/
; Salt Analysis
“eriment Observation inference Reasoning
4 Preliminary Tests:
Colour is Noted colores Absence of Fe™, Cu”, NF
or co”
Odor of Sait is noted
‘Ammoniacal Smell
Presence of NH«”
‘Soluble in water but does not
| Solubitity give precipitate with Sodium Presence of NHy*
| Carbonate solution
| 1. Yellow 7. Presence of Na
Flametest:Alittle ofsattis >" lag AP Biatslich ot
made into a paste with cone: | 3° pate Green 3. Presence of Ba’ —_| Chlorides are more volatile *
_ | HClin awatch glassandis | 4" Crimson red 4, Presence of Sr*
shown toa ue fame 5._Brick red 5, Presence of Ca”
| ; Evolution ofa colorless gas with Evolved gas is CO,, Lime water
‘te toalittle of | attervescence which when Presence of CO; is Ca(OH), turned to milky due
| passed through lime water to formation of insoluble CaCO,
_ | Ifno effervescence, heat the ~ _
H2S04CH3.Coo _| Vinegarsmell Presence of CHsCOO" Ethanoic acid vapors
| cues”
2." Reddish brown vapors | Maybe Br prec
3._Deep violet vapors 3. Mayber has
Wo change, heat above
mixture end added copper__| 4. , Evolution of Brown Gas ‘4. May be NOs” NO2gas
turnings or paper ballsWO3
~
Confirmatory tests for Anions
Carbonate (CO;")
Toa little of salt solution a
White ppt dissolves in HCl acid
Presence of CO;” is
Ppt is MgCOs, releases CO,
Yew drops of MgSO,solution | with effervescence fgg Kf ) | confirmed upon reaction with HCI
isadded
Chloride(Ch),Bromide(er)
lodide (I) 1 ,
little of the salt soln is 2. Pale yellow ppt sparingly - i
cidfied with iLHNO; anda | solublein excess NHOH | 2° Pr confirmed Pptis AgBr
few drops of silver nitrate 3. Yellow ppt insoluble in . Pptis Agi
(AgNO) soln is added excess NH,OH
‘A little of the salt is heated Gls
en Smee Chromyl chloride vapors (red),
Pass red vapors into NaOH in ves NO dyeliow) with
Yellow PPT Clis confirmed NaOH and forms yellow ppt of
another test tube and add Jendch PbCrO,
acetic acid and lead acetate er ad *
solution
Scanned with CamScanner1. Tolitle ofthe salt
solution, BaCl soln is
added
2 Tothetitle ofthe salt
soln, aceticacid and lead
acctate is added
4, White ppt insoluble in
excess dl, HCL
2, White ppt which dissolves
Inhot ammonium acetate
Presence of SO¢*Is
confirmed
. PPtis BaSOx
2. White pptis PESO,
dissolves due to formation
oflead acetate
‘Test for acetate cH,COO.
afr Title of the salt soln
neutral ferric charie is
added.
2. To Amlof salt soinadd
Aml ethanol and 2 drops
Heat the
11. Brown ppt turning red
2. Pleasant fruity smell
Presence of Acetate is
conflemed
1. Red coloration due to
{formation of ron acetate
2 Due to formation of ester
Nitrate NO”
Ly Afew drops of
2. Pptis Zn(OH), ppt dissolves:
Se eee pacts | wadli son 21 confirmed due to formation of sodium
Is added drop by érop Sate
To sal solution few drops of
potas ferocyanide are | White pot 20" confmed Potis zinc errocyanide
‘Ashtente conducted Green ash 25" confirmed 2n0.C00
Scanned with CamScannera
{Group Vpotisisohedin é
acetic acd and divided into
three portions
Parka: Potassium Chromate’s | vetow ppt Presence of Barium is | parium Chromate Is ppt
ated (pa) confirmed
Warum pes White ppt Presence of Barium is Baum Sulphate
Para oapessttsadtes, [WABCO |. =. | Ee eae
Flame testis conducted Gn
T?earium is Absent rashes sto PptissS04
Part 2: (NH) SO, tended (5) WHE PPE confirmed
Presence of Strontium
Fametestisconducted | Crimson red fame confirmed
oath Batam and Sonia
sre absent: Presence of CGMS pprscaliumorate |
art 3: Ammonium Oxalate is_| Wht PPt ‘confiemed
added (Coe)
resence of Clcumis
Flame testiseonducted | Brickred fame isateoal
‘Sop cation EY sence of Magnesium
Tothe salt sole, add NHC, | whit crystline ppt Presence of eens | pptistglPOd
!tioH and Sodium phosphate
[eae mat be secti rte prompt: resence oTwaI | pnisnagok
Bh “OY Pink Achy. | isconfirmed Aghietae 209)
testis cnducted
G Or mmo aegen phaphel> Sheen,
t
Ante nif —> Nal > Nesler ss.
ee denficabion Con Sema £ GPO 4 NAB —9 Neha
4: C05” —y a Hel >. way wb 2. gps Pb ade cl BE,
gp, Cela
| 2: Cig-ceb > il.sey __ Neutral Pec,
|B CL com-YS0, > Agi r ung, 4: gpl athe Ash tes
a “am ay? a ir Eat nites
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Scanned with CamScanner