Method: DLXL-Cal Page 1 Date: 23/10/2019 16:42:10

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Reprocessing Begun
Logged In Analyst: Administrator Technique: ICP Continuous

Results Data Set (original): IDL XL

Results Library (original): C:\Users\Public\PerkinElmer Syngistix\ICP\SystemFiles\Service\
8000 Cyclone\Results.mdb
Results Data Set (reprocessed):
Results Library (reprocessed):

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Sequence No.: 1 Autosampler Location:
Sample ID: IDL-XL (2% HNO3) Date Collected: 23/10/2019 16:36:47
Analyst: Data Type: Reprocessed on 23/10/2019 16:40:38
Logged In Analyst (Original) : Administrator
Initial Sample Wt: Initial Sample Vol:
Dilution: 3X Sample Prep Vol:
Wash Time (before sample):

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Nebulizer Parameters: IDL-XL (2% HNO3)
Analyte Back Pressure Flow
All 97.0 kPa 0.65 L/min

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Mean Data: IDL-XL (2% HNO3)
Mean Corrected Calib
Analyte Intensity Std.Dev. RSD Conc. Units
As 193.696 440.8 52.21 11.85% [0.00] µg/L
Se 196.026 501.9 18.65 3.72% [0.00] µg/L
Tl 190.801 116.1 13.41 11.55% [0.00] µg/L
Pb 220.353 26885.1 193.57 0.72% [0.00] µg/L

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Sequence No.: 1 Autosampler Location:
Sample ID: DL-Standard Date Collected: 23/10/2019 16:23:50
Analyst: Data Type: Reprocessed on 23/10/2019 16:40:46
Logged In Analyst (Original) : Administrator
Initial Sample Wt: Initial Sample Vol:
Dilution: Sample Prep Vol:
Wash Time (before sample):

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Nebulizer Parameters: DL-Standard
Analyte Back Pressure Flow
All 97.0 kPa 0.65 L/min

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Mean Data: DL-Standard
Mean Corrected Calib
Analyte Intensity Std.Dev. RSD Conc. Units
As 193.696 10005.4 127.64 1.28% [1000] µg/L
Se 196.026 7175.4 43.78 0.61% [500] µg/L
Tl 190.801 20232.5 403.49 1.99% [1000] µg/L
Pb 220.353 29768.6 651.51 2.19% [500] µg/L

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Calibration Summary

Analyte Stds. Equation Intercept Slope Curvature Corr. Coef. Reslope

As 193.696 1 Lin, Calc Int 0.0 10.01 0.00000 1.000000
Se 196.026 1 Lin, Calc Int -0.0 14.35 0.00000 1.000000
Tl 190.801 1 Lin, Calc Int 0.0 20.23 0.00000 1.000000
Pb 220.353 1 Lin, Calc Int 0.0 59.54 0.00000 1.000000

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Sequence No.: 1 Autosampler Location:
Sample ID: IDL-XL (2% HNO3) Date Collected: 23/10/2019 16:36:47
Analyst: Data Type: Reprocessed on 23/10/2019 16:41:00
Logged In Analyst (Original) : Administrator
Initial Sample Wt: Initial Sample Vol:
Dilution: 3X Sample Prep Vol:
Wash Time (before sample):
Method: DLXL-Cal Page 2 Date: 23/10/2019 16:42:10

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Nebulizer Parameters: IDL-XL (2% HNO3)
Analyte Back Pressure Flow
All 97.0 kPa 0.65 L/min

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Mean Data: IDL-XL (2% HNO3)
Mean Corrected Calib. Sample
Analyte Intensity Conc. Units Std.Dev. Conc. Units Std.Dev. RSD
As 193.696 0.0 0 µg/L 5.22 0 µg/L 15.66 0.00%
Se 196.026 0.0 0 µg/L 1.30 0 µg/L 3.90 >999.9%
Tl 190.801 0.0 0 µg/L 0.66 0 µg/L 1.99 >999.9%
Pb 220.353 -0.0 -0 µg/L 3.25 -0 µg/L 9.75 >999.9%

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Sequence No.: 1 Autosampler Location:
Sample ID: IDL-XL (2% HNO3) Date Collected: 23/10/2019 16:31:24
Analyst: Data Type: Reprocessed on 23/10/2019 16:41:31
Logged In Analyst (Original) : Administrator
Initial Sample Wt: Initial Sample Vol:
Dilution: 3X Sample Prep Vol:
Wash Time (before sample):

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Nebulizer Parameters: IDL-XL (2% HNO3)
Analyte Back Pressure Flow
All 97.0 kPa 0.65 L/min

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Mean Data: IDL-XL (2% HNO3)
Mean Corrected Calib. Sample
Analyte Intensity Conc. Units Std.Dev. Conc. Units Std.Dev. RSD
As 193.696 23.0 2 µg/L 1.16 7 µg/L 3.48 50.44%
Se 196.026 -0.5 -0 µg/L 2.49 -0 µg/L 7.47 >999.9%
Tl 190.801 42.6 2 µg/L 0.32 6 µg/L 0.95 15.03%
Pb 220.353 1844.7 30 µg/L 4.09 90 µg/L 2.28 13.21%