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Module 6 Optical Properties Lessons 3
Module 6 Optical Properties Lessons 3
ABEn 147
Properties of AB Materials
Module 6 – Lesson 3. STUDENT LEARNING GUIDE
Determination of the Different TP-IMD-02 v0 No. CET.ESC SLG20-03_
Electrical Properties of AB
Materials
College of
ENGINEERING AND
TECHNOLOGY
Department of
AGRICULTURAL AND
BIOSYSTEMS ENGINEERING
2020
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Vision
A globally competitive university for science, technology,
and environmental conservation
Mission
Development of a highly competitive human resource,
cutting-edge scientific knowledge and innovative
technologies for sustainable communities and environment.
It shall be the policy of the university that the quality policies and procedures
are communicated to and understood by all faculty, staff, students and other
stakeholders and that the system shall be continually improved for their
relevance and effectiveness.
Student Learning Guide in
Properties of AB
Materials
ABEn 147. Properties of AB Materials
Table of Contents
Vision i
Mission i
Table of Contents 3
Lesson 6.3 Determination of the Different Electrical Properties of AB
Materials 4
Lesson Summary 4
Learning Outcomes 4
Discussion 4
Electrical Conductivity 4
Electrical Resistivity 6
Electrical Resistance 13
Dielectric Properties 14
Electromagnetic Radiation 19
Assessment 21
References 21
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Lesson 6.3 Determination of the Different
Electrical Properties of AB
Materials
Lesson Summary
This lesson discusses the different methods in measuring the different
mechanical properties of AB materials
Learning Outcomes
At the end of the lesson, the students should be able to:
Discussion
Various methods and mathematical models are used to express and solve
important electrical properties of AB materials, particularly food materials. The
following sections present and discuss these methods.
Electrical Conductivity
Electrical Conductivity or specific conductance, the reciprocal of electrical
resistivity, represents the material’s ability to conduct electric current. It is a
measure of electric current flows through a food of unit cross-sectional area
A, unit length L, and resistance R.
𝐿
𝜎= (1)
𝐴𝑅
Where:
𝜎 = electrical conductivity, S/m; (S=Siemens)
𝐿 = length, m
𝐴 = cross-sectional area, m2
𝑅 = resistance, Ω (ohm)
are connected to a power supply. Care is taken to ensure that the electrodes
make a firm contact with the food sample. Electrical conductivity of foods
increases with temperature in a linear manner. The following equation may be
used to calculate electrical conductivity of a food:
𝜎𝐸 = 𝜎𝑜 (1 + 𝑚" 𝑇) (2)
Where:
𝜎𝑜 = electrical conductivity at 0°C (S/m)
m” = coefficient, (1/°C)
T = temperature (°C)
Values of 𝜎𝑜 , 𝜎𝑟𝑒𝑓 , and coefficients m” and K for different foods are given in
Table 1 shown below.
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6 ABEn 147. Properties of AB Materials
Illustrative Problem 1.
Solution:
Computation:
𝜎𝐸 = 𝜎𝑜 (1 + 𝑚" 𝑇)
𝝈𝑬 = 𝟎. 𝟕𝟒𝟔 𝑺/𝒎
𝝈𝑬 = 𝟎. 𝟕𝟒𝟕 𝑺/𝒎
Electrical Resistivity
Electrical resistivity is a fundamental property of a material that quantifies
how strongly it resists electric current. It is commonly represented by the
Greek letter ρ with SI unit of ohm-meter. It can be solved using the formula:
𝐴
𝜌=𝑅 (4)
𝑙
Where:
𝜌 = electrical resistivity, Ω.m
𝑙 = length, m
𝐴 = cross-sectional area, m2
𝑅 = resistance, Ω (ohm)
Various models and methods have been suggested to measure the electrical
resistance. Factors affecting the suitability of various methods and precision
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ABEn 147. Properties of AB Materials
attainable include contact resistance and shape of the sample i.e. whether is
it in the form of single crystal, thin film, powder pellet or small crystallite.
𝑉𝐴
𝜌= (5)
𝐼𝐿
Where:
𝜎 = electrical resistivity
v = voltage drop, volts
𝐼 = current, A
𝐴 = cross-sectional area, m2
𝑅 = resistance, Ω (ohm)
The potential probe is the most widely used method for resistivity
measurements on the low resistive samples. In this method, the potential
drop is measured across two probes and distance between these probes
D replaces the sample length L in equation 5. When the probes are not
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8 ABEn 147. Properties of AB Materials
point contacts, in that case, the most accurate value for the probe
distance is the distance between the centres rather than the closest
distance between the probes. Figure 3 shows the schematically
arrangement for this method.
𝑉𝐷 𝐴
𝜌= (6)
𝐷𝐼
Four probe method can be used to determine the resistance of the single
crystal as well as the bulk specimen also. Here, current passes through
the outer contacts which are close to the edges of the sample. The
potential difference is measured across the inner contacts. This method
can eliminate the effects of contact resistance between the sample and
electrical contacts and therefore is most suitable for low and accurate
resistance measurements.
Contact and lead resistances are cancelled out by the four point method,
however the contact resistance can still cause error if these produce
enough heat. Thus, it is imperative that the contacts should have low
resistance. Self-induced voltage offsets in the circuit further add to the
error. This problem can be corrected by reversing the flow of current
through the sample. When the low level of the voltage (in the range of µV)
is produced across the sample, signal noise also adds to the error. By
using the proper shielded cables and low thermal contactors, as well as
making single point grounding, noise problem can be reduced.
The ‘four point probe’ method has proven to be a convenient tool for the
resistivity measurement of small size (of the order of mm) specimen. This
method is applicable when the distance between the probes is small
compared to the smallest dimension of the sample, and provided none of
the probe is too close to an edge of the sample. The arrangement of
probes is shown in Figure 4. This gives the functional relationship
between the resistivity ‘ρ’ and the voltage and current ratio for various
geometries.
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ABEn 147. Properties of AB Materials
In the case of a four point probe on a sheet, the two outside current
points represent the dipole. Therefore, the resistivity in this case can be
given by:
𝑉𝐷
𝜌= 𝐼
2𝜋𝑠 (7)
Here, the distance between all the four points is equal. I, is the current
flowing through the sample, 𝑉𝐷 is produced voltage across two inner
points and S is the distance between the adjacent points. If the distance
between contact points is not equal and it is given as S1, S2 and S3
respectively, then the resistivity is given as
𝑉 2𝜋
𝜌= [ ] (8)
𝐼 (1+1− 1
−
1
)
𝑆 𝑆 𝑆
1 3 1 +𝑆2 𝑆2 +𝑆3
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10 ABEn 147. Properties of AB Materials
Figure 6. Samples of any arbitrary shape with four small contacts for
electrical resistivity measurement
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ABEn 147. Properties of AB Materials
𝜋𝑑 𝑅𝐴𝐵,𝐶𝐷 + 𝑅𝐵𝐶,𝐷𝐴 𝑅
𝜌= [ ] 𝑓 ( 𝐴𝐵,𝐶𝐷 ) (9)
ln 2 2 𝑅𝐵𝐶,𝐷𝐴
𝑅𝐴𝐵,𝐶𝐷
Where 𝑓 is a function of ( ) only and satisfies the relation
𝑅𝐵𝐶,𝐷𝐴
ln 2
𝑅𝐴𝐵,𝐶𝐷 𝑓 exp( 𝑓 )
( )= 𝑎𝑟𝑐𝑐𝑜𝑠ℎ { } (10)
𝑅𝐵𝐶,𝐷𝐴 ln 2 2
𝑅𝐴𝐵,𝐶𝐷
𝑓 can be given approximately as and plotted against the ratio ( )
𝑅𝐵𝐶,𝐷𝐴
2 4
𝑅𝐴𝐵,𝐶𝐷− 𝑅𝐵𝐶,𝐷𝐴 ln 2 𝑅 −𝑅 (ln 2)2 (ln 2)3
𝑓 ≅1−[ ] − [ 𝐴𝐵,𝐶𝐷 𝐵𝐶,𝐷𝐴 ] { − } (11)
𝑅𝐴𝐵,𝐶𝐷 + 𝑅𝐵𝐶,𝐷𝐴 2 𝑅𝐴𝐵,𝐶𝐷+ 𝑅𝐵𝐶,𝐷𝐴 4 12
The samples are obtained in powder form, used for pellet study. The
pellet should be made by pressing the powder up to a sufficient and
known pressure without using any binder. Usually these are shaped in the
form of circular discs. A pellet of uniform thickness and circular in shape
has four point contacts on the top surface of it arranged in the form of
rectangle ABCD. The distance between the contacts at A and B is ‘b’ and
that between the contacts at B and c is ‘a’. The thickness of the pellet is
‘d’ must be less than or of the order of 0.3 √𝑎𝑏. This is shown in Figure 7.
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12 ABEn 147. Properties of AB Materials
Consider a rectangular pellet of width ‘b’, length ‘a’ and the thickness ‘d’
and if ABCD represent the corners of the top face of such a pellet, then
according the theory developed by Montgomery, the resistivity can be
given by
𝜌 = 𝐻 𝐸 𝑅1 (12)
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ABEn 147. Properties of AB Materials
In this method, a short pulse of high voltage is applied to the sample and
the current or the potential drop across a pair of probes of the sample is
measured, usually by means of a fast oscilloscope or other amplifying and
recording systems. Since the pulse is of very short duration and repeated
only a few in times in a second or even less. The current density during
the time of application of the pulse is very high without unduly heating or
affecting the sample. This technique is most suitable for the samples
having small dimensions, more fragile and having Joule heating problems.
Electrical Resistance
Electrical resistance is a measure of its opposition to the flow of electric
current. The reciprocal quantity is electrical conductance, and is the ease
with which an electric current passes. The SI units for electrical resistance is
ohm, while electrical conductance is measured in Siemens (S) formerly called
mho.
(https://en.wikipedia.org/wiki/Electrical_resistance_and_conductance)
𝑉
𝑅= (13)
𝐼
𝐼 1
𝐺= = (14)
𝑉 𝑅
Resistance also depend on the material the product is made of as well as the
product’s shape and size. For a given material, resistance is inversely
proportional to the cross-sectional area, meaning the bigger the area, the
lower the resistance. Considering the same given material, resistance is
proportional to length, longer material has higher resistance compared to the
same material with shorter length. The resistance R and conductance G of a
given material of uniform cross-section, therefore, can be computed as:
𝑙
𝑅= 𝜌 (15)
𝐴
𝐴
𝐺= 𝜎 (16)
𝑙
While resistance and conductance are extrinsic properties, both resistivity and
conductivity are intrinsic properties. This means that every material,
irrespective of their shape and size, has their own characteristic resistivity.
For example, all pure copper wires (which have not been subjected to
distortion of their crystalline structure) have the same resistivity, but a long,
thin copper wire has a much larger resistance than a thick, short copper wire.
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14 ABEn 147. Properties of AB Materials
Illustrative Problem 2
Solution
Given:
Length = 10 m
Resistance = 2 ohm
Area = 2 × 10−7 𝑚2
Computation:
𝐴 (2 𝛺) 2 × 10−7 𝑚2
Resistivity, 𝜌=𝑅 =
𝑙 10 𝑚
= 4 × 𝟏𝟎−𝟖 Ω m
1 1
Conductance, 𝐺 = =
𝑅 2
= 0.5 S
𝒍 𝟏 𝟏
Conductivity, 𝝈= = 𝝆 = 𝟒 × 𝟏𝟎−𝟖 𝛀 𝐦
𝑨𝑹
Dielectric Properties
The dielectric properties of biological materials are important in the research
on microwave processing of foods and agricultural materials, and the
destruction of insect pests of postharvest and stored products. Dielectric
properties, among other parameters, are required to provide insight into the
interaction between materials and microwave and radio frequency (RF)
energy during microwave and RF heating. For example, the dielectric
properties of apples are required in modeling microwave and RF heating for
the development of a thermal alternative quarantine treatment against codling
moth.
ε” = ε’ tan δ (17)
The loss tangent, tan δ, provides an indication of how well the material can be
penetrated by an electrical field and how it dissipates electrical energy as
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ABEn 147. Properties of AB Materials
heat. The dielectric constant, loss factor, and loss tangent are dimensionless
quantities.
Illustrative Problem 3
Determine the loss factor of ice (pure distilled water) given that its dielectric
constant at 2450MHz is 3.2 and loss tangent is equal to 0.0009.
Solution:
Given:
ε’ = 3.2
tan δ = 0.0009
Computation:
ε” = ε’ tan δ
ε” = (3.2) (0.0009)
ε” = 0.00288
Illustrative Problem 4
Chicken meat has a dielectric constant of 53.2 and dielectric loss factor of
18.1. Find the loss tangent.
Solution
Given:
ε’ = 53.2; ε” = 18.1
𝛆”
tan δ = 𝛆’
𝟏𝟖.𝟏
= 𝟓𝟑.𝟐
= 0.34
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16 ABEn 147. Properties of AB Materials
The rate of heat generation per unit volume (Q) at a location inside the food
during microwave heating can be characterized by Eq. (18).
Q = 2 f 0 E 2 (18)
where
f = frequency,
0 = dielectric constant of free space (8.854 × 10−12 F/m),
= dielectric loss factor, and
E = electric field.
As microwaves move through the slab at any point, the rate of heat generated
per unit volume decreases. For materials having a high loss factor, the rate of
heat generated decreases rapidly and microwave energy does not penetrate
deeply. A parameter is necessary to indicate the distance that microwaves
will penetrate into the material before it is reduced to a certain fraction of its
initial value.
This parameter is called power penetration depth p , which is defined as the
depth at which power decreases to 1/e or (36.8%) of its original value. It
depends on both dielectric constant and loss factor
of food.
1
0 1 2 1
p
2
(19)
2 2
Dielectric constant and loss factor of various food materials can be seen in
Figures 10 and 11, respectively. As can be seen in the figures, dielectric
properties of cooking oil are very low because of its nonpolar characteristic.
Dielectric properties of water and high-moisture-containing foods such as
fruits, vegetables, and meat are high because of dipolar rotation. The highest
loss factor is observed in the case of salt-containing foods such as ham.
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ABEn 147. Properties of AB Materials
Illustrative Problem 5
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18 ABEn 147. Properties of AB Materials
dielectric loss factor of 18.1. Assume that dielectric properties are constant
during heating.
Solution:
c 3 x 108
0 0.122 m
f 2450 x 106
Using Eq. (4.24):
1
0 1 1
p 2 2
2 2
(4.24)
1
18.1
2 2
p
0.122 1 1 0.00794m
2 253.2 53.2
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ABEn 147. Properties of AB Materials
Electromagnetic Radiation
Electromagnetic radiation encompasses a wide variety of phenomena as
represented by the various regions along its broad spectrum. Only a few
specialized, narrow regions are utilized in food applications which includes
light, infrared, and microwave frequencies. Electromagnetic radiation is
classified by wavelength or frequency. The electromagnetic spectrum
between frequencies of 300 MHz and 300 GHz is represented by
microwaves. Since microwaves are used in radar, navigational equipment,
and communication equipment, their use is regulated by governmental
agencies. In the United States, the Federal communications Commission
(FCC) has set aside two frequencies for industrial, scientific, and medical
(ISM) apparatus in the microwave range, namely 915 ± 13 MHz, and 2450 ±
MHz. Similar frequencies are regulated worldwide through the International
Telecommunication Union (ITU).
𝜆 = 𝑐/𝑓 (20)
Where
λ= wavelength in meters
c = speed of light (3 × 108 m/s)
f = frequency
Illustrative Problem 6
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Solution
𝜆 = 𝑐/𝑓
𝜆 = 𝟎. 𝟏𝟐𝟐 𝒎
Electromagnetic Radiation
As microwaves move through the slab at any point, the rate of heat generated
per unit volume decreases. For materials having a high loss factor, the rate of
heat generated decreases rapidly and microwave energy does not penetrate
deeply. A parameter is necessary to indicate the distance that microwaves
will penetrate into the material before it is reduced to a certain fraction of its
initial value. This parameter is called power penetration depth (δ𝑝 ), which is
defined as the depth at which power decreases to 1/e or (36.8%) of its
original value. It depends on both the dielectric constant and loss factor of
food.
−1
𝜆0 2
𝛿𝑝 = (√1 + (𝜀"/𝜀′)2 − 1) (21)
2𝜋√2𝜀′
Where;
𝛿𝑝 = penetration depth
𝜆0 = wavelength of microwave in free space
𝜀′ = dielectric constant
𝜀" = dielectric loss
Illustrative Problem 7
Solution:
Given:
𝑓 = 2450 MHz; 𝜀′ = 53.2; 𝜀" = 18.1
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ABEn 147. Properties of AB Materials
Required: 𝛿𝑝
𝜆 = 𝑐/𝑓
3 × 108
𝜆= = 𝟎. 𝟏𝟐𝟐 𝒎
2450 × 106
= 0.00794 m
Assessment
References
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AGRICULTURAL AND BIOSYSTEMS ENGINEERING
College of Engineering and Technology