Kelompok-4-Astm F-88-94-Standard Test Method For Seal Strength

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D signation: F 88 - 94

Standard Test Method for


Seal Strength of Flexible Barrier Materials1
This standvd is issued under the fixed designation F 88; the number immediately following the designation indicates the year of
original adoption or, in the case of revision. the year of last revision. A number in parentheses indicates the year of last rcapproval.A
superscript epsilon (,) indicates an editorial change since the last revision or reapproval.

1, Scope
ments of 5.6 of Test Methods D 882 with app'ropriate
1.1 This test method covers the measurement of the seal gripping system to minimize slippage and uneven stress
strength of flexible barrier materials. distribution.
J .2 The techniques and equipment used to form these 4.2 Specimen Cutter, conforming to the requirements of
seals are not covered. . . 5.4 of Test Methods D 882. Generally, samples of 25.4-mm
t .3 This test method does not measure seam continuity or {I-in.) width are used.
any other seam properties beyond the force required to tear
apart a seal of standard width.
J .4 This standard does not purport to address all of the 5. Sampling
safety concerns, 1/ any, associated with its use.· It is the 5.1 The number of test specimens shall be chosen to
responsibility of whoever uses this standard to consult and permit an adequate determination of representative perfor
establish appropriate safety and health practices and deter- mance. Practice D 1898 provides guidance to test specimen
''? the applicabilit;; of regulatory limitations prior to 11se. selection.
'oTE-A former edition of this test method covered a Static Load 5.2 Testing of specimens with visual defects or other
Test 'as an alternative to the Dynamic Load Test covered herein. Since deviations from normality may or may not be appropriate
the property measured by static load may not be the same as dynamic depending on the purpose of the investigation. Indiscrimi nate
load, it is inappropriate to include both in the same test method. elimination of defects can bias results.
2. Referenced Documents
2.1 ASTM Star.c:ards: 6. Conditioning
D 685 Practice for Conditioning Paper and Paper Products 6.1 Condition heat-sealed or adhesive-sealed test speci
for Testing2 mens in accordance with Method D 685. In_place of other
D882 Test Methods for Tensile Properties of Thin Plastic requirements, use 23 ± 2-C (73.4 ± 3.6°F) and 50 ± 5 %
Sbeeting3 relative humidity as the standard conditioning atmosphere.
D 1898 Practice for Sampling of Plastics3 A minimum conditioni'ng time of 40 h is recommended for
E 691 Practice for Conducting an Interlaboratory Study most materials. Some materials may require longer condi
to Determine the Precision of a Test Method5 tioning times and judgement should be exe·rcised as to the
selection of sufTtcienr conditioning time.
J. Significance and Use 6.2 Modification of conditioning practices may be neces
3.1 The force required to pull open a seam is of obvious sary to meet spec1lic test objectives, such as the measurement
relevance to the integrity of a package. At times it is desirable of seal strength at specified storage or handling temperature.
to control the seal strength of packages to facilitate opening..
(t 3.2 A significant ponion of the force measured when·
r: ] materials may actually be a bending component and 7. Procedure
Cl.i, strictly seal·strength alone. A number of fixtures and 7. I Calibrate the tensile testing machine in accordance
"hemes have been devised to hold samples at various angle·s with the manufacturer's recommendations.
ld the pull direction in order to control this bending force. 7.2 Prepare sealed test specimens for testing by cutting to
The design and applicability of these techniques is beyond dimensions shown in; Fig. I. Edges shall be clean-cut and
the scope of this test method. perpendicular to the direction of seal.
7.3 Clamp each leg of the test specimen -in-the tensile
-i. Apparatus testing machine. The ·sealed area of the specimen shall be
4.1 Tensile T;sting Machine, conforming to the require- approximately equidistant between the clamps. A distance

1
" between clamps of25 to 50 mm (I to 2 in.) is recommended,
but under most circumstances is not critical. Align the
_ ·Tois test method is under the jurisdiction of ASTM Committee F-2 on specimen in the clamps so that the seal line is perpendicular
to the direction of pull, allowing sufficient slack so that the
' \ibie Barrier Materials and is the direct responsibilit)' of Subcomm1t1ce F02.J0
"' T ctt Methods. seal is not stressed prior to the initiation of the t st. The rate
Current edition approved Nov. t5; 1994. Published January 1995. Originally of loadine. shall bl! between 250 and 300 mm/min (10 to 12
lubed as F 88 - 68. Last pmious edition F 88 - 85 ( 1994).
:-◄n,11,a/ Book of ASTM Standurds, Vol 15.09. in./min). . . - .
',◄nnua/ Book of ASTM Standards, Vol 08.0 I. 7.4 It mav be appropriate to hold the fin seal tail
• -◄nnua/ Book of ASTM Standuids, Vol 14.02. perpendicula ly to the direction of pull as the specimen is

893

'

L
ITT}, F 88

--, _l

7
X
X

l
.
zM

J
M

'•-;;-; J
I
lllNj l}IN
FIN SEAL
11ilN HOT WIRE SEAL

(Rec ended)
Hinimun
11'-

LI !I I-
L31N J J. X JIN I
Non-Seal dimension marked X Is left undefined to allow inclusion ol various machines and various laboratory sealers.
·FIG. 1 Recommended Sample Dimensions

It . :/ .essed. Alternately the tail can be allowed to hang freely. A 8.1.6 Type of failure (that is, delamination, peel, film
significant differencc in results has been shown to be
dependent on how the tail is oriented and, therefore, the final break).
f , report should cover which method was used. 8.1.7 Number of specimens tested and method of sam
pling.
7.5 Generally, only the maximum force required to tear
8.1.8 Any other pertinent information that may affect tes!
apart the seal is reported. This valve can be read directly
results.
from the chart recorder.
8.1.9 Maximum force required to cause seal failure for
7.6 Additionally, determination of percent elongation,
force tension relationship, and energy to cause separation each test specimen (expressed in pound-force per inch of
width or newtons/metre).
may be appropriate.
8.1.10 Any statistical calculations deemed appropriatt_
(most commonly mean, range, and standard deviation).
8. Report 8.1.11 Other data including percent elongation, for<::.
8.1 Report the following information: extension curves, and integration values. if such data JS
8.1 :I Complete identification of materials being tested. relevant to the specific test purpose.
8.1.2 Test method and equipment used to fonn seals,
including seal width. Equipment used to test seals. . 9. Precision and Bias
8.1.;3 Test conditions-, such as temperature and humidity.
9.1 Three different materials (sampled at various IOC2"
8.1.4 Any and all deviations from standard such as jaw tions across their seals) were tested by six laboratories. Pouch
separation rate and jaw separation distance. samples were taken from large production runs in order to
8.1.5 · Method of holding tail and any special fixtures
ensure minimal sample to sample variation, selected ran
used to hofd test specimens.
domly, cut into one-inch strips by a siQgle laboratory in
4@, F 88
o'eli? d locations within the seal, and distributed to the
c1pants. TABLE 1 Summary of lnterlaboratory Test Results
Repeatability
9.2 Twenty replicates of each material/position were Average
Deviation
Standard Within Repro-
Material Position Between
rested by each laboratory and analyzed in accordance with Strength
Laboratories,
Laboratories, dudbility,

practice E 691. Results are shown in Table I, expressed in S,.b


s, SR

grams-force per inch of seal width. Metallized A 639 49 58 76


9.3 A review of the above data shows the coefficient of Metallized B 648 42 67 79
Paper/LOPE A 1498 179 184 257
variation is consistent among materials and positions tested Clear film A 6460 316 422 527
with values as follows: Clear film B 6486 468 381 604
Coefficient of Variation &sis Average Value,%
Clear film C 6501 403 446 601
Repcai.abiiity 8.S
Reproducibility 11.3

The American Society for Testing and Materials takes no position respecting the va/idiry of any patent rights asserted in connection
with any item mentioned In this standard. Users of this standard are exp,essly advised that determination of the validity of any such
patent rights, and the risk of Infringement of such rights, are entirely their own responsibility.

This standard Is subject to revision at any time by the responsible technical committee end must be reviewed every live years and
If not revised, either reapp,oved or withdrawn. Your comments are invited either for revision of this standard or for additional standards
and should be addressed to ASTM Headquarters. Your comments will receive careful consideration at a meeting of the responsible
technical committ1111, which you may attend. II you feel that your comments have not received a lair hearing you should make your
views known to the ASTM Committee on Standards, 1916 Race St., Philadelphie, PA 19103.

895

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