Boiling Point & Boilup Rate

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Bubble point calculation

Mole Fraction A B C
Mehtylene Dichloride 1 7.0803 1138.91 231.45
Isopropanal 0 8.87829 2010.33 252.636
Temp °C P°b P°T Pb Pt
-44.1384264512486 10.0000689197 0.17230873192 10.00006892 0

Result Boiling Point -44.1 Vaccum 750.0

760
Pb+Pt
10.00006892
O-Xylene MDC
Vaccum Boiling point 600 2.12
mmHG °C 660 -7.27
500 102 680 -11.46
550 96 700 -16.65
600 88.34 710 -19.809
650 78.36 720 -23.55292
700 63.53 730 -28.18852
740 40.14 740 -34.38
750 -44.13
Boilup Rate Calculation
Name of Solvent Isopropanal
Moleculer weight 60
Dansity 0.786 Gm/Ml
Boiling Point 82 °C
Latant Heat 159 Kcal/Kg
Specific Heat 0.61 Kcal/Kg°C
Reactor Capacity 4 KL
Volume of mass 2300 L
Qty to be distilled 1900 L
Qty in Reactor 400 L
Heat Transfer area 8 M2
Effective HTA at mass 4.6 m2
Effective HTA After distillation 0.46
m2
average Heat transfer area 2.53 m2
Vaccum 749 mmhg
At vaccum BP °C 4 °C
Steam Pressure 0.2 Kg/cm2
Steam Temp 104.7 °C
Hot Water 55 °C
Overall Heat Transfer
Coefficient 200 w/M2
Q 25864.1083946009 Kcal
Mass flow rate 162.667348393716 KG/hr
Boiluo rate Hot water 206.955913986916 L/Hr
Q 50993.8464478414
Boilup With Steam 320.716015395229
Boiluo rate volume 408.035642996474 L/Hr
A B C
8.87829 2010.33 252.636

450
1 1.5
2 2.4
3 3.5
4 8
5 7
6 10
7
8
9
10
11
12 20
13
14
15
Moleculer Boiling Latant Specific
Name of the solvent Dansity A
Wt Point Heat Heat
N-pantane 72 0.626 36.1 85 0.56 6.87632
N-Haxane 86 0.659 69 80 0.49 6.91058
N Haptane 100 0.684 98.4 76 0.51 6.89386
Cyclohaxane 84 0.778 80.7 85 0.44 6.85146
Bwnzene 78 0.879 80 94 0.41 6.87987
toluene 92 0.867 110.6 87 0.45 8.53516
ethyle Banzene 106 0.867 136 80 0.41 6.9658
O-Xylene 106 0.882 144 82 0.4 6.99053
m-Xylene 106 0.871 139 82 0.4 6.99053
P-Xylene 106 0.871 138 82 0.4 6.99053
Methenol 32 0.792 64 263 0.61 8.08097
ethenol 46 0.789 78 200 0.59 8.1122
n-Propannol 60 0.804 97 163 0.57 8.37895
Isopropanal 60 0.786 82 159 0.61 8.87829
N-beutenol 74 0.81 118 141 0.55 7.838
Iso -beutenol 74 0.807 108 138 0.72 8.53516
sec Beutanol 74 0.807 99 134 0.54 7.47429
Cyclohaxenol 100 0.947 161 109 0.5 8.35237
Ethylene Glycol 62 1.1135 198 202 0.56 8.09083
mehtyle Cellulose 76 0.975 124 135 0.53 7.8498
Ethyle Cellulose 90 0.929 136 107 0.56 7.8191
Butyle Cellulose 118 0.901 171 88 0.47 7.8448
Mehtylene Dichloride 85 1.326 40 79 0.28 7.0803
Chloroform 119 1.48 61 59 0.23 6.95465
Carban Tetra chloride 154 1.58 76 47 0.21 6.84083
1-2 Dichloro ethane 99 1.253 83.5 77 0.31 7.0253
1,1,1, Trichloro Ethylenen 133 1.329 74 58 0.24 6.90633
Trichloro Ethylenene 131 1.464 87 57 0.23 6.51827
Perchloroethylene 166 1.622 121 50 0.21 7.6293
monochloro benzene 113 1.106 132 78 0.31 7.17294
Acetone 58 0.79 56 122 0.41 7.11714
Methyle Ethyle Ketone 72 0.805 80 109 0.5 7.06356
Methyle isobutyle Ketone 100 0.801 115 85 0.47 6.67272
Cyclohaxanone 98 0.948 156 92 0.45 7.4705
n-Methylene 2- Pyrrolidon 99 1.03 202 127 0.4 8.2789
Di ethyle ethar 74 0.715 34.5 84 0.56 6.98472
Di Isopropyle ether 102 0.724 68 68 0.51 6.84953
1-4 Di oxane 88 1.0336 101 97 0.4 7.43155
Tetra hydrofuran 68 0.888 66 98 0.46 6.99515
Methyle Acetate 74 0.927 57 97 0.5 7.06524
ethyle Acetate 88 0.902 77 88 0.46 7.10179
n-butyle acetate 116 0.883 126 74 0.46 7.02845
Dimethyle Formamide 73 0.945 153 138 0.49 7.1085
Dimethyle Sulfooxide 78 1.101 189 162 0.47 6.88076
Pyridine 79 0.983 115 106 0.43 7.01328
Acetonotrile 41 0.782 81.26 174 0.54 7.33986
Furfuraldehyde 96 1.1598 162 96 0.38 8.402
water 18 0.998 100 539 1 8.07131
B C

1075.78 233.205
1189.64 226.28
1264.37 216.64
1206.47 223.136
1196.76 219.161
1950.94 237.147
1429.55 213.767
1453.43 215.31
1453.43 215.31
1453.43 215.31
1583.271 239.726
1592.864 226.184
1788.02 227.438
2010.33 252.636
1558.19 196.881
1950.94 237.147
1314.188 186.5
2258.56 251.624
2088.936 203.454
1793.982 236.877
1801.9 230
1988.9 230
1138.91 231.45
1170.966 226.232
1210.595 229.664
1271.254 222.927
1211.31 226.816
1018.603 192.731
1803.96 258.976
1549.2 229.26
1210.596 229.664
1261.34 221.969
1168.408 191.9444
1832.2 244.2
2570.3 273.15
1090.64 231.2
1139.34 231.742
1554.679 240.337
1202.29 226.254
1157.63 219.726
1244.95 217.881
1368.5 204
1537.78 210.39
1541.52 191.797
1356.93 212.655
1482.29 250.523
2338.49 261.638
1730.63 233.426
Heat exchanger area
Isopropanal
Boilup rate 600
Dansity ρ 786
Boilup rate 471.6
Specific Heat Cp 0.61
Latent Heat λ 159
Inlet Temp T1 40
Outlet temp T2 25
CW inlet Temp T3 11
CW Outlet Temp T4 8
Overall HTC U 200
LMTD Tlm 21.7738799381987
Specific heat Cp 4315.14
Latent Heat L 74984.4
Total Heat Q 79299.54
Area A 18.2097862726068
Tertery Load 100%
Tertery area Effective A 18.2
L/hr
Kg/m3
Kg/Hr
Kcal/Kg
Kcal/Kg
°C T1 T2 T1 T2
°C 32 14 32 14
°C
°C
W/m2°C
°C 200
Kcal/hr
Kcal/hr
Kcal/hr
m2
%
m2
T1 T2
32 14

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