This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles

for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Designation: D4262 − 05 (Reapproved 2018)

Standard Test Method for

pH of Chemically Cleaned or Etched Concrete Surfaces1
This standard is issued under the fixed designation D4262; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.

1. Scope test method to determine that residual chemicals have been

1.1 This test method covers procedures for determining the removed by measuring the acidity or alkalinity of the final
acidity or alkalinity of concrete surfaces prepared by chemical rinsed surface.
cleaning or etching prior to coating. 4. Apparatus
1.2 This standard does not purport to address all of the 4.1 The specific apparatus for each test is described in
safety concerns, if any, associated with its use. It is the Annex A1 – Annex A3.
responsibility of the user of this standard to establish appro-
priate safety, health, and environmental practices and deter-
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5. Materials
mine the applicability of regulatory limitations prior to use.
5.1 Potable Water, for rinsing chemically cleaned or etched
1.3 This international standard was developed in accor-
concrete surfaces.
dance with internationally recognized principles on standard-
ization established in the Decision on Principles for the 5.2 Wet Concrete Surface, following the final water rinse
Development of International Standards, Guides and Recom- and before the rinse water has completely drained off the
mendations issued by the World Trade Organization Technical surface.
Barriers to Trade (TBT) Committee.
6. Procedure
2. Terminology 6.1 The preparatory actions for each alternative are de-
2.1 Definitions: scribed in Annex A1 – Annex A3.
2.1.1 pH, n—a measure of acidity or alkalinity of a solution 6.2 At least two surface pH readings shall be taken for each
or surface, with neutrality represented by a value of 7, with 500 square feet or portion thereof. Readings shall be taken at
increasing acidity represented by smaller values, and with randomly selected locations immediately following the final
increasing alkalinity represented by increasing values. rinse and before all the rinse water has drained off the surface.
3. Significance and Use 6.3 The pH of the water used for rinsing shall be determined
to establish acceptance criteria. Readings shall be taken at the
3.1 Chemical cleaning and etching is used to prepare beginning and end of the final rinse.
concrete for coating.
6.4 Unless otherwise specified, tests shall be conducted in
3.2 Residual chemicals not removed by water rinsing may accordance with this procedure.
adversely affect the performance and adhesion of coatings
applied over prepared concrete surfaces. It is the intent of this 7. Acceptance Criteria
7.1 The pH readings following the final rinse shall not be
1
This test method is under the jurisdiction of ASTM Committee D33 on more than 1.0 pH lower or 2.0 higher than the pH of the rinse
Protective Coating and Lining Work for Power Generation Facilities and is the direct water unless otherwise specified.
responsibility of Subcommittee D33.05 on Application and Surface Preparation.
Current edition approved Aug. 1, 2018. Published August 2018. Originally 8. Keywords
approved in 1983. Last previous edition approved in 2012 as D4262 – 05 (2012).
DOI: 10.1520/D4262-05R18. 8.1 etched concrete surface; pH

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 D4262 − 05 (2018)
ANNEXES

(Mandatory Information)

A1. pH TEST PAPER, TYPE 1

A1.1 Apparatus A1.2 Procedure

A1.1.1 pH Test Paper, with a minimum range of 1 to 11 pH A1.2.1 Tear off a strip of test paper, wet with test water and
units with a capability of measuring in increments of 0.5 pH after the color develops, compare with color chart to determine
units. pH.

A2. pHYDRION INSTA-CHECK pH PENCIL

A2.1 Apparatus A2.2.2 Moisten the surface with distilled water.

A2.1.1 pH Pencil, a marking instrument capable of measur- A2.2.3 Mark over the scratch with pHydiron pencil.2
ing the surface pH from 0 to 13. A2.2.4 After 15 s, compare the color with the color com-
A2.1.2 Color Comparison Chart. parison chart.

A2.2 Procedure A2.2.5 The color produced is stable for several days.

A2.2.1 Scratch the surface of the concrete with a metallic 2

The pHydrion pencil is available from Micro Essential Laboratories, Inc., 4224
object. Avenue H, Brooklyn, NY 11210.
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A3. pH METER3

A3.1 Apparatus A3.2 Procedure

A3.1.1 Flat Electrode pH Pen, with a minimum range from A3.2.1 Place the tip of the electrode into the test water. The
0 pH to 14 pH units with the capability of measuring in pH reading will appear in the display.
increments of 0.01 pH units.

3
The Model PH100 and PH110 pH meter is available from ExTech Instruments,
285 Bear Hill Road, Waltham, MA 02451–1064.

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