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FLOWSERVE
Flow Control Division
Raleigh, North Carolina

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METHOD SPECIFICATION
MS 8338D
REVISION ~-_,.....;4'­
EFFECTIVE 05119104
SUPERSEDES 3
ORIGINAL DATE -1'""2"""11..,,.51"'03,.....
PAGE 1 of5
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TITLE: SURFACE PREPARATION AND PAINTING FOR CARBO ZINC llSG.
1.0 SCOPE

2.0 EXHIBITS

I. Cleaning and Coating Verification Sheet

11. Paint Certificate of Conformance

3.0 APPLICABLE DOCUMENTS

SSPC-SP1; SSPC-SP10; SSPC-PA2;

ANSI - N-101.2 -.1972; ANSI - N-101.4- 1973

4.0 CERTIFICATION

4.1 Product Identity Certifications from paint supplier are required for all paint, and shall be
supplied to the customer as part of the document package (Exhibit II, Typical).

5.0 CLEANING PRIOR TO BLAST CLEANING

5.1 Requirements

5.1.1 The requirements stated herein shall meet the intent of SPPC-SP1, solvent
cleaning. After cleaning, the surfaces shall be free of detrimental foreign matter
such as oil, grease, soil and other contaminants ..

5.2 Cleaning Procedure

5.2.1 Remove any oil or grease from surface with clean rags soaked in Carboline
Thinner #2 (manufactured by Carboline Co.) or Toluol. Adequate ventilation
should be provided to keep the vapor content in air below flammable
concentration.

5.3 Inspection
5.3.1 After drying, the cleaned surface shall be inspected by Quality Control
personneJ.

6.0 NEAR-WHITE BLAST CLEANING

6.1 Requirements

6.1.1 The requirements stated herein shall meet the intent of SSPC-SP10.

6.2 Cleaning Media

 MS 8338D Rev. 4
Page2 of5

6.2.1 Compressed air used for blasting shall be free of detrimental amounts of oil
and/or water. Adequate separators or traps shall be provided. Air quality shall
be confirmed to be acceptable by blowing the air on a clean white blotter or
cloth for two (2) minutes and checking for contamination visually on the blotter
or cloth.

6.2.2 The largest commercial grade of metal grit permitted by this specification is
SAE No. G-40 abrasive material. The grit shall be clean, dry and oil free.

6.2.3 Contaminated grit shall not be used for finished work.

6.3 Procedure

6.3.1 No blast cleaning shall be allowed when the surface temperature of the item is
within 5 degrees Fahrenheit of the dew point or above 80% relative humidity.
Surface areas exposed to condensation or moisture prior to painting shall be
reblasted. Prior to blast cleaning, record Ambient Conditions for all items on
Exhibit I.

6.3.2 Surfaces are to be grit blasted using compressed air blast nozzles for a
sufficient duration to remove dirt, rust, scale and foreign matter. Surfaces
which are not to be blasted, shall be masked off to avoid being blasted.

6.3.3 The blasting operations shall be done in the blasting chamber. The doors of
the chamber shall be closed during the operation with the ventilation system
on.
6.3.4 Round sharp edges and smooth sharp welds.

6.3.5 All visible burrs, scabs, and weld splatter shall be removed after blast cleaning.

6.3.6 After blast cleaning, the surfaces shall be brushed with clean brushes made of
hair, bristle or fiber, or blown off with clean, oil free, dry air to remove any
traces of blast products from the surface.

6.4 Inspection

6.4.1 After blast cleaning, all surfaces shall be free of grease, dirt, mill scale, rust,
paint or other foreign material. Very light shadows, slight streaks, or slight
discoloration of the cleaned surfaces shall not be considered cause for
rejection. Surface shall be free of all visible residues and the remainder shall
be limited to the light discoloration mentioned above. The profile of the anchor
pattern produced on the surface for all items to be painted shall be 1-3 mils as
determined with a Keane-Tator Surface Profile Comparator manufactured by
KTA Instruments. A minimum of 5 anchor profile readings shall be recorded for
each itell) on Exhibit I.

6.4.2 After acceptance, the surfaces shall be coated per Section 7.0 within four (4)
hours and/or before the surface is exposed to dew point conditions or before
afly rust blooms begin to form. Reblast all surfaces that exceed these
conditions before applying paint.

7.0 PAINTING

7.1 Requirements
 MS 8338D Rev. 4
Page 3 of5

7.1.1 This procedure is intended to meetANSl-N101.2-1972 and ANSI N101.4-

1973.

7.1.2 The coating shall be applied by qualified (certified) personnel. (Carboline

applicator training certificate - nuclear grade coating- TS -120577-1).

7.1.3 The valve shall be coated within four (4) hours or less after being blasted. This
procedure is intended to meetANSl-N101.2-1972 and ANSI N101.4-1973.

7.1.4 Exclusive of the surface condition of the casting, the finish shall be uniform in
color and thickness and free of such imperfections as runs, sags, bare spots,
mud-cracking, air bubbles, and foreign particles.

7.1.5 The coating shall be 3.0 - 6.0 mils dry film thickness

7.2 Paint Materials

7.2.1 Carbo Zinc 11 SG (manufactured by Carboline) color grey.

7.2.2 Carboline Thinner #21 in cool weather (below 60°F, or 16°C) or Carboline
Thinner #26 in warm or windy conditions.

7.3 Painting Procedure

7.3.1 Paint container must be checked to insure paint shelf life requirements are
met.

7.3.2 Size and type of valve shall determine the method of painting to be used.
Spray whenever possible. When spraying is impractical, brushing is
acceptable ifthe desired finish and dry film thickness as stated in Section 7.1.5
is obtained by this method.

7.3.3 No paint shall be applied when the surface or air temperature is below 50
degrees Fahrenheit or above 100 degrees Fahrenheit, when the relative
humidity is above 80%, or when the temperature is within 5 degrees .
Fahrenheit of the dew point or when the surface is wet. It shall be the
responsibility of Quality Control personnel to check these conditions so that the
Carbo Zinc 11 SG is not applied when these conditions are not met. Prior to
painting, record Ambient Conditions for all items on Exhibit I.

7.3.4 Paint that has been stored at low temperature shall be brought up to the
minimum of 60°Fahrenheit before mixing or thinning.

7.3.5 Caution shall be taken to prevent contact of paint with eyes, skin and clothing.
All spraying shall be done inside the spray booth in such a direction that any
over spray is carried away from the painter.

7.3.6 Normal application condition specified below shall be observed.

Paint mixture temperature 60-95°F.

Air/surface temperature 60°F-100°F.
Relative Humidity up to 80%

7.3. 7 Carbo Zinc 11 SG is supplied in two containers as a kit. These materials

should be mixed thoroughly in the following proportions:
 MS 8338D Rev. 4
Page4 of5

Carbo Zinc 11 SG Base 1 gallon

Zinc Filler 14.6-pound unit

Sift zinc filler slowly into base with continuous agitation. Stir until zinc filler is
thoroughly wetted and mixture is free of lumps. Strain the mixture through a
30-mesh screen to remove any lumps. The final color shall be a uniform grey
when the zinc filler is completely mixed in.

Use of additional thinner to lower viscosity after the pot life (8 hours at 75 deg.
F. and less at higher temperatures) shall not be allowed.

7.3.8 To obtain a smooth finish Carbo Zinc 11 SG shall be sprayed on in one coat.

7.3.8.1 For general spraying, it may be necessary to thin each gallon kit with
Y. pint of Carboline Thinner #21 or #26.

7.3.8.2 Hold gun 8-10" from the surface at a right angle to the surface. Use a
50% overlap with each pass of the gun. On irregular surfaces, coat
the edges first making an extra pass later.

7.3.8.3 An agitated pressure pot is necessary in order that zinc filler be

properly dispersed from spraying.

7.3.8.4 If spraying stops for more than 15 minutes, blow material from hose
back into pot.

7.3.9 Prior to handling, the product shall be allowed to dry.

Normal air curing time would be as follows:

Temperature Curing Time Curing Time

(Deg. F.) with over 50% under 50%
R.H. R.H.
40 24 hrs. 35 hrs.
60 16 hrs. 30 hrs.
80 8 hrs. 24 hrs.
100 6 hrs. 12 hrs.

After initial dry time of 1 hour at 75 deg. F, the RH may be raised by applying a
light water spray around the item in order to reduce the cure time.

Adequate cure can be checked by scratching coated surface with a coin. A

cured zinc film will polish and uncured zinc will wrinkle.

7.3.1 O Coating contamination shall be repaired by masking off repair area, reblast per
Section 6.0 and repaint per Section 7.0.

7.3.11 U.nacceptable film thickness shall be corrected by removing coating with a fine
steel wool.

Dry spray and over spray shall be removed by using a fine steel wool.

7.4 Handling after Painting

 MS 8338D Rev. 4
Page 5 of5

7.4.1 All marks and/or blemished areas shall be cleaned with power or hand tools to
the specified profile and cleanliness followed by solvent cleanliness with clean
rags soaked in Carboline Thinner #2 or 10% Caustic Soda Solution. The
cleaned areas shall be touched up by using medium bristle brush if the area is
less than nine (9) square inches in size.

7.5 Inspection

7.5.1 The Quality Control personnel shall inspect the product after painting per
Section 7.0 of this specification. Visual inspection shall be performed to check
the surface condition of the paint and the paint thickness will be checked no
less than five (5) different places with an Inspector Thickness Gauge
(manufactured by Elcometer Co.)or equivalent which is specified in SPPC-
PA2, Measurement of Dry Film Thickness with magnetic gauges. Dry flm
thickness readings for all items shall be recorded on Exhibit I.

7.5.2 No "mud cracking" is allowed.

Prepared by: ~: i:'-0 (B~o >- ~

R. A. Davis, ManufacturlnQng1neering Supervisor
6/18/oy
Date

Approved by: 'l"J!L,.. ,}1.vy }0)< s/;,e/oy

J. P. Tucker, Managi!r, Engineering Dafe

Approved by:
~-A. ~;~surance
-.
di/! /f)Ef
D le I
 ---...
---· Sales Order - Line Item
EXHIBIT 1
FLOWSERVE
MS8338D R/4

CLEANING AND COATING VERIFICATION

PROJECT NAME--------~--- PO/SUBCONTRACT NO.:
----------
VALVE SIZE & FIG. NO.: PS# _ _ _ _ _ _ __ HEAT# _ _ _ _ _ _ _ __

INSTRUCTIONS·: 1. Record all readings, tests, and other data in appropriate boxes on this form for the item, lot or
area identified above. If an appropriate box cannot be found, record data under "Comments".
2. Provide all inspection and test data required by the specification. Mark other boxes "N/A" if ·
the data is not required by the specification.
3. Use a separate Coating Record-Part 2 sheet for each coat applied to the same item, lot or area.

CLEANING RECORD - PART 1

Witness Points Date Time Released Initials Comments
PRE CLEAN
BLAST

MIXING RECORD
Spec'd Material temp. F: > 5 Deg F above Dew Point Pot Life: 8 Hours at 75 F
PRODUCT BATCH MATERIAL MIX
DATE TIME NUMBER NUMBER TEMP. TIME

COATING RECORD - PART 2 I

(Circle One): touch up-r 1st 2nd, 3rd Coat Manufacturer: CARBOLINE
Product/No: CARBOZING 11SG Color: GREY
Date/Time Started: Date/Time Completed :
Witness Points Date Time Released Initials Comments
BEGIN PAINT PROCESS
MIXING
PAINTING

*After initial dry time of 1 hour at 75 deg. F, the RH may be raised by applying a light
water spray around the item in order to reduce the cure time.

SHEET - - - ' - - OF 3

FORM SFA2, T-8, 4A REV. 4 tm

 ~ EXHIBIT1 Sales Order - Line Item
FLOWSERVE
. . . . . . ,= MS8338D R/4

CLEANING AND COATING VERIFICATION

AMBIENT CONDITIONS AT BLAST/SURFACE PREPARATION
Spec'd Air/Surface Temp., F: 50-100F RH,% 80% max Surface Temp. > 5Deg F above DEW pt
Dry/Wet Dew Surf. :;omp. Ai Abrasive Operation MAT'L GAGE
Date Time Bulb Point Temp Test Test Permitted Initials ID IDENTIFICATION

SURFACE PREPARATIONNERIFJGATION OF ANCHOR PROFILE

Substrate : CARBON STEEL Soec'd Surface Preoeration Std: SSPC-SP10 Profile, mils: 1 - 3 mils
Tvpe Abrasive: WHEELABRATOR STEEL Size/Grit: G-40 Inspection instruments : TESTING SIEVE
Profile Instrument : Keane Tator Gauge
MAT'L ID
Date I Time Reading Reading Reading Reading Reading Reading Reading Reading Reading Reading
I Profile Profile Profile Profile Profile Profile Profile Profile Profile Profile

AVERAGE

AMBIENT CONDITIONS AT PAINT PREPARATION

Spec'd Air/Surface Temp., F: 50 - 100F RH,% 80% max Surface Temp. > 5Deg F above DEW pt
Dry/Wet Dew Surf. Comp:.Air Op.eration MAT'L GAGE
Date Time Bulb RH Point Temp. Test Permitted Initials ID IDENTIFICATION
I

FORM SFA2, T-8, 4A REV. 4 Im SHEET 2

---'"----
OF 3
 ~ EXHIBIT 1 Sales Order - Line Item
FLOWSERVE
"'---. MS8338D R/4

CLEANING AND COATING VERIFICATION

Spec'd. Wet Film, mils: N/A Dry Film, mils: 3 - 6 mils Runs, Sags
Inspection Instrument POSITECTOR 6000 .

MATERIAL ID DRY FILM MATERIAL ID DRY FILM

THICKNESS THICKNESS

I AVERAGE AVERAGE

MATERIAL ID DRY FILM MATERIAL ID DRY FILM

THICKNESS THICKNESS

I AVERAGE AVERAGE

MATERIAL ID DRY FILM MATERIAL ID DRY FILM

THICKNESS THICKNESS

AVERAGE AVERAGE

MATERIAL ID DRY FILM MATERIAL ID DRY FILM

THICKNESS THICKNESS

... •.

AVERAGE AVERAGE

MATERIAL ID DRY FILM MATERIAL ID DRY FILM

THICKNESS THICKNESS

AVERAGE I AVERAGE

INSPECTOR: DATE:
-------
FORM SFA2, T-8, 4A REV. 4 Im SHEET 3 OF 3
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 ..
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,

EXHIBIT U
CARBOLINE COMPANY Page : 1 of .3
350 Hanley Industrial Court
St. Louis, MO 63144
(314) 644-1000

03-12-2004
Delivery Address
Energy Steel & Supply .Co Energy Steel & St1pply Co
2715 Paldan St 2715 Paldan St
Aub;u:n Bills, MI Recvq Mon-Fri 80.0-1600 Hrs .\ .·
48326-1827
mr.n Bill•,~~~\t~\.
Project : NUCLEAR \ \
Reference: Carboline Shipment/Release i 701140- 1
Customer Purchase Order i 10884
Subject : Certificate.of Conformance/Nuclear Safety Related
We, Carbolinli! -Company, cert~fy that the following mater~als l\leet the qlfality
control requirements for this product. Also, when used in accordance with
Carboline's printed instructions, the material will perform in accordance with
Carboline's specifications for that product. ·· ·
We further certify that the material was manufactured, tested, and
shipped under a l0CFR50i Appendix B quality assurance program (Carboline
Quality Assurance Manua , Rev 1 dated 09/19/03) and we accept i0CFR21
reporting. Also, the material shipped meets the above referenced purchase order
re~irements and when mixed in accordance wit~ Carboline printed instructions,
it' is wit-h:i.n manufacturing tolerances of the batches originally tested in
accordance with ANSI "NlOl.2, ANSI NlOl.4 ·and ANSI NS.12. .

Quantity Un. Product Description ·

Batch t Quantity Un. Mfg. Date Shelf Life
.-
4. 00 GL 0986S800902D Carboguard 890 White 5800
A: 4B63231 2 01 02-2004 36 Months
B: 4B9487L 2 01 02-2004 15 Months
4.00 . GL · .0986S800902D Carboguard 890 White.5800
A: 4B6323L 2 01 02-2004 36 Months
B: 4B9487L 2 01 02-2004 15 Months
sincerely, .
.;:/IJ a-v~.IYJ; .,I~
. .
----------··
.... •.
.. .
EXHIBIT II Page: 2 of 3

CUSTOMl!R POI: ..;1:::08c:.8""14=--------- "SHIP TO". ~ergy Steel&: Supply Co

-~
ADDIU!SS: 2715 Paldan St '
CARJIOLlNE INVOICE: 701140-1 Au~ HiJls, l\<fi 48326 '
PURCHASER: ...;.-~'"'"'"'=---......,--~
Eru?rgy Steel &: Supply Co

l'ROJECT NAMF.:
---------~

---~
PRODUCT COMPONENT GENERIC TYPE
CARBOGUARD 890 PARTB EPOXY
STANDARD lJATCH Rl!:SULTS
Batch Number N/A 4B9437L
Date o[ Maa.ufacturc N/A Feb'.2004
ShellLl!c 15Jnon1hs May2005 . Exp.Date
Wt. Fer Gallon 13.3 -13.9 lbs. lbs.
VISC<>Sity@75:2"F 1,200-4,.200 cps :2870 CPS
Color- Visual N/A NIA
Color Nlimber N/A 0908

This Baldt Tesi..d by (Initials &: Date): U..., 'Z.-'i- o</

Mixingltatio by Volume: 11'.artComponentAwlPart:C-omponentB

Total Soficls byVollDlle: 75:!:2%. .
l'otlife>·. 3 HOUIS at 75"1' .50% :RH
:F1ash l'oint (lbls Compo11C.t oaly): 7l"F
Tack Free Tune:
&coat Time: 4 HoUIS at 75°F 50% llli
Final DryT1111e: 24 (Mmlmmn) Hours at75"F 5G% ~
Specifkd Carbollne 'lllinncr: 2 (Spray), 33 (Brash and :Roller)
RecommencledDFrpa-Coat: 4-6nUls ...

This product is hereby certified as manufuctared in a.;c0rdalu;e with the Cuboline Quality Assuta11ce Program. When
niliced in accordance with Carl>oline's printed insquqions,_ it is within~ wlerances of !he ba!dles originally
~inaccordaccewithANSIN101.2,ANSIN5.12and.ANSrNl01.4. .

QA/QCSignatnre/Tilie: • • (!;;.,t;~ XJJ,....,_ Date: tl-'1-o'f

~~?:!!*DepartmentSignamre}'f!·%%tm~:tzt~~tttl
 -----------
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-·-·-
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EXHIBIT II Page: 3 of 3

CTJSTOMERl'O#: _1"'0884=~--------
CAlUIOLINEINVOICE: _701:..==.1:::4°"'=1_ _ _ _ __
l'URCHASER: ·Energy Steel &: S!ipply Co

l'ROJECTNAME: - - - - - - - - -

~;!;;;'!,}~
,,...~¢';!}~ ~~~&~~~~~
PRODUCT COMPONENT GENERIC TYPE.
CARBOGUARD 890 PART· A EPOXY :··
STANDARD 'BATCH RESULTS
Batch Number · N/A 4B6323L
Date of Manufacture
Shelf Life
Wt. l'er Gallon (FIMS Ula, 4184)
Viscosity @ 75 :1:2.°F
36months
N/A

Theoretical.± .S Lbs.
1500-7500 cps
__________ ........
Feb2004
...;l'::.;eb=-::200'7=----- Exp. Dale
1L62
4100.
TL

cps
Color- Visual Depends on Color white
Color Number N/A 5800

This Batx:h Tested by {rnllials &: Date): CR

Mixh1g Ratio by Volume: 1 Part Component A to 1 PartComponentB

Total Solids by Volume: 75±2%
l'ot Life: . 3 Homs at 75'1' 50% RH
lilashioint (rhis Component only): 73•p.
"Tacl<FreeT'ime: 3Homsat75'1' 50% RH
ltecoatl]me: . 4HOUISat75'1'-50%RH
Fmal Diy Time: 24 Homs at 75"1' 50% RH
Specified Ca:tPoline Thimtec 2 (Spray), 33 (Brush and Roller)
:S.e«>mmended DFl'per Coat: 4-6mils

. .
nus product is hereby certified as manufactiued. in accordance with the Carboline Quality .Assurance Program. When
· mixed in accordance with Ca:rboline's printed instructions, it 'is within manufactwing' tolerances of the balthes
· orlginally.tested.inaccordaDl:ewithANSJ:NlDl.2;ANSIN5.12andANSINlOL4.

QA/QCS;~titte/Tit1e:· -fl&a-,; ;}?Jk..,.._ Date: J·~S ·O'f ··- _

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