04/05/11 17:47 04/05/11 20:12

Chrysene ND ug/kg 388 1 03/29/11 11:30 03/29/11 19:22 218-01-9

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


Fluorene ND ug/kg 388 1 03/29/11 11:30 03/29/11 19:22 86-73-7
Phenol ND ug/kg 388 1 03/29/11 11:30 03/29/11 19:22 108-95-2
Pyrene ND ug/kg 388 1 03/29/11 11:30 03/29/11 19:22 129-00-0
Nitrobenzene-d5 (S) 56 % 23-110 1 03/29/11 11:30 03/29/11 19:22 4165-60-0
Terphenyl-d14 (S) 79 % 28-110 1 03/29/11 11:30 03/29/11 19:22 1718-51-0
Phenol-d6 (S) 53 % 22-110 1 03/29/11 11:30 03/29/11 19:22 13127-88-3
2-Fluorophenol (S) 53 % 13-110 1 03/29/11 11:30 03/29/11 19:22 367-12-4

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

Acetone ND ug/kg 110 1 03/30/11 17:37 67-64-1

Benzene ND ug/kg 5.5 1 03/30/11 17:37 71-43-2
2-Hexanone ND ug/kg 55.2 1 03/30/11 17:37 591-78-6

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


Styrene ND ug/kg 5.5 1 03/30/11 17:37 100-42-5
Toluene ND ug/kg 5.5 1 03/30/11 17:37 108-88-3
m&p-Xylene ND ug/kg 11.0 1 03/30/11 17:37 179601-23-1
o-Xylene ND ug/kg 5.5 1 03/30/11 17:37 95-47-6
Toluene-d8 (S) 101 % 70-130 1 03/30/11 17:37 2037-26-5

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


o-Terphenyl (S) 72 % 40-140 1 03/29/11 13:30 03/30/11 22:03 84-15-1


Chrysene ND ug/kg 379 1 03/29/11 11:30 03/29/11 20:44 218-01-9

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


Fluorene ND ug/kg 379 1 03/29/11 11:30 03/29/11 20:44 86-73-7
Phenol ND ug/kg 379 1 03/29/11 11:30 03/29/11 20:44 108-95-2
Pyrene ND ug/kg 379 1 03/29/11 11:30 03/29/11 20:44 129-00-0
Nitrobenzene-d5 (S) 62 % 23-110 1 03/29/11 11:30 03/29/11 20:44 4165-60-0
Terphenyl-d14 (S) 77 % 28-110 1 03/29/11 11:30 03/29/11 20:44 1718-51-0
Phenol-d6 (S) 51 % 22-110 1 03/29/11 11:30 03/29/11 20:44 13127-88-3
2-Fluorophenol (S) 51 % 13-110 1 03/29/11 11:30 03/29/11 20:44 367-12-4
Acetone ND ug/kg 108 1 03/30/11 17:57 67-64-1

Benzene ND ug/kg 5.4 1 03/30/11 17:57 71-43-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


2-Hexanone ND ug/kg 54.1 1 03/30/11 17:57 591-78-6

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

Styrene ND ug/kg 5.4 1 03/30/11 17:57 100-42-5

Toluene ND ug/kg 5.4 1 03/30/11 17:57 108-88-3
m&p-Xylene ND ug/kg 10.8 1 03/30/11 17:57 179601-23-1
o-Xylene ND ug/kg 5.4 1 03/30/11 17:57 95-47-6
Toluene-d8 (S) 104 % 70-130 1 03/30/11 17:57 2037-26-5

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


o-Terphenyl (S) 76 % 40-140 1 03/29/11 13:30 03/30/11 22:38 84-15-1


Chrysene ND ug/kg 372 1 03/29/11 11:30 03/29/11 21:11 218-01-9

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


Fluorene ND ug/kg 372 1 03/29/11 11:30 03/29/11 21:11 86-73-7
Phenol ND ug/kg 372 1 03/29/11 11:30 03/29/11 21:11 108-95-2
Pyrene ND ug/kg 372 1 03/29/11 11:30 03/29/11 21:11 129-00-0
Nitrobenzene-d5 (S) 59 % 23-110 1 03/29/11 11:30 03/29/11 21:11 4165-60-0
Terphenyl-d14 (S) 70 % 28-110 1 03/29/11 11:30 03/29/11 21:11 1718-51-0
Phenol-d6 (S) 53 % 22-110 1 03/29/11 11:30 03/29/11 21:11 13127-88-3
2-Fluorophenol (S) 55 % 13-110 1 03/29/11 11:30 03/29/11 21:11 367-12-4
Acetone ND ug/kg 100 1 03/30/11 18:17 67-64-1

Benzene ND ug/kg 5.0 1 03/30/11 18:17 71-43-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


2-Hexanone ND ug/kg 50.0 1 03/30/11 18:17 591-78-6

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

Styrene ND ug/kg 5.0 1 03/30/11 18:17 100-42-5

Toluene ND ug/kg 5.0 1 03/30/11 18:17 108-88-3
m&p-Xylene ND ug/kg 10.0 1 03/30/11 18:17 179601-23-1
o-Xylene ND ug/kg 5.0 1 03/30/11 18:17 95-47-6
Toluene-d8 (S) 103 % 70-130 1 03/30/11 18:17 2037-26-5

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

Sample: MW-02-SB-BQR Lab ID: 9290652058 Collected: 03/23/11 08:00 Received: 03/24/11 17:15 Matrix: Water
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18) ND ug/L 118 1 04/01/11 10:30 04/01/11 22:10 N2

Aromatic (C11-C22) ND ug/L 118 1 04/01/11 10:30 04/01/11 22:10 N2
o-Terphenyl (S) 103 % 40-140 1 04/01/11 10:30 04/01/11 22:10 84-15-1
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08) ND ug/L 30.0 1 03/29/11 04:21 N2

Aromatic (C09-C10) ND ug/L 30.0 1 03/29/11 04:21 N2
2,5-Dibromotoluene (PID)(S) 95 % 70-130 1 03/29/11 04:21
2,5-Dibromotoluene (FID)(S) 97 % 70-130 1 03/29/11 04:21
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthene ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 83-32-9

Acenaphthylene ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 208-96-8
Aniline ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 62-53-3
Anthracene ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 120-12-7
Benzo(a)anthracene ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 56-55-3
Benzo(a)pyrene ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 50-32-8
Benzo(b)fluoranthene ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 205-99-2
Benzo(g,h,i)perylene ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 191-24-2
Benzo(k)fluoranthene ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 207-08-9
Benzoic Acid ND ug/L 62.5 1 03/30/11 13:30 04/01/11 12:31 65-85-0
Benzyl alcohol ND ug/L 25.0 1 03/30/11 13:30 04/01/11 12:31 100-51-6
4-Bromophenylphenyl ether ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 101-55-3
Butylbenzylphthalate ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 85-68-7
4-Chloro-3-methylphenol ND ug/L 25.0 1 03/30/11 13:30 04/01/11 12:31 59-50-7
4-Chloroaniline ND ug/L 25.0 1 03/30/11 13:30 04/01/11 12:31 106-47-8
bis(2-Chloroethoxy)methane ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 111-91-1
bis(2-Chloroethyl) ether ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 111-44-4
bis(2-Chloroisopropyl) ether ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 108-60-1
2-Chloronaphthalene ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 91-58-7
2-Chlorophenol ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 95-57-8
4-Chlorophenylphenyl ether ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 7005-72-3
Chrysene ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 218-01-9
Dibenz(a,h)anthracene ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 53-70-3
Dibenzofuran ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 132-64-9
1,2-Dichlorobenzene ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 95-50-1
3,3'-Dichlorobenzidine ND ug/L 25.0 1 03/30/11 13:30 04/01/11 12:31 91-94-1
2,4-Dichlorophenol ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 120-83-2
Diethylphthalate ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 84-66-2
2,4-Dimethylphenol ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 105-67-9
Dimethylphthalate ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 131-11-3

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Di-n-butylphthalate ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 84-74-2

4,6-Dinitro-2-methylphenol ND ug/L 25.0 1 03/30/11 13:30 04/01/11 12:31 534-52-1
2,4-Dinitrophenol ND ug/L 62.5 1 03/30/11 13:30 04/01/11 12:31 51-28-5
2,4-Dinitrotoluene ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 121-14-2
Di-n-octylphthalate ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 117-84-0
bis(2-Ethylhexyl)phthalate ND ug/L 7.5 1 03/30/11 13:30 04/01/11 12:31 117-81-7
Fluoranthene ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 206-44-0
Fluorene ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 86-73-7
Hexachloro-1,3-butadiene ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 87-68-3
Hexachlorobenzene ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 118-74-1
Hexachlorocyclopentadiene ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 77-47-4
Hexachloroethane ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 67-72-1
Indeno(1,2,3-cd)pyrene ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 193-39-5
Isophorone ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 78-59-1
1-Methylnaphthalene ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 90-12-0
2-Methylnaphthalene ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 91-57-6
2-Methylphenol(o-Cresol) ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 95-48-7
3&4-Methylphenol(m&p Cresol) ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31
Naphthalene ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 91-20-3
2-Nitroaniline ND ug/L 62.5 1 03/30/11 13:30 04/01/11 12:31 88-74-4
Nitrobenzene ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 98-95-3
2-Nitrophenol ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 88-75-5
N-Nitrosodimethylamine ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 62-75-9
N-Nitroso-di-n-propylamine ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 621-64-7
N-Nitrosodiphenylamine ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 86-30-6
Pentachlorophenol ND ug/L 31.2 1 03/30/11 13:30 04/01/11 12:31 87-86-5
Phenanthrene ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 85-01-8
Phenol ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 108-95-2
Pyrene ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 129-00-0
1,2,4-Trichlorobenzene ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 120-82-1
2,4,5-Trichlorophenol ND ug/L 12.5 1 03/30/11 13:30 04/01/11 12:31 95-95-4
Nitrobenzene-d5 (S) 79 % 21-110 1 03/30/11 13:30 04/01/11 12:31 4165-60-0
Terphenyl-d14 (S) 79 % 31-107 1 03/30/11 13:30 04/01/11 12:31 1718-51-0
Phenol-d6 (S) 34 % 10-110 1 03/30/11 13:30 04/01/11 12:31 13127-88-3
2-Fluorophenol (S) 52 % 12-110 1 03/30/11 13:30 04/01/11 12:31 367-12-4
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 25.0 1 03/31/11 17:31 67-64-1

Benzene ND ug/L 1.0 1 03/31/11 17:31 71-43-2
Bromobenzene ND ug/L 1.0 1 03/31/11 17:31 108-86-1

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

Bromochloromethane ND ug/L 1.0 1 03/31/11 17:31 74-97-5

Bromodichloromethane ND ug/L 1.0 1 03/31/11 17:31 75-27-4
Bromoform ND ug/L 1.0 1 03/31/11 17:31 75-25-2
Bromomethane ND ug/L 2.0 1 03/31/11 17:31 74-83-9
2-Butanone (MEK) ND ug/L 5.0 1 03/31/11 17:31 78-93-3
Carbon tetrachloride ND ug/L 1.0 1 03/31/11 17:31 56-23-5
Chlorobenzene ND ug/L 1.0 1 03/31/11 17:31 108-90-7
Chloroethane ND ug/L 1.0 1 03/31/11 17:31 75-00-3
Chloroform ND ug/L 1.0 1 03/31/11 17:31 67-66-3
Chloromethane ND ug/L 1.0 1 03/31/11 17:31 74-87-3
2-Chlorotoluene ND ug/L 1.0 1 03/31/11 17:31 95-49-8
1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 03/31/11 17:31 96-12-8
Dibromochloromethane ND ug/L 1.0 1 03/31/11 17:31 124-48-1
1,2-Dibromoethane (EDB) ND ug/L 1.0 1 03/31/11 17:31 106-93-4
Dibromomethane ND ug/L 1.0 1 03/31/11 17:31 74-95-3
1,2-Dichlorobenzene ND ug/L 1.0 1 03/31/11 17:31 95-50-1
Dichlorodifluoromethane ND ug/L 1.0 1 03/31/11 17:31 75-71-8
1,1-Dichloroethane ND ug/L 1.0 1 03/31/11 17:31 75-34-3
1,1-Dichloroethene ND ug/L 1.0 1 03/31/11 17:31 75-35-4
cis-1,2-Dichloroethene ND ug/L 1.0 1 03/31/11 17:31 156-59-2
trans-1,2-Dichloroethene ND ug/L 1.0 1 03/31/11 17:31 156-60-5
1,2-Dichloropropane ND ug/L 1.0 1 03/31/11 17:31 78-87-5
1,1-Dichloropropene ND ug/L 1.0 1 03/31/11 17:31 563-58-6
cis-1,3-Dichloropropene ND ug/L 1.0 1 03/31/11 17:31 10061-01-5
trans-1,3-Dichloropropene ND ug/L 1.0 1 03/31/11 17:31 10061-02-6
Diisopropyl ether ND ug/L 1.0 1 03/31/11 17:31 108-20-3
Ethylbenzene ND ug/L 1.0 1 03/31/11 17:31 100-41-4
Hexachloro-1,3-butadiene ND ug/L 1.0 1 03/31/11 17:31 87-68-3
2-Hexanone ND ug/L 5.0 1 03/31/11 17:31 591-78-6
p-Isopropyltoluene ND ug/L 1.0 1 03/31/11 17:31 99-87-6
Methylene Chloride ND ug/L 1.0 1 03/31/11 17:31 75-09-2
4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 03/31/11 17:31 108-10-1
Methyl-tert-butyl ether ND ug/L 1.0 1 03/31/11 17:31 1634-04-4
Naphthalene ND ug/L 1.0 1 03/31/11 17:31 91-20-3
Styrene ND ug/L 1.0 1 03/31/11 17:31 100-42-5
1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 03/31/11 17:31 630-20-6
Tetrachloroethene ND ug/L 1.0 1 03/31/11 17:31 127-18-4
Toluene ND ug/L 1.0 1 03/31/11 17:31 108-88-3
1,2,3-Trichlorobenzene ND ug/L 1.0 1 03/31/11 17:31 87-61-6

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

1,1,1-Trichloroethane ND ug/L 1.0 1 03/31/11 17:31 71-55-6

Trichloroethene ND ug/L 1.0 1 03/31/11 17:31 79-01-6
Trichlorofluoromethane ND ug/L 1.0 1 03/31/11 17:31 75-69-4
1,2,3-Trichloropropane ND ug/L 1.0 1 03/31/11 17:31 96-18-4
Vinyl acetate ND ug/L 2.0 1 03/31/11 17:31 108-05-4
Vinyl chloride ND ug/L 1.0 1 03/31/11 17:31 75-01-4
m&p-Xylene ND ug/L 2.0 1 03/31/11 17:31 179601-23-1
o-Xylene ND ug/L 1.0 1 03/31/11 17:31 95-47-6
Dibromofluoromethane (S) 132 % 70-130 1 03/31/11 17:31 1868-53-7 S3
Toluene-d8 (S) 98 % 70-130 1 03/31/11 17:31 2037-26-5

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

Sample: MW-02-SB-45-R Lab ID: 9290652059 Collected: 03/23/11 11:50 Received: 03/24/11 17:15 Matrix: Solid

o-Terphenyl (S) 69 % 40-140 1 03/29/11 13:30 03/30/11 23:14 84-15-1


Chrysene ND ug/kg 396 1 03/29/11 11:30 03/29/11 21:39 218-01-9

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


Fluorene ND ug/kg 396 1 03/29/11 11:30 03/29/11 21:39 86-73-7
Phenol ND ug/kg 396 1 03/29/11 11:30 03/29/11 21:39 108-95-2
Pyrene ND ug/kg 396 1 03/29/11 11:30 03/29/11 21:39 129-00-0
Nitrobenzene-d5 (S) 57 % 23-110 1 03/29/11 11:30 03/29/11 21:39 4165-60-0
Terphenyl-d14 (S) 63 % 28-110 1 03/29/11 11:30 03/29/11 21:39 1718-51-0
Phenol-d6 (S) 50 % 22-110 1 03/29/11 11:30 03/29/11 21:39 13127-88-3
2-Fluorophenol (S) 53 % 13-110 1 03/29/11 11:30 03/29/11 21:39 367-12-4
Acetone ND ug/kg 104 1 03/30/11 19:18 67-64-1

Benzene ND ug/kg 5.2 1 03/30/11 19:18 71-43-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


2-Hexanone ND ug/kg 51.8 1 03/30/11 19:18 591-78-6

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

Styrene ND ug/kg 5.2 1 03/30/11 19:18 100-42-5

Toluene ND ug/kg 5.2 1 03/30/11 19:18 108-88-3
m&p-Xylene ND ug/kg 10.4 1 03/30/11 19:18 179601-23-1
o-Xylene ND ug/kg 5.2 1 03/30/11 19:18 95-47-6
Toluene-d8 (S) 99 % 70-130 1 03/30/11 19:18 2037-26-5

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

Sample: TRIP BLANK Lab ID: 9290652060 Collected: 03/23/11 00:00 Received: 03/24/11 17:15 Matrix: Water
Acetone ND ug/L 25.0 1 03/31/11 17:57 67-64-1

Benzene ND ug/L 1.0 1 03/31/11 17:57 71-43-2
Bromoform ND ug/L 1.0 1 03/31/11 17:57 75-25-2
2-Butanone (MEK) ND ug/L 5.0 1 03/31/11 17:57 78-93-3
2-Hexanone ND ug/L 5.0 1 03/31/11 17:57 591-78-6
p-Isopropyltoluene ND ug/L 1.0 1 03/31/11 17:57 99-87-6
4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 03/31/11 17:57 108-10-1
Styrene ND ug/L 1.0 1 03/31/11 17:57 100-42-5

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

Sample: TRIP BLANK Lab ID: 9290652060 Collected: 03/23/11 00:00 Received: 03/24/11 17:15 Matrix: Water
Toluene ND ug/L 1.0 1 03/31/11 17:57 108-88-3

Vinyl acetate ND ug/L 2.0 1 03/31/11 17:57 108-05-4
m&p-Xylene ND ug/L 2.0 1 03/31/11 17:57 179601-23-1
o-Xylene ND ug/L 1.0 1 03/31/11 17:57 95-47-6
Dibromofluoromethane (S) 132 % 70-130 1 03/31/11 17:57 1868-53-7 S3
Toluene-d8 (S) 98 % 70-130 1 03/31/11 17:57 2037-26-5

(336)623-8921 (828)254-7176 (704)875-9092
QUALITY CONTROL DATA

QC Batch: OEXT/13124 Analysis Method: EPA 8015 Modified

QC Batch Method: EPA 3546 Analysis Description: 8015 Solid GCSV
Associated Lab Samples: 9290652012, 9290652013, 9290652017, 9290652018, 9290652020, 9290652021, 9290652022, 9290652023
METHOD BLANK: 584590 Matrix: Solid

Associated Lab Samples: 9290652012, 9290652013, 9290652017, 9290652018, 9290652020, 9290652021, 9290652022, 9290652023
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Diesel Components mg/kg ND 5.0 03/31/11 13:47
n-Pentacosane (S) % 82 41-119 03/31/11 13:47
LABORATORY CONTROL SAMPLE: 584591

Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Diesel Components mg/kg 167 159 96 49-113
n-Pentacosane (S) % 95 41-119
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 584592 584593

MS MSD
9290652018 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Diesel Components mg/kg ND 205 205 178 190 86 92 10-146 6
n-Pentacosane (S) % 98 94 41-119

(336)623-8921 (828)254-7176 (704)875-9092


Associated Lab Samples: 9290652024, 9290652025, 9290652026, 9290652027, 9290652028, 9290652029, 9290652030, 9290652031,
9290652032, 9290652033, 9290652034, 9290652035, 9290652036, 9290652037, 9290652038, 9290652039,
9290652040, 9290652041, 9290652042, 9290652043

9290652032, 9290652033, 9290652034, 9290652035, 9290652036, 9290652037, 9290652038, 9290652039,
9290652040, 9290652041, 9290652042, 9290652043
Blank Reporting
n-Pentacosane (S) % 83 41-119 04/01/11 01:36

Spike LCS LCS % Rec

MS MSD

(336)623-8921 (828)254-7176 (704)875-9092


Associated Lab Samples: 9290652044, 9290652046, 9290652047, 9290652048, 9290652049, 9290652050, 9290652051

Associated Lab Samples: 9290652044, 9290652046, 9290652047, 9290652048, 9290652049, 9290652050, 9290652051
Blank Reporting
n-Pentacosane (S) % 77 41-119 04/03/11 15:32

Spike LCS LCS % Rec

MS MSD

(336)623-8921 (828)254-7176 (704)875-9092


QC Batch Method: EPA 3535 Analysis Description: 8015 GCS
Associated Lab Samples: 9290652045
METHOD BLANK: 584880 Matrix: Water

Blank Reporting
Diesel Components mg/L ND 0.50 04/01/11 12:54
n-Pentacosane (S) % 86 48-110 04/01/11 12:54

Spike LCS LCS % Rec
Diesel Components mg/L 25 23.8 95 41-114

MS MSD
Diesel Components mg/L ND 55.6 55.6 49.5 48.1 89 87 41-114 3

(336)623-8921 (828)254-7176 (704)875-9092

QC Batch: OEXT/13106 Analysis Method: MADEP EPH

QC Batch Method: MADEP EPH Analysis Description: MADEP EPH NC Soil
Associated Lab Samples: 9290652052, 9290652053, 9290652054, 9290652055, 9290652056, 9290652059

Blank Reporting
Aliphatic (C09-C18) mg/kg ND 10.0 03/31/11 13:43 N2
Aromatic (C11-C22) mg/kg ND 10.0 03/31/11 13:43 N2
2-Bromonaphthalene (S) % 122 40-140 03/31/11 13:43
2-Fluorobiphenyl (S) % 116 40-140 03/31/11 13:43
Nonatriacontane (S) % 76 40-140 03/31/11 13:43
o-Terphenyl (S) % 101 40-140 03/31/11 13:43
LABORATORY CONTROL SAMPLE & LCSD: 583982 583983

Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
Aliphatic (C09-C18) mg/kg 10 ND ND 79 90 40-140 50 N2
Aliphatic (C19-C36) mg/kg 13.3 11.1 12.2 83 92 40-140 10 50 N2
Aromatic (C11-C22) mg/kg 28.3 26.8 26.8 94 95 40-140 0 50 N2
2-Bromonaphthalene (S) % 103 103 40-140
2-Fluorobiphenyl (S) % 106 101 40-140
Nonatriacontane (S) % 82 81 40-140
o-Terphenyl (S) % 90 90 40-140

MS MSD
Aliphatic (C09-C18) mg/kg ND 11.8 11.8 ND ND 69 53 40-140 N2
Aliphatic (C19-C36) mg/kg ND 15.6 15.6 13.1 ND 82 68 40-140 N2
Aromatic (C11-C22) mg/kg ND 33.3 33.3 32.2 25.8 95 76 40-140 22 N2
o-Terphenyl (S) % 91 74 40-140

(336)623-8921 (828)254-7176 (704)875-9092


QC Batch Method: MADEP EPH Analysis Description: MADEP EPH NC Water

Blank Reporting
Aliphatic (C09-C18) ug/L ND 100 04/04/11 19:23 N2
Aromatic (C11-C22) ug/L ND 100 04/04/11 19:23 N2
o-Terphenyl (S) % 83 40-140 04/04/11 19:23

Aliphatic (C09-C18) ug/L 300 262 276 87 92 40-140 5 50 N2
Aromatic (C11-C22) ug/L 850 835 811 98 95 40-140 3 50 N2
o-Terphenyl (S) % 101 101 40-140

MS MSD
Aliphatic (C09-C18) ug/L ND 600 600 422 391 65 60 40-140 8 N2
Aromatic (C11-C22) ug/L ND 1700 1700 1370 1400 80 82 40-140 2 N2
o-Terphenyl (S) % 72 86 40-140

MS MSD

(336)623-8921 (828)254-7176 (704)875-9092


MS MSD
o-Terphenyl (S) % 92 82 40-140

(336)623-8921 (828)254-7176 (704)875-9092

QC Batch: GCV/4843 Analysis Method: EPA 8015 Modified

QC Batch Method: EPA 5035A/5030B Analysis Description: Gasoline Range Organics
9290652009, 9290652010, 9290652011, 9290652012, 9290652013, 9290652014, 9290652015, 9290652016,
9290652017

9290652009, 9290652010, 9290652011, 9290652012, 9290652013, 9290652014, 9290652015, 9290652016,
9290652017
Blank Reporting
Gasoline Range Organics mg/kg ND 6.0 03/29/11 17:01
4-Bromofluorobenzene (S) % 136 70-167 03/29/11 17:01

Spike LCS LCS % Rec
Gasoline Range Organics mg/kg 25 24.2 97 70-165
4-Bromofluorobenzene (S) % 110 70-167

MS MSD
Gasoline Range Organics mg/kg ND 40.2 40.2 47.2 53.4 117 132 47-187 12
4-Bromofluorobenzene (S) % 150 172 70-167 S0

(336)623-8921 (828)254-7176 (704)875-9092


9290652027, 9290652028, 9290652029, 9290652030, 9290652031, 9290652032, 9290652033, 9290652034,
9290652035, 9290652036, 9290652037, 9290652038

9290652027, 9290652028, 9290652029, 9290652030, 9290652031, 9290652032, 9290652033, 9290652034,
9290652035, 9290652036, 9290652037, 9290652038
Blank Reporting

Spike LCS LCS % Rec

MS MSD
4-Bromofluorobenzene (S) % 150 144 70-167

(336)623-8921 (828)254-7176 (704)875-9092


Associated Lab Samples: 9290652048, 9290652049

Blank Reporting

Spike LCS LCS % Rec

MS MSD
Gasoline Range Organics mg/kg 247 30.8 30.8 274 276 86 93 47-187 1

(336)623-8921 (828)254-7176 (704)875-9092


9290652050, 9290652051

9290652050, 9290652051
Blank Reporting

Spike LCS LCS % Rec

MS MSD

(336)623-8921 (828)254-7176 (704)875-9092

QC Batch: GCV/4840 Analysis Method: EPA 5030/8015 Mod.

QC Batch Method: EPA 5030/8015 Mod. Analysis Description: Gasoline Range Organics

Blank Reporting
Gasoline Range Organics mg/L ND 0.080 03/28/11 18:27

Spike LCS LCS % Rec
Gasoline Range Organics mg/L .5 0.49 97 70-150

MS MSD
Gasoline Range Organics mg/L 15.6 2.5 2.5 18.5 18.5 114 113 70-150 0

(336)623-8921 (828)254-7176 (704)875-9092

QC Batch: GCV/4863 Analysis Method: MADEP VPH

QC Batch Method: MADEP VPH Analysis Description: VPH NC Soil

Blank Reporting
Aromatic (C09-C10) mg/kg ND 1.5 04/05/11 17:18 N2
2,5-Dibromotoluene (FID)(S) % 94 70-130 04/05/11 17:18
2,5-Dibromotoluene (PID)(S) % 99 70-130 04/05/11 17:18

Aliphatic (C05-C08) mg/kg 15 15.1 14.6 101 97 70-130 4 25 N2
Aliphatic (C09-C12) mg/kg 15 17.1 17.1 114 114 30-130 0 25 N2
Aromatic (C09-C10) mg/kg 5 5.1 5.0 102 100 70-130 2 25 N2
2,5-Dibromotoluene (FID)(S) % 109 100 70-130
2,5-Dibromotoluene (PID)(S) % 108 103 70-130

(336)623-8921 (828)254-7176 (704)875-9092


QC Batch Method: MADEP VPH Analysis Description: VPH NC Water

Blank Reporting
Aliphatic (C05-C08) ug/L ND 30.0 03/28/11 16:09 N2
Aromatic (C09-C10) ug/L ND 30.0 03/28/11 16:09 N2

Aromatic (C09-C10) ug/L 100 105 100 105 100 70-130 5 25 N2

(336)623-8921 (828)254-7176 (704)875-9092

QC Batch: OEXT/13108 Analysis Method: EPA 8270

QC Batch Method: EPA 3546 Analysis Description: 8270 Solid MSSV Microwave

Blank Reporting
1,2,4-Trichlorobenzene ug/kg ND 330 03/29/11 16:38
1,2-Dichlorobenzene ug/kg ND 330 03/29/11 16:38
1-Methylnaphthalene ug/kg ND 330 03/29/11 16:38
2,4,5-Trichlorophenol ug/kg ND 330 03/29/11 16:38
2,4,6-Trichlorophenol ug/kg ND 330 03/29/11 16:38
2,4-Dichlorophenol ug/kg ND 330 03/29/11 16:38
2,4-Dimethylphenol ug/kg ND 330 03/29/11 16:38
2,4-Dinitrophenol ug/kg ND 1650 03/29/11 16:38
2,4-Dinitrotoluene ug/kg ND 330 03/29/11 16:38
2,6-Dinitrotoluene ug/kg ND 330 03/29/11 16:38
2-Chloronaphthalene ug/kg ND 330 03/29/11 16:38
2-Chlorophenol ug/kg ND 330 03/29/11 16:38
2-Methylnaphthalene ug/kg ND 330 03/29/11 16:38
2-Methylphenol(o-Cresol) ug/kg ND 330 03/29/11 16:38
2-Nitroaniline ug/kg ND 1650 03/29/11 16:38
2-Nitrophenol ug/kg ND 330 03/29/11 16:38
3&4-Methylphenol(m&p Cresol) ug/kg ND 330 03/29/11 16:38
3,3'-Dichlorobenzidine ug/kg ND 1650 03/29/11 16:38
4,6-Dinitro-2-methylphenol ug/kg ND 660 03/29/11 16:38
4-Bromophenylphenyl ether ug/kg ND 330 03/29/11 16:38
4-Chloro-3-methylphenol ug/kg ND 660 03/29/11 16:38
4-Chloroaniline ug/kg ND 1650 03/29/11 16:38
4-Chlorophenylphenyl ether ug/kg ND 330 03/29/11 16:38
4-Nitrophenol ug/kg ND 1650 03/29/11 16:38
Acenaphthene ug/kg ND 330 03/29/11 16:38
Acenaphthylene ug/kg ND 330 03/29/11 16:38
Anthracene ug/kg ND 330 03/29/11 16:38
Benzo(a)anthracene ug/kg ND 330 03/29/11 16:38
Benzo(a)pyrene ug/kg ND 330 03/29/11 16:38
Benzo(b)fluoranthene ug/kg ND 330 03/29/11 16:38
Benzo(g,h,i)perylene ug/kg ND 330 03/29/11 16:38
Benzo(k)fluoranthene ug/kg ND 330 03/29/11 16:38
Benzoic Acid ug/kg ND 1650 03/29/11 16:38
Benzyl alcohol ug/kg ND 660 03/29/11 16:38
bis(2-Chloroethoxy)methane ug/kg ND 330 03/29/11 16:38
bis(2-Chloroethyl) ether ug/kg ND 330 03/29/11 16:38
bis(2-Chloroisopropyl) ether ug/kg ND 330 03/29/11 16:38
bis(2-Ethylhexyl)phthalate ug/kg ND 330 03/29/11 16:38
Butylbenzylphthalate ug/kg ND 330 03/29/11 16:38

(336)623-8921 (828)254-7176 (704)875-9092


Blank Reporting
Chrysene ug/kg ND 330 03/29/11 16:38
Di-n-butylphthalate ug/kg ND 330 03/29/11 16:38
Di-n-octylphthalate ug/kg ND 330 03/29/11 16:38
Dibenz(a,h)anthracene ug/kg ND 330 03/29/11 16:38
Dibenzofuran ug/kg ND 330 03/29/11 16:38
Diethylphthalate ug/kg ND 330 03/29/11 16:38
Dimethylphthalate ug/kg ND 330 03/29/11 16:38
Fluoranthene ug/kg ND 330 03/29/11 16:38
Fluorene ug/kg ND 330 03/29/11 16:38
Hexachloro-1,3-butadiene ug/kg ND 330 03/29/11 16:38
Hexachlorobenzene ug/kg ND 330 03/29/11 16:38
Hexachlorocyclopentadiene ug/kg ND 330 03/29/11 16:38
Hexachloroethane ug/kg ND 330 03/29/11 16:38
Indeno(1,2,3-cd)pyrene ug/kg ND 330 03/29/11 16:38
Isophorone ug/kg ND 330 03/29/11 16:38
N-Nitroso-di-n-propylamine ug/kg ND 330 03/29/11 16:38
N-Nitrosodimethylamine ug/kg ND 330 03/29/11 16:38
N-Nitrosodiphenylamine ug/kg ND 330 03/29/11 16:38
Naphthalene ug/kg ND 330 03/29/11 16:38
Nitrobenzene ug/kg ND 330 03/29/11 16:38
Pentachlorophenol ug/kg ND 1650 03/29/11 16:38
Phenanthrene ug/kg ND 330 03/29/11 16:38
Phenol ug/kg ND 330 03/29/11 16:38
Pyrene ug/kg ND 330 03/29/11 16:38
2,4,6-Tribromophenol (S) % 63 27-110 03/29/11 16:38
2-Fluorophenol (S) % 54 13-110 03/29/11 16:38
Nitrobenzene-d5 (S) % 56 23-110 03/29/11 16:38
Phenol-d6 (S) % 53 22-110 03/29/11 16:38
Terphenyl-d14 (S) % 77 28-110 03/29/11 16:38

Spike LCS LCS % Rec
1,2,4-Trichlorobenzene ug/kg 1670 1150 69 39-101
1,2-Dichlorobenzene ug/kg 1670 1200 72 36-110
1-Methylnaphthalene ug/kg 1670 1170 70 45-105
2,4,5-Trichlorophenol ug/kg 1670 1250 75 48-109
2,4,6-Trichlorophenol ug/kg 1670 1410 85 45-111
2,4-Dichlorophenol ug/kg 1670 1230 74 51-116
2,4-Dimethylphenol ug/kg 1670 1210 72 42-103
2,4-Dinitrophenol ug/kg 8330 5570 67 28-103
2,4-Dinitrotoluene ug/kg 1670 1330 80 46-114

(336)623-8921 (828)254-7176 (704)875-9092


Spike LCS LCS % Rec
2,6-Dinitrotoluene ug/kg 1670 1370 82 48-112
2-Chloronaphthalene ug/kg 1670 1390 83 44-105
2-Chlorophenol ug/kg 1670 1230 74 36-110
2-Methylnaphthalene ug/kg 1670 1140 68 39-112
2-Methylphenol(o-Cresol) ug/kg 1670 1240 74 39-101
2-Nitroaniline ug/kg 3330 2970 89 44-111
2-Nitrophenol ug/kg 1670 1290 77 41-100
3&4-Methylphenol(m&p Cresol) ug/kg 1670 1250 75 43-103
3,3'-Dichlorobenzidine ug/kg 3330 1960 59 10-150
4,6-Dinitro-2-methylphenol ug/kg 3330 2940 88 38-118
4-Bromophenylphenyl ether ug/kg 1670 1390 83 47-115
4-Chloro-3-methylphenol ug/kg 3330 2560 77 43-127
4-Chloroaniline ug/kg 3330 1810 54 34-109
4-Chlorophenylphenyl ether ug/kg 1670 1250 75 44-115
4-Nitrophenol ug/kg 8330 5650 68 21-152
Acenaphthene ug/kg 1670 1380 83 38-117
Acenaphthylene ug/kg 1670 1370 82 46-107
Anthracene ug/kg 1670 1390 83 50-110
Benzo(a)anthracene ug/kg 1670 1290 77 47-116
Benzo(a)pyrene ug/kg 1670 1240 75 47-106
Benzo(b)fluoranthene ug/kg 1670 1210 72 47-109
Benzo(g,h,i)perylene ug/kg 1670 1390 84 39-115
Benzo(k)fluoranthene ug/kg 1670 1350 81 45-117
Benzoic Acid ug/kg 8330 4150 50 16-110
Benzyl alcohol ug/kg 3330 2580 77 38-105
bis(2-Chloroethoxy)methane ug/kg 1670 1170 70 39-110
bis(2-Chloroethyl) ether ug/kg 1670 1260 75 19-119
bis(2-Chloroisopropyl) ether ug/kg 1670 1300 78 21-110
bis(2-Ethylhexyl)phthalate ug/kg 1670 1270 76 35-116
Butylbenzylphthalate ug/kg 1670 1320 79 38-110
Chrysene ug/kg 1670 1360 81 49-110
Di-n-butylphthalate ug/kg 1670 1320 79 43-109
Di-n-octylphthalate ug/kg 1670 1120 67 37-109
Dibenz(a,h)anthracene ug/kg 1670 1340 81 43-116
Dibenzofuran ug/kg 1670 1310 78 45-106
Diethylphthalate ug/kg 1670 1270 76 41-114
Dimethylphthalate ug/kg 1670 1250 75 43-110
Fluoranthene ug/kg 1670 1270 76 50-114
Fluorene ug/kg 1670 1350 81 46-114
Hexachloro-1,3-butadiene ug/kg 1670 1170 70 28-111
Hexachlorobenzene ug/kg 1670 1450 87 46-120
Hexachlorocyclopentadiene ug/kg 1670 1220 73 18-119
Hexachloroethane ug/kg 1670 1240 74 33-110
Indeno(1,2,3-cd)pyrene ug/kg 1670 1360 81 42-115
Isophorone ug/kg 1670 1360 82 44-109
N-Nitroso-di-n-propylamine ug/kg 1670 1210 72 43-104

(336)623-8921 (828)254-7176 (704)875-9092


Spike LCS LCS % Rec
N-Nitrosodimethylamine ug/kg 1670 1300 78 29-110
N-Nitrosodiphenylamine ug/kg 1670 1420 85 48-113
Naphthalene ug/kg 1670 1190 71 41-110
Nitrobenzene ug/kg 1670 1230 74 38-110
Pentachlorophenol ug/kg 3330 2270 68 32-128
Phenanthrene ug/kg 1670 1360 82 50-110
Phenol ug/kg 1670 1340 80 28-106
Pyrene ug/kg 1670 1470 88 45-114
2,4,6-Tribromophenol (S) % 92 27-110
2-Fluorobiphenyl (S) % 78 30-110
2-Fluorophenol (S) % 73 13-110
Nitrobenzene-d5 (S) % 74 23-110
Phenol-d6 (S) % 71 22-110
Terphenyl-d14 (S) % 86 28-110

MS MSD
1,2,4-Trichlorobenzene ug/kg ND 1960 1960 975 838 50 43 18-119 15
1,2-Dichlorobenzene ug/kg ND 1960 1960 991 890 51 45 50-110 11 M0,M1
1,3-Dichlorobenzene ug/kg ND 1960 1960 974 882 50 45 27-110 10
1,4-Dichlorobenzene ug/kg ND 1960 1960 978 875 50 45 28-110 11
1-Methylnaphthalene ug/kg ND 1960 1960 977 834 50 43 24-116 16
2,4,5-Trichlorophenol ug/kg ND 1960 1960 1080 926 55 47 28-110 16
2,4,6-Trichlorophenol ug/kg ND 1960 1960 1170 985 60 50 17-117 17
2,4-Dichlorophenol ug/kg ND 1960 1960 1020 864 52 44 21-128 17
2,4-Dimethylphenol ug/kg ND 1960 1960 990 854 51 44 10-120 15
2,4-Dinitrophenol ug/kg ND 9790 9790 4440 4250 45 43 10-107 4
2,4-Dinitrotoluene ug/kg ND 1960 1960 1210 1050 62 53 36-109 14
2,6-Dinitrotoluene ug/kg ND 1960 1960 1170 1010 60 52 32-110 15
2-Chloronaphthalene ug/kg ND 1960 1960 1170 1000 60 51 30-107 16
2-Chlorophenol ug/kg ND 1960 1960 991 883 51 45 14-106 11
2-Methylnaphthalene ug/kg ND 1960 1960 956 812 49 41 10-135 16
2-Methylphenol(o-Cresol) ug/kg ND 1960 1960 990 857 51 44 10-124 14
2-Nitroaniline ug/kg ND 3920 3920 2590 2240 66 57 26-116 15
2-Nitrophenol ug/kg ND 1960 1960 1050 873 54 45 28-103 19
3&4-Methylphenol(m&p ug/kg ND 1960 1960 1010 869 52 44 10-109 15
Cresol)
3,3'-Dichlorobenzidine ug/kg ND 3920 3920 1870J 1710J 48 44 10-150
3-Nitroaniline ug/kg ND 3920 3920 2150 1850J 55 47 22-110
4,6-Dinitro-2-methylphenol ug/kg ND 3920 3920 2310 2170 59 55 13-121 6
4-Bromophenylphenyl ether ug/kg ND 1960 1960 1140 986 58 50 31-109 14
4-Chloro-3-methylphenol ug/kg ND 3920 3920 2100 1850 54 47 13-128 13
4-Chloroaniline ug/kg ND 3920 3920 1810J 1570J 46 40 18-102
4-Chlorophenylphenyl ether ug/kg ND 1960 1960 1120 958 57 49 29-112 16
4-Nitroaniline ug/kg ND 3920 3920 2160 1840 55 47 16-111 16

(336)623-8921 (828)254-7176 (704)875-9092


MS MSD
4-Nitrophenol ug/kg ND 9790 9790 5390 4830 55 49 14-135 11
Acenaphthene ug/kg ND 1960 1960 1200 1040 61 53 26-114 14
Acenaphthylene ug/kg ND 1960 1960 1180 1000 60 51 32-108 16
Anthracene ug/kg ND 1960 1960 1220 1040 62 53 32-111 16
Benzo(a)anthracene ug/kg ND 1960 1960 1110 967 56 49 25-117 13
Benzo(a)pyrene ug/kg ND 1960 1960 1060 917 54 47 25-106 15
Benzo(b)fluoranthene ug/kg ND 1960 1960 1010 856 51 44 24-110 16
Benzo(g,h,i)perylene ug/kg ND 1960 1960 1140 1020 58 52 19-112 11
Benzo(k)fluoranthene ug/kg ND 1960 1960 1150 989 59 50 24-114 15
Benzoic Acid ug/kg ND 9790 9790 3330 3200 34 33 10-110 4
Benzyl alcohol ug/kg ND 3920 3920 2070 1790 53 46 24-106 15
bis(2-Chloroethoxy)methane ug/kg ND 1960 1960 996 837 51 43 13-119 17
bis(2-Chloroethyl) ether ug/kg ND 1960 1960 1030 911 52 46 10-134 12
bis(2-Chloroisopropyl) ether ug/kg ND 1960 1960 1090 936 56 48 10-113 15
bis(2-Ethylhexyl)phthalate ug/kg ND 1960 1960 1020 857 52 44 10-125 17
Butylbenzylphthalate ug/kg ND 1960 1960 1120 933 57 48 18-110 18
Chrysene ug/kg ND 1960 1960 1190 1060 61 54 30-110 12
Di-n-butylphthalate ug/kg ND 1960 1960 1150 970 59 49 19-112 17
Di-n-octylphthalate ug/kg ND 1960 1960 868 718 44 37 17-105 19
Dibenz(a,h)anthracene ug/kg ND 1960 1960 1080 979 55 50 23-111 10
Dibenzofuran ug/kg ND 1960 1960 1160 993 59 51 35-103 15
Diethylphthalate ug/kg ND 1960 1960 1160 990 59 51 27-113 16
Dimethylphthalate ug/kg ND 1960 1960 1100 958 56 49 26-111 14
Fluoranthene ug/kg ND 1960 1960 1170 1020 60 52 33-109 14
Fluorene ug/kg ND 1960 1960 1210 1040 62 53 32-113 15
Hexachloro-1,3-butadiene ug/kg ND 1960 1960 987 842 50 43 16-116 16
Hexachlorobenzene ug/kg ND 1960 1960 1200 1050 61 54 27-120 13
Hexachlorocyclopentadiene ug/kg ND 1960 1960 927 815 47 42 10-108 13
Hexachloroethane ug/kg ND 1960 1960 1030 920 53 47 10-117 12
Indeno(1,2,3-cd)pyrene ug/kg ND 1960 1960 1080 981 55 50 10-122 9
Isophorone ug/kg ND 1960 1960 1170 990 60 51 28-114 17
N-Nitroso-di-n-propylamine ug/kg ND 1960 1960 1020 880 52 45 27-113 15
N-Nitrosodimethylamine ug/kg ND 1960 1960 1050 942 53 48 10-109 11
N-Nitrosodiphenylamine ug/kg ND 1960 1960 1180 1030 60 53 10-128 13
Naphthalene ug/kg ND 1960 1960 1010 861 52 44 25-110 16
Nitrobenzene ug/kg ND 1960 1960 1060 884 54 45 18-114 18
Pentachlorophenol ug/kg ND 3920 3920 1850J 1780J 47 45 10-122
Phenanthrene ug/kg ND 1960 1960 1180 1030 60 52 30-114 14
Phenol ug/kg ND 1960 1960 1070 948 55 48 11-102 12
Pyrene ug/kg ND 1960 1960 1220 1020 62 52 25-116 17
2,4,6-Tribromophenol (S) % 62 55 27-110
2-Fluorophenol (S) % 48 45 13-110
Nitrobenzene-d5 (S) % 53 45 23-110
Phenol-d6 (S) % 47 42 22-110
Terphenyl-d14 (S) % 61 50 28-110

(336)623-8921 (828)254-7176 (704)875-9092


QC Batch Method: EPA 3510 Analysis Description: 8270 Water MSSV

Blank Reporting
1,2,4-Trichlorobenzene ug/L ND 10.0 03/31/11 12:56
1,2-Dichlorobenzene ug/L ND 10.0 03/31/11 12:56
1-Methylnaphthalene ug/L ND 10.0 03/31/11 12:56
2,4,5-Trichlorophenol ug/L ND 10.0 03/31/11 12:56
2,4-Dichlorophenol ug/L ND 10.0 03/31/11 12:56
2,4-Dimethylphenol ug/L ND 10.0 03/31/11 12:56
2,4-Dinitrophenol ug/L ND 50.0 03/31/11 12:56
2,4-Dinitrotoluene ug/L ND 10.0 03/31/11 12:56
2-Chloronaphthalene ug/L ND 10.0 03/31/11 12:56
2-Chlorophenol ug/L ND 10.0 03/31/11 12:56
2-Methylnaphthalene ug/L ND 10.0 03/31/11 12:56
2-Methylphenol(o-Cresol) ug/L ND 10.0 03/31/11 12:56
2-Nitroaniline ug/L ND 50.0 03/31/11 12:56
2-Nitrophenol ug/L ND 10.0 03/31/11 12:56
3&4-Methylphenol(m&p Cresol) ug/L ND 10.0 03/31/11 12:56
3,3'-Dichlorobenzidine ug/L ND 20.0 03/31/11 12:56
4,6-Dinitro-2-methylphenol ug/L ND 20.0 03/31/11 12:56
4-Bromophenylphenyl ether ug/L ND 10.0 03/31/11 12:56
4-Chloro-3-methylphenol ug/L ND 20.0 03/31/11 12:56
4-Chloroaniline ug/L ND 20.0 03/31/11 12:56
4-Chlorophenylphenyl ether ug/L ND 10.0 03/31/11 12:56
Acenaphthene ug/L ND 10.0 03/31/11 12:56
Acenaphthylene ug/L ND 10.0 03/31/11 12:56
Aniline ug/L ND 10.0 03/31/11 12:56
Anthracene ug/L ND 10.0 03/31/11 12:56
Benzo(a)anthracene ug/L ND 10.0 03/31/11 12:56
Benzo(a)pyrene ug/L ND 10.0 03/31/11 12:56
Benzo(b)fluoranthene ug/L ND 10.0 03/31/11 12:56
Benzo(g,h,i)perylene ug/L ND 10.0 03/31/11 12:56
Benzo(k)fluoranthene ug/L ND 10.0 03/31/11 12:56
Benzoic Acid ug/L ND 50.0 03/31/11 12:56
Benzyl alcohol ug/L ND 20.0 03/31/11 12:56
bis(2-Chloroethoxy)methane ug/L ND 10.0 03/31/11 12:56
bis(2-Chloroethyl) ether ug/L ND 10.0 03/31/11 12:56
bis(2-Chloroisopropyl) ether ug/L ND 10.0 03/31/11 12:56
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 03/31/11 12:56

(336)623-8921 (828)254-7176 (704)875-9092


Blank Reporting
Butylbenzylphthalate ug/L ND 10.0 03/31/11 12:56
Chrysene ug/L ND 10.0 03/31/11 12:56
Di-n-butylphthalate ug/L ND 10.0 03/31/11 12:56
Di-n-octylphthalate ug/L ND 10.0 03/31/11 12:56
Dibenz(a,h)anthracene ug/L ND 10.0 03/31/11 12:56
Dibenzofuran ug/L ND 10.0 03/31/11 12:56
Diethylphthalate ug/L ND 10.0 03/31/11 12:56
Dimethylphthalate ug/L ND 10.0 03/31/11 12:56
Fluoranthene ug/L ND 10.0 03/31/11 12:56
Fluorene ug/L ND 10.0 03/31/11 12:56
Hexachloro-1,3-butadiene ug/L ND 10.0 03/31/11 12:56
Hexachlorobenzene ug/L ND 10.0 03/31/11 12:56
Hexachlorocyclopentadiene ug/L ND 10.0 03/31/11 12:56
Hexachloroethane ug/L ND 10.0 03/31/11 12:56
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 03/31/11 12:56
Isophorone ug/L ND 10.0 03/31/11 12:56
N-Nitroso-di-n-propylamine ug/L ND 10.0 03/31/11 12:56
N-Nitrosodimethylamine ug/L ND 10.0 03/31/11 12:56
N-Nitrosodiphenylamine ug/L ND 10.0 03/31/11 12:56
Naphthalene ug/L ND 10.0 03/31/11 12:56
Nitrobenzene ug/L ND 10.0 03/31/11 12:56
Pentachlorophenol ug/L ND 25.0 03/31/11 12:56
Phenanthrene ug/L ND 10.0 03/31/11 12:56
Phenol ug/L ND 10.0 03/31/11 12:56
Pyrene ug/L ND 10.0 03/31/11 12:56
2-Fluorophenol (S) % 38 12-110 03/31/11 12:56
Nitrobenzene-d5 (S) % 63 21-110 03/31/11 12:56
Phenol-d6 (S) % 24 10-110 03/31/11 12:56
Terphenyl-d14 (S) % 86 31-107 03/31/11 12:56

Spike LCS LCS % Rec
1,2,4-Trichlorobenzene ug/L 50 24.5 49 10-110
1,2-Dichlorobenzene ug/L 50 32.7 65 10-110
1-Methylnaphthalene ug/L 50 31.2 62 21-110
2,4,5-Trichlorophenol ug/L 50 37.8 76 23-116
2,4-Dichlorophenol ug/L 50 31.3 63 22-120
2,4-Dimethylphenol ug/L 50 32.4 65 15-109
2,4-Dinitrophenol ug/L 250 191 76 10-103

(336)623-8921 (828)254-7176 (704)875-9092


Spike LCS LCS % Rec
2,4-Dinitrotoluene ug/L 50 42.0 84 24-119
2-Chloronaphthalene ug/L 50 46.2 92 18-110
2-Chlorophenol ug/L 50 38.4 77 10-104
2-Methylnaphthalene ug/L 50 30.2 60 16-110
2-Methylphenol(o-Cresol) ug/L 50 38.1 76 13-110
2-Nitroaniline ug/L 100 92.5 92 20-117
2-Nitrophenol ug/L 50 28.7 57 16-108
3&4-Methylphenol(m&p Cresol) ug/L 50 35.4 71 14-110
3,3'-Dichlorobenzidine ug/L 100 80.7 81 13-131
4,6-Dinitro-2-methylphenol ug/L 100 84.5 84 13-119
4-Bromophenylphenyl ether ug/L 50 37.5 75 23-120
4-Chloro-3-methylphenol ug/L 100 71.1 71 21-119
4-Chloroaniline ug/L 100 58.9 59 10-122
4-Chlorophenylphenyl ether ug/L 50 38.4 77 22-112
4-Nitrophenol ug/L 250 113 45 10-110
Acenaphthene ug/L 50 43.1 86 20-105
Acenaphthylene ug/L 50 42.0 84 23-106
Aniline ug/L 50 36.5 73 10-110
Anthracene ug/L 50 42.2 84 25-120
Benzo(a)anthracene ug/L 50 42.6 85 21-128
Benzo(a)pyrene ug/L 50 38.7 77 25-116
Benzo(b)fluoranthene ug/L 50 43.1 86 23-117
Benzo(g,h,i)perylene ug/L 50 42.8 86 17-128
Benzo(k)fluoranthene ug/L 50 44.3 89 25-127
Benzoic Acid ug/L 250 24.4J 10 10-110
Benzyl alcohol ug/L 100 75.2 75 10-101
bis(2-Chloroethoxy)methane ug/L 50 38.8 78 19-107
bis(2-Chloroethyl) ether ug/L 50 41.2 82 10-108
bis(2-Chloroisopropyl) ether ug/L 50 41.2 82 10-108
bis(2-Ethylhexyl)phthalate ug/L 50 40.8 82 16-123
Butylbenzylphthalate ug/L 50 42.4 85 20-118
Chrysene ug/L 50 42.2 84 24-125
Di-n-butylphthalate ug/L 50 40.4 81 23-115
Di-n-octylphthalate ug/L 50 36.2 72 20-115
Dibenz(a,h)anthracene ug/L 50 43.1 86 18-131
Dibenzofuran ug/L 50 41.5 83 23-106
Diethylphthalate ug/L 50 40.5 81 24-115
Dimethylphthalate ug/L 50 39.3 79 22-113
Fluoranthene ug/L 50 43.0 86 24-125
Fluorene ug/L 50 43.9 88 24-114
Hexachloro-1,3-butadiene ug/L 50 21.3 43 10-110
Hexachlorobenzene ug/L 50 41.8 84 22-127
Hexachlorocyclopentadiene ug/L 50 36.5 73 10-110
Hexachloroethane ug/L 50 34.8 70 10-110
Indeno(1,2,3-cd)pyrene ug/L 50 42.5 85 18-130

(336)623-8921 (828)254-7176 (704)875-9092


Spike LCS LCS % Rec
Isophorone ug/L 50 34.1 68 23-114
N-Nitroso-di-n-propylamine ug/L 50 47.4 95 21-114
N-Nitrosodimethylamine ug/L 50 25.7 51 10-110
N-Nitrosodiphenylamine ug/L 50 40.8 82 24-123
Naphthalene ug/L 50 30.0 60 14-110
Nitrobenzene ug/L 50 31.5 63 16-106
Pentachlorophenol ug/L 100 88.6 89 10-123
Phenanthrene ug/L 50 42.3 85 25-119
Phenol ug/L 50 23.7 47 10-110
Pyrene ug/L 50 41.5 83 22-127
Phenol-d6 (S) % 34 10-110
Terphenyl-d14 (S) % 79 31-107

(336)623-8921 (828)254-7176 (704)875-9092

QC Batch: MSV/14634 Analysis Method: EPA 8260

QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Landfill

Blank Reporting
1,1,1,2-Tetrachloroethane ug/L ND 1.0 03/31/11 14:08
1,1,1-Trichloroethane ug/L ND 1.0 03/31/11 14:08
1,1-Dichloroethane ug/L ND 1.0 03/31/11 14:08
1,1-Dichloroethene ug/L ND 1.0 03/31/11 14:08
1,1-Dichloropropene ug/L ND 1.0 03/31/11 14:08
1,2,3-Trichloropropane ug/L ND 1.0 03/31/11 14:08
1,2-Dibromo-3-chloropropane ug/L ND 5.0 03/31/11 14:08
1,2-Dibromoethane (EDB) ug/L ND 1.0 03/31/11 14:08
1,2-Dichloropropane ug/L ND 1.0 03/31/11 14:08
2-Butanone (MEK) ug/L ND 5.0 03/31/11 14:08
2-Chlorotoluene ug/L ND 1.0 03/31/11 14:08
2-Hexanone ug/L ND 5.0 03/31/11 14:08
4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 03/31/11 14:08
Acetone ug/L ND 25.0 03/31/11 14:08
Benzene ug/L ND 1.0 03/31/11 14:08
Bromobenzene ug/L ND 1.0 03/31/11 14:08
Bromochloromethane ug/L ND 1.0 03/31/11 14:08
Bromodichloromethane ug/L ND 1.0 03/31/11 14:08
Bromoform ug/L ND 1.0 03/31/11 14:08
Bromomethane ug/L ND 2.0 03/31/11 14:08
Carbon tetrachloride ug/L ND 1.0 03/31/11 14:08
Chlorobenzene ug/L ND 1.0 03/31/11 14:08
Chloroethane ug/L ND 1.0 03/31/11 14:08
Chloroform ug/L ND 1.0 03/31/11 14:08
Chloromethane ug/L ND 1.0 03/31/11 14:08
cis-1,2-Dichloroethene ug/L ND 1.0 03/31/11 14:08
cis-1,3-Dichloropropene ug/L ND 1.0 03/31/11 14:08
Dibromochloromethane ug/L ND 1.0 03/31/11 14:08
Dibromomethane ug/L ND 1.0 03/31/11 14:08
Dichlorodifluoromethane ug/L ND 1.0 03/31/11 14:08
Diisopropyl ether ug/L ND 1.0 03/31/11 14:08
Ethylbenzene ug/L ND 1.0 03/31/11 14:08

(336)623-8921 (828)254-7176 (704)875-9092


Blank Reporting
Hexachloro-1,3-butadiene ug/L 1.0 1.0 03/31/11 14:08 B-
m&p-Xylene ug/L ND 2.0 03/31/11 14:08
Methyl-tert-butyl ether ug/L ND 1.0 03/31/11 14:08
Methylene Chloride ug/L ND 1.0 03/31/11 14:08
o-Xylene ug/L ND 1.0 03/31/11 14:08
p-Isopropyltoluene ug/L ND 1.0 03/31/11 14:08
Styrene ug/L ND 1.0 03/31/11 14:08
Tetrachloroethene ug/L ND 1.0 03/31/11 14:08
Toluene ug/L ND 1.0 03/31/11 14:08
trans-1,2-Dichloroethene ug/L ND 1.0 03/31/11 14:08
trans-1,3-Dichloropropene ug/L ND 1.0 03/31/11 14:08
Trichloroethene ug/L ND 1.0 03/31/11 14:08
Trichlorofluoromethane ug/L ND 1.0 03/31/11 14:08
Vinyl acetate ug/L ND 2.0 03/31/11 14:08
Vinyl chloride ug/L ND 1.0 03/31/11 14:08
1,2-Dichloroethane-d4 (S) % 122 70-130 03/31/11 14:08
Dibromofluoromethane (S) % 122 70-130 03/31/11 14:08
Toluene-d8 (S) % 98 70-130 03/31/11 14:08

Spike LCS LCS % Rec
1,1,1,2-Tetrachloroethane ug/L 50 52.0 104 70-130
1,1,1-Trichloroethane ug/L 50 51.1 102 70-130
1,1-Dichloroethane ug/L 50 51.2 102 70-130
1,1-Dichloroethene ug/L 50 51.0 102 70-132
1,1-Dichloropropene ug/L 50 51.0 102 70-130
1,2,3-Trichloropropane ug/L 50 53.1 106 70-130
1,2-Dibromo-3-chloropropane ug/L 50 51.8 104 70-130
1,2-Dibromoethane (EDB) ug/L 50 53.7 107 70-130
1,2-Dichloropropane ug/L 50 51.6 103 70-130
2-Butanone (MEK) ug/L 100 108 108 70-145
2-Chlorotoluene ug/L 50 56.2 112 70-130

(336)623-8921 (828)254-7176 (704)875-9092


Spike LCS LCS % Rec
2-Hexanone ug/L 100 98.7 99 70-144
4-Methyl-2-pentanone (MIBK) ug/L 100 96.3 96 70-140
Acetone ug/L 100 103 103 50-175
Benzene ug/L 50 50.9 102 70-130
Bromobenzene ug/L 50 52.1 104 70-130
Bromochloromethane ug/L 50 47.8 96 70-130
Bromodichloromethane ug/L 50 51.6 103 70-130
Bromoform ug/L 50 55.7 111 70-130
Bromomethane ug/L 50 57.8 116 54-130
Carbon tetrachloride ug/L 50 47.5 95 70-132
Chlorobenzene ug/L 50 50.8 102 70-130
Chloroethane ug/L 50 51.2 102 64-134
Chloroform ug/L 50 50.7 101 70-130
Chloromethane ug/L 50 47.6 95 64-130
cis-1,2-Dichloroethene ug/L 50 49.5 99 70-131
cis-1,3-Dichloropropene ug/L 50 47.4 95 70-130
Dibromochloromethane ug/L 50 52.5 105 70-130
Dibromomethane ug/L 50 51.2 102 70-131
Dichlorodifluoromethane ug/L 50 43.2 86 56-130
Diisopropyl ether ug/L 50 52.4 105 70-130
Ethylbenzene ug/L 50 54.8 110 70-130
m&p-Xylene ug/L 100 106 106 70-130
Methyl-tert-butyl ether ug/L 50 54.1 108 70-130
Methylene Chloride ug/L 50 48.9 98 63-130
o-Xylene ug/L 50 51.4 103 70-130
p-Isopropyltoluene ug/L 50 52.3 105 70-130
Styrene ug/L 50 50.8 102 70-130
Tetrachloroethene ug/L 50 53.8 108 70-130
Toluene ug/L 50 51.0 102 70-130
trans-1,2-Dichloroethene ug/L 50 49.8 100 70-130
trans-1,3-Dichloropropene ug/L 50 47.0 94 70-132
Trichloroethene ug/L 50 54.5 109 70-130
Trichlorofluoromethane ug/L 50 52.2 104 62-133
Vinyl acetate ug/L 100 104 104 66-157
Vinyl chloride ug/L 50 50.6 101 69-130
1,2-Dichloroethane-d4 (S) % 93 70-130
Dibromofluoromethane (S) % 96 70-130
Toluene-d8 (S) % 101 70-130

(336)623-8921 (828)254-7176 (704)875-9092


MS MSD
1,1-Dichloroethene ug/L ND 50 50 54.6 53.5 109 107 70-166 2
Benzene ug/L ND 50 50 54.2 53.5 108 107 70-148 1
Chlorobenzene ug/L ND 50 50 60.0 60.1 120 120 70-146 0
Toluene ug/L ND 50 50 56.3 55.5 113 111 70-155 1
Trichloroethene ug/L ND 50 50 52.0 50.8 104 102 69-151 2
1,2-Dichloroethane-d4 (S) % 112 114 70-130
Dibromofluoromethane (S) % 111 115 70-130
Toluene-d8 (S) % 90 88 70-130

(336)623-8921 (828)254-7176 (704)875-9092


QC Batch Method: EPA 8260 Analysis Description: 8260 MSV 5035A Volatile Organics

Blank Reporting
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 03/29/11 02:04
1,1,1-Trichloroethane ug/kg ND 5.0 03/29/11 02:04
1,1-Dichloroethane ug/kg ND 5.0 03/29/11 02:04
1,1-Dichloroethene ug/kg ND 5.0 03/29/11 02:04
1,1-Dichloropropene ug/kg ND 5.0 03/29/11 02:04
1,2,3-Trichlorobenzene ug/kg ND 5.0 03/29/11 02:04
1,2,3-Trichloropropane ug/kg ND 5.0 03/29/11 02:04
1,2,4-Trimethylbenzene ug/kg ND 5.0 03/29/11 02:04
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 03/29/11 02:04
1,2-Dibromoethane (EDB) ug/kg ND 5.0 03/29/11 02:04
1,2-Dichlorobenzene ug/kg ND 5.0 03/29/11 02:04
1,2-Dichloropropane ug/kg ND 5.0 03/29/11 02:04
2-Butanone (MEK) ug/kg ND 100 03/29/11 02:04
2-Chlorotoluene ug/kg ND 5.0 03/29/11 02:04
2-Hexanone ug/kg ND 50.0 03/29/11 02:04
4-Methyl-2-pentanone (MIBK) ug/kg ND 50.0 03/29/11 02:04
Acetone ug/kg ND 100 03/29/11 02:04
Benzene ug/kg ND 5.0 03/29/11 02:04
Bromobenzene ug/kg ND 5.0 03/29/11 02:04
Bromochloromethane ug/kg ND 5.0 03/29/11 02:04
Bromodichloromethane ug/kg ND 5.0 03/29/11 02:04
Bromoform ug/kg ND 5.0 03/29/11 02:04
Bromomethane ug/kg ND 10.0 03/29/11 02:04
Carbon tetrachloride ug/kg ND 5.0 03/29/11 02:04
Chlorobenzene ug/kg ND 5.0 03/29/11 02:04
Chloroethane ug/kg ND 10.0 03/29/11 02:04
Chloroform ug/kg ND 5.0 03/29/11 02:04
Chloromethane ug/kg ND 10.0 03/29/11 02:04
cis-1,2-Dichloroethene ug/kg ND 5.0 03/29/11 02:04
cis-1,3-Dichloropropene ug/kg ND 5.0 03/29/11 02:04
Dibromochloromethane ug/kg ND 5.0 03/29/11 02:04
Dibromomethane ug/kg ND 5.0 03/29/11 02:04
Dichlorodifluoromethane ug/kg ND 10.0 03/29/11 02:04

(336)623-8921 (828)254-7176 (704)875-9092


Blank Reporting
Diisopropyl ether ug/kg ND 5.0 03/29/11 02:04
Ethylbenzene ug/kg ND 5.0 03/29/11 02:04
Hexachloro-1,3-butadiene ug/kg ND 5.0 03/29/11 02:04
Isopropylbenzene (Cumene) ug/kg ND 5.0 03/29/11 02:04
m&p-Xylene ug/kg ND 10.0 03/29/11 02:04
Methyl-tert-butyl ether ug/kg ND 5.0 03/29/11 02:04
Methylene Chloride ug/kg ND 20.0 03/29/11 02:04
n-Butylbenzene ug/kg ND 5.0 03/29/11 02:04
n-Propylbenzene ug/kg ND 5.0 03/29/11 02:04
Naphthalene ug/kg ND 5.0 03/29/11 02:04
o-Xylene ug/kg ND 5.0 03/29/11 02:04
p-Isopropyltoluene ug/kg ND 5.0 03/29/11 02:04
sec-Butylbenzene ug/kg ND 5.0 03/29/11 02:04
Styrene ug/kg ND 5.0 03/29/11 02:04
tert-Butylbenzene ug/kg ND 5.0 03/29/11 02:04
Tetrachloroethene ug/kg ND 5.0 03/29/11 02:04
Toluene ug/kg ND 5.0 03/29/11 02:04
trans-1,2-Dichloroethene ug/kg ND 5.0 03/29/11 02:04
trans-1,3-Dichloropropene ug/kg ND 5.0 03/29/11 02:04
Trichloroethene ug/kg ND 5.0 03/29/11 02:04
Trichlorofluoromethane ug/kg ND 5.0 03/29/11 02:04
Vinyl acetate ug/kg ND 50.0 03/29/11 02:04
Vinyl chloride ug/kg ND 10.0 03/29/11 02:04
Toluene-d8 (S) % 99 70-130 03/29/11 02:04

Spike LCS LCS % Rec
1,1,1,2-Tetrachloroethane ug/kg 50 51.0 102 70-131
1,1,1-Trichloroethane ug/kg 50 47.6 95 70-141
1,1-Dichloroethane ug/kg 50 48.5 97 70-143
1,1-Dichloroethene ug/kg 50 47.8 96 70-137
1,1-Dichloropropene ug/kg 50 43.5 87 70-135
1,2,3-Trichlorobenzene ug/kg 50 53.7 107 69-153
1,2,3-Trichloropropane ug/kg 50 48.0 96 70-130
1,2,4-Trimethylbenzene ug/kg 50 48.4 97 70-149
1,2-Dibromo-3-chloropropane ug/kg 50 47.1 94 68-141
1,2-Dibromoethane (EDB) ug/kg 50 51.1 102 70-130
1,2-Dichlorobenzene ug/kg 50 49.3 99 70-140

(336)623-8921 (828)254-7176 (704)875-9092


Spike LCS LCS % Rec
1,2-Dichloropropane ug/kg 50 46.6 93 70-133
2-Butanone (MEK) ug/kg 100 93.9J 94 70-149
2-Chlorotoluene ug/kg 50 48.8 98 70-141
2-Hexanone ug/kg 100 102 102 70-149
4-Methyl-2-pentanone (MIBK) ug/kg 100 105 105 70-153
Acetone ug/kg 100 98.9J 99 70-157
Benzene ug/kg 50 47.5 95 70-130
Bromobenzene ug/kg 50 47.1 94 70-141
Bromochloromethane ug/kg 50 48.6 97 70-149
Bromodichloromethane ug/kg 50 51.5 103 70-130
Bromoform ug/kg 50 51.5 103 70-131
Bromomethane ug/kg 50 58.2 116 64-136
Carbon tetrachloride ug/kg 50 47.6 95 70-154
Chlorobenzene ug/kg 50 47.7 95 70-135
Chloroethane ug/kg 50 52.3 105 68-151
Chloroform ug/kg 50 50.6 101 70-130
Chloromethane ug/kg 50 52.1 104 70-132
cis-1,2-Dichloroethene ug/kg 50 48.2 96 70-140
cis-1,3-Dichloropropene ug/kg 50 49.9 100 70-137
Dibromochloromethane ug/kg 50 48.2 96 70-130
Dibromomethane ug/kg 50 50.5 101 70-136
Dichlorodifluoromethane ug/kg 50 58.0 116 36-148
Diisopropyl ether ug/kg 50 50.6 101 70-139
Ethylbenzene ug/kg 50 47.4 95 70-137
Hexachloro-1,3-butadiene ug/kg 50 47.7 95 70-145
Isopropylbenzene (Cumene) ug/kg 50 49.3 99 70-141
m&p-Xylene ug/kg 100 95.7 96 70-140
Methyl-tert-butyl ether ug/kg 50 50.8 102 45-150
Methylene Chloride ug/kg 50 47.0 94 70-133
n-Butylbenzene ug/kg 50 50.7 101 65-155
n-Propylbenzene ug/kg 50 47.4 95 70-148
Naphthalene ug/kg 50 54.6 109 70-148
o-Xylene ug/kg 50 48.9 98 70-141
p-Isopropyltoluene ug/kg 50 49.8 100 70-148
sec-Butylbenzene ug/kg 50 48.4 97 70-145
Styrene ug/kg 50 50.9 102 70-138
tert-Butylbenzene ug/kg 50 47.8 96 70-143
Tetrachloroethene ug/kg 50 42.6 85 70-140
Toluene ug/kg 50 46.9 94 70-130
trans-1,2-Dichloroethene ug/kg 50 45.9 92 70-136
trans-1,3-Dichloropropene ug/kg 50 51.9 104 70-138

(336)623-8921 (828)254-7176 (704)875-9092


Spike LCS LCS % Rec
Trichloroethene ug/kg 50 47.7 95 70-132
Trichlorofluoromethane ug/kg 50 51.5 103 69-134
Vinyl acetate ug/kg 100 90.5 91 24-161
Vinyl chloride ug/kg 50 49.9 100 55-140
Toluene-d8 (S) % 100 70-130
MATRIX SPIKE SAMPLE: 583931

9290652052 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
1,1-Dichloroethene ug/kg ND 52.6 50.1 95 49-180
Benzene ug/kg ND 52.6 52.6 100 50-166
Chlorobenzene ug/kg ND 52.6 55.4 105 43-169
Toluene ug/kg ND 52.6 55.8 106 52-163
Trichloroethene ug/kg ND 52.6 54.9 104 49-167
Toluene-d8 (S) % 98 70-130
SAMPLE DUPLICATE: 583930

9290680050 Dup
Parameter Units Result Result RPD Qualifiers
1,1,1,2-Tetrachloroethane ug/kg ND ND
1,1,1-Trichloroethane ug/kg ND ND
1,1,2,2-Tetrachloroethane ug/kg ND ND
1,1,2-Trichloroethane ug/kg ND ND
1,1-Dichloroethane ug/kg ND ND
1,1-Dichloroethene ug/kg ND ND
1,1-Dichloropropene ug/kg ND ND
1,2,3-Trichlorobenzene ug/kg ND ND
1,2,3-Trichloropropane ug/kg ND ND
1,2,4-Trichlorobenzene ug/kg ND ND
1,2,4-Trimethylbenzene ug/kg ND ND
1,2-Dibromo-3-chloropropane ug/kg ND ND
1,2-Dibromoethane (EDB) ug/kg ND ND
1,2-Dichlorobenzene ug/kg ND ND
1,2-Dichloroethane ug/kg ND ND
1,2-Dichloropropane ug/kg ND ND
1,3,5-Trimethylbenzene ug/kg ND ND

(336)623-8921 (828)254-7176 (704)875-9092


9290680050 Dup
2-Butanone (MEK) ug/kg ND ND
2-Chlorotoluene ug/kg ND ND
2-Hexanone ug/kg ND ND
4-Chlorotoluene ug/kg ND ND
4-Methyl-2-pentanone (MIBK) ug/kg ND ND
Acetone ug/kg ND 20.5J
Benzene ug/kg ND ND
Bromobenzene ug/kg ND ND
Bromochloromethane ug/kg ND ND
Bromodichloromethane ug/kg ND ND
Bromoform ug/kg ND ND
Bromomethane ug/kg ND ND
Carbon tetrachloride ug/kg ND ND
Chlorobenzene ug/kg ND ND
Chloroethane ug/kg ND ND
Chloroform ug/kg ND ND
Chloromethane ug/kg ND ND
cis-1,2-Dichloroethene ug/kg ND 5.2
cis-1,3-Dichloropropene ug/kg ND ND
Dibromochloromethane ug/kg ND ND
Dibromomethane ug/kg ND ND
Dichlorodifluoromethane ug/kg ND ND
Diisopropyl ether ug/kg ND ND
Ethylbenzene ug/kg ND ND
Hexachloro-1,3-butadiene ug/kg ND ND
Isopropylbenzene (Cumene) ug/kg ND ND
m&p-Xylene ug/kg ND ND
Methyl-tert-butyl ether ug/kg ND ND
Methylene Chloride ug/kg ND ND
n-Butylbenzene ug/kg ND ND
n-Propylbenzene ug/kg ND ND
Naphthalene ug/kg ND ND
o-Xylene ug/kg ND ND
p-Isopropyltoluene ug/kg ND ND
sec-Butylbenzene ug/kg ND ND
Styrene ug/kg ND ND
tert-Butylbenzene ug/kg ND ND
Tetrachloroethene ug/kg 15.0 5.0 100 R1
Toluene ug/kg ND ND
trans-1,2-Dichloroethene ug/kg ND ND
trans-1,3-Dichloropropene ug/kg ND ND
Trichloroethene ug/kg ND ND
Trichlorofluoromethane ug/kg ND ND
Vinyl acetate ug/kg ND ND
Vinyl chloride ug/kg ND ND
1,2-Dichloroethane-d4 (S) % 102 106 3
4-Bromofluorobenzene (S) % 95 94 2

(336)623-8921 (828)254-7176 (704)875-9092


9290680050 Dup
Dibromofluoromethane (S) % 105 107 1
Toluene-d8 (S) % 99 100 1

(336)623-8921 (828)254-7176 (704)875-9092


QC Batch Method: EPA 8260 Analysis Description: 8260 MSV 5035A Volatile Organics
Associated Lab Samples: 9290652053, 9290652054, 9290652055, 9290652056, 9290652059

Blank Reporting
1,1-Dichloroethene ug/kg ND 5.0 03/30/11 11:09
1,1-Dichloropropene ug/kg ND 5.0 03/30/11 11:09
1,2,3-Trichloropropane ug/kg ND 5.0 03/30/11 11:09
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 03/30/11 11:09
1,2-Dibromoethane (EDB) ug/kg ND 5.0 03/30/11 11:09
2-Butanone (MEK) ug/kg ND 100 03/30/11 11:09
2-Hexanone ug/kg ND 50.0 03/30/11 11:09
4-Methyl-2-pentanone (MIBK) ug/kg ND 50.0 03/30/11 11:09
Acetone ug/kg ND 100 03/30/11 11:09
Benzene ug/kg ND 5.0 03/30/11 11:09
Bromobenzene ug/kg ND 5.0 03/30/11 11:09
Bromochloromethane ug/kg ND 5.0 03/30/11 11:09
Bromodichloromethane ug/kg ND 5.0 03/30/11 11:09
Bromoform ug/kg ND 5.0 03/30/11 11:09
Bromomethane ug/kg ND 10.0 03/30/11 11:09
Carbon tetrachloride ug/kg ND 5.0 03/30/11 11:09
Chlorobenzene ug/kg ND 5.0 03/30/11 11:09
Chloroethane ug/kg ND 10.0 03/30/11 11:09
Chloroform ug/kg ND 5.0 03/30/11 11:09
Chloromethane ug/kg ND 10.0 03/30/11 11:09
cis-1,2-Dichloroethene ug/kg ND 5.0 03/30/11 11:09
cis-1,3-Dichloropropene ug/kg ND 5.0 03/30/11 11:09
Dibromochloromethane ug/kg ND 5.0 03/30/11 11:09
Dibromomethane ug/kg ND 5.0 03/30/11 11:09
Dichlorodifluoromethane ug/kg ND 10.0 03/30/11 11:09

(336)623-8921 (828)254-7176 (704)875-9092


Blank Reporting
Diisopropyl ether ug/kg ND 5.0 03/30/11 11:09
Ethylbenzene ug/kg ND 5.0 03/30/11 11:09
Hexachloro-1,3-butadiene ug/kg ND 5.0 03/30/11 11:09
Isopropylbenzene (Cumene) ug/kg ND 5.0 03/30/11 11:09
m&p-Xylene ug/kg ND 10.0 03/30/11 11:09
Methyl-tert-butyl ether ug/kg ND 5.0 03/30/11 11:09
Methylene Chloride ug/kg ND 20.0 03/30/11 11:09
n-Butylbenzene ug/kg ND 5.0 03/30/11 11:09
n-Propylbenzene ug/kg ND 5.0 03/30/11 11:09
Naphthalene ug/kg ND 5.0 03/30/11 11:09
o-Xylene ug/kg ND 5.0 03/30/11 11:09
p-Isopropyltoluene ug/kg ND 5.0 03/30/11 11:09
sec-Butylbenzene ug/kg ND 5.0 03/30/11 11:09
Styrene ug/kg ND 5.0 03/30/11 11:09
tert-Butylbenzene ug/kg ND 5.0 03/30/11 11:09
Tetrachloroethene ug/kg ND 5.0 03/30/11 11:09
Toluene ug/kg ND 5.0 03/30/11 11:09
trans-1,2-Dichloroethene ug/kg ND 5.0 03/30/11 11:09
trans-1,3-Dichloropropene ug/kg ND 5.0 03/30/11 11:09
Trichloroethene ug/kg ND 5.0 03/30/11 11:09
Trichlorofluoromethane ug/kg ND 5.0 03/30/11 11:09
Vinyl acetate ug/kg ND 50.0 03/30/11 11:09
Vinyl chloride ug/kg ND 10.0 03/30/11 11:09
Toluene-d8 (S) % 101 70-130 03/30/11 11:09

Spike LCS LCS % Rec
1,1-Dichloroethene ug/kg 50 48.4 97 70-137
1,1-Dichloropropene ug/kg 50 46.6 93 70-135
1,2,3-Trichloropropane ug/kg 50 45.4 91 70-130
1,2-Dibromo-3-chloropropane ug/kg 50 48.0 96 68-141
1,2-Dibromoethane (EDB) ug/kg 50 48.0 96 70-130

(336)623-8921 (828)254-7176 (704)875-9092


Spike LCS LCS % Rec
2-Butanone (MEK) ug/kg 100 89.9J 90 70-149
2-Hexanone ug/kg 100 93.5 93 70-149
4-Methyl-2-pentanone (MIBK) ug/kg 100 97.6 98 70-153
Acetone ug/kg 100 87.9J 88 70-157
Benzene ug/kg 50 48.4 97 70-130
Bromobenzene ug/kg 50 50.0 100 70-141
Bromochloromethane ug/kg 50 50.3 101 70-149
Bromodichloromethane ug/kg 50 50.1 100 70-130
Bromoform ug/kg 50 48.4 97 70-131
Bromomethane ug/kg 50 56.1 112 64-136
Carbon tetrachloride ug/kg 50 51.4 103 70-154
Chlorobenzene ug/kg 50 49.8 100 70-135
Chloroethane ug/kg 50 51.7 103 68-151
Chloroform ug/kg 50 51.8 104 70-130
Chloromethane ug/kg 50 44.5 89 70-132
cis-1,2-Dichloroethene ug/kg 50 47.7 95 70-140
cis-1,3-Dichloropropene ug/kg 50 49.1 98 70-137
Dibromochloromethane ug/kg 50 44.1 88 70-130
Dibromomethane ug/kg 50 48.7 97 70-136
Dichlorodifluoromethane ug/kg 50 34.0 68 36-148
Diisopropyl ether ug/kg 50 48.3 97 70-139
Ethylbenzene ug/kg 50 51.0 102 70-137
Hexachloro-1,3-butadiene ug/kg 50 53.1 106 70-145
Isopropylbenzene (Cumene) ug/kg 50 53.4 107 70-141
m&p-Xylene ug/kg 100 105 105 70-140
Methyl-tert-butyl ether ug/kg 50 47.6 95 45-150
Methylene Chloride ug/kg 50 45.9 92 70-133
n-Butylbenzene ug/kg 50 60.8 122 65-155
n-Propylbenzene ug/kg 50 55.2 110 70-148
Naphthalene ug/kg 50 53.2 106 70-148
o-Xylene ug/kg 50 51.3 103 70-141
p-Isopropyltoluene ug/kg 50 57.5 115 70-148
sec-Butylbenzene ug/kg 50 54.3 109 70-145
Styrene ug/kg 50 52.2 104 70-138
tert-Butylbenzene ug/kg 50 51.7 103 70-143
Tetrachloroethene ug/kg 50 46.6 93 70-140
Toluene ug/kg 50 51.2 102 70-130
trans-1,2-Dichloroethene ug/kg 50 47.1 94 70-136
trans-1,3-Dichloropropene ug/kg 50 51.2 102 70-138

(336)623-8921 (828)254-7176 (704)875-9092


Spike LCS LCS % Rec
Trichloroethene ug/kg 50 52.4 105 70-132
Trichlorofluoromethane ug/kg 50 54.0 108 69-134
Vinyl acetate ug/kg 100 318 318 24-161 L3
Vinyl chloride ug/kg 50 45.7 91 55-140
Toluene-d8 (S) % 99 70-130

MS MSD
1,1,1,2-Tetrachloroethane ug/kg ND 60.8 50.8 65.4 49.0 108 96 70-130 29
1,1,1-Trichloroethane ug/kg ND 60.8 50.8 66.0 51.6 109 102 70-130 24
1,1,2,2-Tetrachloroethane ug/kg ND 60.8 50.8 65.1 45.0 107 89 70-130 36 R1
1,1,2-Trichloroethane ug/kg ND 60.8 50.8 69.4 48.6 114 96 70-130 35 R1
1,1-Dichloroethane ug/kg ND 60.8 50.8 65.2 49.2 107 97 70-130 28
1,1-Dichloroethene ug/kg ND 60.8 50.8 63.5 50.2 105 99 49-180 23
1,1-Dichloropropene ug/kg ND 60.8 50.8 62.5 46.8 103 92 70-130 29
1,2,3-Trichlorobenzene ug/kg ND 60.8 50.8 70.9 52.5 117 103 70-130 30
1,2,3-Trichloropropane ug/kg ND 60.8 50.8 62.0 42.5 102 84 70-130 37 R1
1,2,4-Trichlorobenzene ug/kg ND 60.8 50.8 74.1 56.6 122 112 70-130 27
1,2,4-Trimethylbenzene ug/kg ND 60.8 50.8 66.9 51.3 110 101 70-130 26
1,2-Dibromo-3-chloropropane ug/kg ND 60.8 50.8 64.3 47.2 106 93 70-130 31 R1
1,2-Dibromoethane (EDB) ug/kg ND 60.8 50.8 63.0 45.4 104 89 70-130 32 R1
1,2-Dichlorobenzene ug/kg ND 60.8 50.8 66.6 50.1 110 99 70-130 28
1,2-Dichloroethane ug/kg ND 60.8 50.8 66.9 47.7 110 94 70-130 34 R1
1,2-Dichloropropane ug/kg ND 60.8 50.8 62.5 47.4 103 93 70-130 27
1,3,5-Trimethylbenzene ug/kg ND 60.8 50.8 69.0 52.9 114 104 70-130 26
1,3-Dichloropropane ug/kg ND 60.8 50.8 62.0 44.9 102 88 70-130 32 R1
2,2-Dichloropropane ug/kg ND 60.8 50.8 65.8 48.9 108 96 70-130 30
2-Butanone (MEK) ug/kg ND 121 102 121 81.3J 100 80 70-130
2-Chlorotoluene ug/kg ND 60.8 50.8 68.3 52.3 113 103 70-130 27
2-Hexanone ug/kg ND 121 102 141 93.0 116 92 70-130 41 R1
4-Chlorotoluene ug/kg ND 60.8 50.8 71.1 53.7 117 106 70-130 28
4-Methyl-2-pentanone (MIBK) ug/kg ND 121 102 136 92.7 112 91 70-130 38 R1
Acetone ug/kg ND 121 102 127 91.2J 105 90 70-130
Benzene ug/kg ND 60.8 50.8 62.9 48.5 104 96 50-166 26
Bromobenzene ug/kg ND 60.8 50.8 66.8 48.8 110 96 70-130 31 R1
Bromochloromethane ug/kg ND 60.8 50.8 65.1 49.6 107 98 70-130 27
Bromodichloromethane ug/kg ND 60.8 50.8 68.0 51.1 112 101 70-130 28
Bromoform ug/kg ND 60.8 50.8 64.4 44.3 106 87 70-130 37 R1
Bromomethane ug/kg ND 60.8 50.8 79.3 68.3 131 135 70-130 15 M0
Carbon tetrachloride ug/kg ND 60.8 50.8 74.0 57.5 122 113 70-130 25

(336)623-8921 (828)254-7176 (704)875-9092


MS MSD
Chlorobenzene ug/kg ND 60.8 50.8 64.6 48.4 106 95 43-169 29
Chloroethane ug/kg ND 60.8 50.8 65.8 48.6 108 96 70-130 30
Chloroform ug/kg ND 60.8 50.8 69.6 52.2 115 103 70-130 28
Chloromethane ug/kg ND 60.8 50.8 57.9 43.4 95 85 70-130 29
cis-1,2-Dichloroethene ug/kg ND 60.8 50.8 63.9 48.1 105 95 70-130 28
cis-1,3-Dichloropropene ug/kg ND 60.8 50.8 64.3 48.4 106 95 70-130 28
Dibromochloromethane ug/kg ND 60.8 50.8 60.1 43.1 99 85 70-130 33 R1
Dibromomethane ug/kg ND 60.8 50.8 62.4 48.3 103 95 70-130 26
Dichlorodifluoromethane ug/kg ND 60.8 50.8 45.6 33.9 75 67 70-130 29 M0
Diisopropyl ether ug/kg ND 60.8 50.8 64.2 48.4 106 95 70-130 28
Ethylbenzene ug/kg ND 60.8 50.8 66.2 49.9 109 98 70-130 28
Hexachloro-1,3-butadiene ug/kg ND 60.8 50.8 65.3 51.0 107 100 70-130 25
Isopropylbenzene (Cumene) ug/kg ND 60.8 50.8 68.6 51.9 113 102 70-130 28
m&p-Xylene ug/kg ND 121 102 136 101 112 100 70-130 29
Methyl-tert-butyl ether ug/kg ND 60.8 50.8 63.8 45.8 105 90 70-130 33 R1
Methylene Chloride ug/kg ND 60.8 50.8 66.0 52.0 109 103 70-130 24
n-Butylbenzene ug/kg ND 60.8 50.8 74.7 57.4 123 113 70-130 26
n-Propylbenzene ug/kg ND 60.8 50.8 70.7 54.1 116 107 70-130 27
Naphthalene ug/kg ND 60.8 50.8 66.7 48.5 110 96 70-130 32 R1
o-Xylene ug/kg ND 60.8 50.8 66.5 49.4 109 97 70-130 29
p-Isopropyltoluene ug/kg ND 60.8 50.8 72.4 55.2 119 109 70-130 27
sec-Butylbenzene ug/kg ND 60.8 50.8 67.9 55.0 112 108 70-130 21
Styrene ug/kg ND 60.8 50.8 50.7 36.4 83 72 70-130 33 R1
tert-Butylbenzene ug/kg ND 60.8 50.8 66.8 52.4 110 103 70-130 24
Tetrachloroethene ug/kg ND 60.8 50.8 60.7 44.7 100 88 70-130 30
Toluene ug/kg ND 60.8 50.8 65.6 50.5 108 99 52-163 26
trans-1,2-Dichloroethene ug/kg ND 60.8 50.8 62.3 47.4 103 93 70-130 27
trans-1,3-Dichloropropene ug/kg ND 60.8 50.8 66.4 49.0 109 97 70-130 30
Trichloroethene ug/kg ND 60.8 50.8 65.3 50.7 108 100 49-167 25
Trichlorofluoromethane ug/kg ND 60.8 50.8 71.6 51.1 118 101 70-130 33 R1
Vinyl acetate ug/kg ND 121 102 161 111 133 109 70-130 37 M0,R1
Vinyl chloride ug/kg ND 60.8 50.8 60.0 44.8 99 88 70-130 29
Toluene-d8 (S) % 100 101 70-130

(336)623-8921 (828)254-7176 (704)875-9092

QC Batch: PMST/3817 Analysis Method: ASTM D2974-87

QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
9290652009, 9290652010, 9290652011, 9290652012, 9290652013, 9290652014, 9290652015

9290650001 Dup
Percent Moisture % 31.3 30.8 2

9290671001 Dup

(336)623-8921 (828)254-7176 (704)875-9092


9290652025, 9290652026, 9290652027, 9290652028, 9290652029, 9290652030, 9290652031, 9290652032,
9290652033, 9290652034, 9290652035

9290652016 Dup

9290652035 Dup

(336)623-8921 (828)254-7176 (704)875-9092


9290652044, 9290652046, 9290652047, 9290652048, 9290652049, 9290652050, 9290652051, 9290652052,
9290652053, 9290652054, 9290652055, 9290652056

9290652036 Dup

9290652056 Dup

(336)623-8921 (828)254-7176 (704)875-9092



9290591001 Dup

9290680072 Dup
Percent Moisture % 12.4

(336)623-8921 (828)254-7176 (704)875-9092
QUALIFIERS

DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
LABORATORIES
PASI-C Pace Analytical Services - Charlotte
SAMPLE QUALIFIERS
Sample: 9290652012
[1] A
Sample: 9290652013
[1] A
Sample: 9290652014
[1] A
Sample: 9290652015
[1] A
Sample: 9290652016
[1] A
Sample: 9290652017
[1] A
Sample: 9290652018
[1] A
Sample: 9290652020
[1] A
Sample: 9290652021
[1] A
Sample: 9290652022
[1] A

(336)623-8921 (828)254-7176 (704)875-9092
QUALIFIERS

SAMPLE QUALIFIERS
Sample: 9290652023
[1] A
Sample: 9290652024
[1] A
Sample: 9290652025
[1] A
Sample: 9290652026
[1] A
Sample: 9290652027
[1] A
Sample: 9290652028
[1] A
Sample: 9290652029
[1] A
Sample: 9290652030
[1] A
Sample: 9290652031
[1] A
Sample: 9290652032
[1] A
Sample: 9290652033
[1] A
Sample: 9290652034
[1] A
Sample: 9290652035
[1] A
Sample: 9290652036
[1] A
Sample: 9290652037
[1] A
Sample: 9290652038
[1] A
Sample: 9290652039
[1] A
Sample: 9290652040
[1] A
Sample: 9290652041
[1] A
Sample: 9290652042
[1] A
Sample: 9290652043
[1] A

(336)623-8921 (828)254-7176 (704)875-9092
QUALIFIERS

SAMPLE QUALIFIERS
Sample: 9290652044
[1] A
Sample: 9290652045
[1] A
Sample: 9290652046
[1] A
Sample: 9290652047
[1] A
Sample: 9290652048
[1] A
Sample: 9290652049
[1] A
Sample: 9290652050
[1] A
Sample: 9290652051
[1] A
Sample: 9290652052
[1] A
Sample: 9290652053
[1] A
Sample: 9290652054
[1] A
Sample: 9290652055
[1] A
Sample: 9290652056
[1] A
Sample: 9290652058
[1] A
Sample: 9290652059
[1] A
Sample: 9290652060
[1] A
ANALYTE QUALIFIERS
1g Surrogate fails after Moisture Correction for Methanol.
B- Analyte detected in method blank but was not detected in the associated samples.
L3 Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.
M0 Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold NELAC accreditation for this parameter.
P3 Sample extract could not be concentrated to the routine final volume, resulting in elevated reporting limits.
R1 RPD value was outside control limits.

(336)623-8921 (828)254-7176 (704)875-9092
QUALIFIERS

ANALYTE QUALIFIERS
S0 Surrogate recovery outside laboratory control limits.
S2 Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re-analysis).
S3 Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated samples.
Results unaffected by high bias.
S4 Surrogate recovery not evaluated against control limits due to sample dilution.
S5 Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis).

(336)623-8921 (828)254-7176 (704)875-9092
LIMS USE: FR - LISA MANNING

LIMS OBJECT ID: 9290693
April 08, 2011
Ms. Lisa Manning

Altamont Environmental
231 Haywood St.
Asheville, NC 28801
RE: Project: McGill Kings Mountain 3/25

Dear Ms. Manning:

Enclosed are the analytical results for sample(s) received by the laboratory on March 28, 2011. The
results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lorri Patton
lorri.patton@pacelabs.com
Project Manager
Enclosures
cc: Mr. Adam Tripp, Altamont Environmental

(336)623-8921 (828)254-7176 (704)875-9092
CERTIFICATIONS

Charlotte Certification IDs

9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Drinking Water Cert. #: 99006003
Louisiana/LELAP Certification #: 04034 Virginia Certification #: 00213
New Jersey Certification #: NC012 Connecticut Certification #: PH-0104
North Carolina Drinking Water Certification #: 37706 Florida/NELAP Certification #: E87627
North Carolina Field Services Certification #: 5342 Kentucky UST Certification #: 84
North Carolina Wastewater Certification #: 12 Louisiana DHH Drinking Water # LA 100031
Pennsylvania Certification #: 68-00784 West Virginia Certification #: 357
South Carolina Certification #: 99006001
Asheville Certification IDs

2225 Riverside Dr., Asheville, NC 28804 North Carolina Wastewater Certification #: 40
Connecticut Certification #: PH-0106 Pennsylvania Certification #: 68-03578
Florida/NELAP Certification #: E87648 South Carolina Bioassay Certification #: 99030002
Massachusetts Certification #: M-NC030 South Carolina Certification #: 99030001
New Jersey Certification #: NC011 Virginia Certification #: 00072
North Carolina Bioassay Certification #: 9 West Virginia Certification #: 356
North Carolina Drinking Water Certification #: 37712

(336)623-8921 (828)254-7176 (704)875-9092

Analytes
9290693001 MW-1 MADEP EPH RES 5 PASI-C

EPA 200.7 JMW 1 PASI-A
SM 6200B TLS 65 PASI-C
9290693004 MW-3 DUPLICATE MADEP EPH RES 5 PASI-C
9290693005 Field Blank MADEP EPH RES 7 PASI-C
9290693006 Trip Blank SM 6200B TLS 65 PASI-C

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

Sample: MW-1 Lab ID: 9290693001 Collected: 03/25/11 14:10 Received: 03/28/11 08:25 Matrix: Water

o-Terphenyl (S) 89 % 40-140 1 04/01/11 10:30 04/01/11 23:57 84-15-1

200.7 MET ICP, 3030C Analytical Method: EPA 200.7 Preparation Method: SM 3030C
Lead ND ug/L 5.0 1 03/28/11 11:10 03/30/11 19:29 7439-92-1
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625

Chrysene ND ug/L 5.0 1 04/01/11 14:30 04/04/11 21:58 218-01-9

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


Fluorene ND ug/L 5.0 1 04/01/11 14:30 04/04/11 21:58 86-73-7
Phenol ND ug/L 5.0 1 04/01/11 14:30 04/04/11 21:58 108-95-2
Pyrene ND ug/L 5.0 1 04/01/11 14:30 04/04/11 21:58 129-00-0
Nitrobenzene-d5 (S) 75 % 10-120 1 04/01/11 14:30 04/04/11 21:58 4165-60-0
Terphenyl-d14 (S) 99 % 11-131 1 04/01/11 14:30 04/04/11 21:58 1718-51-0
Phenol-d6 (S) 25 % 10-120 1 04/01/11 14:30 04/04/11 21:58 13127-88-3
2-Fluorophenol (S) 39 % 10-120 1 04/01/11 14:30 04/04/11 21:58 367-12-4
6200B MSV Analytical Method: SM 6200B
Benzene 2.3 ug/L 0.50 1 04/02/11 02:11 71-43-2

Bromoform ND ug/L 0.50 1 04/02/11 02:11 75-25-2
n-Butylbenzene ND ug/L 0.50 1 04/02/11 02:11 104-51-8
sec-Butylbenzene ND ug/L 0.50 1 04/02/11 02:11 135-98-8
tert-Butylbenzene ND ug/L 0.50 1 04/02/11 02:11 98-06-6

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


1,2-Dichloroethane 17.7 ug/L 0.50 1 04/02/11 02:11 107-06-2
1,2-Dichloropropane 1.5 ug/L 0.50 1 04/02/11 02:11 78-87-5
Diisopropyl ether 195 ug/L 0.50 1 04/02/11 02:11 108-20-3
Ethanol ND ug/L 200 1 04/02/11 02:11 64-17-5
Ethylbenzene 1.8 ug/L 0.50 1 04/02/11 02:11 100-41-4
Isopropylbenzene (Cumene) ND ug/L 0.50 1 04/02/11 02:11 98-82-8
Methyl-tert-butyl ether 1.3 ug/L 0.50 1 04/02/11 02:11 1634-04-4
Naphthalene 3.9 ug/L 2.0 1 04/02/11 02:11 91-20-3
n-Propylbenzene ND ug/L 0.50 1 04/02/11 02:11 103-65-1
Styrene ND ug/L 0.50 1 04/02/11 02:11 100-42-5
Toluene ND ug/L 0.50 1 04/02/11 02:11 108-88-3
1,1,2-Trichloroethane 1.3 ug/L 0.50 1 04/02/11 02:11 79-00-5
1,2,4-Trimethylbenzene 0.50 ug/L 0.50 1 04/02/11 02:11 95-63-6
1,3,5-Trimethylbenzene ND ug/L 0.50 1 04/02/11 02:11 108-67-8
m&p-Xylene ND ug/L 1.0 1 04/02/11 02:11 179601-23-1
o-Xylene 0.71 ug/L 0.50 1 04/02/11 02:11 95-47-6

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


Toluene-d8 (S) 101 % 70-130 1 04/02/11 02:11 2037-26-5

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


o-Terphenyl (S) 98 % 40-140 1 04/01/11 10:30 04/04/11 21:47 84-15-1
Aliphatic (C05-C08) 260 ug/L 30.0 1 04/07/11 06:32 N2

Aliphatic (C09-C12) 737 ug/L 30.0 1 04/07/11 06:32 N2
Aromatic (C09-C10) 153 ug/L 30.0 1 04/07/11 06:32 N2
Lead ND ug/L 5.0 1 03/28/11 11:10 03/30/11 19:32 7439-92-1

Chrysene ND ug/L 5.0 1 04/01/11 14:30 04/04/11 22:26 218-01-9

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


Fluorene ND ug/L 5.0 1 04/01/11 14:30 04/04/11 22:26 86-73-7
Phenol ND ug/L 5.0 1 04/01/11 14:30 04/04/11 22:26 108-95-2
Pyrene ND ug/L 5.0 1 04/01/11 14:30 04/04/11 22:26 129-00-0
Nitrobenzene-d5 (S) 91 % 10-120 1 04/01/11 14:30 04/04/11 22:26 4165-60-0
Terphenyl-d14 (S) 106 % 11-131 1 04/01/11 14:30 04/04/11 22:26 1718-51-0
Phenol-d6 (S) 22 % 10-120 1 04/01/11 14:30 04/04/11 22:26 13127-88-3
2-Fluorophenol (S) 32 % 10-120 1 04/01/11 14:30 04/04/11 22:26 367-12-4
Benzene ND ug/L 0.50 1 04/02/11 02:34 71-43-2

Bromoform ND ug/L 0.50 1 04/02/11 02:34 75-25-2
Chloroform 1.6 ug/L 0.50 1 04/02/11 02:34 67-66-3

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


Ethanol ND ug/L 200 1 04/02/11 02:34 64-17-5
Styrene ND ug/L 0.50 1 04/02/11 02:34 100-42-5
Toluene ND ug/L 0.50 1 04/02/11 02:34 108-88-3
m&p-Xylene ND ug/L 1.0 1 04/02/11 02:34 179601-23-1
o-Xylene ND ug/L 0.50 1 04/02/11 02:34 95-47-6

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


Toluene-d8 (S) 96 % 70-130 1 04/02/11 02:34 2037-26-5

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


o-Terphenyl (S) 81 % 40-140 1 04/01/11 10:30 04/04/11 22:23 84-15-1

Lead ND ug/L 5.0 1 03/28/11 11:10 03/30/11 18:59 7439-92-1

Chrysene ND ug/L 5.0 1 04/01/11 14:30 04/04/11 22:53 218-01-9

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


Fluorene ND ug/L 5.0 1 04/01/11 14:30 04/04/11 22:53 86-73-7
Phenol ND ug/L 5.0 1 04/01/11 14:30 04/04/11 22:53 108-95-2
Pyrene ND ug/L 5.0 1 04/01/11 14:30 04/04/11 22:53 129-00-0
Nitrobenzene-d5 (S) 70 % 10-120 1 04/01/11 14:30 04/04/11 22:53 4165-60-0
Terphenyl-d14 (S) 97 % 11-131 1 04/01/11 14:30 04/04/11 22:53 1718-51-0
Phenol-d6 (S) 25 % 10-120 1 04/01/11 14:30 04/04/11 22:53 13127-88-3
2-Fluorophenol (S) 34 % 10-120 1 04/01/11 14:30 04/04/11 22:53 367-12-4
Benzene ND ug/L 0.50 1 04/02/11 02:57 71-43-2

Bromoform ND ug/L 0.50 1 04/02/11 02:57 75-25-2
Chloroform 1.5 ug/L 0.50 1 04/02/11 02:57 67-66-3

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


Ethanol ND ug/L 200 1 04/02/11 02:57 64-17-5
Styrene ND ug/L 0.50 1 04/02/11 02:57 100-42-5
Toluene ND ug/L 0.50 1 04/02/11 02:57 108-88-3
m&p-Xylene ND ug/L 1.0 1 04/02/11 02:57 179601-23-1
o-Xylene ND ug/L 0.50 1 04/02/11 02:57 95-47-6

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


Toluene-d8 (S) 96 % 70-130 1 04/02/11 02:57 2037-26-5

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

Sample: MW-3 DUPLICATE Lab ID: 9290693004 Collected: 03/25/11 12:00 Received: 03/28/11 08:25 Matrix: Water

o-Terphenyl (S) 103 % 40-140 1 04/01/11 10:30 04/02/11 01:09 84-15-1

Lead ND ug/L 5.0 1 03/28/11 11:10 03/30/11 19:19 7439-92-1

Chrysene ND ug/L 5.0 1 04/01/11 14:30 04/05/11 00:16 218-01-9

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


Fluorene ND ug/L 5.0 1 04/01/11 14:30 04/05/11 00:16 86-73-7
Phenol ND ug/L 5.0 1 04/01/11 14:30 04/05/11 00:16 108-95-2
Pyrene ND ug/L 5.0 1 04/01/11 14:30 04/05/11 00:16 129-00-0
Nitrobenzene-d5 (S) 73 % 10-120 1 04/01/11 14:30 04/05/11 00:16 4165-60-0
Terphenyl-d14 (S) 102 % 11-131 1 04/01/11 14:30 04/05/11 00:16 1718-51-0
Phenol-d6 (S) 25 % 10-120 1 04/01/11 14:30 04/05/11 00:16 13127-88-3
2-Fluorophenol (S) 38 % 10-120 1 04/01/11 14:30 04/05/11 00:16 367-12-4
Benzene ND ug/L 0.50 1 04/06/11 23:41 71-43-2

Bromoform ND ug/L 0.50 1 04/06/11 23:41 75-25-2
Chloroform 1.5 ug/L 0.50 1 04/06/11 23:41 67-66-3

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


Ethanol ND ug/L 200 1 04/06/11 23:41 64-17-5
Styrene ND ug/L 0.50 1 04/06/11 23:41 100-42-5
Toluene ND ug/L 0.50 1 04/06/11 23:41 108-88-3
m&p-Xylene ND ug/L 1.0 1 04/06/11 23:41 179601-23-1
o-Xylene ND ug/L 0.50 1 04/06/11 23:41 95-47-6

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


Toluene-d8 (S) 96 % 70-130 1 04/06/11 23:41 2037-26-5

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

Sample: Field Blank Lab ID: 9290693005 Collected: 03/25/11 16:40 Received: 03/28/11 08:25 Matrix: Water

o-Terphenyl (S) 89 % 40-140 1 04/01/11 10:30 04/05/11 11:45 84-15-1

Lead ND ug/L 5.0 1 03/28/11 11:10 03/30/11 19:35 7439-92-1

Chrysene ND ug/L 5.0 1 04/01/11 14:30 04/05/11 00:44 218-01-9

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


Fluorene ND ug/L 5.0 1 04/01/11 14:30 04/05/11 00:44 86-73-7
Phenol ND ug/L 5.0 1 04/01/11 14:30 04/05/11 00:44 108-95-2
Pyrene ND ug/L 5.0 1 04/01/11 14:30 04/05/11 00:44 129-00-0
Nitrobenzene-d5 (S) 68 % 10-120 1 04/01/11 14:30 04/05/11 00:44 4165-60-0
Terphenyl-d14 (S) 101 % 11-131 1 04/01/11 14:30 04/05/11 00:44 1718-51-0
Phenol-d6 (S) 24 % 10-120 1 04/01/11 14:30 04/05/11 00:44 13127-88-3
2-Fluorophenol (S) 37 % 10-120 1 04/01/11 14:30 04/05/11 00:44 367-12-4
Benzene ND ug/L 0.50 1 04/02/11 03:43 71-43-2

Bromoform ND ug/L 0.50 1 04/02/11 03:43 75-25-2

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


Ethanol ND ug/L 200 1 04/02/11 03:43 64-17-5
Styrene ND ug/L 0.50 1 04/02/11 03:43 100-42-5
Toluene ND ug/L 0.50 1 04/02/11 03:43 108-88-3
m&p-Xylene ND ug/L 1.0 1 04/02/11 03:43 179601-23-1
o-Xylene ND ug/L 0.50 1 04/02/11 03:43 95-47-6

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS


Toluene-d8 (S) 96 % 70-130 1 04/02/11 03:43 2037-26-5

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

Sample: Trip Blank Lab ID: 9290693006 Collected: 03/25/11 00:00 Received: 03/28/11 08:25 Matrix: Water
Benzene ND ug/L 0.50 1 04/02/11 04:06 71-43-2

Bromoform ND ug/L 0.50 1 04/02/11 04:06 75-25-2
Ethanol ND ug/L 200 1 04/02/11 04:06 64-17-5
Styrene ND ug/L 0.50 1 04/02/11 04:06 100-42-5

(336)623-8921 (828)254-7176 (704)875-9092
ANALYTICAL RESULTS

Sample: Trip Blank Lab ID: 9290693006 Collected: 03/25/11 00:00 Received: 03/28/11 08:25 Matrix: Water

Toluene ND ug/L 0.50 1 04/02/11 04:06 108-88-3
m&p-Xylene ND ug/L 1.0 1 04/02/11 04:06 179601-23-1
o-Xylene ND ug/L 0.50 1 04/02/11 04:06 95-47-6
Toluene-d8 (S) 96 % 70-130 1 04/02/11 04:06 2037-26-5

(336)623-8921 (828)254-7176 (704)875-9092


QC Batch Method: MADEP EPH Analysis Description: MADEP EPH NC Water

Blank Reporting
Aromatic (C11-C22) ug/L ND 100 04/04/11 19:23 N2
o-Terphenyl (S) % 83 40-140 04/04/11 19:23

Aromatic (C11-C22) ug/L 850 835 811 98 95 40-140 3 50 N2
o-Terphenyl (S) % 101 101 40-140

MS MSD
o-Terphenyl (S) % 72 86 40-140

MS MSD

(336)623-8921 (828)254-7176 (704)875-9092


MS MSD
o-Terphenyl (S) % 92 82 40-140

(336)623-8921 (828)254-7176 (704)875-9092


Associated Lab Samples: 9290693003, 9290693004, 9290693005

Associated Lab Samples: 9290693003, 9290693004, 9290693005
Blank Reporting

Aromatic (C09-C10) ug/L 100 101 102 101 102 70-130 0 25 N2

(336)623-8921 (828)254-7176 (704)875-9092



Blank Reporting

Aromatic (C09-C10) ug/L 100 100 99.0 100 99 70-130 1 25 N2

(336)623-8921 (828)254-7176 (704)875-9092

QC Batch: MPRP/8096 Analysis Method: EPA 200.7

QC Batch Method: SM 3030C Analysis Description: 200.7 MET 3030C

Blank Reporting
Lead ug/L ND 5.0 03/30/11 18:52

Spike LCS LCS % Rec
Lead ug/L 500 549 110 85-115

MS MSD
Lead ug/L ND 500 500 517 514 103 102 70-130 1

MS MSD
Lead ug/L ND 500 500 520 530 104 106 70-130 2

MS MSD
Lead ug/L ND 500 500 541 543 108 108 70-130 0

(336)623-8921 (828)254-7176 (704)875-9092


QC Batch Method: EPA 625 Analysis Description: 625 MSS

Blank Reporting
2,4-Dichlorophenol ug/L ND 5.0 04/04/11 21:03
2,4-Dimethylphenol ug/L ND 10.0 04/04/11 21:03
2,4-Dinitrophenol ug/L ND 50.0 04/04/11 21:03
2-Chloronaphthalene ug/L ND 5.0 04/04/11 21:03
2-Chlorophenol ug/L ND 5.0 04/04/11 21:03
3,3'-Dichlorobenzidine ug/L ND 25.0 04/04/11 21:03
4,6-Dinitro-2-methylphenol ug/L ND 20.0 04/04/11 21:03
4-Bromophenylphenyl ether ug/L ND 5.0 04/04/11 21:03
4-Chloro-3-methylphenol ug/L ND 5.0 04/04/11 21:03
4-Chlorophenylphenyl ether ug/L ND 5.0 04/04/11 21:03
Acenaphthene ug/L ND 5.0 04/04/11 21:03
Acenaphthylene ug/L ND 5.0 04/04/11 21:03
Anthracene ug/L ND 5.0 04/04/11 21:03
Benzo(a)anthracene ug/L ND 5.0 04/04/11 21:03
Benzo(a)pyrene ug/L ND 5.0 04/04/11 21:03
Benzo(b)fluoranthene ug/L ND 5.0 04/04/11 21:03
Benzo(g,h,i)perylene ug/L ND 5.0 04/04/11 21:03
Benzo(k)fluoranthene ug/L ND 5.0 04/04/11 21:03
bis(2-Chloroethoxy)methane ug/L ND 10.0 04/04/11 21:03
bis(2-Chloroethyl) ether ug/L ND 5.0 04/04/11 21:03
bis(2-Chloroisopropyl) ether ug/L ND 5.0 04/04/11 21:03
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 04/04/11 21:03
Butylbenzylphthalate ug/L ND 5.0 04/04/11 21:03
Chrysene ug/L ND 5.0 04/04/11 21:03
Di-n-butylphthalate ug/L ND 5.0 04/04/11 21:03
Di-n-octylphthalate ug/L ND 5.0 04/04/11 21:03
Dibenz(a,h)anthracene ug/L ND 5.0 04/04/11 21:03
Diethylphthalate ug/L ND 5.0 04/04/11 21:03
Dimethylphthalate ug/L ND 5.0 04/04/11 21:03
Fluoranthene ug/L ND 5.0 04/04/11 21:03
Fluorene ug/L ND 5.0 04/04/11 21:03
Hexachlorobenzene ug/L ND 5.0 04/04/11 21:03
Hexachlorocyclopentadiene ug/L ND 10.0 04/04/11 21:03
Hexachloroethane ug/L ND 5.0 04/04/11 21:03
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 04/04/11 21:03
Isophorone ug/L ND 10.0 04/04/11 21:03

(336)623-8921 (828)254-7176 (704)875-9092


Blank Reporting
N-Nitroso-di-n-propylamine ug/L ND 5.0 04/04/11 21:03
N-Nitrosodimethylamine ug/L ND 5.0 04/04/11 21:03
N-Nitrosodiphenylamine ug/L ND 10.0 04/04/11 21:03
Nitrobenzene ug/L ND 5.0 04/04/11 21:03
Pentachlorophenol ug/L ND 25.0 04/04/11 21:03
Phenanthrene ug/L ND 5.0 04/04/11 21:03
Phenol ug/L ND 5.0 04/04/11 21:03
Pyrene ug/L ND 5.0 04/04/11 21:03
2-Fluorophenol (S) % 35 10-120 04/04/11 21:03
Nitrobenzene-d5 (S) % 59 10-120 04/04/11 21:03
Phenol-d6 (S) % 23 10-120 04/04/11 21:03
Terphenyl-d14 (S) % 94 11-131 04/04/11 21:03

Spike LCS LCS % Rec
2,4-Dichlorophenol ug/L 50 33.3 67 1-191
2,4-Dimethylphenol ug/L 50 32.9 66 32-119
2,4-Dinitrophenol ug/L 250 193 77 1-181
2-Chloronaphthalene ug/L 50 43.7 87 60-118
2-Chlorophenol ug/L 50 38.8 78 23-134
2-Nitrophenol ug/L 50 32.5 65 29-182
3,3'-Dichlorobenzidine ug/L 100 79.1 79 1-262
4,6-Dinitro-2-methylphenol ug/L 100 97.2 97 1-181
4-Bromophenylphenyl ether ug/L 50 44.6 89 53-127
4-Chloro-3-methylphenol ug/L 100 77.4 77 22-147
4-Chlorophenylphenyl ether ug/L 50 43.2 86 25-158
4-Nitrophenol ug/L 250 95.0 38 1-132
Acenaphthene ug/L 50 46.8 94 47-145
Acenaphthylene ug/L 50 44.6 89 33-145
Anthracene ug/L 50 45.9 92 1-166
Benzo(a)anthracene ug/L 50 44.2 88 33-143
Benzo(a)pyrene ug/L 50 42.1 84 17-163
Benzo(b)fluoranthene ug/L 50 44.1 88 24-159
Benzo(g,h,i)perylene ug/L 50 44.9 90 1-219
Benzo(k)fluoranthene ug/L 50 48.4 97 11-162
bis(2-Chloroethoxy)methane ug/L 50 42.8 86 33-184
bis(2-Chloroethyl) ether ug/L 50 42.4 85 12-158

(336)623-8921 (828)254-7176 (704)875-9092


Spike LCS LCS % Rec
bis(2-Chloroisopropyl) ether ug/L 50 46.5 93 36-166
bis(2-Ethylhexyl)phthalate ug/L 50 43.0 86 8-158
Butylbenzylphthalate ug/L 50 45.6 91 1-152
Chrysene ug/L 50 46.1 92 17-168
Di-n-butylphthalate ug/L 50 42.1 84 1-118
Di-n-octylphthalate ug/L 50 35.2 70 4-146
Dibenz(a,h)anthracene ug/L 50 43.1 86 1-227
Diethylphthalate ug/L 50 42.9 86 1-114
Dimethylphthalate ug/L 50 41.6 83 1-112
Fluoranthene ug/L 50 43.4 87 26-137
Fluorene ug/L 50 47.0 94 59-121
Hexachlorobenzene ug/L 50 44.8 90 1-152
Hexachlorocyclopentadiene ug/L 50 34.7 69 25-150
Hexachloroethane ug/L 50 30.0 60 40-113
Indeno(1,2,3-cd)pyrene ug/L 50 43.4 87 1-171
Isophorone ug/L 50 37.6 75 21-196
N-Nitroso-di-n-propylamine ug/L 50 44.6 89 1-230
N-Nitrosodimethylamine ug/L 50 26.4 53 25-150
N-Nitrosodiphenylamine ug/L 50 44.4 89 25-150
Nitrobenzene ug/L 50 33.4 67 35-180
Pentachlorophenol ug/L 100 77.7 78 14-176
Phenanthrene ug/L 50 44.9 90 54-120
Phenol ug/L 50 22.6 45 5-112
Pyrene ug/L 50 49.9 100 52-115
Phenol-d6 (S) % 34 10-120
Terphenyl-d14 (S) % 100 11-131

MS MSD
1,2,4-Trichlorobenzene ug/L ND 100 100 60.0 60.5 60 60 44-142 1
2,4,6-Trichlorophenol ug/L ND 100 100 86.3 95.4 86 95 37-144 10
2,4-Dichlorophenol ug/L ND 100 100 66.4 67.3 66 67 1-191 1
2,4-Dimethylphenol ug/L ND 100 100 64.4 67.1 64 67 32-119 4
2,4-Dinitrophenol ug/L ND 500 500 697 449 139 90 1-181 43 R1
2,4-Dinitrotoluene ug/L ND 100 100 110 87.9 110 88 39-139 22
2,6-Dinitrotoluene ug/L ND 100 100 102 90.5 102 91 50-158 12
2-Chloronaphthalene ug/L ND 100 100 84.9 101 85 101 60-118 18
2-Chlorophenol ug/L ND 100 100 78.5 82.6 79 83 23-134 5
2-Nitrophenol ug/L ND 100 100 67.7 71.0 68 71 29-182 5

(336)623-8921 (828)254-7176 (704)875-9092


MS MSD
3,3'-Dichlorobenzidine ug/L ND 200 200 162 166 81 83 1-262 3
4,6-Dinitro-2-methylphenol ug/L ND 200 200 246 228 123 114 1-181 8
4-Bromophenylphenyl ether ug/L ND 100 100 88.5 95.3 89 95 53-127 7
4-Chloro-3-methylphenol ug/L ND 200 200 144 136 72 68 22-147 6
4-Chlorophenylphenyl ether ug/L ND 100 100 98.0 84.9 98 85 25-158 14
4-Nitrophenol ug/L ND 500 500 444 289 89 58 1-132 42 R1
Acenaphthene ug/L ND 100 100 96.6 96.1 97 96 47-145 1
Acenaphthylene ug/L ND 100 100 91.0 93.2 91 93 33-145 2
Anthracene ug/L ND 100 100 94.9 97.5 95 97 1-166 3
Benzo(a)anthracene ug/L ND 100 100 92.4 93.4 92 93 33-143 1
Benzo(a)pyrene ug/L ND 100 100 88.1 88.5 88 89 17-163 1
Benzo(b)fluoranthene ug/L ND 100 100 90.6 94.4 91 94 24-159 4
Benzo(g,h,i)perylene ug/L ND 100 100 92.4 100 92 100 1-219 8
Benzo(k)fluoranthene ug/L ND 100 100 101 100 101 100 11-162 1
bis(2-Chloroethoxy)methane ug/L ND 100 100 84.3 87.0 84 87 33-184 3
bis(2-Chloroethyl) ether ug/L ND 100 100 85.1 86.8 85 87 12-158 2
bis(2-Chloroisopropyl) ether ug/L ND 100 100 91.1 95.3 91 95 36-166 5
bis(2-Ethylhexyl)phthalate ug/L ND 100 100 86.5 88.5 86 89 8-158 2
Butylbenzylphthalate ug/L ND 100 100 90.7 94.9 91 95 1-152 4
Chrysene ug/L ND 100 100 96.0 97.6 96 98 17-168 2
Di-n-butylphthalate ug/L ND 100 100 88.5 101 88 101 1-118 13
Di-n-octylphthalate ug/L ND 100 100 76.8 75.6 77 76 4-146 2
Dibenz(a,h)anthracene ug/L ND 100 100 91.2 95.4 91 95 1-227 4
Diethylphthalate ug/L ND 100 100 103 83.9 103 84 1-114 21
Dimethylphthalate ug/L ND 100 100 92.5 83.8 92 84 1-112 10
Fluoranthene ug/L ND 100 100 97.0 114 97 114 26-137 16
Fluorene ug/L ND 100 100 108 91.5 108 92 59-121 16
Hexachloro-1,3-butadiene ug/L ND 100 100 62.5 65.5 63 66 24-116 5
Hexachlorobenzene ug/L ND 100 100 91.1 96.9 91 97 1-152 6
Hexachlorocyclopentadiene ug/L ND 100 100 80.7 102 81 102 25-150 23
Hexachloroethane ug/L ND 100 100 72.3 78.4 72 78 40-113 8
Indeno(1,2,3-cd)pyrene ug/L ND 100 100 90.6 93.9 91 94 1-171 4
Isophorone ug/L ND 100 100 70.7 73.8 71 74 21-196 4
N-Nitroso-di-n-propylamine ug/L ND 100 100 87.1 93.7 87 94 1-230 7
N-Nitrosodimethylamine ug/L ND 100 100 65.9 71.9 66 72 25-150 9
N-Nitrosodiphenylamine ug/L ND 100 100 87.8 93.7 88 94 25-150 7
Naphthalene ug/L ND 100 100 65.9 68.3 66 68 21-133 4
Nitrobenzene ug/L ND 100 100 66.5 67.8 66 68 35-180 2
Pentachlorophenol ug/L ND 200 200 193 177 96 88 14-176 9
Phenanthrene ug/L ND 100 100 92.7 95.1 93 95 54-120 3
Phenol ug/L ND 100 100 67.3 65.6 67 66 5-112 3
Pyrene ug/L ND 100 100 90.7 96.3 91 96 52-115 6
2,4,6-Tribromophenol (S) % 117 87 10-137
2-Fluorophenol (S) % 59 63 10-120
Nitrobenzene-d5 (S) % 68 68 10-120
Phenol-d6 (S) % 52 51 10-120

(336)623-8921 (828)254-7176 (704)875-9092


MS MSD
Terphenyl-d14 (S) % 90 94 11-131

(336)623-8921 (828)254-7176 (704)875-9092

QC Batch: MSV/14647 Analysis Method: SM 6200B

QC Batch Method: SM 6200B Analysis Description: 6200B MSV

Blank Reporting
1,2,4-Trimethylbenzene ug/L ND 0.50 04/01/11 22:45
Benzene ug/L ND 0.50 04/01/11 22:45
Bromoform ug/L ND 0.50 04/01/11 22:45
Ethanol ug/L ND 200 04/01/11 22:45

(336)623-8921 (828)254-7176 (704)875-9092


Blank Reporting
Isopropylbenzene (Cumene) ug/L ND 0.50 04/01/11 22:45
m&p-Xylene ug/L ND 1.0 04/01/11 22:45
n-Butylbenzene ug/L ND 0.50 04/01/11 22:45
n-Propylbenzene ug/L ND 0.50 04/01/11 22:45
o-Xylene ug/L ND 0.50 04/01/11 22:45
sec-Butylbenzene ug/L ND 0.50 04/01/11 22:45
Styrene ug/L ND 0.50 04/01/11 22:45
tert-Butylbenzene ug/L ND 0.50 04/01/11 22:45
Toluene ug/L ND 0.50 04/01/11 22:45
Toluene-d8 (S) % 97 70-130 04/01/11 22:45

Spike LCS LCS % Rec
1,2,4-Trimethylbenzene ug/L 50 59.1 118 60-140

(336)623-8921 (828)254-7176 (704)875-9092


Spike LCS LCS % Rec
Benzene ug/L 50 51.0 102 60-140
Bromoform ug/L 50 53.6 107 60-140
Chloroform ug/L 50 50.3 101 60-140
Ethanol ug/L 2000 1970 99 60-140
Isopropylbenzene (Cumene) ug/L 50 52.5 105 60-140
m&p-Xylene ug/L 100 113 113 60-140
n-Butylbenzene ug/L 50 57.2 114 60-140
n-Propylbenzene ug/L 50 55.0 110 60-140
o-Xylene ug/L 50 58.2 116 60-140
sec-Butylbenzene ug/L 50 57.4 115 60-140
Styrene ug/L 50 52.0 104 60-140
tert-Butylbenzene ug/L 50 58.0 116 60-140
Toluene ug/L 50 50.5 101 60-140
Toluene-d8 (S) % 101 70-130

(336)623-8921 (828)254-7176 (704)875-9092


MS MSD
1,1,1,2-Tetrachloroethane ug/L ND 20 20 20.0 19.6 100 98 60-140 2
1,1,1-Trichloroethane ug/L ND 20 20 20.6 20.4 103 102 60-140 1
1,1-Dichloroethane ug/L ND 20 20 20.2 20.1 101 101 60-140 1
1,1-Dichloropropene ug/L ND 20 20 17.6 17.6 88 88 60-140 0
1,2,3-Trichloropropane ug/L ND 20 20 18.1 17.7 90 88 60-140 2
1,2,4-Trimethylbenzene ug/L ND 20 20 21.1 20.6 105 102 60-140 3
1,2-Dibromo-3-chloropropane ug/L ND 20 20 18.3 17.2 92 86 60-140 6
1,2-Dibromoethane (EDB) ug/L ND 20 20 18.9 18.4 94 92 60-140 3
1,2-Dichlorobenzene ug/L ND 20 20 18.3 17.8 91 89 60-140 3
1,2-Dichloropropane ug/L ND 20 20 18.3 18.4 91 92 60-140 1
2-Chlorotoluene ug/L ND 20 20 20.0 19.6 100 98 60-140 2
Benzene ug/L ND 20 20 18.3 18.3 91 91 60-140 0
Bromobenzene ug/L ND 20 20 19.2 18.9 96 95 60-140 2
Bromochloromethane ug/L ND 20 20 18.4 18.4 92 92 60-140 0
Bromodichloromethane ug/L ND 20 20 18.9 18.5 95 93 60-140 2
Bromoform ug/L ND 20 20 18.5 18.1 92 90 60-140 2
Bromomethane ug/L ND 20 20 28.0 29.8 140 149 60-140 6 M0
Carbon tetrachloride ug/L ND 20 20 19.6 19.5 98 97 60-140 0
Chloroethane ug/L ND 20 20 20.7 21.0 104 105 60-140 1
Chloroform ug/L 1.5 20 20 21.5 21.5 100 100 60-140 0
Chloromethane ug/L ND 20 20 20.0 20.1 100 100 60-140 0
cis-1,2-Dichloroethene ug/L ND 20 20 19.2 19.3 96 97 60-140 1
cis-1,3-Dichloropropene ug/L ND 20 20 16.6 16.7 83 84 60-140 1
Dibromochloromethane ug/L ND 20 20 18.9 18.0 95 90 60-140 5
Dibromomethane ug/L ND 20 20 18.1 17.9 91 89 60-140 1
Dichlorodifluoromethane ug/L ND 20 20 20.5 21.1 102 106 60-140 3
Diisopropyl ether ug/L ND 20 20 20.1 19.7 100 98 60-140 2
Ethanol ug/L ND 800 800 799 759 100 95 60-140 5
Ethylbenzene ug/L ND 20 20 19.5 19.4 98 97 60-140 1
Isopropylbenzene (Cumene) ug/L ND 20 20 18.5 18.6 92 93 60-140 1
m&p-Xylene ug/L ND 40 40 41.4 41.6 104 104 60-140 0
Methyl-tert-butyl ether ug/L ND 20 20 19.5 19.1 98 96 60-140 2
Methylene Chloride ug/L ND 20 20 19.7 19.9 98 99 60-140 1

(336)623-8921 (828)254-7176 (704)875-9092


MS MSD
n-Butylbenzene ug/L ND 20 20 19.4 19.5 97 97 60-140 0
n-Propylbenzene ug/L ND 20 20 20.4 20.3 102 101 60-140 0
o-Xylene ug/L ND 20 20 20.7 20.7 103 103 60-140 0
sec-Butylbenzene ug/L ND 20 20 21.0 21.2 105 106 60-140 1
Styrene ug/L ND 20 20 16.4 16.6 82 83 60-140 1
tert-Butylbenzene ug/L ND 20 20 20.3 20.6 102 103 60-140 1
Tetrachloroethene ug/L ND 20 20 18.3 18.7 92 93 60-140 2
Toluene ug/L ND 20 20 18.3 18.1 92 90 60-140 1
trans-1,2-Dichloroethene ug/L ND 20 20 19.5 19.7 97 98 60-140 1
trans-1,3-Dichloropropene ug/L ND 20 20 19.4 19.0 97 95 60-140 2
Trichlorofluoromethane ug/L ND 20 20 20.5 20.5 103 102 60-140 0
Vinyl chloride ug/L ND 20 20 19.8 20.1 99 100 60-140 1
Toluene-d8 (S) % 98 99 70-130

MS MSD
1,1,2-Trichloroethane ug/L ND 20 20 27.6 30.0 138 150 60-140 8 M0
1,1-Dichloropropene ug/L ND 20 20 15.0 17.5 75 88 60-140 16
1,2,3-Trichloropropane ug/L ND 20 20 14.5 17.1 73 86 60-140 17
1,2,4-Trimethylbenzene ug/L ND 20 20 17.3 33.8 86 169 60-140 65 M0,R1
1,2-Dibromo-3-chloropropane ug/L ND 20 20 20.2 24.8 101 124 60-140 20
1,2-Dibromoethane (EDB) ug/L ND 20 20 16.8 19.6 84 98 60-140 16

(336)623-8921 (828)254-7176 (704)875-9092


MS MSD
Benzene ug/L ND 20 20 22.0 24.8 110 124 60-140 12
Bromobenzene ug/L ND 20 20 16.6 19.9 83 99 60-140 18
Bromochloromethane ug/L ND 20 20 15.2 17.8 76 89 60-140 16
Bromodichloromethane ug/L ND 20 20 14.0 17.0 70 85 60-140 20
Bromoform ug/L ND 20 20 14.2 17.7 71 89 60-140 22
Bromomethane ug/L ND 20 20 23.5 25.7 118 129 60-140 9
Carbon tetrachloride ug/L ND 20 20 15.3 18.1 77 91 60-140 17
Chloroethane ug/L ND 20 20 16.9 19.8 84 99 60-140 16
Chloroform ug/L 1.1 20 20 17.0 19.8 79 94 60-140 16
Chloromethane ug/L ND 20 20 16.1 18.9 80 95 60-140 16
cis-1,2-Dichloroethene ug/L ND 20 20 15.9 18.7 79 94 60-140 17
cis-1,3-Dichloropropene ug/L ND 20 20 15.6 18.7 78 94 60-140 18
Dibromochloromethane ug/L ND 20 20 14.7 17.8 74 89 60-140 19
Dibromomethane ug/L ND 20 20 15.0 18.0 75 90 60-140 18
Dichlorodifluoromethane ug/L ND 20 20 16.8 19.5 84 97 60-140 15
Diisopropyl ether ug/L ND 20 20 19.3 23.1 96 115 60-140 18
Ethanol ug/L 657 768 16
Ethylbenzene ug/L ND 20 20 33.1 36.8 166 184 60-140 11 M0
Isopropylbenzene (Cumene) ug/L ND 20 20 19.3 23.0 97 115 60-140 17
m&p-Xylene ug/L ND 40 40 33.2 39.9 83 100 60-140 18
Methyl-tert-butyl ether ug/L ND 20 20 16.0 19.8 80 99 60-140 21
Methylene Chloride ug/L ND 20 20 15.9 18.9 79 95 60-140 18
n-Butylbenzene ug/L ND 20 20 28.0 31.3 140 157 60-140 11 M0
n-Propylbenzene ug/L ND 20 20 27.1 30.3 135 152 60-140 11 M0
o-Xylene ug/L ND 20 20 17.4 21.2 87 106 60-140 20
sec-Butylbenzene ug/L ND 20 20 22.7 26.3 114 132 60-140 15
Styrene ug/L ND 20 20 14.4 18.0 72 90 60-140 23
tert-Butylbenzene ug/L ND 20 20 18.2 21.9 91 110 60-140 18
Tetrachloroethene ug/L ND 20 20 15.4 18.6 77 93 60-140 19
Toluene ug/L ND 20 20 16.2 19.1 81 95 60-140 17
trans-1,2-Dichloroethene ug/L ND 20 20 15.8 19.2 79 96 60-140 19
trans-1,3-Dichloropropene ug/L ND 20 20 16.3 19.5 81 98 60-140 18
Trichlorofluoromethane ug/L ND 20 20 16.3 18.9 82 94 60-140 15
Vinyl chloride ug/L ND 20 20 16.5 19.3 82 97 60-140 16
Toluene-d8 (S) % 104 103 70-130

(336)623-8921 (828)254-7176 (704)875-9092

QC Batch: MSV/14715 Analysis Method: SM 6200B

QC Batch Method: SM 6200B Analysis Description: 6200B MSV

Blank Reporting
Benzene ug/L ND 0.50 04/06/11 14:09
Bromoform ug/L ND 0.50 04/06/11 14:09
Ethanol ug/L ND 200 04/06/11 14:09

(336)623-8921 (828)254-7176 (704)875-9092


Blank Reporting
Isopropylbenzene (Cumene) ug/L ND 0.50 04/06/11 14:09
m&p-Xylene ug/L ND 1.0 04/06/11 14:09
n-Butylbenzene ug/L ND 0.50 04/06/11 14:09
n-Propylbenzene ug/L ND 0.50 04/06/11 14:09
o-Xylene ug/L ND 0.50 04/06/11 14:09
sec-Butylbenzene ug/L ND 0.50 04/06/11 14:09
Styrene ug/L ND 0.50 04/06/11 14:09
tert-Butylbenzene ug/L ND 0.50 04/06/11 14:09
Toluene ug/L ND 0.50 04/06/11 14:09
Toluene-d8 (S) % 94 70-130 04/06/11 14:09

Spike LCS LCS % Rec

(336)623-8921 (828)254-7176 (704)875-9092


Spike LCS LCS % Rec
Benzene ug/L 50 52.3 105 60-140
Bromoform ug/L 50 56.0 112 60-140
Chloroform ug/L 50 52.4 105 60-140
Ethanol ug/L 2000 1890 95 60-140
Isopropylbenzene (Cumene) ug/L 50 55.0 110 60-140
m&p-Xylene ug/L 100 117 117 60-140
n-Butylbenzene ug/L 50 60.5 121 60-140
n-Propylbenzene ug/L 50 56.7 113 60-140
o-Xylene ug/L 50 60.1 120 60-140
sec-Butylbenzene ug/L 50 59.4 119 60-140
Styrene ug/L 50 54.1 108 60-140
tert-Butylbenzene ug/L 50 59.6 119 60-140
Toluene ug/L 50 50.9 102 60-140
Toluene-d8 (S) % 97 70-130

(336)623-8921 (828)254-7176 (704)875-9092
QUALIFIERS

DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
LABORATORIES
PASI-A Pace Analytical Services - Asheville

PASI-C Pace Analytical Services - Charlotte
SAMPLE QUALIFIERS
Sample: 9290693004
[1]
Sample: 9290693005
[1]
Sample: 9290693006
[1]
ANALYTE QUALIFIERS
M0 Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
N2 The lab does not hold NELAC accreditation for this parameter.
R1 RPD value was outside control limits.

APPENDIX B
Boring Log for Monitoring Well MW-2

Boring Log Form
Project Name McGills Service Station
LITHOLOGIC LOG SHEET
Project No. 2354.02 Boring Name MW-2
Geologist Adam Tripp Sheet 1 of 1
Driller EarthCon Total Depth 53'
Rig Type Geoprobe 7720 DT Date Begun 3/22/2011 Groundwater 46.61'
Method Used 3¹/₄" ID HAS Date Completed 3/22/2011
Weather ______________
Sampling Location Diagram
Location Sampled
Sampling Method
Depth in Feet
Sample No.
Blow Count
Soil Graph
Recovery
Lithologic Description
DPT
with
Macro- 5
Core (5-10') Red, sandy silt with some clay. Damp.
Sleeves 10
15
(15-20') Tan, micaceous, silty sand. Dry. Contains relic structures (saprolite).
20
25
30
35
40
(40-45') Tan, micaceous, silty sand. Damp. Contains relic structures (saprolite).
45
P:\Isothermal PDC\Former McGills Service Station\Brownfield Site Assessment\Reports\BSA Report\Appendices\Boring Log MW-2.xls
APPENDIX C
Monitoring Well Construction Logs for MW-1, MW-2,

and MW-3
MONITORING WELL CONSTRUCTION DATA
DATE INSTALLED: 3/22/11 CLIENT: Isothermal PDC PROJECT NO: 2354.02
WELL/BORING NO: MW-1 PLANE COORDINATES: Well not surveyed to NGVD.

GEOLOGIST/ENGINEER: Adam Tripp, P.G. NORTH
PROJECT NAME: Former McGills Service Station EAST
ADDRESS: King Street and Piedmont Street
Kings Mountain NC TOP OF SLAB ELEVATION:
WELL CONTRACTOR: EarthCon TOP OF CASING ELEVATION:
CONSTRUCTION DATA
WELL SCHEMATIC CASING INFORMATION

TOP OF CASING
MATERIAL: x PVC STAINLESS CARBON
PROTECTIVE CASING OTHER
DIAMETER: x 2" 4" 6"
TOP OF CONCRETE PAD LENGTH OF STICKUP OTHER IN.
0 FT. JOINTS: x THREADED WELDED
GROUND SURFACE SCREWED COUPLED
OTHER
SCHEDULE: 40
SCREEN INFORMATION
MATERIAL: x PVC
CEMENT/BENTONITE STAINLESS
GROUT DEPTH TO TEFLON
BASE OF OTHER
GROUT SEAL DIAMETER: x 2"
39.0 FT. 4"
6"
TOTAL BOREHOLE OTHER IN
BOREHOLE DIAMETER SLOT: x 0.010
DEPTH 3 and 1/4 IN. LENGTH 0.020
FROM OF OTHER IN
GRADE RISER
59.0 FT. 43.0 FT. CENTRALIZER: YES X NO
SHOW LOCATION OF CENTRALIZER(S) ON SCHEMATIC
SEAL
2.0 FT. FILTER PACK MATERIAL
20/40 SAND x
OTHER
TOTAL
WELL SECONDARY FILTER PACK MATERIAL
DEPTH SUGAR SAND
FROM OTHER
GRADE
58.0 FT.
BENTONITE WELL SEAL
FILTER LENGTH 1/2-INCH PELLETS
PACK OF 1/4-INCH PELLETS
17.0 FT. SCREEN x CHIPS
15.0 FT. OTHER
SURFACE PROTECTION
CONCRETE PAD: x 2'X2'
4'X4'
OTHER FT
WELL SUMP/CAP WELL SUMP/CAP

YES
x NO
LENGTH FT.
P:\Isothermal PDC\Former McGills Service Station\Brownfield Site Assessment\Reports\BSA Report\Appendices\Well Construction Log MW-1-2-3.xls

CONSTRUCTION DATA

TOP OF CASING
OTHER
SCHEDULE: 40
SCREEN INFORMATION
MATERIAL: x PVC
BASE OF OTHER
39.0 FT. 4"
6"
FROM OF OTHER IN
GRADE RISER
SEAL
20/40 SAND x
OTHER
TOTAL
DEPTH SUGAR SAND
FROM OTHER
GRADE
53.0 FT.
BENTONITE WELL SEAL
10.0 FT. OTHER
SURFACE PROTECTION
4'X4'
OTHER FT

YES
x NO
LENGTH FT.

CONSTRUCTION DATA

TOP OF CASING
OTHER
SCHEDULE: 40
SCREEN INFORMATION
MATERIAL: x PVC
BASE OF OTHER
39.0 FT. 4"
6"
FROM OF OTHER IN
GRADE RISER
SEAL
20/40 SAND x
OTHER
TOTAL
DEPTH SUGAR SAND
FROM OTHER
GRADE
53.0 FT.
BENTONITE WELL SEAL
10.0 FT. OTHER
SURFACE PROTECTION
4'X4'
OTHER FT

YES
x NO
LENGTH FT.
APPENDIX D
Equipment Calibration Logs

APPENDIX E
Well Development and Low-Flow Sampling Logs

APPENDIX F
Form UST-61
UST-61 24-Hour Release and UST Leak Reporting Form.
For Releases This form should be completed and submitted to the UST Section’s regional office following a known or suspected release from
an underground storage tank (UST) system. This form is required to be submitted within 24 hours of discovery of a known or
in NC suspected release
(DWM USE ONLY) Y

Suspected Contamination? (Y/N) ________ N/A
Facility ID Number ______________
Incident # ________ Risk (H,I,L,U)_______ Y
Confirmed GW Contamination? (Y/N) ______ Date Leak Discovered4/18/2011
___________
Received On ________ Received By ________ Y
Confirmed Soil Contamination ?(Y/N) ______ Comm
Comm/Non-Commercial? ________
Reported by (circle one): Phone, Fax or Report Y
Samples Taken?(Y/N) ______ Regulated
Reg/Non-regulated? _____________
Region _______ N If Yes, State Greatest
Free Product? (Y/N) _____
N/A
Thickness ______________
INCIDENT DESCRIPTION
Incident Name: Former McGills Service Station
Address: 100 East King Street County: Cleveland
Regional Office (circle one): Asheville, Mooresville, Fayetteville,
City/Town: Kings Mountain Zip Code: 28086 Raleigh, Washington, Wilmington, Winston-Salem
Latitude (decimal degrees): 35.240680 Longitude (decimal degrees) : -81.342156 Obtained by:
Briefly describe suspected or confirmed release: (including but not limited to: nature of release, date of release, amount T GPS
of release, amount of free product present and recovery efforts, initial responses conducted, impacts to receptors)
T Topographic map
Soil sampling conducted 3/23-3/24/2011 indicated presence
of petroleum constituents in soil. Groundwater contamination T GIS Address matching
was also detected. See attached Tables 3 and 5. T

x Other
Non-petroleum constituents (1,2-DCA) detected in groundwater. T Unknown
Describe location:
Google Earth
HOW RELEASE WAS DISCOVERED (Release Code)

(Check one)
T Release Detection Equipment or Methods T Visual/Odor T

x Groundwater Contamination
T During UST Closure/Removal T Water in Tank T Surface Water Contamination
T Property Transfer T Water Supply Well Contamination T
x soil
Other (specify) _______________
contam.
SOURCE OF CONTAMINATION
Source of Release Cause of Release Type of Release Product Type Released
(Check one to indicate primary (Check one to indicate primary (Check one) (Check one to indicate primary product type
source) cause) released)
T
x Tank TSpill T
x Petroleum T
x Gasoline/ Diesel/ T Diesel/Veg. Oil
Kerosene Blend
TPiping T
x Overfill T
x Non-Petroleum ?
T Heating Oil T Vegetable Oil 100%
TDispenser T
x Corrosion ? TBoth T Other Petroleum T E10 – E20
TSubmersible Turbine Pump TPhysical or Mechanical Products
T E21 – E84
Location T Metals
TDelivery Problem Damage
T T E85 – E99
TOther TInstall Problem (Check one) Other Inorganics
T Other Organics T Ethanol 100%
TUnknown TOther T
x Facility
TUnknown T Residence T E01 – E09
Definitions presented on reverse Definitions presented on reverse T Other
Ownership
1. Municipal 2. Military 3. Unknown 4. Private 5. Federal 6. County 7. State
Operation Type
1. Public Service 2. Agricultural 3. Residential 4. Education/Relig. 5. Industrial 6. Commercial 7. Mining
UST Form 61 (02/08) Page 1 of 2

IMPACT ON DRINKING WATER SUPPLIES
Water Supply Wells Affected? 1. Yes 2. No 3. Unknown
Number of Water Supply Wells Affected __________________
Water Supply Wells Contaminated: (Include Users Names, Addresses and Phone Numbers. Attach additional sheet if necessary)
1. N/A
2.
3.
UST SYSTEM OWNER
UST Owner/Company
Wallace Properties, Inc. and Patterson Oil Company of Kings Mountain?
Point of Contact Address
Steve Wallace PO Box 470407
City State Zip Code Telephone Number
Charlotte NC 28247 (704) 541-1133
UST SYSTEM OPERATOR
UST Operator/Company Address
Former McGills Service Station 100 East King Street
Kings Mountain NC 28086 N/A
LANDOWNER AT LOCATION OF UST INCIDENT
Landowner Address
Wallace Properties, Inc. PO Box 470407
Charlotte NC
28247 (704) 541-1133
Draw Sketch of Area (showing two major road intersections) or Attach Map
See attached Figure 3.
828-
Person Reporting Incident
Lisa Company Altamont
Manning Environmental, Inc. 281-3350 Telephone Number
Title Project Engineer Address231 Haywood Street, Asheville Date 05/03/2011
UST Form 61 (02/08) Page 2 of 2
Definitions of Sources
Tank: means the tank that stores the product and is part of the underground storage tank system
Piping: means the piping and connectors running from the tank or submersible turbine pump to the dispenser or other end-use equipment (Vent, vapor recovery, or fill
lines are excluded.)
Dispenser: includes the dispenser and the equipment used to connect the dispenser to the piping (e.g., a release from a suction pump or from components located above
the shear valve)
Submersible Turbine Pump (STP) Area includes the submersible turbine pump head (typically located in the tank sump), the line leak detector, and the piping that
connects the submersible turbine pump to the tank
Delivery Problem: identifies releases that occurred during product delivery to the tank. (Typical causes associated with this source are spills and overfills.)
Other: serves as the option to use when the release source is known but does not fit into one of the preceding categories (e.g., for releases from vent lines, vapor
recovery lines, and fill lines)
Unknown: identifies releases for which the source has not been determined
Definitions of Causes
Spill: use this cause when a spill occurs (e.g., when the delivery hose is disconnected from the tank fill pipe or when the nozzle is removed from the dispenser)
Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser)
Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion (e.g., puncture of tank or piping, loose fittings, broken
components, and components that have changed dimension)
Corrosion: use when a metal tank, piping, or other component has a release due to corrosion (e.g., for steel, corrosion takes the form of rust)
Installation Problem: use when the problem is determined to have occurred specifically because the UST system was not installed properly
Other: use this option when the cause is known but does not fit into one of the preceding categories (e.g., putting regulated substances into monitoring wells)
Unknown: use when the cause has not been determined

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3 Former McGills Service Station BSA Report

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Brownfields Site Assessment

Former McGills Service Station

2.0 General Information ......................................................................................................... 3

3.0 Site History and Characterization .................................................................................... 5

4.0 Site Investigation.............................................................................................................. 7

5.0 Data Evaluation ............................................................................................................. 12

6.0 Conclusions and Recommendations ............................................................................ 15

7.0 References .................................................................................................................... 16

1.0 Executive Summary

2.0 General Information

3.0 Site History and Characterization

3.2 Site Characteristics

4.0 Site Investigation

4.2 Ground-Penetrating Radar and UST Survey

4.3 Soil Sampling

4.4 Monitoring Well Installation

4.4.1 Monitoring Well Soil Boring Sampling

4.4.2 Monitoring Well Development

• Temperature, DO, and turbidity ± 10%

4.4.3 Monitoring Well Surveying and Water Level Gauging

4.5 Monitoring Well Sampling

4.6 Quality Control Measures

5.0 Data Evaluation

5.1 Soil Sampling

5.1.2 UST Soil Sampling Results

5.1.3 Product Line Soil Sampling Results

5.1.4 Monitoring Well Soil Boring Sampling Results

5.2 Monitoring Well Sampling

5.2.2 Laboratory Analytical Results

5.3 Initial Response and Reporting

5.4 Receptor Survey

5.5 Investigative Derived Waste Management

6.0 Conclusions and Recommendations

Brownfields Site Assessment

Current/ Last Capacity Date Tank Approximate Last Did a Release

Yes (fill port area

4 Gasoline ~6,000 Unknown Unknown Filling Station In Place No

5 Unknown ~4,000 Unknown Unknown Filling Station In Place No

6 Unknown ~4,000 Unknown Unknown Filling Station In Place Yes

7 Unknown ~1,000 Unknown Unknown Filling Station In Place Yes

8 Oil ~1,000 Unknown Unknown Filling Station In Place Yes

Brownfields Site Assessment

Brownfields Site Assessment

Brownfields Site Assessment

Brownfields Site Assessment

Volatile Organics (µg/kg) Soil to GW

Brownfields Site Assessment

Volatile Organics (µg/kg) Soil to GW

Brownfields Site Assessment

Semi-Volatile Organics (µg/kg) Soil to GW

Brownfields Site Assessment

Hydrocarbon Fractions (mg/kg) Soil to GW

Aliphatic (C09-C18) 3,300 ND ND ND ND ND ND

Brownfields Site Assessment

Sample ID: MW-1 MW-2 MW-3 MW-3-Dup Field Blank

Brownfields Site Assessment

Sample ID: MW-1 MW-2 MW-3 MW-3-Dup Field Blank

Brownfields Site Assessment

Sample ID: MW-1 MW-2 MW-3 MW-3-Dup Field Blank

Brownfields Site Assessment

Sample ID: MW-1 MW-2 MW-3 MW-3-Dup Field Blank

Laboratory Analytical Reports and Chain-of-Custody

LIMS USE: FR - LISA MANNING