MenAMU Oxytrace 00

AMU Oxytrace
Version 4.11 and later
Operator’s Manual
SWAN sets the standard
A-96.250.541 / 080117
Customer Support
SWAN and its representatives maintain a fully trained staff of technical specialists
around the world. For any technical question, contact your nearest
SWAN representative, or the manufacturer:
SWAN ANALYTISCHE INSTRUMENTE AG

Studbachstrasse 13
8340 Hinwil
Switzerland
Internet: www.swan.ch
E-mail: support@swan.ch
Document Status
Title: AMU Oxytrace Operator’s Manual
ID: A-96.250.541
Revision Issue
00 January 2008
© 2008, SWAN ANALYTISCHE INSTRUMENTE AG, Switzerland, all rights reserved
Information contained in this document is subject to change without notice.

AMU Oxytrace
Table of Contents
Table of Contents
1. Safety Instructions. . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
1.1 General . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
1.2 Warning Notices. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
1.3 General Safety Regulations . . . . . . . . . . . . . . . . . . . . . . . 5
1.3.1 Legal Requirements . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
1.3.2 General Inspection and Maintenance Duties . . . . . . . . 5
1.3.3 Spare Parts and Disposables . . . . . . . . . . . . . . . . . . . 5
1.3.4 Modifications . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
1.3.5 Electrical shock hazard . . . . . . . . . . . . . . . . . . . . . . . . 5
2. Description of the system . . . . . . . . . . . . . . . . . . . . . . . 6

2.1 Technical Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
2.2 Swansensor Oxytrace G . . . . . . . . . . . . . . . . . . . . . . . . . 9
2.3 Flow cells . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
2.3.1 QV-Flow PMMA OTG . . . . . . . . . . . . . . . . . . . . . . . . . 10
2.3.2 B-Flow SS316L OTG . . . . . . . . . . . . . . . . . . . . . . . . . . 11
2.4 Software. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
2.4.1 Display . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
2.4.2 Menu Navigation Keys . . . . . . . . . . . . . . . . . . . . . . . . . 13
2.4.3 Software Structure . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14
2.5 Changing Parameters and values . . . . . . . . . . . . . . . . . . 15
3. Installation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16
3.1 Installation Checklist . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16
3.2 Mounting of the Instrument . . . . . . . . . . . . . . . . . . . . . . . 17
3.3 Electrical Connection Scheme . . . . . . . . . . . . . . . . . . . . . 18
3.4 Power Supply. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19
3.5 Relay Contacts. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
3.5.1 Alarm Relay . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
3.5.2 Relay Contacts 1 and 2 . . . . . . . . . . . . . . . . . . . . . . . . 20
3.6 Signal Outputs 1 and 2 . . . . . . . . . . . . . . . . . . . . . . . . . . 20
3.7 Input . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
3.8 Sensor Connections. . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21
3.9 Interfaces . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21
3.9.1 RS232 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21
3.9.2 Profibus (optional) . . . . . . . . . . . . . . . . . . . . . . . . . . . . 22
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AMU Oxytrace
Table of Contents
4. Instrument Setup . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23
4.1 Establish sample flow. . . . . . . . . . . . . . . . . . . . . . . . . . . . 23
5. Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23
5.1 Maintenance Schedule. . . . . . . . . . . . . . . . . . . . . . . . . . . 23
5.2 Stop Operation before Maintenance . . . . . . . . . . . . . . . . 24
5.3 Maintenance of Oxygen Sensor. . . . . . . . . . . . . . . . . . . . 24
5.4 Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26
5.4.1 Calibration Procedure. . . . . . . . . . . . . . . . . . . . . . . . . . 26
5.4.2 Zero-Verification . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28
6. Error list . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29
6.1 Error messages . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29
6.2 Error Codes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30
A. Programm Overview . . . . . . . . . . . . . . . . . . . . . . . . . . . 32
B. RS232 Interface . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35
B.1 Connection of the Communication Cable. . . . . . . . . . . . . 35
B.2 Configuration of the AMU Transmitter . . . . . . . . . . . . . . . 36
B.3 HyperTerminal Configuration on the PC . . . . . . . . . . . . . 37
B.4 Functions of the AMU RS232 Interface . . . . . . . . . . . . . . 41
B.4.1 Logger Download . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 41
B.4.2 Log download . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 42
B.4.3 Clear Logger . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44
B.5 Firmware Upload . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45
C. Profibus (option) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47
C.1 Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47
C.2 Cyclic Data Telegram. . . . . . . . . . . . . . . . . . . . . . . . . . . . 48
B.3 Customizing the Cyclic Data Telegram . . . . . . . . . . . . . . 49
B.4 Data Formats . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 50
B.5 Configuration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 54
B.5.1 Device Master Files (GSD). . . . . . . . . . . . . . . . . . . . . . 54
B.5.2 GSD File Types . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 54
B.6 Acyclic Data Communication . . . . . . . . . . . . . . . . . . . . . . 55
2 A-96.250.541 / 080117
AMU Oxytrace
Table of Contents
C. Modbus (option). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 56
C.1 Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 56
C.2. Data and Control Functions . . . . . . . . . . . . . . . . . . . . . . . 58
C.3 Function Description . . . . . . . . . . . . . . . . . . . . . . . . . . . . 60
D. Program List and Explanations . . . . . . . . . . . . . . . . . . 64

1 Messages. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 64
2 Diagnostics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 64
3 Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 66
4 Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 66
5 Installation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 69
F. MSDS Filling electrolyte . . . . . . . . . . . . . . . . . . . . . . . . 79
G. Default Values . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 80
H. Index . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 82
A-96.250.541 / 080117 3
AMU Oxytrace
Safety Instructions
AMU Oxytrace - Operator’s Manual

This document describes the main steps for instrument setup,
operation and maintenance.
1. Safety Instructions
This chapter contains general information assuring safe operation
of the instrument. More safety instructions are given throughout this
manual, at the respective locations where observation is most
important.
Strictly follow all safety instructions in this publication.
1.1 General
The instructions included in this section explain the potential risks
associated with instrument operation and provide important safety
practices designed to minimize these risks.
If you carefully follow the information contained in this section, you
can protect yourself from hazards and create a safer work
environment.
Target audience
Operator: Qualified person who uses the equipment

for its intended purpose.
Instrument operation requires thorough knowledge of applications,
instrument functions and software program as well as all applicable
safety rules and regulations.
Qualification, Training
To be qualified for instrument operation, you must read and

understand the written instructions in this operator’s manual, have
appropriate training (by SWAN Service Technician), and know the
safety rules and regulations.
Operator’s Manual Location
The AMUAMU Oxytrace Operator’s Manual shall be kept in

proximity of the instrument.
4 A-96.250.541 / 080117
AMU Oxytrace
Safety Instructions
1.2 Warning Notices

The symbols used for safety-related notices have the following
significance:
WARNING Warning
Symbols
Generally, the triangular warning symbol indicates the possibility
of personal injury or even loss of life if instructions are not followed,
e.g.
electrical shock hazard
caustic
Attention Attention
Symbols The attention symbol indicates the possibility of equipment
damage, malfunctions or incorrect process results if instructions
are not followed.
Warning
For safe instrument installation and operation you must read and
understand the instructions in this manual.
Only SWAN trained and authorized personnel shall perform the
tasks described in this document.
A-96.250.541 / 080117 5
AMU Oxytrace
Safety Instructions
1.3 General Safety Regulations
1.3.1 Legal Requirements

The user is responsible for proper system operation.
All precautions must be followed to ensure safe operation of the
instrument.
1.3.2 General Inspection and Maintenance Duties

The SWAN instrument shall only be operated in optimal running
condition. The preventive maintenance procedures listed in this
manual must be performed.
In case of safety relevant deficiencies, SWAN must immediately be
informed.
1.3.3 Spare Parts and Disposables

Use only official SWAN spare parts and disposables. If other parts
are used during the normal warranty period, the manufacturer’s
warranty is voided.
1.3.4 Modifications
Modifications and instrument upgrades shall only be carried out by
an authorized Service Technician. SWAN will not accept
responsibility for any claim resulting from unauthorized modification
or alteration.
1.3.5 Electrical shock hazard

WARNING
If proper operation is no longer possible, the instrument must be

disconnected from all power lines, and measures must be taken to
prevent inadvertent operation.
To prevent from electrical shock, always make sure that
the ground wire is connected.
Service shall be performed by authorized personnel only.
Whenever electronic service is required, disconnect
instrument power and power of devices connected to
• relay 1 and 2
• alarm relay.
6 A-96.250.541 / 080117
AMU Oxytrace
Description of the system
2. Description of the system

Application AMU Oxytrace is used to measure low levels of oxygen in high-
purity water. Especially in power plant water cycles (e.g.
feedwater), a very low level of oxygen is needed to prevent
corrosion.
Measuring Clark principle:

principle The sensor consists of one noble metal electrode (e.g. platinum or
gold), a reference electrode (mostly Ag/AgCl) and optionally a
guard electrode (mostly platinum or gold)
The Clark-type electrode is the most used oxygen sensor for
measuring oxygen dissolved in a liquid. The basic principle is that
there is a cathode and an anode submersed in an electrolyte and a
voltage is applied between the two parts. Oxygen enters the sensor
through a permeable membrane by diffusion, and is reduced at the
cathode, creating a measurable electrical current.
O2 + 2 e- + 2 H2O --> H2O2 + 2 OH-
There is a linear correlation between the oxygen concentration and
the electrical current.
The guard electrode is mounted circularly around the cathode is on
the same voltage as that but there is no current measurement.
Oxygen which diffuses from the electrolyte to the cathode is
consumed by the guard. As a consequence, residual oxygen in the
electrolyte will no more disturb the measurement signal and the
run-in time will be shorter.
The measuring signal depends on temperature, but is automatically
compensated to 25°C. The sample temperature is determined
continuously by a temperature sensor inside the oxygen electrode.
On-line Swansensor Oxytrace combined with QV-flow cell: The sample

operation enters the flow cell at the sample inlet, passes the flow regulating
valve and fills the flow cell. The oxygen concentration will be
determined. Exiting the flow cell, the rotor of the flowmeter (for flow
monitoring) will be driven and the sample leaves the flow cell
through the pressure-free outlet.
A-96.250.541 / 080117 7
AMU Oxytrace
2.1 Technical Data

The AMU measuring and control transmitter is used for panel
installation.
Input for an oxygen sensor with a built-in Nt5k temperature probe,
e.g. Swansensor Oxytrace G and for a digital sample flow meter.
Electronic case: Noryl® resin
Protection degree: IP54 (front)
RUN 10:56:03
11.3 ppb Large backlit LC-Display,

75 x 45mm
8.5 l/h 25.2 °C
AMU Oxytrace
Dimensions: 96 x 96 x 119mm (DIN 43700)

Weight: 0.45kg
Ambient temperature: -10 to +50°C
Limit range of operation: +25 to +65°C
Storage and transport: -30 to +85°C
Humidity: 10 to 90% relative, non-condensing
Voltage: 85 - 265VAC, 47 - 63Hz,
or 24VDC ±15%
Power consumption: max. 7VA
Measuring range Resolution

0.0 - 199.9 ppb 0.1 ppb
200 - 1999 ppb 1 ppb
2 - 20 ppm 0.01 ppm
0 - 200% saturation 0.1 %
Automatic range switching.
8 A-96.250.541 / 080117
AMU Oxytrace
Temperature for NT5k type sensor

Input Measuring range: -30 to +130°C
Resolution: 0.1°C
Temperature Transmitter temperature monitoring with programmable high/low

monitoring alarm limits.
Safety No data loss after power failure, all data is saved in a non-volatile
features memory. Over voltage protection of in- and outputs.
Galvanic separation of measuring inputs and signal outputs.
Alarm Relay One potential free contact for summary alarm indication for
programmable alarm values and instrument faults.
Maximum load: 100mA / 50V
Input One input for potential-free contact. Programmable ‘HOLD’ or

‘OFF’ function.
Relays Two potential-free contacts programmable as

• limit switches for measuring values
• controllers
• timer for system cleaning with automatic hold function
Rated load: 100 mA / 50 V
Signal Two programmable signal outputs for measured values

Outputs (freely scaleable, linear or bilinear) or as continuous control output
(control parameters programmable).
Current loop: 0/4 - 20 mA
Maximum burden: 510 Ω
Control Relays or current outputs programmable for 1 or 2 pulse dosing

Function pumps, solenoid valves or for one motor valve.
Programmable P, PI, PID or PD control parameters.
Communica- Optional RS485 interface with Fieldbus protocol PROFIBUS DP or

tion Interface Modbus, galvanically separated.
Serial RS232 for data logger download to PC with Microsoft

Interface HyperTerminal and for Firmware updates.
A-96.250.541 / 080117 9
AMU Oxytrace
2.2 Swansensor Oxytrace G

The Swansensor Oxytrace G is used for the measurement of
dissolved oxygen in high purity water and is designed for low level
measurement.
Cable with sleeves
Sensor head
Sensor cap
Measuring range: 0 - 15 ppm O2 (at 1°C)

0 - 100% saturation
Accuracy: 0.3%, if cal temp. = measurement temp
1.5%, at +/- 10°C deviation to cal temp.
Temperature sensor: NT5k
Operating temp: 0 - 50 °C
Operating pressure: 0 - 3 bar
Sensor mounting: thread
Material: shaft: polyacetal copolymer
cathode/anode/guard: gold/silver/silver
membrane: fluoropolymer
Response time: t90 < 30 seconds
Minimal sample flow: 50cm / s
10 A-96.250.541 / 080117
AMU Oxytrace
2.3 Flow cells

2.3.1 QV-Flow PMMA OTG
Flow cell made of acrylic glass with integrated flow sensor.
Sample temperature: max. 45 °C
Pressure inlet QV-Flow : max. 1 bar
The sample outlet has to be pressure-free against atmosphere.
Sample flow QV-Flow: 6 - 25 l/h
Process connection inlet: Swagelok connection for 1/4” tube
Outlet: SERTO angle +6mm flexible tube
Dimensions: see picture below
Sample
outlet
Flow
meter
Oxygen
sensor
Sample
inlet
A-96.250.541 / 080117 11
AMU Oxytrace
2.3.2 B-Flow SS316L OTG

B-Flow SS316L OTG is made of stainless steel and can be used for
higher operating pressures and temperatures. There is no flow
sensor.
Sample temperature: 0 - 50 °C
Pressure inlet max. 5 bar at 50 °C
The sample outlet has to be pressure-free against atmosphere.
Process connection inlet and outlet:
Swagelok connections for 1/4” tube
Dimensions: see picture below:
Sample
outlet
Sample
inlet
12 A-96.250.541 / 080117
AMU Oxytrace
2.4 Software
2.4.1 Display
RUN 10:56:03
11.3 ppb
8.5 l/h 25.2 °C
AMU Oxytrace
Menu navigation keys
RUN normal operation

HOLD input closed or cal delay: Instrument on hold (shows status of signal
outputs). Add. info see Program List and Explanations, p. 65.
OFF input closed: Control/limit is interrupted (shows status of signal
outputs). Add. info see Program List and Explanations, p. 65.
error
blinking: fatal error
Status Time
R1 Process dissolved oxygen
xx.x ppb
R2
Values
sample sample
flow l/h °C temperature
Relay Status
upper / lower limit not yet reached
upper / lower limit reached
control upw. / dnw.: no action
control upw. / dnw.: active, dark bar indicates control intensity
motor valve: valve closed
motor valve: open, dark bar indicates approx. position
timer
timer: timing active (hand rotating)
A-96.250.541 / 080117 13
AMU Oxytrace
2.4.2 Menu Navigation Keys

Keys
to exit a menu or command (without accepting)
Exit
to move back to the previous menu level
to move DOWN in a menu list and

to decrease digits
to move UP in a menu list and

to increase digits
to open a selected sub-menu

Enter
to confirm an entry
Program
Navigation RUN 14:10:45 Main Menu 1
R1 Enter Messages
R2 x ppb Diagnostics
Maintenance
Exit Operation
25.0°C Installation
For a detailed listing of the menu see 5 Programm Overview, p. 33
14 A-96.250.541 / 080117
AMU Oxytrace
2.4.3 Software Structure
Main Menu 1
Messages 1.1 Menu Messages 1
Messages Pending Errors Reveals pending errors as
Diagnostics Message List well as an event history
Maintenance (time and state of events
Operation
that have occured at an
Installation
earlier point in time).
Diagnostics 2.1 Menu Diagnostics 2

Identification Provides user relevant
Sensors instrument and sample
Sample data.
I/O State
Interface
Menu Maintenance 3
Maintenance 3.1
For relay and signal output
Simulation simulation, to set the
Set Time 02.04.05 16:49:30 instrument time, and to
Transmitter check off
issue the transmitter
Fine adjust
check. It is used by the
service personnel.
Menu Operation 4
Operation 4.1
Sensors Subset of menu
Relay Contacts Installation 5, but process-
Logger related. User relevant
parameters that might
need to be modified during
daily routine. Normally
password protected and
used by the process-
operator.
Menu Installation 5
Installation 5.1
Sensors For initial instrument set up
Signal Outputs by SWAN authorized
Relay Contacts person, to set all
Miscellaneous instrument parameters.
Interface Normally password
protected.
A-96.250.541 / 080117 15
AMU Oxytrace
2.5 Changing Parameters and values

Changing The following example shows how to change the current loop from
parameters 4-20 mA to 0-20 mA (see Programm Overview, p. 33 Installation):
Signal output 1 5.2.1 Highlight the menu item
Parameter Hydrazine indicating the parameter you
Current loop 4-20 mA want to change.
Function lin
Scaling Enter
Press .
Signal output 1 5.2.1

Parameter Curr. loop. x Sec
Current loop.
0-20 mA
Press or to highlight
Function Free chlorine the required parameter.
4-20 mA
Scaling 1 Min
Press Enter to confirm the
selection (or [Exit] to keep the
previous parameter).
Parameter Hydrazine
Current loop 0-20 mA
Function lin
The selected parameter is
Scaling indicated (but not saved yet).
Press Exit .
Yes highlighted, press Enter to
ParameterSave ? Hydrazine
save the new parameter. The
Current loop 0-20 mA
Yes system reboots, the new
Function No lin
Scaling parameter is set.
Changing
parameter Alarm Dis 5.3.1.1 Enter
Select parameter and press .
values Alarm High 1000 ppb
Alarm Low 0.00 ppb
Hysteresis 1.0 ppb to set required value.
Delay 5 Sec
Alarm Dis 5.3.1.1 Enter to confirm new value.
Alarm High 30.0 ppb
Alarm Low 0.00 ppb Exit to exit the menu.
Hysteresis 1.0 ppb
Delay 5 Sec
16 A-96.250.541 / 080117
AMU Oxytrace
Installation
3. Installation
3.1 Installation Checklist
Check Instrument’s specification must conform to

your AC power ratings. Do not turn on
power until instructed to do so.
On site 85-265 VAC, 47-63 Hz or 24 VDC power
requirements outlet with ground
connection and 20 VA.
Installation Mount the instrument in vertical position.
Display should be at eye level.
Electrical Wiring Connect all external devices like limit
switches, current loops and pumps. Con-
nect power cord; do NOT switch on power
yet!
Electrode Connect the sensor to the AMU transmitter
Turn-on power Switch on power.
First, the transmitter performs a self test,
displays the firmware version and then
starts normal operation
Run-in Period Please consult the respective sensor oper-
ation manual for more information.
Programming Program all parameters for external
devices (interface, etc.). Set all parameters
for instrument operation (limits, alarms).
Calibration Perform an air calibration if needed
A-96.250.541 / 080117 17
AMU Oxytrace
Installation
3.2 Mounting of the Instrument

Transmitter Standard housing according to DIN 43700: 96 x 96 x 119 mm
89.8
96
89.8
96
112
18 A-96.250.541 / 080117
AMU Oxytrace
Installation
3.3 Electrical Connection Scheme
Use only the terminals shown in this diagram, and only for
the mentioned purpose. Use of any other terminals will
cause short circuits with possible damage to material and
personnel.
A-96.250.541 / 080117 19
AMU Oxytrace
Installation
Rear view
SENSOR
LINE
RS232
RELAYS - INPUT - SIGNAL OUT
OPTION
PROFIBUS or MODBUS
SHIELD
3.4 Power Supply
Power Supply Connector
Neutral
Phase
20 A-96.250.541 / 080117
AMU Oxytrace
Installation
3.5 Relay Contacts
3.5.1 Alarm Relay

Note: Max. load 100mA / 50V
Terminal 5/6
3.5.2 Relay Contacts 1 and 2

Note: Max. load 100mA / 50V
Relay 1: Terminal 1/2

Relay 2: Terminal 3/4
3.6 Signal Outputs 1 and 2

Note: Max. burden 510Ω
If signals are sent to two different receivers,
use a signal isolator (loop isolator).
Signal Output 1: Terminal 13 (+) and 12 (-)

Signal Output 2: Terminal 14 (+) and 12 (-)
Current loop: 0 - 20mA resp. 4 - 20mA
3.7 Input
Use only potential-free (dry contacts).
Terminal: 11/10
A-96.250.541 / 080117 21
AMU Oxytrace
Installation
3.8 Sensor Connections
Swansensor Connect the sensor as given bellow:

Oxytrace G
Black Brown Green White
19 20 21 22
Swan Connect the Swan flow meter of the QV-Flow cell as given below.
flow meter
Black White Brown
7 8 9
3.9 Interfaces
3.9.1 RS232
The interface RS232 is on the backside of

the AMU transmitter.
For connecting the communication cable and the configuration

(using RS232 for data logger download to PC and for firmware
updates)
22 A-96.250.541 / 080117
AMU Oxytrace
Installation
3.9.2 Profibus (optional)
The interface RS485,

galvanically separated.
To connect several instruments by means of a network, use a

PROFIBUS cable with free ends. See picture below.
Please buy a PROFIBUS cable with free endsfrom your local suppli-
er.
NOTE: The color of the wires might be different. Before connecting
them to the transmitter, please check the corresponding data sheet.
In-and outcoming leads have to be bridged, as shown in the picture
above.
This bridging allows the replacement of an AMU transmitter without
interruption of the Profibus.
NOTE: Terminate bus by means of ON/OFF switch on the RS485

interface only. If only one instrument is installed, or on the last
instrument in a bus, the termination switch must be ON.
A-96.250.541 / 080117 23
AMU Oxytrace
Instrument Setup
4. Instrument Setup
4.1 Establish sample flow

Sensor Check if:
Power is available
Sensor is in working condition
Establish 1 Check if sample is available. Open sample flow.

Sample Flow 2 Connect the instrument to power. If applicable, adjust sample
flow. To achieve the precise determination the sample flow
should be in the range of 6-25 l/h.
5. Maintenance
Maintenance frequency depends strongly on the water quality.
5.1 Maintenance Schedule

Weekly Check sample flow.
Make manual measurement.
If necessary, correct.
Monthly If necessary, perform an air calibration.
Half a year Clean Oxytrace G membrane with a soft tissue.
Yearly Replace Oxytrace G electrode membrane and
filling electrolyte. If the sensor is exposed to air
frequently and during long time intervals, the
electrolyte and membrane may have to be
changed earlier (see below*).
Clean flow cell and flow meter, if dirty.
*A change of membrane and electrolyte is recommended:

if the response of the sensor is slow
if the sensor can not be calibrated any more and/or the
instrument shows a corresponding error message
if the sensor signal is very unstable.
24 A-96.250.541 / 080117
AMU Oxytrace
Maintenance
5.2 Stop Operation before Maintenance

Stop sample flow.
Shut off power of the instrument.
To take the sensor out of the flow cell, turn the fastening of the
sensor counter clockwise. Unscrew it completely. Open the
sample valve slightly for a moment. This will loosen the tight
seal of the sealing ring, and the electrode may be taken out of
the flow cell easily. Do NOT pull the sensor with force!
5.3 Maintenance of Oxygen Sensor

From time to time it is necessary to exchange the electrolyte and
membrane.
Warning: The filling solution is alkaline and caustic. It contains less

than 1% of potassium hydroxide.
Do not ingest. Wear protective goggles and gloves during
handling. Avoid contact with clothes.
In case of accidental contact with the eyes, wash immediately
with clear water and contact a physician. Show him the label of
the bottle or this section of the manual.
Short contact with skin is harmless, nevertheless wash with lots
of water
A-96.250.541 / 080117 25
AMU Oxytrace
Maintenance
Filling and • Switch of power.

membrane • Screw off the the sensor cap. Exhaust the remaining electrolyte.
exchange
.
Thread
Anode
Sensor cap
Cathode
Guard electrode
• Take the new cap of the replacement kit (A-87.290.050) and fill
it completely with fresh electrolyte.
• There is a groove in the electrode thread, where excessive air
and electrolyte can escape while mounting the sensor cap. Hold
the sensor in upright position, sensor tip pointing downwards,
with the groove on the upper side.
• Slowly fix the electrode head and the sensor cap to allow the
excess electrolyte to escape without building up too much
pressure inside the electrode. Fasten sensor cap finger-tight.
• Clean the electrode thoroughly and dry the sensing membrane
with a soft tissue.
• Switch on power. Let the sensor run-in at air for at least 30 min,
better 1 h. Afterwards perform an air calibration and install the
sensor into the flow cell again.
26 A-96.250.541 / 080117
AMU Oxytrace
Maintenance
5.4 Calibration
5.4.1 Calibration Procedure
Go into Maintenance, select Calibration.
If the instrument is in operation, turn off the sample flow by turning
the needle valve.
To take the electrode out of the flow cell, turn the fastening of the
sensor counter clockwise. Unscrew it completely. Open the sample
valve slightly for a moment. This will loosen the tight seal of the
sealing ring, and the electrode may be taken out of the flow cell
easily. Avoid pulling the electrode with force.
Dry the electrode's body and sensing membrane with a soft paper
tissue. This is very important!
Place the electrode slightly tilted into the flow cell, so that the
sensor cap of the electrode rests on the rim for the sealing ring.
A-96.250.541 / 080117 27
AMU Oxytrace
Maintenance
In the wet flow cell, the atmosphere will be saturated with water
vapour. This atmosphere will produce the most accurate calibration
results. The sensing part of the electrode must not be in direct
contact with water!
Choose menu 3 (maintenance), then calibration (point 3.1). Press
Enter.
The calibration is now done automatically. As soon as the reading
is stable, the microprocessor will store the calibration data in the
memory.
The required time for a calibration depends mainly on the
difference between temperature and oxygen content in the sample
and in the air. It can take 15 - 20 minutes. This is also the case, if
the electrolyte was exchanged. The end of the calibration is
indicated on the display.
Push Enter to confirm the calibration.
Insert the electrode back into the flow cell, push down completely.
Tighten the sensor fastening.
Turn the sample flow on and off until all air bubbles are flushed out.
During calibration, control is interrupted. The signal outputs are

frozen if hold after calibration has been programmed (menu
4.3.4.2). Otherwise the outputs track the measuring value. Hold
after calibration is indicated by Hold in the display.
For additional explanations see Error Codes, p. 31
The calibration value should be verified monthly. Leave the sensor

with clean and dry membrane at air. Set the display to % saturation
and check the calibration value. The air pressure is automatically
acquired during calibration. Therefore the influence of altitude and
pressure variations because of the weather are eliminated.
28 A-96.250.541 / 080117
AMU Oxytrace
Maintenance
5.4.2 Zero-Verification
SWANSENSOR OXYTRACE G for the measurement of low
oxygen content (< 1 ppb).
Prepare a 5%-sodium sulfite solution with demineralized water.
If necessary, install the electrode according to the description in
the manual (Maintenance of Oxygen Sensor, p. 25), i. e. place a
measuring membrane into the head screw cap of the electrode
and fill it with electrolyte.
Calibrate according to the manual
(Calibration Procedure, p. 27).
Put the electrode into the sodium sulfite solution afterwards.
Assure that there are no air bubbles at the electrode.
The measured value should now be < 1 ppb.
Depending on the state of the electrode this process can take
several hours. In case of an electrode-refill, this can take days
until the measured value is lower than 1 ppb.
A-96.250.541 / 080117 29
AMU Oxytrace
Error list
6. Error list
6.1 Error messages

The menu 1 - Messages - reveals pending errors as well as the
message list with text, time and state of errors that have occured
before.
Error
Nonfatal error. The system continues to operate normally, except
for the defective part.
Fatal error (blinking symbol)

If used for control relay 1, 2 as well as the Signal Outputs are
deactivated, i. e. any control is interrupted. The indicated measured
values are incorrect. Depending on the error the system may stop
operating.
To solve the problem, please consult Error Codes, p. 31
Errors remain in the Pending

Pending Errors 1.1.5
Errors window until
Error Code E010
corrected, even if
Sample Flow low acknowledged.
Acknowledging the error only
<Enter> to Acknowledge deactivates the Alarm Relay,
i.e. it switches off an alarm
device if available.
If an error is corrected, by intervention or by the system itself, it is
listed in the the Message List (Menu 1.2). The symbol
disappears.
The last 64 messages are stored for viewing. They are deleted if
SET Default Values (Menu 5.4.2) is carried out.
30 A-96.250.541 / 080117
AMU Oxytrace
Error list
6.2 Error Codes

E0xx (bold and red) are fatal errors.
Error Error text Corrective action
E001 Oxygen Alarm high check process
E002 Oxygen Alarm low check process
E003 Saturation Alarm high check process
E004 Saturation Alarm low check process
E007 Sample Temp. high check sample temperature
E008 Sample Temp. low check sample temperature
E009 Sample Flow high check sample inlet pressure,

check sample flow, check alarm
value in Installation/Relays/
Alarm relay/Sample
E010 Sample Flow low establish sample flow, check

sample inlet pressure, check
alarm value in Installation/
Relays/Alarm relay/Sample,
clean instrument
E011 Temp. shorted check wiring of temperature sen-

sor, check temp. sensor
E012 Temp. disconnected check wiring of temperature sen-

sor, check temp. sensor
E013 Case Temp. high check environment temperature
E014 Case Temp. low check environment temperature
E017 Control time-out check control device or program-

ming in Installation, Relay con-
tact, Relay 1/2
E024 Input active Information that the Input is

active (see programming Instal-
lation, Input, Fault “Yes”)
A-96.250.541 / 080117 31
AMU Oxytrace
Error list
Error Error text Corrective action
E025 IC MK41T56 call service
E026 IC LM75 call service
E027 IC PCF8574 call service
E028 EEProm Microcon call service
E029 EEProm Motherboard call service
E030 EEprom Front-End call service
E031 Calibration RecOut call service
E032 Wrong Front-End call service
E033 Power-on none, status message
E034 Power-down none, status message
32 A-96.250.541 / 080117
AMU Oxytrace
Programm Overview
A. Programm Overview
Pending Errors 1.1*
Messages Message List 1.2*

(Main Menu 1)
Designation AMU Oxytrace 2.1.1*
Version e.g 4.11 – 11/07 2.1.2*
Instrument 2.1.3.1*
Identification 2.1* Factory Test 2.1.3* Motherboard
Front End
Years 2.1.4.1*
Operating Time 2.1.4* Days
Hours
:
Current Value 2.2.1.4*

Oxytrace G Raw Value tc
2.2.1* Raw Value
Sensors 2.2* Saturation
Cal. History 2.2.1.5*
Case Temp. 2.2.2.1*

Diagnostics Miscellaneous Air pressure
(Main Menu 2) 2.2.2*
Sample ID 2.3.1*
Temperature (°C)
Sample 2.3* Nt5k (Ohm)
Sample Flow (l/h)
Sample flow raw value (Hz)
Alarm Relay 2.4.1/2.4.2*

Relay 1/2
I/O State 2.4* Input
Signal Output 1/2
Protocol 2.5.1*
Interface 2.5* (only with RS485
Baud rate 2.5.2* or RS232 interface)
* Menu numbers
Menu Messages may be protected by a password. Menu

Diagnostics is always accessible for everybody. No password
protection. In both menus, no settings can be modified.
A-96.250.541 / 080117 33
AMU Oxytrace
Programm Overview
Calibration 3.1*
Maintenance Alarm Relay 3.2.1*

(Main Menu 3) Simulation 3.2* Relay 1/2 3.2.2-3.2.3*
Signal Output 1/2 3.2.4-3.2.5*
Set Time 3.3*
Sensors 4.1* Filter Time Const. 4.1.1*

Hold after Cal. 4.1.2*
Operation Alarm Relay 4.2.1* Alarm Oxygen 4.2.1.1*

(Main Menu 4) Alarm Saturation 4.2.1.2*
Relay Contacts
4.2* Relay 1/2 4.2.2/4.2.3* Parameters depend on chosen settings
in menu Installation
Active 4.2.4.1*
Signal Outputs 4.2.4.2*
Input 4.2.4* Output/Control 4.2.4.3*
Fault 4.2.4.4*
Delay 4.2.4.5*
Logger 4.3* Log Interval 4.3.1*

Clear Logger 4.3.2*
* Menu numbers
Menu Maintenance is for service: Calibration, simulation of outputs

and set time/date. Please protect with password.
Menu Operation is for the user, allowing to set limits, alarm values,
etc. The presetting is done in the menu Installation (only for the
System engineer). Please protect with password.
34 A-96.250.541 / 080117
AMU Oxytrace
Programm Overview
Flow 5.1.1* None

Q-Flow
Sensors 5.1*
O2 Offset 5.1.2*
Parameter 5.2.X.1*
Signal Outputs Signal Output 1/2 Current Loop 5.2.X.2*
5.2* 5.2.1*/5.2.2* Function 5.2.X.3*
Scaling / Control Parameters 5.2.X.4X*
Alarm Oxygen 5.3.1.1*

Alarm Relay Sample Flow 5.3.1.2*
5.3.1* Sample Temp 5.3.1.3*
Alarm Saturation 5.3.1.4*
Case Temp. 5.3.1.5*
Installation
(Main Menu 5) Function 5.3.X.1*
Relay Contacts Relay 1/2 Parameter 5.3.X.20*
5.3* 5.3.1*/5.3.2* further settings depends on chosen function
Active 5.3.4.1*
Signal Outputs 5.3.4.2*
Input 5.3.4* Output/Control 5.3.4.3*
Fault 5.3.4.4*
Delay 5.3.4.5*
Language 5.4.1*
Miscellaneous 5.4* Set defaults 5.4.2*
Load Firmware 5.4.3*
Password 5.4.4*
Sample ID 5.4.5*
Protocol 5.5.1*
Interface 5.5* (only with RS485
Baud rate 5.5.2* or RS232 interface)
* Menu numbers
Menu Installation: Defining assignment of all inputs and outputs, measuring

parameters, interface, passwords, etc. Menu for the system engineer. Password
stronlgy recommended
A-96.250.541 / 080117 35
AMU Oxytrace
RS232 Interface
B. RS232 Interface
B.1 Connection of the Communication Cable

1 Disconnect the instrument from the mains!
2 Connect the communication cable for AMU transmitters to the
transmitter.
RS232 with connected communication

cable
3 Connect the other end of the cable to the PC.
4 Connect the instrument to power.
36 A-96.250.541 / 080117
AMU Oxytrace
RS232 Interface
B.2 Configuration of the AMU Transmitter

1 Enter the menu 5.5.1 on the AMU transmitter and choose
HyperTerminal for the sub-menu Protocol.
Interface 5.5.1
Protocol HyperTerminal Protocol
Baud Rate 115200 Baud Profibus
Modbus RTU
SWAN Bus
HyperTerminal
Webserver
Confirm with <Enter>
2 Enter menu 5.5.2 and choose 115200 Baud for the Baud rate.
Interface 5.5.2
Protocol HyperTerminal
Baud Rate 115200 Baud Baud Rate
2400 Baud
4800 Baud
9600 Baud
19200 Baud
38400 Baud
57600 Baud
115200 Baud
Confirm with <Enter>
A-96.250.541 / 080117 37
AMU Oxytrace
RS232 Interface
B.3 HyperTerminal Configuration on the PC
38 A-96.250.541 / 080117
AMU Oxytrace
RS232 Interface
* Note:
If your computer has no COM port, you have to use an USB-COM-
Converter to connect the cable to the PC.
After connection find out via the Device Manager which port you
are using (Settings/Control Panel/System/Hardware/Device
Manager).
Clicking on the Device

Manager leads you to the
following scheme:
Clicking on Ports
(COM & LPT) shows
you which port is
used.
This address of the port should be used for the configuration of the
HyperTerminal.
A-96.250.541 / 080117 39
AMU Oxytrace
RS232 Interface
40 A-96.250.541 / 080117
AMU Oxytrace
RS232 Interface
A-96.250.541 / 080117 41
AMU Oxytrace
RS232 Interface
B.4 Functions of the AMU RS232 Interface

The AMU RS232 Interface has two functions:
transfer of log datas onto a PC
upgrade of AMU instruments with a new firmware.
B.4.1 Logger Download

Log interval The internal logger can save approx. 1’500 data records, stored at
a selectable time interval. The following table shows the period of
time covered with the corresponding record interval.
Operation 4.4
Sensors
Signal Outputs
Relay Contacts
Logger
Log Interval
Logger 4.4.1
1 Second
Log Interval x Sec/Min/Hour 5 Seconds
Clear Logger no/yes 1 Minute
5 Minutes
10 Minutes
30 Minutes
1 Hour
Interval 1s 5s 1 min 5 min 10 min 30 min 1h
Time 25 min 2h 25 h 5d 10 d 31 d 62 d
Default value for the the interval is set on 30 min.
42 A-96.250.541 / 080117
AMU Oxytrace
RS232 Interface
B.4.2 Log download

Download
Procedure Choose the configured
connection.
On the keyboard,
press Esc.
Browse to the
folder you have
created to archive
printouts.
A text file AMU*.TXT is created. Existing files are renamed

AMU*0.TXT, AMU*1.TXT, AMU*2.TXT, etc.
A-96.250.541 / 080117 43
AMU Oxytrace
RS232 Interface
Changing the To change the folder where the files are saved,
folder for 1 press the “Receive”-button.
download
data 2 choose the directory and the folder
3 and the receiving protocol must be Zmodem.
44 A-96.250.541 / 080117
AMU Oxytrace
RS232 Interface
B.4.3 Clear Logger

To delete all log data, proceed as follow
:
Operation 4.4
Sensors
Signal Outputs
Relay Contacts
Logger
Logger 4.4.2
Log Interval 30 Minutes
Clear Logger no
Enter
Clear Logger Select yes and press
no to accept.
yes
Exit
Press .
Logger 4.4.2
Log Interval
Save? 30 Minutes
Clear Logger yes yes highlighted, press Enter
Yes to clear logger. The system
No
reboots, all log data is
deleted.
A-96.250.541 / 080117 45
AMU Oxytrace
RS232 Interface
B.5 Firmware Upload

Only SWAN trained and authorized personnel shall perform the
tasks described in this section.
Requirements The HyperTerminal connection must be configured. See

HyperTerminal Configuration on the PC, p. 38
Firmware 1
upload
Choose the
configured
connection.
AMU Rescon
3 Press <Enter> and

confirm it by
pressing “y”.
46 A-96.250.541 / 080117
AMU Oxytrace
RS232 Interface
If upload fails (instrument

does not restart), repeat
steps 1 and .2
Perform Set defaults 5.4.2 > completely and setup the

instrument according to user specifications.
A-96.250.541 / 080117 47
AMU Oxytrace
Profibus (option)
C. Profibus (option)
C.1 Introduction
The AMU family of transmitters provides a common base for a
number of analytical instruments with application specific sensor
interfaces. Each instrument has a basic structure with identical
functionality.
AMU instruments can (optionally) be equipped with a PROFIBUS

DP-V1 interface. The interface supports the PROFIBUS-PA Profile
3.0. This part of the manual describes the functionality of the
interface and the integration of the AMU family of transmitters into
an automation system.
Hardware Wiring, bus terminals and connectors are not part of this manual. It
should, however, be noted that the observation of the
corresponding standards is of paramount importance to proper
operation. Setting the transmission rate to reasonable values will
help avoid communication errors.
GSD File for The PROFIBUS system requires a description of the device
AMU parameters, e. g. output data, input data, data format, data volume
Oxytrace and supported transmission rate, so that it can integrate the field
devices into the bus system. These data are contained in a
Device Master File (GSD file) which is placed at the disposal of
the PROFIBUS master while communication system is
being commissioned.
Device bitmaps can also be integrated. These appear as icons in

the network tree.
The manufacturer-specific GSD file SW17E1.gsd is available for
download from http://www.swan.ch
48 A-96.250.541 / 080117
AMU Oxytrace
Profibus (option)
C.2 Cyclic Data Telegram

AMU Oxytrace makes the following modules available as input data
for the cyclic data exchange:
1 Main Process Value (ppb)

2 Main Temperature
3 Main Flow (l/h)
4 2nd Process Value (%)
5 Control AMI
6 Diagnostic Values (5 values)
a Raw Current Temperature Compensated in nA
b Raw Current in nA
c Air Pressure in hPa
d Reserved (for internal use)
e Case Temperature in °C
The input data is transferred from AMU Oxytrace in the following

structure :
Figure 1: Input data structure of AMU Oxytrace

Index
Data format /
input Data Access Configuration data
comments
data
0 ... 4 Analog Input block 1 read Measured value (32-bit 0x42, 0x84, 0x08, 0x05 or
Main Process Value floating point number) 0x42, 0x84, 0x81, 0x81 or
Status byte 0x94
Main Temperature floating point number) 0x42, 0x84, 0x81, 0x81 or
Status byte 0x94
Main Flow floating point number) 0x42, 0x84, 0x81, 0x81 or
Status byte 0x94
nd
2 Process Value floating point number) 0x42, 0x84, 0x81, 0x81 or
Status byte 0x94
20 ... 39 Diagnostic Values read 5 Measured values (32-bit 0x45, 0x93, 0x08, 0x08,
floating point numbers) 0x08, 0x08, 0x08, 0xE9
A-96.250.541 / 080117 49
AMU Oxytrace
Profibus (option)
The output data is transferred to AMU Oxytrace in the following structure:

Index
Data format /
output Data Access Configuration data
comments
data
0 ... 1 Control AMI (SP_D) write Byte 0 0x82, 0x81, 0x05, 0x05 or
Bit Description 0x82, 0x81, 0x84, 0x82 or
0 Relay 1 0xA1
0 = open
1 = close
1 Relay 2
0 = open
1 = close
2 Not used
3 Not used
4..7 Not used
Byte 1
Bit Description
0 Hold
1 Control Off
2..7 Not used
B.3 Customizing the Cyclic Data Telegram

You can customize the cyclic telegram to better meet the
requirements of a process. The tables above represent the
maximum contents of the cyclic data telegram. If you do not want to
use all the cyclic data of AMU Oxytrace, you can use the device
configuration (Chk_Cfg) to eliminate individual data blocks from the
cyclic telegram via the PLC software. Shortening the telegram
improves the data throughput rate of a PROFIBUS system. You
should only keep those blocks active which you process further in
the system. You can do this by means of a "negative" selection in
the configuration tool.
To achieve the correct structure of the cyclic data telegram, the
PROFIBUS master must send the identification FREE_PLACE
(00h) for the non-active blocks.
50 A-96.250.541 / 080117
AMU Oxytrace
Profibus (option)
B.4 Data Formats

Each measured value has the same format: one four-byte (32-bit)
floating-point value in IEEE 754 Short Real Number format and a
status code byte referring to the measured value. There are four
quality states, 16 sub-status values (not all defined) for each quality
state, and four limit states for the measured value indicated in its
associated status byte (See Figures 2 ,3, 4 and 5).
Figure 2: Out Value + Status

Byte 1 Byte 2 Byte 3 Byte 4 Byte 5
Analog values in IEEE 754 Format Status
Figure 3: IEEE 754 floating point number:
Byte n Byte n+1 Byte n+2 Byte n+3

Bit 7 Bit 6 Bit 0 Bit 7 Bit 6 Bit 0 Bit 7 Bit 0 Bit 7 Bit 0
Sign 27 26 25 24 23 22 21 20 2–1 2–2 2–3 2–4 2–5 2–6 2–7 2–8 2–9 2–10 2–11 2–12 2–13 2–14 2–15 2–16 2–17 2–18 2–19 2–20 2–21 2–22 2–23
Exponent Mantissa Mantissa Mantissa
Formula: Value = (-1) sign * 2(exponent - 127) * (1 + mantissa)

Example: 40 F0 00 00 h = 0100 0000 1111 0000 0000 0000 0000
0000 b
Value = (-1)0 * 2(129 - 127) * (1 + 2-1 + 2-2 + 2-3)
= 1 * 22* (1 + 0.5 + 0.25 + 0.125)
= 1 * 4 * 1.875
= 7.5
Figure 4: Status Code Byte

7 6 5 4 3 2 1 0
Quality Sub-status Limits Meaning
0 0 bad
0 1 uncertain
1 0 good
The sub-status has
a different quality 0 0 ok
depending on the coding
0 1 low limited
1 0 high limited
1 1 constant
A-96.250.541 / 080117 51
AMU Oxytrace
Profibus (option)
Figure 5: Status codes of the measured value

Status Device status Meaning Limits
code
0x08 BAD Not connected (Temp Sensor not
connected)
0x0C BAD device failure
0x10 BAD sensor failure (Temp Sensor Short Circuit)
0x47 UNCERTAIN last usable value (HOLD) CONST
0x50 UNCERTAIN sensor conversion not accurate (No Flow) OK
0x64 UNCERTAIN sensor calibration OK
0x67 sensor calibration, hold CONST
0x80 GOOD ok OK
0x89 GOOD Warning Low LOW_LIM
0x8A Warning High HIGH_LIM
0x8D GOOD Alarm Low LOW_LIM
0x8E Alarm High HIGH_LIM
Figure 6: DP Diagnostics
Byte Description
0 Status 1 Standard DP Diagnostics
1 Status 2
2 Status 3
3 Master address
4 Ident number (high byte)
5 Ident number (low byte)
6 Header (block length incl. Header byte) = 14 Status coding according
7 Status Type (0x81) to DP/V1
8 Slot Number (0x00)
9 Status Specifier
10 ..13 Diagnosis
14 ..19 Diagnosis Extension
52 A-96.250.541 / 080117
AMU Oxytrace
Profibus (option)
The diagnosis object consists of 4 Bytes
Byte Bit Meaning when “1” Abbreviation

0 0 Hardware failure electronics DIA_HW_ELECTR
1 Hardware failure mechanics DIA_HW_MECH
2 -
3 Electronic temperature too high DIA_TEMP_ELECTR
4 -
5 Measurement failure DIA_MEASUREMENT
6 -
7 -
1 0 -
1 -
2 -
3 -
4 -
5 Maintenance required DIA_MAINTENANCE
6 -
7 -
2 0 -
1 -
2 -
3 -
4 -
5 -
6 -
7 -
3 0 -
1 -
2 -
3 -
4 -
5 -
6 -
7 Extension Available EXTENSION_AVAILABLE
A-96.250.541 / 080117 53
AMU Oxytrace
Profibus (option)
The diagnosis extension object consists of 6 Bytes

.
Byte Bit Meaning when “1”
0 0 Oxygen Alarm high -
1 Oxygen Alarm low -
2 Saturation Alarm high -
3 Saturation Alarm low -
4 - -
5 - -
6 Sample Temp. high DIA_MEASUREMENT
7 Sample Temp. low DIA_MEASUREMENT
1 0 Sample Flow high DIA_MEASUREMENT
1 Sample Flow low DIA_MEASUREMENT
2 Temp. shorted DIA_HW_ELECTR
3 Temp. disconnected DIA_HW_ELECTR
4 Case Temp. high DIA_TEMP_ELECTR
5 Case Temp. low DIA_TEMP_ELECTR
6 -
7 -
2 0 Control Timeout -
1 - -
2 - -
3 - -
4 - -
5 - -
6 - -
7 Input Active DIA_HW_ELECTR
3 0 IC MK41T56 DIA_HW_ELECTR
1 IC LM75 DIA_HW_ELECTR
2 IC PCF8574 DIA_HW_ELECTR
3 EEprom Microcon DIA_HW_ELECTR
4 EEProm Motherboard DIA_HW_ELECTR
5 EEProm Frontend DIA_HW_ELECTR
6 Cal. Recout DIA_HW_ELECTR
7 Wrong Frontend DIA_HW_ELECTR
Bytes 4 and 5 are reserved for future extensions.
54 A-96.250.541 / 080117
AMU Oxytrace
Profibus (option)
B.5 Configuration
B.5.1 Device Master Files (GSD)

The device is ready for system integration once commissioning has
been effected via the local display or the Class 2 master. The
PROFIBUS system requires a description of the device
parameters, e.g. output data, input data, data format, data volume
and supported transmission rate, so that it can integrate the field
devices into the bus system. These data are contained in a Device
Master File (GSD file) which is placed at the disposal of the
PROFIBUS master while the communication system is being
commissioned. Device bitmaps can also be integrated. These
appear as icons in the network tree.
The Profile 3.0 Device Master File (GSD) allows field devices from
various manufacturers to be exchanged without having to
reconfigure.
B.5.2 GSD File Types

Prior to configuration, decide which GSD you want to use to
operate the system.
You can change the setting by means of a Class 2 master (under
Physical Block-Parameter Ident_Number_Selector).
The following two Device Master Files with different functionalities

are available:
Manufacturer-specific GSD with Profile 3.0 functionality
(default setting):
This GSD guarantees the unlimited functionality of the field device.
Device-specific process parameters and functions are therefore
available.
Profile GSD's:
If a system is configured with profile GSD's, it is possible to
exchange devices that are supplied by various manufacturers. It is,
however, essential that the cyclic process values follow the same
sequence. The transmitter supports the profiles Analyzer and
Multivariable (IEC 61158-2). These GSD's comprise Analog Input
blocks (AI).
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AMU Oxytrace
Profibus (option)
GSD files for AMU Oxytrace:
Device name Ident_number_ ID number GSD Bitmaps

Selector
Manufacturer-specific GSD with Profile 3.0 functionality:
AMI Oxytrace 1 17E1Hex SW17E1.gsd SW17E1_D.bmp

SW17E1_N.bmp
SW17E1_D.bmp
Profile 3.0 GSD Analyzer:
AMI Oxytrace 0 9750 Hex PA039750.gsd PA_9750n.bmp
Profile 3.0 GSD Multivariable:
AMI Oxytrace 3 9760 Hex PA039760.gsd PA_9760n.bmp
Working with GSD files

The GSDs must be integrated into the automation system.
Depending on the software that is being used, the GSD files can be
copied to the program-specific directory or can be read into the
database using the import function within the configuration
software.
B.6 Acyclic Data Communication

The AMU Series of analytical instruments is available for a wide
range of parameters. Instrument configuration depends on
connected sensors and application. Therefore, configuration must
be performed by trained personnel with a background in
analytical methods.
It should be noted that there is a clear distinction between

instruments that are configured and calibrated in an application
(flow, level, pressure) and instruments that are calibrated with a
known standard (pH, chlorine). AMU instruments are of the
second type.
To ensure reliability and consistency of the measurement, remote

configuration has not been enabled at this time.
56 A-96.250.541 / 080117
AMU Oxytrace
Modbus (option)
C. Modbus (option)
C.1 Introduction
The AMU Oxytrace is an electronic transmitter / controller for the
measurement of dissolved oxygen in high purity water. It can be
operated as an intelligent slave device on the Modbus/JBUS using
twisted pair RS485 lines.
Modbus/Jbus The Modbus / Jbus Protocol communicates using a master-slave
technique, in which only one device (the master) can initiate
transactions (queries). The other devices (the slaves) respond by
supplying the requested data to the master, or by taking the action
requested in the query. Typical master devices include host
processors, PLCs etc. Typical slaves can be PLCs or intelligent
transmitter/controller like the AMU family of the instruments.
The Query The function code in the query tells the addressed slave device
what kind of action to perform. The data bytes contain any
additional information the slave will need to function. For example,
function code 03 will query the slave to read holding registers and
respond with their contents. The data field must contain the
information telling the slave which register to start at and how many
registers to read.
The Re- If the slave makes a normal response, the function code in the
sponse response is an echo of the function code in the query.
The data bytes contain the data collected by the slave.
Serial Modbus supports two transmission modes: ASCII or RTU.
Transmission The AMU Instruments support Modbus RTU (Remote Terminal
modes Unit) mode only.
RTU Mode In RTU mode, each 8-bit byte in a message contains two 4-bit
hexadecimal characters. The main advantage of this mode is that
its greater character density allows better data throughput than
ASCII for the same baud rate. Each message must be transmitted
in a continuous stream. Users select the desired serial port
communication parameters (baud rate, parity mode, etc). The serial
parameters must be the same for all devices on a Modbus network.
A-96.250.541 / 080117 57
AMU Oxytrace
Modbus (option)
Coding System
Eight bit binary
1 start bit
8 data bits, least significant bit sent first
1 bit for even / odd parity, no bit for no parity
1 stop bit if parity is used, 2 bits if no parity
Cyclic Redundancy Check (CRC)
RTU framing: messages start with a silent interval of at least 3 ½
character times. A similar interval of at least 3 ½ character times
marks the end of the message.
A typical message frame is shown below
Slave
Start Function Data CRC END
Address
T1-T2-T3-T4 8 Bits 8 Bits n x 8 Bits 16 Bits T1-T2-T3-T4
58 A-96.250.541 / 080117
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Modbus (option)
C.2. Data and Control Functions

Data adress Data Addresses in Modbus Messages
All data addresses in Modbus Messages are referenced to zero.
The first occurrence of a data item is addressed as item number
zero. For example:
Holding Register 40001 is addressed as register 0000 in the
data address field of the message. The function code field
already specifies a holding register operation. Therefore the 4x
reference is implicit.
Function Modbus Function Codes
codes The list below shows the function codes supported by the AMU
Instruments. Codes are listed in decimal. Function codes not
supported return an exception response 02 to the master.
Table 1: Modbus function codes
Code Name Description

02 Read Input Status Read Alarm & Status Bits
03 Read Holding Registers Read Parameter Data
04 Read Input Registers Read Process Data
05 Force Single Coil Set Relays, fake Keystrokes etc.
16 Preset Multiple Registers Preset Parameter Data (SWAN Use only)
Data re- Data representation

presentation The process- and parameter data of the AMU Instruments are
represented by float (IEEE 754), signed- or unsigned integer
values. Depending on the range of the value, float, integer8,
unsigned8, integer16, unsigned16, integer32 or unsigned32
representation is used.
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AMU Oxytrace
Modbus (option)
Discrete Inputs
Alarm &Status bits are packed as one input per bit of the data field.
Definition: big-endian and little-endian

Big-endian and little-endian are terms that describe the order in
which a sequence of bytes are stored in computer memory. Big-
endian is an order in which the "big end" (most significant value in
the sequence) is stored first (at the lowest storage address). Little-
endian is an order in which the "little end" (least significant value in
the sequence) is stored first. For example, in a big-endian
computer, the two bytes required for the hexadecimal number 4F52
would be stored as 4F52 in storage.
In a little-endian system, it would be stored as 524F.
Attention: big-endian format is used !!!
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Modbus (option)
C.3 Function Description

Input status Read Input Status (Alarm &Status Bits), Function 02
Up to 32 bits of Alarm are available as summarised in the table
below:
Table 2: Alarm and Status addresses
Addr. Type Description
0 Alarm Oxygen Alarm high
1 Alarm Oxygen Alarm low
2 Alarm Saturation Alarm high
3 Alarm Saturation Alarm low
4 Alarm -
5 Alarm -
6 Alarm Sample Temp. high
7 Alarm Sample Temp. low
8 Alarm Sample Flow high
9 Alarm Sample Flow low
10 Alarm Temp. shorted
11 Alarm Temp. disconnected
12 Alarm Case Temp. high
13 Alarm Case Temp. low
14 Alarm -
15 Alarm -
16 Alarm Control Timeout
17 Alarm Reagent Empty
18 Alarm -
19 Alarm -
20 Alarm -
21 Alarm -
22 Alarm
23 Alarm Input Active
24 Alarm IC MK41T56
25 Alarm IC LM75
26 Alarm IC PCF8574
27 Alarm EEprom Microcon
28 Alarm EEprom Motherboard
29 Alarm EEprom Front-end
30 Alarm Cal. Recout
31 Alarm Wrong Front-end
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AMU Oxytrace
Modbus (option)
Input register Read Input Registers (Process data): Function 04

The process data are made up of the measuring values of the AMU
Powercon.
Table 3: Input registers
Byte- Data type Description Range of physical value
Offset
0 Float Oxygen 0.. 20’000 ppb
4 Float Temperature -30 … 120 ºC
8 Float Flow 0... 50 l/h
12 Float Saturation 0… 200 %
16 Float Air Pressure 500... 1200 hPa
20 Float Raw Oxygen temp. compensated 0... 50000 nA
24 Float Raw Oxygen uncompensated 0... 50000 nA
28 Float Raw Temp. (NT5k) 150 … 66’000 Ω
32 Float Raw Flow 0.. 100 Hz
36 Float Odometer 0.. 100 mAh
40 Float Case Temperature -55... 125 ºC
44 Float Signal Output 1 0.. 20 mA
48 Float Signal Output 2 0.. 20 mA
52 INSTRUMENT_STATUS Instrument Display Status
Single coil Force Single Coil: Function 05

function This function is used to set relays and reset the instrument. Relays
can only be forced if set to fieldbus function.
Table 4: single coil function
Addr. Description OFF (0) ON (1)
0.. 1 Relay Contacts 1..2 open close
2 Hold no yes
3 Remote Off no yes
4 Channel Select Channel 0 Channel 1
15 Reset Instrument (like hardware reset) reset
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Modbus (option)
Holding Read Holding Registers (Parameter data): Function 03

register Read Parameter data (see Parameter Table). All objects of type
Record are defined in the Manufacturer specific tables following the
parameter table.
Note: The Address is used in a proprietary way to select the
designated record.
see parameter table on the next page.
Table 5: parameter table

Address Modbus Addr Parameter Object Type Data Type Description Acc.
2300 1151 Version Record FIRMWARE_REC Firmware Version r
2400 1201 Num_Evt Simple Unsigned16 No. of Event Records r

2402 1202 Num_Log Simple Unsigned16 No. of Log Records r
3000 1501 Cal_History_1 Array Array of CAL_HIST_1[15] Cal. History Dis. r
4000.. 4126 2001.. 2064 Event_Rec Record EVENT_REC Get Event Record r
64 Records max.
5000.. 8070 2501.. 4036 Log_Rec Record LOG_REC Get Logger Record r
1536 Records max.
Specific data Manufacturer-specific Data Types & Records

DATE_STAMP Format
31.. 26 25..22 21..17 16..12 11.. 6 5.. 0
YYYYYY MMMM DDDDD HHHHH MMMMMM SSSSSS
Year Month Date Hour Minutes Seconds
0... 63 1... 12 1... 31 0... 23 0... 59 0... 59
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AMU Oxytrace
Modbus (option)
Parameter Size Data Type Description Range

INSTRUMENT_STATUS 32 Record Instrument Display Status
Language 1 Unsigned8 Language Selection 0 = German
1 = English
2 = French
3 = Spanish
RunMode 1 Unsigned8 Run Mode 0 = Run
1 = Hold
2 = Off
3 = Grab
AlaMode 1 Unsigned8 Alarm Mode 0 = Off
1 = on
2 = Blinking
MaintMode 1 Unsigned8 Maintenance Mode 0 = Off
1 = on
2 = Blinking
RelMode1 1 Unsigned8 Relais 1 Display Mode 0 = None
1 = Limit Hi On
2 = Limit Hi Off
3 = Limit Lo On
4 = Limit Lo Off
5 = Timer Off
6 = Timer On
7 = Percent Control
8 = Valve
9 = Bus
RelMode2 1 Unsigned8 Relais 2 Display Mode 0 = None
1 = Limit Hi On
2 = Limit Hi Off
3 = Limit Lo On
4 = Limit Lo Off
5 = Timer Off
6 = Timer On
7 = Percent Control
8 = Valve
9 = Bus
PercDos1 2 Unsigned16 Percent Dosage Relais 1 0.. 100 %
PercDos2 2 Unsigned16 Percent Dosage Relais 2 0.. 100 %
MaintValue 2 Unsigned16 Maintenance Value 0.. 100 %
AlarmsActive 4 Unsigned32 Alarms Pending AlarmsActive
AlarmsLatched 4 Unsigned32 Alarms no Acknowledged AlarmsLatched
AlarmsActiveE 4 Unsigned32 Extended Alarms Pending AlarmsActiveE
AlarmsLatchedE 4 Unsigned32 Extended Alarms not Acknowledged AlarmsLatchedE
TimeStamp 4 DATE_STAMP Current Time
end Record
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Program List and Explanations
D. Program List and Explanations

1 Messages
1.1 Pending Errors
Provides the list of active errors with their status (active,
acknowledged). If an active error is acknowledged, the alarm relay
opens again. Cleared errors are moved to the Message list.
1.2 Message List

Shows the error history: Error code, date and time of issue, and
status (active, acknowledged, cleared).
65 errors are memorized. Then the oldest error is cleared to save
the newest error (circular buffer).
2 Diagnostics
In diagnostics mode, the values can only be viewed, not modified.
2.1 Identification
2.1.1 View the Designation of instrument: Always AMU Oxytrace
2.1.2 Version: firmware of instrument, e.g. V4.11-11/07
2.1.3 Factory test of the instrument; date of mother board and front-end
QC test
2.1.5 Operating time: years, days, hours, minutes, seconds
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AMU Oxytrace
2.2 Sensors
2.2.1 Oxytrace G
Current value: in ppb
Raw value tc: raw value in nA, temperature compensated.
Raw value: raw value in nA, uncompensated.
Saturation: Current saturation in %
2.2.1.5 Cal history:
Review the diagnostic values of the last calibration of the oxygen
sensor. Only for diagnostic purpose.Max. 65 data records are
memorized.
2.2.2 Miscellaneous
Case Temp.: Actual temperature in °C inside the transmitter.
Air pressure: Displaying of the current air pressure in hPa
2.3 Sample
2.3.1 Sample ID
Sample ID: Review the programmed code. The code is defined by
the user to identify the sample point in the plant.
Temperature
Current sample temperature in °C and additionally the resistance of
the Nt5k temperature probe in Ohm
2.4 I/O State

2.4.1- 2.4.2 Reveals the actual status of all in and outputs:
Alarm relay: Open or closed
Relay 1 and Relay 2: Open or closed
Input: Open or closed
Signal output 1, 2 (and 3, if option is installed):
Actual current in mA.
2.5 Interface
Review programmed communication settings.
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3 Maintenance
3.1 Calibration
3.1.5 Start a calibration and follow the instructions on the screen.
Displayed values are saturation in % and the saturation current in
nA. The indication bar shows the progress.
3.2 Simulation
3.2.1-3.2.6 Select alarm relay, relay 1 /2 or signal output 1/2 to be tested with
the <Enter> key and press the up/down key to change the value.
After confirming the setting with the Enter key, the value is
simulated by the relay/signal output.
At the absence of any key activities, the instrument will switch back
to normal mode after 20 min.
If you quit the menu, all simulated values will be reseted.
3.3 Set Time

Adjust date and time.
4 Operation
4.1 Sensors
4.1.1 Filter time constant:
Used to damp noisy signals. The higher the filter time constant, the
slower the system reacts to changes of the measured value.
Range: 5-300 sec
4.1.2 Hold after cal:
To allow the instrument to stabilize again after calibration. During
cal. and hold time the signal outputs are frozen, alarms and limits
are not active.
Range: 0 - 6000 sec
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AMU Oxytrace
4.2 Relay Contacts

4.2.1 Alarm Relay
The alarm relay is used as cumulative error indicator.
Under normal operating conditions, the contact is open.
The contact closes upon:
power loss
detection of system faults like defective sensors or electronic
parts
high case temperature
process values out of programmed ranges
See chapter 5 for a complete list and description of parameters.
Program process value alarm levels here or in menu 5.3.1
4.2.2 and Relay 1 and 2
4.2.3 The function of relay contacts 1 or 2 are defined by the user:
Start by defining the function of each relay in menu 5.3.2 and 5.3.3.
These functions may be selected:
limit switch, controller, timer or fieldbus driven.
Then enter the necessary data in this menu or in the submenus of
5.3.2 / 5.3.3. The description of each function is given in chapter 5.
4.2.4 Input:
The functions of the relays and signal outputs can be defined
depending on the position of the input contact, i.e. no function,
closed or open. See menu 5.3.4 for parameter description
68 A-96.250.541 / 080117
AMU Oxytrace
4.3 Logger
The instrument is equipped with an internal logger. The data can be
downloaded to a PC by Hyperterminal interface (see Log
download, p. 43 for more details)
The logger can save approx. 1500 data records. Records consists
of: Date, time, alarms, measured value, measured value
uncompensated, temperature, flow.
4.3.1 Log Interval: Select a convenient log interval. Consult the table
below to estimate the max logging time. When the loggin buffer is
full, the oldest data record is erased to make room for the newest
one. (circular buffer)
Interval 1s 5s 1 min 5 min 10 min 30 min 1h
Time 25 min 2h 25 h 5d 10 d 31 d 62 d
4.3.2 Clear logger: If confirmed with yes, all data is erased and a new
data series is started.
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AMU Oxytrace
5 Installation
5.1 Sensors
5.1.1 Flow:
If a flow cell without flow measurement (B-Flow) is used, choose
none. With flow measurement select Q-Flow
5.1.2 O2 Offset:
Manual, small correction of the offset. Range 0-3 ppb
5.2 Signal outputs

5.2.1 - 5.2.3 Signal output 1, Signal output 2, Signal output 3:
Signal output 3 is only available if option 3rd signal output has been
installed.
Assign process value, the current loop range and a function to each
signal output.
5.2.1.1 Parameter: Assign one of the process values to the signal output.
Available values: Oxygen, Temperature, Sample flow and
Saturation.
5.2.1.2 Current loop: Select the current range of the signal output. Make
sure the connected device works with the same current range.
Available ranges: 0-20 mA or 4-20 mA.
5.2.1.3 Function: Define if the signal output is used to transmit a process
value or to drive a control unit:
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As process values:
The process value can be represented in 3 ways: linear, bilinear or
logarithmic. See graphs below
mA
20
e ar
bilin
0-20 mA: 10
4-20 mA: 12
e ar
lin
0/4
0.0 0.1 0.2 0.3 0.4 0.5 0.6 unit
meas. value
mA
20
0-20 mA:10
4-20 mA: 12
0/4
1 2 3 6 30
10 100 1000 10000 value
0 1 2 3 4 log
5.2.1.40 Scaling: Enter beginning and end point of the linear or

logarithmic scale. In addition, the midpoint for the bilinear scale.
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AMU Oxytrace
As control output:
Signal outputs can be used for driving control units.
We distinguish different kinds of controls:
P-controller:
The controller action is proportional to the deviation from the
setpoint. The controller is characterized by the P-Band. In the
steady-state, the setpoint will never be reached. The deviation is
called steady-state error.
Parameters: setpoint, P-Band
PI-controller:
The combination of a P-controller with an I-controller will minimize
the steady-state error. If the reset time is set to zero, the I-controller
is switched off.
Parameters: setpoint, P-Band, reset time
PD-controller:
The combination of a P-controller with a D-controller will minimize
the response time to a fast change of the process value. If the
derivative time is set to zero, the D-controller is switched off.
Parameters: setpoint, P-Band, derivative time.
PID-controller:
The combination of a P-, an I- and a D-controller allows a proper
control of the process.
parameters: setpoint, P-Band, reset time, derivative time
Ziegler-Nichols method for the optimization of a PID controller:

parameters: setpoint
P-Band: Xp = 1.2 / a
reset time: Tn = 2 L
derivative time: Tv = L / 2
measure
tangent on the inflection
response on maximum
control output
a time
The point of intersection of the tangent with the respective axis will
result in the parameters a and L .
Consult the manual of the control unit for connecting and
programming details. Choose control upwards or downwards.
72 A-96.250.541 / 080117
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Control upwards/downwards:
5.2.x.43.10 Setpoint: User-defined process value (Oxygen, Temperature,
Sample flow or Saturation).
5.2.x.43.20 P-Band: Range below (upwards control) or above (downwards
control) the set-point, within the dosing intensity is reduced from
100% to 0% to reach the set-point without overshooting.
5.2.X.43.3 Reset time: The reset time is the time till the step response of a
single I-controller will reach the same value as it will be suddenly
reached by a P-controller.
Range: 0-9000 sec.
5.2.X.43.4 Derivative time: The derivative time is the time till the ramp
response of a single P-controller will reach the same value as it will
be suddenly reached by a D-controller.
Range: 0 - 9000 sec.
5.2.X.43.5 Control timeout: If a controller action (dosing intensity) is constantly
over 90% during a defined period of time and the process value
does not come closer to the setpoint, the dosing process will be
stopped to safety reasons. Range: 0 - 720 min.
5.3 Relay contacts

5.3.1 Alarm relay
The alarm relay is used as cumulative error indicator.
Under normal operating conditions the contact is open.
The contact closes upon:
power loss
detection of system faults like defective sensors or electronic
parts
high case temperature
process values out of programmed ranges.
Program alarm levels, hysteresis values and delay times for the
following parameters:
Oxygen, Sample Temp, Sample Flow, Saturation and Case temp.
The alarm values of Oxygen and Saturation can also be
programmed in menu 4.2.1.1 or 4.2.1.2
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5.3.1.1 Alarm Oxygen:

5.3.1.1.1 Alarm high: If the measured value rises above the alarm high
value, the alarm relay closes and E001 is displayed
in the message list. Range: 0-10 ppm
5.3.1.1.23 Alarm low: If the measured value falls below the alarm low
in the message list. Range: 0-10 ppm
5.3.1.1.33 Hysteresis: Within the hyst. range, the relay does not switch.
This prevents damage of relais contacts when the measured
value fluctuates around the alarm value.
Range. 0-10 ppm
5.3.1.1.43 Delay: During run time plus the delay time the signal and control
outputs are held in the operating mode. Range: 0-28800 sec
5.3.1.2 Alarm Sample Flow:
5.3.1.2.1- Flow Alarm high (E009) and low (E010)
5.3.1.2.36 Range alarm high: 10-50 l/h
Range alarm low: 0.5-9 l/h
5.3.1.3 Alarm Sample Temperature:
5.3.1.3.1- Alarm Sample Temperature high (E007) and low (E008)
5.3.1.3.23 Range alarm high: 30-100 °C
Range alarm low: -10-20 °C
5.3.1.4 Alarm Saturation:
5.3.1.4.1 Alarm high: If the measured value rises above the alarm high
in the message list. Range: 0-200 %
5.3.1.4.23 Alarm low: If the measured value falls below the alarm low
in the message list. Range: 0-200 %
5.3.1.4.33 Hysteresis: Within the hyst. range, the relay does not switch.
Range. 0-200 %
5.3.1.4.43 Delay: During run time plus the delay time the signal and control
outputs are held in the operating mode. Range: 0-28800 sec
5.3.1.4-5.3.1.5 Case temperature alarm high (E013) and low (E014)
Range alarm high: 30 - 75 °C
Range alarm low: -10 - 20 °C
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5.3.2 - 5.3.3 Relay 1 and 2

The function of relay contacts 1 or 2 are defined by the user:
First select the functions as:
limit switch, controller, timer or fieldbus driven.
Then enter the necessary data depending on the selected function.
The same values may also be entered in menu 4.2.2 and 4.2.3.
5.3.X.1 Function
Select Limit upper, Limit lower, Control upw., Control dnw., Timer or
Fieldbus
Limit upper/lower:
5.3.X.20 Parameter: Select Oxygen, Temperature, Sample flow or

Saturation
5.3.X.300 Set-point: User-defined process value (Oxygen, Temperature,
Sample flow or Saturation).
5.3.X.400 Hysteresis: Within the hysteresis range, the relay does not switch.
5.3.2.50 Delay: uring run time plus the delay time the signal and control
outputs are held in the operating mode.
Range: 0-28800 sec
Control upwards / downwards:

The relays may be used to drive control units such as solenoid
valves, membrane dosing pumps or motor valves. When driving a
motor valve both relays are needed, relay 1 to open and relay 2 to
close the valve.
5.3.X.22 Parameter
select the process parameter to be controlled (Oxygen,
Temperature, Sample flow or Saturation)
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5.3.X.32 Settings
Choose the respective actuator:
Time proportional
Examples of metering devices that are driven time proportional are
solenoid valves, peristaltic pumps.
Dosing is controlled by the operating time
Parameters:
Cycle time: duration of one control cycle (on/off change).
Range: 10-600 sec.
Response time: Minimal time the metering device needs to react
Range: 0-240 sec.
Frequency
Examples of metering devices that are puls frequency driven are
the classic membrane pumps with a potential free triggering input.
Dosing is controlled by the repetition speed of dosing shots
Parameters:
Pulse frequency: Max. pulses per minute the device is able to
respond to. Range: 20-300/min.
Motor valve
Dosing is controlled by the position of a motor driven mixing valve.
Parameters:
Run time: Time needed to open a completly closed valve
Range: 5-300 sec.
Neutral zone: Minimal response time in % of the of the runtime. If
the requested dosing output is smaller than the response time, no
change will take place.
Range: 0-240 sec.
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5.3.X.32.31 Control Parameters

Define the control parameters for the respective actuator
5.3.X.32.31.10 Set-point:User-defined process value (Oxygen, Temperature,
Sample flow or Saturation)
5.3.X.32.31.20 P-Band: Range below (upwards control) or above (downwards
control) the set-point, within the dosing intensity is reduced from
100% to 0% to reach the set-point without overshooting.
5.3.X.32.31.3 Reset time: The reset time is the time till the step response of a
single I-controller will reach the same value as it will be suddenly
reached by a P-controller.
Range: 0-9000 sec.
5.3.X.32.31.4 Derivative time: The derivative time is the time till the ramp
response of a single P-controller will reach the same value as it will
be suddenly reached by a D-controller.
Range: 0 - 9000 sec.
5.3.X.32.31.5 Control timeout: If a controller action (dosing intensity) is constantly
over 90% during a defined period of time and the process value
does not come closer to the setpoint, the dosing process will be
stopped to safety reasons. Range: 0 - 720 min.
Timer
The relay will be closed repetitively depending on the programmed
time scheme.
This function is intended mainly to run Swan's cleaning modules or
to program an automatic filter flush.
5.3.X.24 Operation mode: Select the operation mode (interval, daily, weekly)
of the signal outputs.
5.3.X.340 Interval: Set interval time. range 1-1440 min.
5.3.X.44 Run Time: Time the relay stays closed. Range: 5-6000 sec.
5.3.X.54 Delay: during run time plus the delay time the signal and
control outputs are held as programmed below .
5.3.X.6 Signal Outputs:
Select the behavior of the signal outputs when the relay closes
Continuous: Signal output continues normally.
Hold: Signal output continues on the last valid value.
Off: Signal output is switched off and goes to 0/4 mA
4.2.2.6 Output / Control:
Select the behavior of the control outputs when the relay closes
Continuous: Controller continues normally.
Hold: Controller continues on the last valid value.
Off: Controller is switched off.
A-96.250.541 / 080117 77
AMU Oxytrace
Fieldbus
The relay will be switched via the Profibus input. No further
parameters are needed.
See section Profibus (option), p. 48 for more details
5.3.4 Input
5.3.4.1 Define when the input should be active:

No: Input is never active
When closed: Input is active if the input relay is closed
When open: Input is active if the input relay is open
5.3.4.2 Signal output: Select the operation mode of the signal outputs
when the relay is active (closed):
Continuous: Signal outputs continue to issue the
measured value.
Hold: Signal outputs issue the last valid measured value.
Off: set to 0 or 4 mA respectively.
5.3.4.3 Output/Control (relay or signal output):
Continuous: Controller continues normally..
Hold: Controller continues on the last valid value.
Off: Controller is switched off.
5.3.4.4 Fault:
No: No message is issued and the alarm relay does not close
when input is active.
Yes: Message E024 is issued and alarm relay closes when
input is active.
5.3.4.5 Delay:
Time which the instrument waits, after the input is deactivated,
before returning to normal operation.
Range: 0 - 6000 s
78 A-96.250.541 / 080117
AMU Oxytrace
5.4 Miscellaneous
5.4.1 Language: Set the desired language.
Available settings: Deutsch / English / Français / Español
5.4.2 Set default values: Reset the instrument to factory default values
in three different ways:
Calibration: Sets calibration values back to default. All other
values are kept in memory.
In parts: Communication parameters are kept in memory. All other
values
are set back to default values.
Completely: Sets back all values including communication
parameters.
5.4.3 Load firmware: Firmware updates should be done by instructed
service personnel only.
5.4.4 Password: Select a password different from 0000 to prevent
unauthorized access to the menus “Messages”, “Maintenance”,
“Operation” and “Installation”.
Each menu may be protected by a different password.
If you forgot the passwords, contact the closest SWAN
representative.
5.4.5 Sample ID: Identify the process value with any meaning full text,
such as KKS number.
5.5 Interface
5.5.1 Select one of the following communication protocols. Depending on
your selection, different parameters must be defined.
Profibus: Device Address: 0 - 126
ID Number: Analyzer, Manufacturer, Multivariable
Local operation: enable, disable
see Profibus (option), p. 48 for details.
Modbus RTU: Device Address: 0 - 126
Baud Rate: 2400 - 115200
Parity: none, even, odd
see Modbus (option), p. 57 for details
HyperTerminal: Baud Rate: 2400 - 115200
see RS232 Interface, p. 36
Webserver: Device Address: 0-126
see separate Webserver Manual.
A-96.250.541 / 080117 79
AMU Oxytrace
MSDS Filling electrolyte
F. MSDS Filling electrolyte
COMERCIAL PRODUCT NAME Filling solution “1ALK”

for oxygen sensor, 50 ml, 102751.10
Chemical characterization : contains less than 1% KOH (caustic potassium

solution)
Form : liquid
Color : clear
Odor : Odorless
Change in physical state : Boiling point roughly 100 °C
Density (20 qC) : -
Solubility in water : good
pH - Value lower than pH 13
Flash point : ---
Autoignition temperature : ---
Explosion limits : ---
Hazardous decomposition products : Not any
Hazardous reactions : Not any
Transport :
IMDG-code 8/II
UN No. 1814
ICAO/IATA Class 8
8 UN 1814 PAX 809 CAO 813
Regulations : Requirement under the classification, packaging

and labeling of dangerous substances
regulations.
Warning symbol C
Risk phrases R 35
Safety phrases S 2-26-27-37/39
Protective Measures, Storage and Handling
Technical protective measures : Store in cool room, away from sunlight.

Personal protective equipment : Eye protection and PE-gloves.
Do not swallow.
Measures in case of Accidents and Fires
After spillage/leakage : Dilute with water.
First Aid :
- Inhalation : --
- Eyes : Wash with lot of water, summon eye specialist
immediately.
- Contact with skin : Wash with lot of water
Information on toxicology : -
Information on ecology : Less than 1% caustic potassium solution (KOH)
80 A-96.250.541 / 080117
AMU Oxytrace
Default Values
G. Default Values
Operation:
Sensors: Filter time constant: 30s
Hold after cal: 300 s
Relay 1, same as in Installation
Relay 2, Input:
Log. Interval: 30 min
Clear Logger no
Installation:
Sensors: Flow: None
O2 Offset: 0.0 ppb
Signal Outputs: Parameter Output 1: Oxygen
Parameter Output 2: Temperature
Current loop: 4-20 mA
Function: linear
Scaling:
Oxygen range low: 0.0 ppb
Oxygen range high: 10.00 ppm
Temperature range low: 0.0 °C
Temperature range high: 50.0 °C
Flow range low: 0 .0 l/h
Flow range high: 50.0 l/h
Saturation range low: 0.0 %
Saturation range high: 100 %
Alarm Relay: Alarm Oxygen high: 10 ppm
Alarm Oxygen low: 0.0 ppb
Hysteresis: 100 ppb
Delay: 5 s
Flow alarm: yes
Flow alarm high: 20.0 l/h
Flow alarm low: 5 l/h
Sample temp. alarm high: 100 °C
Sample temp. alarm low: 0 °C
Saturation alarm high: 120 %
Saturation alarm low: 0.0 %
Hysteresis: 2 %
Delay: 5 s
Case temp. high: 65 °C
Case temp. low: 0 °C
A-96.250.541 / 080117 81
AMU Oxytrace
Default Values
Relay1/2 Function: limit upper

Parameter: Oxygen
Setpoint: 10 ppm
Hysteresis: 100.0 ppb
Delay: 30 s
Control: Actuator: Frequency
Control: Frequency: Frequency: 120/min
Control: Time prop.: Cycle time: 60s, Response time: 10 s
Control: Motor valve: Run time: 60s, Neutral zone: 5%
Control: Control parameter Setpoint: 10 ppm
Control: Control parameter P-band: 100.0 ppb
Control: Control parameter Reset time: 0 s
Control: Control parameter Derivative time: 0 s
Control: Control parameter Control time-out: 0 min
Timer: Mode: Interval:
Timer: Interval:1 min
Timer: Mode: daily/weekly: Starting time: 00.00.00
Timer: Run time: 10s
Timer: Delay: 5s
Timer: Signal output: cont.
Timer: Output/Control: cont.
Input Active: when closed
Signal Outputs: hold
Output/Control: off
Fault: no
Delay: 10 s
Miscellaneous Language: English
Set default: no
Load firmware: no
Password: for all modes 0000
Sample ID: --
Interface Protocol: Hyperterminal
Baud Rate: 115200 Baud
82 A-96.250.541 / 080117
AMU Oxytrace
Index
H. Index
A
Alarm Relay . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9, 21, 69
Attention Symbols . . . . . . . . . . . . . . . . . . . . . . . . . 5
B
B-Flow SS316L OTG . . . . . . . . . . . . . . . . . . . . . . 12
C
Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27
Communication Cable . . . . . . . . . . . . . . . . . . . . . . 36
Control Function . . . . . . . . . . . . . . . . . . . . . . . . . . 9
D
Data Communication, acyclic . . . . . . . . . . . . . . . . 57
Data Communication, cyclic . . . . . . . . . . . . . . . . . 50
Data logger . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 70
Default Values . . . . . . . . . . . . . . . . . . . . . . . . . . . . 82
Delay . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 75
Description of the system . . . . . . . . . . . . . . . . . . . 7
Diagnostics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 66
Display . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
E
Electrical Connection Scheme. . . . . . . . . . . . . . . . 19
Error Codes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31
Error list . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30
F
Filter time constant . . . . . . . . . . . . . . . . . . . . . . . . 68
Firmware Upload . . . . . . . . . . . . . . . . . . . . . . . . . . 46
G
GSD File Types . . . . . . . . . . . . . . . . . . . . . . . . . . 56
H
HyperTerminal . . . . . . . . . . . . . . . . . . . . . . . . . . . . 38
Hysteresis . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 75
I
Input . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9, 21, 69
Instrument Setup . . . . . . . . . . . . . . . . . . . . . . . . . . 24
Interface . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9, 22
L
Logger Download . . . . . . . . . . . . . . . . . . . . . . . . . 42, 43
Logger, clear . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45
A-96.250.541 / 080117 83
AMU Oxytrace
Index
M
Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 68
Maintenance of Oxygen Sensor . . . . . . . . . . . . . . 25
Maintenance Schedule . . . . . . . . . . . . . . . . . . . . . 24
Measuring principle . . . . . . . . . . . . . . . . . . . . . . . . 7
Measuring range . . . . . . . . . . . . . . . . . . . . . . . . . . 8, 10
Modbus . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 58
Mounting . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18
MSDS Filling electrolyte. . . . . . . . . . . . . . . . . . . . . 81
O
On-line operation . . . . . . . . . . . . . . . . . . . . . . . . . . 7
Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 68
P
Power Supply . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
Profibus . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23, 49
Program List and Explanations . . . . . . . . . . . . . . . 66
Programm Overview . . . . . . . . . . . . . . . . . . . . . . . 33
Q
QV-Flow PMMA OTG . . . . . . . . . . . . . . . . . . . . . . 11
R
Relays . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9, 21, 69
RS232 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 22, 36
S
Sensor Connections . . . . . . . . . . . . . . . . . . . . . . . 22
Sensors . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 68
Signal Outputs . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9, 21, 71, 74
Software. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
Software Structure . . . . . . . . . . . . . . . . . . . . . . . . . 15
Swansensor Oxytrace G . . . . . . . . . . . . . . . . . . . . 10
T
Technical Data. . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
Temperature Input . . . . . . . . . . . . . . . . . . . . . . . . . 9
Temperature monitoring . . . . . . . . . . . . . . . . . . . . 9
W
Warning Symbols . . . . . . . . . . . . . . . . . . . . . . . . . 5
Z
Zero-Verification . . . . . . . . . . . . . . . . . . . . . . . . . . 29
84 A-96.250.541 / 080117
AMU Oxytrace
A-96.250.541 / 080117 85
AMU Oxytrace
SWAN
is represented worldwide by subsidiary companies
and distributors.
cooperates with independent representatives

all over the world.
SWAN Products
Analytical Instruments for:
High Purity Water
Feedwater, Steam and Condensate
Potable Water
Pool and Sanitary Water
Cooling Water
Waster Water and Effluents
Made in Switzerland.
86 A-96.250.541 / 080117

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AMU Oxytrace

Version 4.11 and later

SWAN sets the standard

SWAN ANALYTISCHE INSTRUMENTE AG

Title: AMU Oxytrace Operator’s Manual

© 2008, SWAN ANALYTISCHE INSTRUMENTE AG, Switzerland, all rights reserved

Information contained in this document is subject to change without notice.

2. Description of the system . . . . . . . . . . . . . . . . . . . . . . . 6

D. Program List and Explanations . . . . . . . . . . . . . . . . . . 64

F. MSDS Filling electrolyte . . . . . . . . . . . . . . . . . . . . . . . . 79

AMU Oxytrace - Operator’s Manual

Operator: Qualified person who uses the equipment

To be qualified for instrument operation, you must read and

The AMUAMU Oxytrace Operator’s Manual shall be kept in

1.2 Warning Notices

electrical shock hazard

1.3 General Safety Regulations

1.3.1 Legal Requirements

1.3.2 General Inspection and Maintenance Duties

1.3.3 Spare Parts and Disposables

1.3.5 Electrical shock hazard

If proper operation is no longer possible, the instrument must be

2. Description of the system

Measuring Clark principle:

On-line Swansensor Oxytrace combined with QV-flow cell: The sample

2.1 Technical Data

11.3 ppb Large backlit LC-Display,

Dimensions: 96 x 96 x 119mm (DIN 43700)

Measuring range Resolution

Automatic range switching.

Temperature for NT5k type sensor

Temperature Transmitter temperature monitoring with programmable high/low

Input One input for potential-free contact. Programmable ‘HOLD’ or

Relays Two potential-free contacts programmable as

Signal Two programmable signal outputs for measured values

Control Relays or current outputs programmable for 1 or 2 pulse dosing

Communica- Optional RS485 interface with Fieldbus protocol PROFIBUS DP or

Serial RS232 for data logger download to PC with Microsoft

2.2 Swansensor Oxytrace G

Cable with sleeves

Measuring range: 0 - 15 ppm O2 (at 1°C)

2.3 Flow cells

2.3.2 B-Flow SS316L OTG

8.5 l/h 25.2 °C

Menu navigation keys

RUN normal operation

2.4.2 Menu Navigation Keys

to move DOWN in a menu list and

to move UP in a menu list and

to open a selected sub-menu

For a detailed listing of the menu see 5 Programm Overview, p. 33

2.4.3 Software Structure

Diagnostics 2.1 Menu Diagnostics 2

2.5 Changing Parameters and values

Signal output 1 5.2.1

3.1 Installation Checklist

Check Instrument’s specification must conform to