Mz-000-Ccx-Mc-Spc-00004-Ext. Coating For Buried Pipeline and Piping Components - Fbe and FJC Rev0

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External Coating for Buried Pipeline and Piping

Components - FBE and FJC

MOZAMBIQUE LNG – 6.44 MTPA

0 20-JAN-2020 Issue for Design M. Turetta P. Khoei C. Borghesan

A 09-DEC-2019 Issued for Review and Acceptance M. Turetta P. Khoei C. Borghesan

Revision Date Description Prepared by: Reviewed by: Approved by:

Security COMPANY USE Total number of Pages (including Cover sheet): 18

For Contract No. Contractor Document No. Contractor Rev.


Contractor
Documents LNG19-00079 000-KA-E-093004 0

Company Project System Originator Discipline Doc. Type Sequence Language Revision
Document
No. MZ 000 CCX MC SPC 00004 - 0

This document is Work Product under the Agreement between ANADARKO


MOÇAMBIQUE AREA 1, LIMITADA (“COMPANY”) and CCS JV S.c.a.r.l. (“CONTRACTOR”).
All rights, title and interest in this Work Product, including any and all copyrights therein,
are owned by COMPANY, except as reserved under the Agreement.
Uncontrolled if Printed
Mozambique LNG – 6.44 MTPA
External Coating for Buried Pipeline and Piping
Components - FBE and FJC
Document No. MZ-000-CCX-MC-SPC-00004
Rev. 0 Rev Date: 20-JAN-2020

REVISION MODIFICATION LOG

Page No. Section Description of Changes

Update of Purpose and Scope of the document to expand on intended


4 1.2 / 1.3 use and Field Joint Coatings (FJC).
5/6 2.1 Addition of ISO standards noted in the specification.
6/7/8 3.0 Sectioning and sub-sectioning terms improved
3.1.3 / Applicator’s documentation encloses now the Cure time, Tg, Moisture
7 4.2 Size. Inspection of Prepared surfaces added.
Coating Process description Added. Reference to Inspection
8 4.3 / 5 requirements set in APPENDIX 2 added for consistency.
Repetition in the requirement removed, Repair procedure submittal
9 6.0 added.
10 7.2 Rewording of the subsection title
APP 2 Updated the sequencing and addition of bullets to cover In-line inspection
16 Tab.4 and measurement of Finish, Cleanliness, Travel Speed.

HOLD LOG

HOLD No. Description of Holds

INPUTS / REFERENCE DOCUMENTS

Document Number Title Status

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Mozambique LNG – 6.44 MTPA
External Coating for Buried Pipeline and Piping
Components - FBE and FJC
Document No. MZ-000-CCX-MC-SPC-00004
Rev. 0 Rev Date: 20-JAN-2020

TABLE OF CONTENTS
1.0 INTRODUCTION .................................................................................................................4
1.1 Project Description ...........................................................................................................4
1.2 Document Purpose ...........................................................................................................4
1.3 Document Scope ..............................................................................................................4
1.4 Acronyms, Abbreviations and Definitions.......................................................................... 4
2.0 REFERENCES ....................................................................................................................5
2.1 Codes and Standards ....................................................................................................... 5
3.0 MATERIALS ........................................................................................................................6
3.1 Coating .............................................................................................................................6
3.1.1 Approved Coatings .................................................................................................... 6
3.1.2 Storage of Powder Coating........................................................................................ 6
3.1.3 Batch Information and Segregation ........................................................................... 6
4.0 APPLICATION.....................................................................................................................7
4.1 General ............................................................................................................................7
4.2 Surface Preparation.......................................................................................................... 7
4.3 Application ........................................................................................................................8
5.0 INSPECTION .......................................................................................................................8
6.0 COATING REPAIR ..............................................................................................................8
7.0 FIELD JOINT COATINGS ................................................................................................... 9
7.1 Surface Preparation.......................................................................................................... 9
7.2 Liquid Epoxy Coating...................................................................................................... 10
8.0 STORAGE AND HANDLING ............................................................................................. 11
9.0 MARKING.......................................................................................................................... 11
10.0 SUBMITTALS .................................................................................................................... 11
11.0 APPENDICES.................................................................................................................... 12
APPENDIX 1 COATING MATERIALS QUALIFICATION .......................................................... 13
APPENDIX 2 PRODUCTION TESTING REQUIREMENTS ....................................................... 15

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Mozambique LNG – 6.44 MTPA
External Coating for Buried Pipeline and Piping
Components - FBE and FJC
Document No. MZ-000-CCX-MC-SPC-00004
Rev. 0 Rev Date: 20-JAN-2020

1.0 INTRODUCTION

1.1 Project Description


Mozambique LNG is a two-train, nominal 6.44 MTPA per train, LNG facility using APCI
liquefaction technology. Hydrocarbon condensate, separated from the feed is processed
and exported separately.

The facility will be constructed at a remote coastal location in the Cabo Delgado province of
Mozambique.

The feed stream is fed to the LNG plant which comprises gas/liquid separation, gas
treatment (removal of acid gas, dehydration and mercury), heavy component (C5+)
removal followed by gas liquefaction, storage and export. Condensate stabilization and
export facilities are also included.

Phase 1a of the project consists of the first two (2) LNG trains and relevant utilities.

1.2 Document Purpose


The purpose of this specification is to provide the minimum requirements for coating
underground piping and pipelines for External corrosion protection using Fusion Bonded
Epoxy (FBE). FBE is intended to provide corrosion protection, preventing it when used in
conjunction with cathodic protection.

1.3 Document Scope


This specification describes the requirements for surface preparation and the application
and inspection of shop-applied and field-applied protective coatings on pipe, fittings,
flanges, field joints, valves, and special fabrications made of carbon steel intended for
underground service.
This specification applies to shop fabricated items, purchased items and to field joint
coatings (FJC).

1.4 Acronyms, Abbreviations and Definitions


The following acronyms, abbreviations and definitions apply to this document:

TERM DEFINITION

COMPANY Anadarko Moçambique Area 1 Limitada

CCS JV Chiyoda, CB&I and Saipem Joint Venture


LNG Liquefied Natural Gas
Imperfection consisting of cracked, missing, or insufficient
coating thickness, and/or a foreign inclusion in the coating
Holiday
that significantly lowers the dielectric strength on a
surface that has been coated
Party who owns the facility wherein the coating system
Owner will be used, for the scope of the project this is referred to
COMPANY

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Mozambique LNG – 6.44 MTPA
External Coating for Buried Pipeline and Piping
Components - FBE and FJC
Document No. MZ-000-CCX-MC-SPC-00004
Rev. 0 Rev Date: 20-JAN-2020

TERM DEFINITION
Party who awards the contract to the supplier. The
purchaser may be the owner or the owner’s authorized
Purchaser
agent. For the scope of the project this is referred to CCS
JV
Purchaser’s authorized representative with authority to
Purchaser’s Inspector act in the interest of, and on behalf of, the purchaser in all
quality assurance matters
Party responsible for furnishing and/or installing the
Applicator
coating

2.0 REFERENCES
Use the latest edition of codes available at the release of the Purchase Order unless otherwise
specified.
The order of precedence of the document is Local Laws and regulations, This Technical
Specification, the Standards referenced into this specification.

2.1 Codes and Standards


ASTM - American Society for Testing and Materials
ASTM D4417 Standard Test Methods for Field Measurement of Surface
Profile of Blast Cleaned Steel
AWWA - American Water Works Association
AWWA C203 Coal Tar Protective Coatings & Linings for Steel Water
Pipelines, Enamel & Tape, Hot Applied
AWWA C213 Fusion-Bonded Epoxy Coating for the Interior and Exterior
of Steel Water Pipelines
NACE - National Association of Corrosion Engineers
NACE SP0394 Application, Performance, and Quality Control of Plant-
(formerly RP0394) Applied, Fusion-Bonded Epoxy External Pipe Coating
NACE SP0490 Holiday Detection of Fusion-Bonded Epoxy External
(formerly RP0490) Pipelines Coatings of 250 to 760 μm (10 to 30 mils)
SSPC - The Society for Protective Coatings
SSPC-PA2 Measurement of Dry Coating Thickness with Magnetic
Gages
SSPC-SP-10 Near White Metal Blast Cleaning
SSPC-VIS-1 Guide and Reference Photographs for Steel Surfaces
Prepared by Dry Abrasive Blast Cleaning
ISO - International Organization for Standardization
ISO 8501-1 Preparation of steel substrates before application of paints
and related products — Visual assessment of surface
cleanliness — Part 1: Rust grades and preparation grades
of uncoated steel substrates and of steel substrates after
overall removal of previous coatings

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Mozambique LNG – 6.44 MTPA
External Coating for Buried Pipeline and Piping
Components - FBE and FJC
Document No. MZ-000-CCX-MC-SPC-00004
Rev. 0 Rev Date: 20-JAN-2020

ISO 8502-6 Preparation of steel substrates before application of paints


and related products — Tests for the assessment of surface
cleanliness — Part 6: Extraction of soluble contaminants for
analysis — The Bresle method
ISO 8503-5 Preparation of steel substrates before application of paints
and related products — Tests for the assessment of surface
cleanliness — Part 5: Measurement of chloride on steel
surfaces prepared for painting (ion detection tube method)

3.0 FUSION BONDED EXTERNAL COATING

3.1 FBE Coating

3.1.1 Approved Coatings


Shop applied external coating material shall be one of the following fusion bond epoxy
powders:
• 3M Scotchkote 6233
• NAPGARD 7-2503
• Or Company Approved Equal,
details of Material Qualification per NACE SP 0394 are given in APPENDIX 1.
Coatings will be subject to a design Temperature envelope of -29°C to +70°C.

3.1.2 Storage of Powder Coating


Powder shall not be used for pipe coating if it or the powder containers (boxes or bags) have
been allowed to become wet, damaged, or if the powder has been stored beyond
manufacturer’s recommended self-life or beyond the manufacturer’s recommended
maximum storage temperature.
Coating material shall be delivered in the manufacturer’s unopened, original container.
Coating material shall be handled and stored in accordance with the manufacturer’s latest
published instruction and shall be protected from damage, moisture, direct sunlight, and
temperature below 4.5°C (40°F) and above 39°C (100°F).
Thinners, solvents, and cleaners shall be as recommended by the coating manufacturer and
shall be identified by product number and/or generic formulation.

3.1.3 Batch Information and Segregation


Each container of powdered coating materials used by the Applicator shall be marked with
the following information:
• The manufacturer’s name
• The material identification number
• The batch number
• Date of manufacture
• Shelf life and storage temperature limits
The fusion bond epoxy manufacturer shall supply the information listed below to the
Applicator for each batch of powder. Standards for comparison shall also be provided for

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Mozambique LNG – 6.44 MTPA
External Coating for Buried Pipeline and Piping
Components - FBE and FJC
Document No. MZ-000-CCX-MC-SPC-00004
Rev. 0 Rev Date: 20-JAN-2020

each item. This information will be used to check that no changes have been made in the
epoxy formulation. The Applicator shall maintain these document and they shall be available
for review or duplication by the Purchaser’s representative.
• Infrared scan of powder and typical powder scan for comparison.
• Gel time at recommended application temperature.
• Particle size distribution.
• Cure Time.
• Glass Transition Temperature (first heating, second heating, enthalpy).
• Moisture Content.
Coating powder shall be segregated by batch number during shipment, storage, and
handling. Batches shall be used consecutively during coating application and shall not be
mixed except when necessary to keep the coating process continuous.

4.0 APPLICATION

4.1 General
The fusion bond epoxy shall be applied in accordance with the coating manufacturer’s
application official procedures. The Applicator must have a copy of these procedures at the
site where the coating is being applied. Any deviation from the coating manufacturer’s
application procedures shall be submitted to the Purchaser for approval.
It shall be the Applicator’s responsibility to stop the coating process at any time when
condition may exist that might adversely affect the coating quality. The Purchaser’s
representative may reject any product not proven by the Applicator to be in compliance with
this Specification.
Proper equipment for the handling, unloading, and temporary storage of bare pipe shall be
used to avoid any damage to bare pipe and pipe ends. The Applicator shall also take special
care to avoid damage to any internal coating during all phase of the external coating process.
The finish coating shall have a cutback at each end to the pipe. Unless otherwise specified,
the length of the cutback shall be 75 mm (3 inches) minimum, measured from the exterior
shoulder of the bevel at the end of the pipe. On pipes requiring PWHT/Pre-heating and/or
post-heating minimum cutback length is 150mm.

4.2 Surface Preparation


All oil base paints, mill lacquer, oil coatings, heavy rust scale, weld splatter, burrs, soil
deposits, dirt, loose rust and mill scale, oil, grease, moisture, dust and foreign matter shall
be removed.
Pipe shall be preheated following surface preparation by passing through gas impinging
heaters to burn off any remaining oil, grease, etc. and dry off all moisture and increase the
temperature of the pipe sufficiently to prevent sweating of the pipe between cleaning and
coating.
All surfaces to be coated shall be blast cleaned in accordance with SSPC SP-10 Near White
Blast Cleaning. The abrasive shall produce an average surface profile of 65 µm (2.5 mils).
All blast-cleaned surfaces shall be inspected for proper cleaning before painting. After
abrasive blast cleaning, all dust and traces of abrasives shall be removed from the pipe
surface by brushing, compressed air or vacuum cleaning. Each pipe shall be inspected for

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Mozambique LNG – 6.44 MTPA
External Coating for Buried Pipeline and Piping
Components - FBE and FJC
Document No. MZ-000-CCX-MC-SPC-00004
Rev. 0 Rev Date: 20-JAN-2020

surface cleanliness. SSPC VIS-1 (ISO 8501-1 to be confirmed by purchaser) shall be used
as a visual standard for confirming the degree of surface cleanliness.
Anchor profile shall be verified in accordance with ASTM D4417, Method C. Anchor profile
may also be verified in accordance with ISO 8503-5, when approved by purchaser.

4.3 Application
The time between blast cleaning and the coating operations shall be kept to a maximum of
four hours to avoid formation of oxides on the cleaned surface. Visible formation of such
oxides shall require re-blasting of pipe surface.
The pipes shall be coated on a continuous coating line without any risk of deterioration during
the various heating, powder spraying, curing and quenching operations.
The pipe shall be uniformly preheated to a temperature specified by the coating
manufacturer. The preheat temperature shall not exceed 246°C (475°F). Optical pyrometers
shall be used to measure preheat temperature. A procedure for calibrating pyrometers on a
minimum twice-daily basis shall be followed. As an alternate, preheat temperature may be
checked with temperature sticks providing care is exercised not to contaminate any surface
to be coated with deposits left by the melt stick. Care shall be taken during the preheating
operation to prevent any contamination of the cleaned pipe surface.
Following preheating, the fusion bond coating shall be applied to the pipe by electrostatic
spray or fluidized bed to provide uniform cured film thickness of 300 µm to 350 µm (12 to 14
mils).
The coating may be water cooled provided that the minimum curing time schedule has been
met. Cooling shall be accomplished in graduated stages, using water jets operating at
carefully controlled flow and temperatures, according to the manufacturer’s
recommendation.

5.0 INSPECTION
Each length of coated pipe shall be checked with an approved holiday detector and shall be
subject for approval by Purchaser’s Inspection. Holiday detection voltage shall be set at an
appropriate voltage. The coating shall be 100 percent holiday-free. The detector shall travel
at a rate not to exceed 1 ft. per second, nor shall it be allowed to remain stationary while the
power is on. Holiday detection test shall be in accordance with NACE SP0490-2007, Holiday
Detection of Fusion Bonded Epoxy External Pipelines Coatings 250 to 760 µm (10 to 30 mils)
and specific requirements set forth in APPENDIX 2.
Any pinholes or missed spots located by the detector shall be repaired or replace and
retested prior to shipment.
Each length of coated pipe shall be checked to measure the coating dry film thickness (DFT)
by using Mikrotest film thickness gauge or Purchaser’s approved equal. The dry film
thickness shall be checked in accordance with the procedure defined by SSPC PA-2.
For critical applications, such as hydrocarbon service and/or severe corrosive environments,
a procedure for the control of Degree of Cure shall be submitted for Purchaser approval.

6.0 COATING REPAIR


All defects disclosed by the holiday detector and defect resulting from mechanical damage
to the coated surface shall be repaired.

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Mozambique LNG – 6.44 MTPA
External Coating for Buried Pipeline and Piping
Components - FBE and FJC
Document No. MZ-000-CCX-MC-SPC-00004
Rev. 0 Rev Date: 20-JAN-2020

Scars, dents, damaged areas and holidays are to be cleaned by removing all rust, scale,
loose coating, dirt or other foreign material. The area to be patched shall be suitable
roughened. Dust generated by the sanding shall be removed prior to patching.
FBE manufacturer’s recommended patching compound shall be used for patching holidays
and damaged coating. The patching compound shall be mixed and applied strictly in
accordance with FBE coating manufacturer’s specification. Patching shall overlap the
surrounding undamaged coating by a minimum 12 mm (0.5 inch) and shall be applied to
attain the minimum thickness recommended by the coating manufacturer.
All coating defects should be repaired using materials that are compatible with and adhere
well to the FBE coating, and are approved by the purchaser.
Repair materials typically consist of:
- Heat melting sticks; and
- Two-part epoxy or equivalent.
All repairs shall be holiday free.
The surface to be repaired should be suitably prepared to ensure adhesion of the repair
material. Minimum thickness of the repaired coating shall be in accordance with the repair
coating manufacturer’s recommendations.
Areas 6.4 mm (0.25 in) in diameter and less may be repaired with the supplier’s
recommended hot-melt stick, two-part epoxy, or equivalent.
Areas greater than 6.4 mm (0.25 in) in diameter and less than 0.013 m2 (20 in2) shall be
repaired with the purchaser’s or powder supplier’s recommended two-part epoxy or
equivalent.
The total maximum repaired areas for each pipe shall not exceed 0.052 m2 (80 in2).
For stripping, pipe shall be heated to a temperature not exceeding 260 °C (500 °F) to soften
the coating to permit removal by scraping, followed by abrasive blasting. All coating shall be
removed before recoating. The identity of each stripped and recoated pipe shall be recorded.
The repair procedure shall be proposed jointly by Applicator and submitted to Contractor and
Company for Approval.

7.0 FIELD JOINT COATINGS


Field joints (girth weld) shall be painted with two-part liquid epoxy coating. Cold apply tape,
shrink sleeves, or petroleum tape shall not be used.
Liquid epoxy shall be as listed below or approved equal:
• 3M Scotchkote Liquid Epoxy Coating 323
• Denso Protal 7200
• Sherwin Williams Dura-Plate UHS

7.1 Surface Preparation


Prior to blast cleaning at the field joints, contamination shall be removed from the steel
surfaces. Oil and grease shall be removed by solvent cleaning in accordance with SSPC SP-
1.
Surfaces shall be tested for soluble salt contamination using the Bresle method in
accordance with ISO 8502 Part 6. Surface preparation may proceed if the level of soluble
salt contamination is less than 5μg/cm2.

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Mozambique LNG – 6.44 MTPA
External Coating for Buried Pipeline and Piping
Components - FBE and FJC
Document No. MZ-000-CCX-MC-SPC-00004
Rev. 0 Rev Date: 20-JAN-2020

If contamination exceeds 5μg/cm2, the girth weld area shall be pressure washed with fresh
water and retested. Washing shall be repeated as needed. Surface preparation shall not
proceed until soluble salt contamination has been reduced to less than 5μg/cm2.
All burned damaged or loose FBE adjacent to the bare the girth weld area shall be removed
leaving and edge of sound, intact and tightly adhered FBE.
The leading edge of the intact shop applied FBE shall be feathered at least 25 mm (1 inch)
back from the bare steel producing a transition zone where the girth weld coating will overlap
onto the existing FBE. Feathering shall be performed by sanding to completely remove the
surface and roughen the coating and to producing a smooth taper from the exiting FBE
coating down to the bare steel.
The temperature of the substrate shall be per the manufacturer’s data sheet or a minimum
of 3°C (5°F) above the dew point during surface preparation, whichever is more stringent.
Surfaces to be coated shall be blast cleaned in accordance with SSPC SP-10 with a
minimum profile of 62 microns (2.5 mils) and a maximum profile of 127 microns (5.0 mils)
unless otherwise required by the coating material manufacturer’s latest published
instructions.
FBE coated surfaces beyond the transition (overlap) area shall be protected from abrasive
blast cleaning.
Burrs, slivers, scabs, sharp edges, and weld spatter visible after blasting shall be referred to
the Purchaser for removal. Surface preparation shall be restored to these repair areas in
accordance with original specification requirements.
If rusting occurs or if the cleaned surfaces become wet or otherwise contaminated prior to
coating, the surface shall be re-cleaned to the degree specified above.
After blast cleaning and immediately before coating, dust shall be removed with clean soft
bristle brushes, vacuuming, or other methods accepted by Buyer.

7.2 Application of Liquid Epoxy Coating


Only qualified applicator shall be allowed to apply liquid epoxy coating. Applicator shall
prepare application procedure and submit for approval.
Mixing time, “sweat-in” time, application window, and curing time of the coating material shall
be in accordance with the manufacturer’s latest published instructions and the requirements
specified herein. When multiple component units are mixed, each component shall be mixed
separately prior to the mixing of the combined materials. Only complete, pre-measured units
shall be mixed. After mixing, the coating material shall be applied within the material’s pot-
life.
Coating materials shall be thoroughly mixed until they are smooth and free from lumps, and
if required by the application strained through a suitably sized screen.
The temperature of the substrate shall be warmer than 10°C (50°F) and colder than 100°C
(212°F), and minimum of 3°C (5°F) above the dew point. Relative humidity shall not exceed
85% during lining application and curing.
Coating materials shall not be applied when there is moisture, dust, dirt or other
contaminants on the surface. The coating shall be applied by spray, brush or roller using
equipment recommended by the coating material manufacturer. When brush or roller
applied, several coats may be required to achieve the proper DFT.
The final cure of the completed coating shall be as recommended by the coating
manufacturer prior to backfilling the excavation.

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Mozambique LNG – 6.44 MTPA
External Coating for Buried Pipeline and Piping
Components - FBE and FJC
Document No. MZ-000-CCX-MC-SPC-00004
Rev. 0 Rev Date: 20-JAN-2020

Runs, sags, voids, drips, overspray, loss of adhesion, blistering, peeling, inadequate cure,
or rusting of the substrate are not permitted. Defects shall be corrected as detected during
or after application of the coating.

8.0 STORAGE AND HANDLING


Coated pipe shall be stored per Section 6 AWWA Standard C213 and Section 4.2 AWWA
Standard C203. Coated pipe shall be laid on pads designed to prevent damage to coating
by penetration. Stacked pipe shall be “nested” so that adjacent pipe lengths bear equally
against each other throughout their coated lengths. High stacks, which result in excessive
pressure and damage the coating to the coating or pipe, shall be avoided. When storing, the
bottom row of pipe shall be supported with 6-inch wide blocks spaced at internals of no more
than 5 feet. The ground shall be free of sharp objects that could damage coating.
The coated pipe shall be handled per Section 4.1 of AWWA Standard C203. The coated pipe
shall be handled (loading or unloading) at all times so as not to damage the coating before,
during or after transit.
Pipe shall not be allowed to ram into other pipe or to drop on rocky ground. Bare cables,
chains, hooks, metal bars or narrow skids shall not be used in handling coated pipe. Pipe
shall be lifted from carrier with wide padded slings and stockpiled on wide padded skids.
Coating that is damaged during handling, storage, or shipping shall be repaired. The
applicator is responsible for repairing damage that occurs during the handling, storage, and
shipping activities under its control. Repair to damage that occurs after the applicator no
longer controls the pipe activity is the responsibility of the Purchaser. While under the control
of the applicator, coating damage that exceeds the limits of Section 6 shall be stripped and
recoated, unless accepted by the Purchaser. Coating damage that occurs after the pipe
leaves control of the applicator and exceeds the limits of Chapter 6 shall be the responsibility
of the Purchaser.
Repair methods shall be such that no reduction to the thickness of metallic component is
possible.

9.0 MARKING
The following identification markings shall be placed on the coating:
1) Applicator’s name or mark (work order number);
2) Markings required by the applicable pipe specification or standard (grade, size, weight,
manufacturer, class, etc.);
3) Date of coating application;
4) Coating material identification; and
5) Purchase order number.

10.0 SUBMITTALS
To be provided at enquiry for qualification:
- Coating Material Datasheets
- Coating Application Procedure
- Quality Procedures and Plan
- Reference IR Scan
- Material Qualification Plan, if FBE proposed is different from those accepted
- Qualification Schedule, if FBE proposed is different from those accepted
To be provided during production, on each production lot:
- Material report, inclusive of

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Mozambique LNG – 6.44 MTPA
External Coating for Buried Pipeline and Piping
Components - FBE and FJC
Document No. MZ-000-CCX-MC-SPC-00004
Rev. 0 Rev Date: 20-JAN-2020

o IR-Scan
o Gel-Time
o Tg Control
o Particle Size Distribution
- Surface Preparation Report
- Defect Correction Report
- DFT report
- Holiday Detection Report
- Test Ring Report

11.0 APPENDICES
APPENDIX 1 COATING MATERIALS QUALIFICATION
APPENDIX 2 PRODUCTION TESTING REQUIREMENTS

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Mozambique LNG – 6.44 MTPA
External Coating for Buried Pipeline and Piping
Components - FBE and FJC
Document No. MZ-000-CCX-MC-SPC-00004
Rev. 0 Rev Date: 20-JAN-2020

APPENDIX 1 COATING MATERIALS QUALIFICATION


The suppliers shall provide the following:
1) Directions for handling and storage of coating materials
2) Materials Safety Data Sheets (MSDS)
3) Certification of the determined physical properties of batch in accordance with Table 1
4) Product Quality Certificate in accordance with Table 2 and
5) Technical datasheet (TDS) with basic physical properties including operating
temperature limits of the products.
6) Application Procedures
Labelling:
All boxes of epoxy powder supplied shall be labeled with the following minimum
information:
- Epoxy powder manufacturer’s name;
- Product description;
- Product Number;
- Batch Number;
- Manufacturing Location;
- Manufacturing Date;
- Shelf life / Expiration date;
- Temperature requirement for storage and transportation.

Each Batch of powder shall be provided with a test certificate in accordance with table 1.

Table 1 Epoxy Powder Properties

Property Value Limits Test Method


Density / Specific In accordance with supplier’s specification NACE SP0394
Gravity Appendix A
Particle Size Max. Retained on 150 μm (100 mesh) sieve; max. NACE SP0394
retained on 250 μm (60 mesh) sieve within the Appendix L
manufacturer’s recommendation
Shelf Life In accordance with supplier’s specifications and NACE SP0394
recommended storage conditions Appendix B
Gel Time In accordance with supplier’s specification or within 20% NACE SP0394
of the published value Appendix C
Cure Cycle Capable of cure at temperatures and time specified by In accordance
the supplier with supplier’s
specification
Moisture Content 0.5% max. in accordance with Appendix E or 0.6 % in NACE SP0394
or Total Volatile accordance with Appendix M Appendix E,
Content Appendix M

The coating supplier shall provide a product quality certificate in accordance with Table 2. The test
Specimens shall be either laboratory-prepared coupons in accordance with NACE SP0394 sec.
3.5 or coupons collected from pipe coated at the factory. A minimum of two test specimens are
needed unless otherwise specified in each test requirement (see table 2).

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Mozambique LNG – 6.44 MTPA
External Coating for Buried Pipeline and Piping
Components - FBE and FJC
Document No. MZ-000-CCX-MC-SPC-00004
Rev. 0 Rev Date: 20-JAN-2020

The product qualification tests must be repeated if the epoxy powder formulation, composition, or
manufacturing location changes.
Table 2 FBE Coating Qualities

No. of Test
Test Acceptance Criteria Test Method
Specimens
Cross-section porosity Rating 1 to 4, inclusive 2 NACE SP0394,
Interface Porosity Rating 1 to 4, inclusive 2 Appendix G
Flexibility: 3.0°/PD No cracks, tears, 3 NACE SP0394,
(Degrees per pipe diameter), - delamination, or Appendix H
30°C disbondment
Hot-water adhesion: 48 hours at Rating 1 to 2, inclusive 3 NACE SP0394,
(75 ± 3)°C Appendix J
Cathodic disbondment: Equal to or less than 3 NACE SP0394,
24 hours, (65 ± 3)°C, –3.5 Volt 6.5 mm radial disbondment Appendix F
Cathodic Disbondment: Equal to or less than 3
28 days (20 ± 3)°C -1.5V, -1.5Volt 8 mm radial disbondment
Cathodic Disbondment: Equal to or less than 3
28 days (65 ± 3)°C -1.5V, -1.5Volt 15 mm radial disbondment
Strained coating cathodic No cracking, no 3 NACE SP0394,
Disbondment: 28 days, -1.5Volt, delamination or Appendix N
(20 ± 3)°C disbondment
Thermal characteristics Coating Tg should be at 1 NACE SP0394,
least 5 °C above the Appendix D
pipeline design
temperature, or in
accordance with supplier’s
specification
Delta H (heat of reaction) In accordance with 1
supplier’s specification
Impact Resistance ≥ 1.5 J 3 NACE SP0394,
Appendix I
NOTE: Testing for pipelines operating above the glass transition temperature of the coating shall be adjusted
for atypical service applications such as elevated operating temperatures. Test methods and acceptance
criterion shall be based on the product TDS and recommendations by the coating manufacturers.

Uncontrolled if Printed Page 14 of 18


Mozambique LNG – 6.44 MTPA
External Coating for Buried Pipeline and Piping
Components - FBE and FJC
Document No. MZ-000-CCX-MC-SPC-00004
Rev. 0 Rev Date: 20-JAN-2020

APPENDIX 2 PRODUCTION TESTING REQUIREMENTS


The minimum requirements for production testing are given in this appendix, this appendix
shall be read in conjunction with NACE SP 0394.
Production Test Ring
The applicator is responsible for and shall have suitable equipment and trained personnel
at the plant to perform Type A, B and C Tests as required by Table 3, on each production
Lot.
Test rings shall be obtained from locations at least 0.30 m (12 in) from the end and shall be
of sufficient size to provide the tests described in Table 3. Heat-affected and cold-hardened
zones should be considered when preparing test specimens. Test rings shall be a
minimum length of 0.46 m. (18 in.).

Table 3 Production Test Ring Requirements

Test Test Acceptance Criteria No. Of Test Test


Type Specimens Method
Cathodic disbondment: (24 A Max. radius: 8 mm 1 NACE
hours (65 ± 3)°C, -3.5 Volts SP0394,
Appendix F
Flexibility: (3.0 °/PD permanent A No cracks, tears, or 3 NACE
strain) delamination (unaided visual) SP0394,
Test temperature: -30 °C Appendix H
Hot-water soak A Rating of 1 to 3, inclusive 1 NACE
Hot-water adhesion: (48 hours) SP0394,
75 ± 3 °C Appendix J
Interface contamination B Max: 30% 1 NACE
SP0394,
Appendix K
Cross-section porosity B Rating of 1 to 3, inclusive 1 NACE
SP0394,
Appendix G
Thermal characteristics C ΔTg of 5 °C, max, or 95% 1 NACE
conversion, minimum. SP0394,
Appendix D
Impact resistance C 1.5 J 1 NACE
SP0394,
Appendix I

Failure to meet the acceptance criteria for Type A tests shall be grounds for rejection of all pipe
coated after the previous acceptable test result and before the next acceptable test result.
Additional Type A testing of the affected day’s production may be conducted in an attempt to
reduce the amount of rejected pipe. Failure to meet the acceptance criteria for Type B or C tests
shall be grounds for requiring changes to the application process parameters.
The purchaser may require that the applicator limit the application process until the cause of the
failure is remedied.
For each pipe size (distinct combination of diameter and wall thickness), the minimum frequency of
obtaining test rings should be one sample for each of the following lots or fraction thereof:

Uncontrolled if Printed Page 15 of 18


Mozambique LNG – 6.44 MTPA
External Coating for Buried Pipeline and Piping
Components - FBE and FJC
Document No. MZ-000-CCX-MC-SPC-00004
Rev. 0 Rev Date: 20-JAN-2020

- One during each shift (maximum shift of 12 hours), unless the pipe size or wall thickness is
changed during the shift. At least one test should be made on each pipe size or wall
thickness.
The tests to be conducted by the applicator and the acceptance criteria for test rings are
shown in Table 3.
If the test results do not meet the criteria of Table 3, additional test rings can be taken and
retested. If these tests pass, all pipes between this test and the last successful test can be
accepted. If the second set of tests fails, additional bracket tests can be performed to isolate
problem pipes.

FBE Powder Verification


The minimum testing shall be one sample from each vehicle shipment of FBE powder received.
For stock-stored FBE powder, gel time shall be retested before each use, in accordance with
NACE SP0394 Appendix C.
Laboratory-coated test specimens shall be prepared at the proposed plant application
temperature. The tests to be conducted with the laboratory prepared panels and the acceptance
criteria are shown in Table 4. To meet the acceptance criteria in Table 4, the thickness shall be
between 350 μm (14 mil) and 450 μm (18 mil) for any thickness reading.

Table 4 In-Plant Verification of Epoxy Powder Quality

Test Acceptance Criteria No of Test Test Method


Specimens
Moisture Content Less than 0.6% in accordance with Appendix N/A NACE SP0394,
M, or 0.5 in accordance with Appendix E Appendix E or
M
Flexibility: (2.5 °/PD No cracks, tears, delamination, or 3 NACE SP0394,
Permanent Strain) at disbondment Appendix H
–30 °C
Gel Time In accordance with supplier’s specification 1 NACE SP0394,
Appendix C
Hot water adhesion: (48 Rating of 1 to 3, inclusive 1 NACE SP0394,
hours) (75 ± 3)°C Appendix J

In-line inspection and measurement

The inspection and measurements required shall be made and recorded by the applicator under
the supervision of a person qualified by experience and training in coating inspection methods.

1. Air for blasting, cleaning, drying, or powder application shall be checked and information
recorded at least every four hours to ensure no water, oil, or other contaminants are
present.
2. All temperature, dew point, humidity, and other such measurements as required by the
coating manufacturer or applicator shall be taken and recorded at the start of each shift
and at least once every two hours.
3. Surface finish shall be monitored hourly before heating: it shall be minimum ISO 8501-1 Sa
2.5 and surface roughness shall not exceed 100µm.

Uncontrolled if Printed Page 16 of 18


Mozambique LNG – 6.44 MTPA
External Coating for Buried Pipeline and Piping
Components - FBE and FJC
Document No. MZ-000-CCX-MC-SPC-00004
Rev. 0 Rev Date: 20-JAN-2020

4. Surface cleanliness per ISO 8502-3 (Pressure sensitive Tape). The maximum level shall
be class 2.
5. Pipe travel speed shall be recorded for blasting and coating setting phase and shall be
checked during production.
6. At least once every four hours of production, the surface profile shall be measured using a
replicating film or approved equivalent. The surface profile shall note exceed the limits of
the Approved Coating Procedure
7. Each cleaned pipe shall be visually inspected for surface defects and surface imperfections
that may cause holidays in the coating. Surface imperfections shall be removed by grinding
or other suitable means. Pipe containing surface defects shall be rejected or repaired at the
purchaser’s option. Repaired pipe that falls below the required minimum in wall thickness
shall be rejected.
8. The surface temperature of the pipe immediately before the application of the FBE powder
shall be monitored and controlled within the limits agreed to by the applicator, the
purchaser, and the coating supplier. (Optical pyrometers, graduated heat-indicating sticks,
or other purchaser-approved methods shall be used to monitor and control the
temperature.)
9. Once the coating temperature is established, the temperature of every fifth pipe shall be
taken and recorded
10. The use of recycled powder, curing temperature, and cure shall be controlled and
monitored.
11. The coating thickness shall be measured at five locations along the length of each coated
pipe using a coating thickness gauge calibrated at least once every four hours during
production. Each reading shall be at least 2 m (6 ft) from any other reading. All five of the
thickness measurements shall be recorded.
12. If any individual measured thickness value is less than the specified minimum value of 300
μm (12 mil), two coating thickness measurements shall be measured within 150 mm (6.0
in) of the original measurement. The average of these measurements shall exceed the
specified average value of 350 μm (14 mil) or greater minimum as specified by the
purchaser, and no individual value shall be more than 50 μm (2.0 mil) below the specified
minimum value. All these thickness measurements shall be recorded.
13. Pipe failing to meet the requirements of item 10, at the purchaser’s option, be repaired or
stripped and recoated.
14. If the purchaser’s maximum thickness is exceeded, the pipe shall be placed on hold for
further inspection, special marking, or stripping and recoating, as agreed to by the
purchaser’s representative and the applicator.

Final Testing

The entire pipe shall be inspected with a holiday detector having a search electrode made of
conducting electrode or phosphor bronze wire in accordance with NACE SP0490. The direct
current potential shall be set to exceed 5 V for each μm (125 V/mil). The detector shall be
calibrated in accordance with the manufacturer’s procedures at least once every shift, not
exceeding 12 hours).
The coated surface shall be 100% visually inspected to ensure it is free of blisters, bubbles, sags,
voids, and other irregularities.
Pipe containing holidays shall be repaired or recoated. No holidays are allowed on accepted pipe.

Uncontrolled if Printed Page 17 of 18


Mozambique LNG – 6.44 MTPA
External Coating for Buried Pipeline and Piping
Components - FBE and FJC
Document No. MZ-000-CCX-MC-SPC-00004
Rev. 0 Rev Date: 20-JAN-2020

The maximum number of repairs is on average one for every 2 m2 (22 ft2) of coated pipe surface,
for pipes of all diameters.
The allowable number and type of coating surface defects shall be agreed with the purchaser.

Uncontrolled if Printed Page 18 of 18


Mozambique LNG

Comment Sheet

ACTION BY ACTION BY
doCS Date: 13/01/2020 FINAL AGREEMENT
CLIENT CCS JV
doCS No: MZ-000-CCX-MC-SPC-00004.pdf

Document STATUS
Drawing / Document Number, Title and Revision: code
By CLIENT
Code 2 - Accepted with
Doc. No.: MZ-000-CCX-MC-SPC-00004 comments

Rev. No. : A
Rev. Date: 10/12/2019
Title:
EXTERNAL COATING FOR BURIED PIPELINE AND PIPING COMPONENTS - FBE AND FJC
PROTECTIVE COATING AND
Discipline:
INSULATION

Company Originator Company Consolidator Contractor Action by


CP No. Rev. Page number COMPANY Comments Description Comment Action Confirmation / Explanation CLIENT REPLY STATUS
NAME NAME position NAME

pbk168 anadarko\www187 A. Noted, Comment will be implemented Minor Wording Improvement is confirmed. M. Turetta

Created by: anadarko\www187


On: 1/13/2020 19:08
1 A 04 Section 1.3 Last sentance Agreed Agreed Closed
CCSJV should delete "field paint" and add "field joint coatings (FJC)"

--------- 0 Replies ---------


OJX035 anadarko\www187 A. Noted, Comment will be implemented Minor Wording Improvement is confirmed. M. Turetta

Created by: anadarko\www187


On: 1/13/2020 19:08
2 A 04 1.2 (Add): The purpose of such coatings is to prevent corrosion when used in Agreed Agreed Closed
conjunction with cathodic protection.

--------- 0 Replies ---------


OJX035 anadarko\www187 A. Noted, Comment will be implemented Referenced ISO Standards Added. M. Turetta

Created by: anadarko\www187


On: 1/13/2020 19:08
2.1 (add)
3 A 05 ISO 8501-1 Agreed Agreed Closed
ISO 8502-6
ISO 8503-5

--------- 0 Replies ---------

OJX035 anadarko\www187 A. Noted, Comment will be implemented Agreed to add clarity to the sectioning. M. Turetta

Created by: anadarko\www187


On: 1/13/2020 19:08
4 A 06 Sections 3 to 6 cover Fusion Bonded Epoxy External Coating. Hence, indicate Agreed Agreed Closed
here the main paragraph  Fusion Bonded Epoxy External Coatingand then
the subsections shall follow accordingly.

--------- 0 Replies ---------


OJX035 anadarko\www187 A. Noted, Comment will be implemented Agreed, such are standard production control. M. Turetta

Created by: anadarko\www187


On: 1/13/2020 19:08
5 A 06 3.1.3 (add) Agreed Agreed Closed
Cure time, Glass transition temperature (first heating, second heating,
enthalpy), Moisture content.

--------- 0 Replies ---------


OJX035 anadarko\www187 A. Noted, Comment will be implemented Agreed, addition of such details added. M. Turetta

Created by: anadarko\www187


On: 1/13/2020 19:08
4.2 (add) After abrasive blast cleaning, all dust and traces of abrasives shall be
6 A 07 removed from the pipe surface by brushing and vacuum cleaning. Agreed Agreed Closed
100% of the prepared surface of each pipe shall be inspected.

--------- 0 Replies ---------

OJX035 anadarko\www187 A. Noted, Comment will be implemented Agreed M. Turetta

Created by: anadarko\www187


On: 1/13/2020 19:08
7 A 07 4.3 (add) The pipes shall be coated on a continuous coating line without any Agreed Agreed Closed
risk of deterioration during the various heating, powder spraying, curing and
quenching operations.

--------- 0 Replies ---------

File: Copy of MZ-000-CCX-MC-SPC-00004_EXTERNAL COATING FOR BURIED PIPELINE AND PIPING - CPY reply Pavol P Jan-30-2020.xlsx Page 1/2
Mozambique LNG

Comment Sheet

ACTION BY ACTION BY
doCS Date: 13/01/2020 FINAL AGREEMENT
CLIENT CCS JV
doCS No: MZ-000-CCX-MC-SPC-00004.pdf

Document STATUS
Drawing / Document Number, Title and Revision: code
By CLIENT
Code 2 - Accepted with
Doc. No.: MZ-000-CCX-MC-SPC-00004 comments

Rev. No. : A
Rev. Date: 10/12/2019
Title:
EXTERNAL COATING FOR BURIED PIPELINE AND PIPING COMPONENTS - FBE AND FJC
PROTECTIVE COATING AND
Discipline:
INSULATION

Company Originator Company Consolidator Contractor Action by


CP No. Rev. Page number COMPANY Comments Description Comment Action Confirmation / Explanation CLIENT REPLY STATUS
NAME NAME position NAME

OJX035 anadarko\www187 A. Noted, Comment will be implemented Alignement of requirement included. M. Turetta

Created by: anadarko\www187


On: 1/13/2020 19:08
8 A 08 5.0 (update) Holiday inspection is addressed in App 2 under final testing. Agreed Agreed Closed
Please align both sections so as to avoid redundancy.

--------- 0 Replies ---------


OJX035 anadarko\www187 A. Noted, Comment will be implemented Duplication Removed. M. Turetta

Created by: anadarko\www187


On: 1/13/2020 19:08
9 A 08 6.0 (update) Information on overlap of repaired areas is repeated in this Agreed Agreed Closed
paragraph twice.

--------- 0 Replies ---------


OJX035 anadarko\www187 A. Noted, Comment will be implemented Sentence will be updated. M. Turetta

Created by: anadarko\www187


On: 1/13/2020 19:08
10 A 08 6.0 (update) Minimum thickness of the repaired coating shall be in accordance Agreed Agreed Closed
with the repair coating manufacturer's recommendations (see below).

--------- 0 Replies ---------

OJX035 anadarko\www187 A. Noted, Comment will be implemented Company and Contractor approval of repair M. Turetta
procedure added.
Created by: anadarko\www187
On: 1/13/2020 19:08
11 A 08 6.0 (add) The repair procedure shall be proposed jointly by Applicator and Agreed Agreed Closed
Manufacturer and submitted to CCSJV and Company for approval.

--------- 0 Replies ---------


OJX035 A. Noted, Comment will be implemented Sectioning will be updated. M. Turetta

Created by: anadarko\www187


12 A 10
On: 1/13/2020 19:08 Closed
anadarko\www187 Agreed Agreed
7.2 (update) The section to be called P
reparation and
application of Liquid Epoxy Coating
.

--------- 0 Replies ---------


OJX035 A. Noted, Comment will be implemented This comment is not relevant to the table and the M. Turetta
Product Qualification test in itself. This will be
addressed under sh.16, via a new item (item 5 in
Created by: anadarko\www187
appendix 2).
On: 1/13/2020 19:08 Agreed during the clarification meeting.
13 A 13 App 1 (add) Pipe travel speed shall be recorded for blasting anadarko\www187 Agreed
CCS JV shall address CPY comments
Closed
and coating processes during product qualification test. Then, under Appendix 2.
it shall be checked during production.

--------- 0 Replies ---------


OJX035 A. Noted, Comment will be implemented Dust Level and Pipe Travel added. M. Turetta

Created by: anadarko\www187


On: 1/13/2020 19:08
14 A 15
App 2, In-line inspection and measurement (add):
anadarko\www187 Agreed Agreed Closed
Add following inspection:
- Dust level of prepared surface
- Pipe travel speed for blasting and coating process

--------- 0 Replies ---------


EVEN IF THIS DOCUMENT IS ISSUED AS IFD AND, ACCORDING TO NORMAL CONTRACT PROCEDURE, THE DOCUMENT SHALL NOT INCLUDE COMMENT SHEETS, CLOUDS, TRACK CHANGES OR HOLDS, IT HAS BEEN AGREED TO ISSUE IT ANYWAY AND TO PROCEED TO THE NEXT REVISION. CONTRACTOR WILL RE-ISSUE AS SOON AS PRACTICAL THE SAME DOCUMENT/DRAWING WITHOUT HOLDS,
CLOUDS, TRACK CHANGES AND COMMENT SHEETS.

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