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Smart Materials and Structures

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Smart Materials and Structures

Smart Mater. Struct. 32 (2023) 034006 (24pp) https://doi.org/10.1088/1361-665X/acb6d9

3D printed negative stiffness


meta-structures with superior energy
absorption and super-elastic
shape-recovery features
M Hosseinabadi1, E Etemadi1, A Serjouei2 and M Bodaghi2,∗
1
Department of Mechanical Engineering, Hakim Sabzevari University, Sabzevar, Iran
2
Department of Engineering, School of Science and Technology, Nottingham Trent University,
Nottingham NG11 8NS, United Kingdom

E-mail: mahdi.bodaghi@ntu.ac.uk

Received 15 December 2022, revised 9 January 2023


Accepted for publication 28 January 2023
Published 10 February 2023

Abstract
The aim of this paper is to create novel 3D cubic negative stiffness (NS) structures (NSSs) with
superior mechanical performances such as high energy absorption, shape recovery,
super-elasticity, and reversibility. The conceptual design is based on an understanding of
geometrical influences, non-linear buckling-type instability, snap-through mechanism,
elasto-plastic deformation growth and plastic hinges. A finite element (FE) based computational
model with an elasto-plastic material behavior is developed to design and analyze NSSs, saving
time, material, and energy consumption. Material samples and meta-structures are 3D printed
by selective laser sintering printing method. Material properties are determined via mechanical
testing revealing that the printing process does not introduce much anisotropy into the fabricated
parts. Experimental tests are then conducted to study the behavior of novel designs under
loading–unloading cycles verifying the accuracy of the computational model. A good
correlation is observed between experimental and numerical data revealing the high accuracy of
the FE modeling. The structural model is then implemented to digitally design and test NSSs.
Effects of the geometrical parameters of the negative stiffness members under three cyclic
loading are investigated, and their implications on the non-linear mechanical behavior of NSSs
under cyclic loading are put into evidence, and pertinent conclusions are outlined. In addition,
the dissipated energy and loss factor values of the designed structures are studied and the
proposed unit cell is presented for the energy absorbing systems. The results show that the
structural and geometry of energy absorbers are key parameters to improve the energy
absorption capability of the designed structures. This paper is likely to fill a gap in the
state-of-the-art NS meta-structures and provide guidelines that would be instrumental in the
design of NSS with superior energy absorption, super-elasticity and reversibility features.


Author to whom any correspondence should be addressed.

Original content from this work may be used under the terms
of the Creative Commons Attribution 4.0 licence. Any fur-
ther distribution of this work must maintain attribution to the author(s) and the
title of the work, journal citation and DOI.

1361-665X/23/034006+24$33.00 Printed in the UK 1 © 2023 The Author(s). Published by IOP Publishing Ltd
Smart Mater. Struct. 32 (2023) 034006 M Hosseinabadi et al

Supplementary material for this article is available online


Keywords: negative stiffness, meta-structure, snap-through, energy absorption, shape recovery,
3D printing
(Some figures may appear in colour only in the online journal)

1. Introduction the snap-through mechanism on its performance. Zhang et al


[26, 35] improved the energy dissipation capability of NSSs by
The ability to absorb and dissipate kinetic energy by differ- increasing the bending stiffness of a curved beam and main-
ent static and dynamic loadings or vibrations is an essen- taining a constant volume to mass ratio. They designed two
tial requirement for many engineering applications. Energy types of lattices and hollow cross-sections as building blocks
absorbers like car bumpers and bicycle helmets absorb mech- for multi-stable structures. Recently, Ma et al [36] proposed a
anical energies via permanent deformations of foams or multiple-use and self-recoverable NSS with tetrahedral motif
cellular materials mostly made of plastics [1]. In general, the unit cells (UCs) and curved beams with an ability to dissipate
mechanical energy can be dissipated through non-recoverable energy in three directions.
methods, such as auxetic structures with permanent deform- The 3D printing technology is one of the common high-
ation in the plastic domain that unlike traditional structures, precision methods to manufacture conventional [37, 38] and
auxetic meta-materials show lateral shrinkage under com- meta-material [38] structures. NSSs can be manufactured
pressive loading or lateral expansion under tensile loading through various 3D printing technologies such as fused depos-
[2–7] or recoverable methods such as non-linear instability ition modeling (FDM) [38–40], selective laser sintering (SLS)
[8, 9] and viscoelastic mechanisms [10, 11]. Practically, thin, stereolithography (SLA) [41, 42], and multi-jet fusion
energy absorbing structures should be lightweight and capable [43]. For instance, Ha et al [44] presented a 3D cubic NS
of energy absorption in a reversible manner. lattice structure including multiple UCs with a high energy
Negative stiffness (NS) structure (NSS) is a class of meta- absorption capacity and shape recovery in the elastic domain
material structures designed to operate based on magnetic with 20% strain. They used SLS printing technology to man-
interactions [12] and the buckling mechanism in its members ufacture the structure and verified the results with FE method
to absorb energy, maintain their original configuration, and (FEM). Ha et al [45] designed and printed an NSS including
prevent vibration of structures through cyclic loadings [13]. multiple tetra-beam-plate UCs and investigated the mechan-
During buckling in a member of the NSS, with an increase ical behavior of the structure through numerical and experi-
in the applied compressive loading, a force-drop occurs, a mental analyses. They concluded that the snap-through mech-
snap-through mechanism is activated in the structure, and anism of the NSS is due to the nonlinear geometry of the elastic
it reveals an NS behavior [14]. Such structures have been beam members. Tan et al [46] designed disk elements on the
used as actuators [15, 16], bumpers [17], energy absorbers face sides of cubic UCs and introduced a 3D NS disk struc-
[18–22], and vibration absorbers [23, 24]. While other energy ture. They fabricated the structure using SLA printing method,
absorber structures such as auxetics are disposable, NSSs have evaluated its mechanical behavior and energy absorption val-
the advantage of multiple-use applications [25–28]. Further- ues under compressive loading, and compared their results
more, the load bearing ability of viscoelastic materials is under with those from FEM. Gao et al [47] introduced negative stiff-
question [14, 15]. ness UCs manufactured by SLS printing technique with the
Qiu et al [29] proposed the possibility of using curved ability to absorb energy and recover their original configur-
beams to create the NS behavior. They developed analytical ation in two loading directions. They investigated the mech-
equations to characterize the behavior of curved beams. Izard anical behavior of the UC and 3D cubic NS lattice structures
et al [30] designed an NSS based on a curved beam. Their res- under compressive and tensile loadings through theoretical,
ults showed that using a buckling beam as a member with the FE simulation, and experimental studies. Gholikord et al [48],
NS property improved the energy absorption in comparison assembled the positive and negative stiffness members man-
with other conventional structures. Tan et al [31, 32] studied ufactured by FDM method as new NSSs and evaluated their
the mechanical behavior of NSSs, including V-shaped, curved energy absorption capabilities under cyclic loadings and veri-
and arched beams with different configurations, through ana- fied the energy absorption values with FEM.
lytical, finite element (FE) simulation, and experimental tests. The literature review reveals that although NSSs have
They concluded that the use of the curved and V-shaped beams been investigated in the recent years, their capabilities for
in NSSs exhibited better NS behavior than the arched beams. energy dissipation, super-elasticity, shape recovery and re-
Virk et al [33] designed cellular structures with zero stiff- usability have not yet been discovered. This paper aims at
ness and NS effects. Their cellular structures demonstrated presenting novel designs of 3D cubic NS UCs with new
a large deformation capability with zero stiffness and NS features like high energy absorption, shape recovery, super-
regimes for a special range of strain rates. Yoon and Mo [34] elasticity, and reversibility. The design approach is based on
designed a new structure with a bidirectional NS mechanism an understanding of geometrical effects, non-linear buckling-
and conducted an experimental test to determine the effect of type instability and elasto-plastic deformation mechanism. A

2
Smart Mater. Struct. 32 (2023) 034006 M Hosseinabadi et al

FEM based on the elasto-plastic model is established as a larger than UC-1 to delay the corner beams connected to
digital tool to study geometrical effects on the structural beha- the plates from entering into the plastic region. In addi-
viors reducing material waste and experimental efforts. Sev- tion, the ends of the beams are chamfered to decrease the
eral dog-bone samples and NSSs are 3D printed by SLS print- stress concentration at the attached places of the beams and
ing technology. Experiments are first conducted to determine stalks.
mechanical material properties of the fabricated part revealing UC-3, UC-4, and UC-5 are then designed based on the
that the printing process does not introduce much anisotropy addition of different energy absorber members to UC-2, see
into the printed parts. Experimental studies are then carried out figures 3–5(c). The energy absorbers are proposed to improve
to investigate novel designs’ energy absorption in response to the energy absorption and dissipation capability of the UCs
loading-unloading cycles. A good correlation between experi- and recover their original configurations in the loading direc-
mental and numerical results is seen confirming high accuracy tion. They include curved members embedded in the middles
of the FEM. FE solution is then applied to digitally design and of the UCs. Their design is based on the allocation of suffi-
test NSSs mechanically. A detailed analysis of the influence of cient space for expansion during the compressive loading. The
geometrical parameters on the mechanical behaviors of NSSs geometry of the energy absorber members should be designed
under cyclic loading is carried out. Due to the absence of sim- such that they can restore their original configuration dur-
ilar design and results in the specialized literature, it is expec- ing the unloading process. Furthermore, energy absorbers are
ted that the results of this research will contribute to a better designed from curved corners instead of sharp ones to decrease
understanding of the mechanical behavior of energy absorb- their stress concentration and improve their energy absorption
ing NS meta-structures with super-elasticity and reversibility mechanism.
features. It is expected that the energy absorption and specific energy
absorption values of UC-3 to UC-5 are improved compared to
UC-2 and UC-1. That is due to the fact that upon the applic-
2. Materials and methods
ation the compressive load, the applied energy is transmit-
2.1. Conceptual design of novel NSSs
ted from the moving loading plate to the stalks and then to
the plates and finally it propagates through the internal and
This section discusses the design of five NSSs (namely external energy absorbing elements for performing buckling
UC-1, UC-2, UC-3, UC-4, and UC-5) with NS properties. in the elastic and plastic regions. As a result, by having more
Figures 1(a)–(c) shows UC-1 schematic of the side view, iso- energy absorbing elements in UC-3, UC-4, and UC-5, the
metric view, and one of the face views, respectively. All UCs energy absorption values are expected to increase signific-
consist of 12 frame members, 6 plates, and 24 cross beams, antly. Furthermore, in UC-1 and UC-2, the plates enter the
see figure 1(b). Beams are connected from two sides to the plastic region sooner than the other members during the com-
corner of the frames and plates and the stalks are embedded pressive loading. With the addition of energy absorbers to the
on upon the plates. All of them are placed on each side face of foresaid UCs, the stress concentration is expected to decrease
the NSSs. In figure 1, the geometrical parameters include the in UC-3, UC-4, and UC-5, and as a result they could properly
height of the beam (tb ), width of the beam (bb ), inclined angle recover their original configuration. In section 4.2, the values
(α), length of the beam (Lb ), inclined height of the beam (hb ), of the energy absorption and specific energy absorption are
side length of the plate (Lp ), thickness of the plate (tp ), side presented and compared.
length of the frame (Lf ), and the thickness of the frame(tf ). Figures 3(a)–(c) shows different views of UC-3. A camber-
Table 1 also lists the values of geometric parameters of UC-1– arch as shown in figure 3(c) is added to UC-2, named UC-3, see
5. The inclined angle α is 15◦ for all NSSs. The snap-through figure 3(b). The camber-arch, as an energy absorber member,
mechanism in NSSs is expected to be based on the buckling could exhibit a snap-through type buckling under compress-
of cross beams. ive loading and recover its original shape during unloading.
UC-1 is a basic design and is drawn according to [44] with Table 1 lists the dimensions of the camber-arch.
changing its geometrical parameters. The frame and plates are UC-4 as illustrated in figure 4 is designed by adding another
designed with larger dimensions than the beams leading to energy absorber between the top and bottom stalks of UC-2,
more deformation of the beams than the frames and plates to named rhombus, see figure 4(c). Table 1 presents dimensions
prevent undesired buckling. The maximum displacements of of the rhombus members. The geometry of the rhombus is
the UCs are 12 mm (εmax = 17.05%), and for displacements designed in such a way that the UC-4 has enough space for
greater than 12 mm, the frames would start to buckle and col- buckling to exhibit NS behaviors.
lapse. The importance of maximum displacement loading will Finally, UC-5 as demonstrated in figure 5 is innovated
be discussed in section 4.3.1. by adding another energy absorber with an DNA shape (see
Subsequently, based on the limitations of UC-1 in terms figure 5(c)) with different structural geometries compared to
of energy absorption and energy dissipation capabilities, new UC-3 and UC-4 to investigate the effects of the geometrical
NSSs with a high mechanical performance are designed here. parameters on the energy absorption, dissipation and shape
Figures 2(a) and (b) show side and isometric views of UC- recovery capabilities. The advantage of DNA members com-
2, respectively. The difference between UC-2 and UC-1 is pared to the camber-arch in UC-3 and rhombus in UC-4 is that
that in UC-2, the geometric dimensions of the plates are by designing small curves in DNA member, the stiffness of

3
Smart Mater. Struct. 32 (2023) 034006 M Hosseinabadi et al

Figure 1. UC-1: (a) side view, (b) isotropic view, (c) face view.

the member and, as a result, the energy absorption and shape Among the designed UCs, UC-2 and UC-3 are
recovery could increase. manufactured using 3D SLS printing technology to check
their performance under two cyclic loading. Three UC-2 and
2.2. Materials and 3D printing UC-3 are printed to achieve trustable results, and their mean
mechanical properties are reported. However, the testing val-
Polyamide material, PA 12, with an elastic-plastic behavior ues of fabricated samples exhibit close correlations. Figure 8
is selected as a base material to fabricate UCs. Lisa Pro Sin- (a) and (b) shows the side and isotropic views of UC-2 and
terit 3D printer with SLS technology is utilized to manufac- UC-3 printed samples.
ture tensile test samples and the UC-2 and UC-3. PA 12 with a
layer thickness of 0.125 mm is used for printing. The method
of printing is as follows: after designing a sample in the Solid-
2.3. Mechanical testing procedure
works software, it is exported as printable STL files. After that,
a thin layer of the powder is spread on a printing bed, and then The Shimadzu® universal machine is used to perform two
a laser fuses it in the shape of the designed sample. loading/unloading quasi-static compression tests on UC-2 and
By performing some mechanical testing, it is observed that UC-3 at the room temperature (25 ± 1 ◦ C). Figure 12 in
after SLS printing of the samples, the mechanical properties of section 4.1 shows the deformation sequences of UC-3 through
the tensile samples are differed in 0◦ , 45◦ , and 90◦ directions the cyclic loading. Furthermore, the experimental movie S1-
relative to the bed plate [49, 50]. To evaluate the mechanical EXP (see the supplementary section) shows the experimental
properties of PA 12, twelve tensile samples are fabricated in recording of the UC-3 behavior during two cyclic loadings.
three directions according to the ASTM D638 standard [51]. In the loading process, the top plate moves down and com-
Figure 6 shows geometric dimensions of a standard tensile presses the UCs to a maximum displacement of 12 mm with
sample. The room-temperature mechanical properties includ- a loading velocity of 2 mm min−1 and then moves up with
ing Young’s moduli (E0 , E45 , E90 ), 0.2% offset yield strength the same velocity to start an unloading process. Furthermore,
(σ 0 , σ 45 , σ 90 ) and Poisson’s ratio (v) of PA 12 are determ- the bottom plate is fixed during the cyclic loadings. The cyc-
ined by the Shimadzu® tensile testing machine and digital lic loading is repeated twice for both UC-2 and UC-3. Dur-
image correlation (DIC) method (to measure axial and trans- ing the test, the machine applies the displacement (d). The
verse strains and hence Poisson’s ratio) at loading rate of normal force (F) applied to the structure in all the loading
2 mm min−1 . Typical engineering stress–strain curves are and unloading processes is detected by a 50 kN load-cell.
shown in figure 7 and the respective results are presented in Force–displacement and stress–strain diagrams are obtained
table 2. at the end.

4
Smart Mater. Struct. 32 (2023) 034006 M Hosseinabadi et al

Table 1. Geometry parameters; dimensions are in mm. analysis, an element with the dimension 2.6 mm is selected,
Unit cell and the equivalent von Mises stress of the marked node in UC-
Parameters UCs 5 (see figure 9) is measured. Meanwhile, the element dimen-
sion is reduced until the von-Mises stress change is negligible.
Lf 44.7 Figure 10 shows the process of mesh sensitivity analysis for
Ls 2.4 UC-5 structure. Considering figure 10, the element size with
bb 8 a dimension of 1.6 mm is selected as a reference element.
Ds 14.6
The same process is implemented to mesh other designed
tf 4
tb 2
structures.
In this study, a static-general step is considered to simulate
UC-1 the cyclic loading of the UCs. To apply the boundary condi-
tions as shown in figure 6, a displacement-control loading is
Lb 23
Lp 16
applied to the top plate in the z-direction and the other five
degrees are constrained. Furthermore, the bottom area of the
UC-2, UC-3, UC-4, UC-5 bottom stalk of the UC is constrained to all six degrees of free-
dom (three translations and three rotations).
Lb 19.08
Lp 24
To plot the force–displacement diagrams for a designed
lb 5 UC, the sum of the element forces (F) and vertical displace-
lp 12 ment (δ) of a node in the top plate are evaluated, respectively. It
should be noted that the top plate nodes have the same vertical
Camber arch (UC-3) displacement, and it is adequate to measure the displacement
Rc1 14.1 of only one node. Again, all UCs are subjected to maximum
Rc2 13.5 displacement of 12 mm. Then, the applied stress (σ) and strain
bc 4 (ε) of the UCs are calculated by:
tc 2
F
Rhombus (UC-4) σ= (1)
A
LR 34.1
lR 32 δ
ε= (2)
RR 14.7 L
tR 2.6
bR 4 where A and L are the area of the top plate and initial height of
the UCs, respectively. In this paper, the A value is 167.33 mm2
DNA (UC-5) for all the UCs. After obtaining the stress–strain diagram, the
LD 28.3 energy absorption (E) values are obtained during the loading
lD 16.5 through equation (3) as:
RD 2.7
ˆε
tD 2
bD 4 E= σ dε. (3)
0

To conduct weight sensitive analysis of UCs, specific


3. FE simulation energy absorption (Em ) is investigated. This parameter is
defined as the ratio of energy absorption to the mass (m) of
The ABAQUS/standard FE software package is implemented the UCs as:
to investigate the mechanical properties of the designed UCs
under quasi-static cyclic loadings. An elastic–plastic mater- E
Em = . (4)
ial model is selected to determine the mechanical properties m
of PA 12. The elastic-plastic model is considered to investig- Furthermore, the hysteresis loops in stress–strain diagrams
ate the possibility of entering the UCs into the plastic region. which are enclosed during loading/unloading show the val-
Since, the Young’s modulus and yield stress are approximately ues of dissipated energy of the UCs. The values of dissip-
the same in three foresaid directions (see table 2), an isotropic ated energy in a hysteresis loop, ∆E, are calculated using
material with E = 933 MPa, σ 0 = 28.7 MPa is considered equation (5):
for UCs to simplify the FE simulation; also, Poisson’s ratio
ν = 0.33 calculated from DIC measurements is assumed. ∆E = E − E ′ (5)
The top plate and all components of each UC are meshed
using ten-node tetrahedral elements (C3D10). Mesh sensitiv- where E ′ is the energy release during unloading. Non-zero val-
ity analysis is performed according to [4]. For all the UCs to ues of ∆E in the cyclic loading indicate that the NSSs could
ensure high accuracy for the results. For the mesh sensitivity dissipate energy and have damping capabilities. The loss factor

5
Smart Mater. Struct. 32 (2023) 034006 M Hosseinabadi et al

Figure 2. UC-2: (a) side view and (b) isotropic view.

ψ is defined to investigate the ability of the NSSs to dissipate in the simulations and also visco-elasticity that is not included
and dampen energy as: in the simulations.
( ) According to figures 13 and 14 respectively for UC-2 and
∆E UC-3, two snap-through mechanical instabilities are observed
ψ= . (6)
E during two cyclic loadings in both the experiment and the FE
simulation. The structural behavior also changes from the first
Among the designed UCs, the UC with the highest ψ value cycle to the second one. It means that UC-2 and UC-3 may
can dissipate more energy than the others. experience some inelastic deformations that affect their beha-
vior in the following mechanical loading cycles. A similar
behavior would be expected for the other structures designed
4. Results and discussions
in this paper. The behavior of UC-3 in the first loading cycle is
now analyzed to get a better understanding of the defamation
4.1. Validation of FE modeling
mechanism. Considering the behavior of UC-3 in figures 11,
Figures 11 and 12 show the FE simulation and experimental 12 and 14 and S1-EXP- and S2-FEM movies, it is seen that
test of UC-3 for different displacements during one load- during the first loading cycle, in the deformations less than
ing/unloading, respectively. Furthermore, the behavior of UC- 4.9 mm, the entire UC-3 first deforms uniformly in an elastic
3 under two loading/unloading cycles is recorded in the manner. Then, at displacement 4.9 mm, four top cross beams
S2-FEM movie (see the attached file in the supplementary start to buckle, and the first snap-through-like mechanical
section). The other UCs show a general behavior to that of instability happens and as a result, the first peak in figure 15
UC-3. The detailed behavior analysis of the UCs through is observed. The structure softens and the force drops drastic-
FE simulation will be explained in section 4.2. Figures 13 ally with an increase in the displacement until displacement
and 14 demonstrate the force–displacement response for two of 7.8 mm when the buckling of the top cross beams is com-
cyclic loadings for UC-2 and UC-3, respectively, obtained pleted. Subsequently, with an increase in the applied displace-
from experiments and FE simulation. Furthermore, table 3 ment, the structure hardens and the force increases, and the
presents the force values at the first and second peaks and UC shows the capability to absorb more energy. At displace-
the error percentages between the FE modeling and exper- ment of 10 mm, the four bottom cross beams buckle and initi-
imental results in two cyclic loadings for UC-2 and UC-3. ate the second snap-through instability, and the force drops
Focusing figures 13 and 14 and table 3 reveal that the main fea- again with an increase of the displacement. The two snap-
tures of NNSs such as softening–hardening–softening beha- through-like mechanical instabilities could be associated to
viors, length of the snap-through instability, hysteresis loop the asymmetrical deformations during the mechanical load-
area, peak force value, loading history pattern, irrecoverable ing. Upon unloading, the meta-structures start recovering their
residual deformation and shape recovery behaviors are well initial shape while an irrecoverable residual plastic deform-
simulated by the present FE model. The differences between ation remains into the structure. It is seen that the meta-
the experimental and FE results could be due to some random structure experiences a free-stress shape recovery at the end
defects introduced during SLS printing technology that make of unloading and the force–displacement curve tracks the
the structures imperfect while perfect geometries are assumed horizontal displacement axis towards the origin. That is why,

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Smart Mater. Struct. 32 (2023) 034006 M Hosseinabadi et al

Figure 3. UC-3: (a) side view and (b) isotropic view, (c) camber-arch part.

in the second loading cycle, the force–displacement curve The stress and strain values are calculated using equations (1)
starts growing before the first unloading cycle curve. Plastic and (2), respectively. Furthermore, table 4 presents the val-
deformation grows in each load cycle and is captured by the ues of E, Em , E ′ , ∆E and ψ for every cyclic loading. E and
simulation very well. The overall dissipated energy observed Em are calculated for the first and second loading cycle using
in the experiment can be attributed slightly to visco-elasticity equations (3) and (4), respectively. Also, the values of ∆E and
and mainly to mechanical instability through compression and ψ for every cyclic loading are evaluated using equations (5)
plasticity. The mechanical behaviors of UCs and the influence and (6), respectively.
of geometrical parameters on their responses will be studied in According to figure 15 and table 4, the response of the
the next sections by implementing the developed FE modeling. fist loading/unloading cycle does not coincide to the response
of the second cycle. That shows the presence of the inelastic
deformation in the first cycle that makes the mechanical beha-
vior be cycle dependent. It is seen that all UCs dissipate
4.2. Mechanical behaviors of UCs under cyclic loadings
some energy during the first loading/unloading cycle. By
Figures 15(a)–(e) shows the stress–strain behaviors of UC-1 to mechanical unloading, mechanical hysteresis, characterized
UC-5 for two cyclic loadings obtained from the FE analysis. by noncoincident loading–unloading curves, is observed in all

7
Smart Mater. Struct. 32 (2023) 034006 M Hosseinabadi et al

Figure 4. UC-4: (a) side view and (b) isotropic view, and (c) rhombus part.

cases. UCs recover their original shape partially while some produce any plastic deformation during the second loading/un-
strains remain in the meta-structure due to the plastic deform- lading cycle and dissipates the mechanical energy via the non-
ation. The energy dissipation may arise from mechanical linear mechanical instability. Therefore, it can be concluded
instability and plasticity. As per the second loading/unloading that UC-1 and 5 have a super-elastic behavior with a full shape
cycle, it is seen that, while UC-2–5 show hysteresis loop and recovery feature in the second loading/unloading cycle. Spe-
consequently dissipate energy, UC-1 behaves elastically and cifically, UC-1 behaves like non-linear elastic material with
releases all energy stored during loading upon unloading in the no energy dissipation while UC-5 behaves like super-elastic
second cycle as ψ value of UC-1 in the second loading cycle shape memory alloys with a fully shape recovery response.
becomes zero. UC-1 acts like a springer that releases all the While the energy dissipation mechanism in shape memory
stored energy upon unloading. Considering stress–strain dia- alloy (SMA)s is due to the martensitic phase transformation
grams of second cycle loading in figure 15, it is observed that [52, 53], solid-state non-linear mechanical instability in NSS
while UC-2–4 experience some residual plastic deformation at UC-5 dissipates the energy. UCs provide the designers with a
the end of second unloading cycle, interestingly, UC5 does not variety of mechanical behaviors and options to meet different

8
Smart Mater. Struct. 32 (2023) 034006 M Hosseinabadi et al

Figure 5. UC-5: (a) side view and (b) isotropic view, and (c) DNA member.

requirements. They can expand the design space for propos- an effective way to improve energy absorption and dissipa-
ing large recoverable energy absorbers and dissipaters with tion capabilities. Also, against UC-1, UC-2 has ψ value in the
different capacities. The first cycle could also be considered second loading/unloading cycle, and as a result, chamfering its
as a training stage to produce shape memory devices where a plate corners causes the original configuration to be properly
super-elastic behavior where a large energy absorption and/or recovered. According to figures 15(b)–(e) and table 4, it can
dissipation is required. From a numerical point of view, among be observed that, for UC-2 to UC-5, ψ values in the second
the designed UCs, UC-1 has the minimum values of Em , ∆E cyclic loading decreases in comparison with the first load
and ψ for both the first and second cycles. UC-2 has more cycle. It implies that plastic deformation growth and mech-
values of Em than UC-1, and therefore it is concluded that anical instability reduce by further loading cycles for UC-2-4
changing the plate dimensions of UC-1 to achieve UC-2 is and UC-5, respectively.

9
Smart Mater. Struct. 32 (2023) 034006 M Hosseinabadi et al

Figure 6. Geometry of the standard tensile sample designed according to the standard ASTM D638 [51] (dimensions are in mm).

Figure 7. Typical engineering tensile stress–strain curves for PA 12 samples printed in 0◦ , 45◦ , and 90◦ directions.

Table 2. Mechanical properties of PA 12 in different directions.

E0 (MPa) E45 (MPa) E90 (MPa) σ 0 (MPa) σ 45 (MPa) σ 90 (MPa) v

933 933 943 28.7 28.7 24.2 0.33

Figure 8. Side and isotropic views of 3D printed (a) UC-2 and (b) UC-3.

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Smart Mater. Struct. 32 (2023) 034006 M Hosseinabadi et al

Figure 9. Meshing and boundary conditions of UC-5.

Figure 10. Mesh-sensitivity analysis for UC-5 structure.

The results in figure 15 and table 4 reveal that UC-2 has found that UC-5 has the maximum values of E, Em and ψ.
higher E and less Em than UC-3 in the first and second load- It implies that UC-5 can absorb and dissipate more energy
ing cycles. It means that the designing of camber-arch energy compared to other UCs. For more investigation, the stress–
absorber should be modified. Therefore, rhombus and DNA strain response of UC-5 under three cyclic loadings is demon-
members have been designed for UC-4 and UC-5, respect- strated in figure 16. Also, E, Em and ψ for the third cycle
ively. Indeed, the higher values of E and Em in UC-4, and of UC5 are calculated and added to table 4. Surprisingly,
UC-5 in comparison with UC-1 and UC-2 show that adding it is seen that E, Em and ψ remain almost constant for the
foresaid energy absorbers could increase the E and Em values. second and third cycles and stress–strain graphs coincide each
Therefore, the energy absorber members in UC-4 and UC-5 other. It is an interesting observation and implies that the
can improve the mechanical performance of NSSs. The reason plastic deformation growth stops after the first loading/un-
is that the energy absorbers have been designed to decrease loading cycle and UC-5 shows a stable shape recovery fea-
the concentration stress in the cross beams and plates and help ture onwards. The energy dissipation mechanism after the first
them recover their original configurations. cycle is completely attributed to the non-linear mechanical
By comparing E and Em values of the UCs with the energy instability through compression. The stable super-elastic beha-
absorber members (UC-3, UC-4, and UC-5) in table 4, it is vior in UC-5 has can be exploited for applications such as

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Smart Mater. Struct. 32 (2023) 034006 M Hosseinabadi et al

Figure 11. FE simulation of UC-3 under a loading/unloading cycle.

strong-yet-flexible instruments. The large recoverable beha- response can be exploited to create structural polymeric ele-
vior also gives rise to large hysteretic loss during load cycles ments with high energy dissipation for stabilizing sensitive
due to the solid-state energy dissipation. This dissipative lightweight structures.

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Smart Mater. Struct. 32 (2023) 034006 M Hosseinabadi et al

Figure 12. Sequences of UC-3 experimental test under a loading/unloading cycle.

4.3. Geometric parametric studies absorption capabilities, and maintaining the original configur-
ation of the NSSs [54]. As mentioned in section 4.2, UC-5 is
The NS member dimensions are effective parameters in the selected for further investigations. Therefore, the effects of the
activation of the snap-through mechanism, improving energy inclined cross beam angle, α, and DNA member thickness, tD ,

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Smart Mater. Struct. 32 (2023) 034006 M Hosseinabadi et al

Figure 13. Force–displacement response of UC-2 for (a) first load cycle and (b) second load cycle from experimental tests and FE
simulations.

parameters on the mechanical performance of UC-5 are stud- For further discussion, figures 18(a) and (b) exhibits a
ied in sections 4.3.1 and 4.3.2, respectively. plastic strain (PE) contour of UC-5 with α = 5◦ and 8◦ at
dmax = 12 mm, respectively. Following figures 18(a) and (b)
for the deformation of UC-5 with α = 5◦ and 8◦ , it can be
4.3.1. Effect of inclined cross beam angle. As shown in observed that the top and bottom cross beams do not have
section 4.1, the cross beams are NS members that could enough space to buckle, and cross beams do not soften and
improve the mechanical performance of the designed NSSs stay stable during the bending. It is seen that the frame and
through the snap-through mechanism. Therefore, in this members connected to the frame, including plates, and cross
section, the effect of the inclined cross beam angle, α, on the beams stay in the elastic domain while the DNA member
snap-through mechanism and energy absorption capability is enters into the plastic region for both angles of α = 5◦ and
studied. To examine the effect of α on the UC-5’s mechanical 8◦ at dmax = 12 mm. Plastic hinges are developed in the cen-
stability, the force–displacement responses for the first com- ter, nodes and the end of the beam due to bending moment
pressive loading are presented in figure 17 for α = 5◦ , 8◦ , in the span of the beam and a high level of the stress at these
12.5◦ , and 15◦ . It is seen that the force increases monotonically points. For α = 12.5◦ , because of the sufficient space for the
with an increase in the compressive displacement for α = 5◦ cross beams, they become unstable and buckle in the elastic
and 8◦ . The mechanical behavior is completely stable during region. As shown in figure 17, the force values decrease with
the compression and the material response is hardening. an increase in the displacement with a low slope. In addition,

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Smart Mater. Struct. 32 (2023) 034006 M Hosseinabadi et al

Figure 14. Force–displacement response of UC-3 for (a) first load cycle and (b) second load cycle from experimental tests and FE
simulations.

Table 3. The peak force values obtained from experimental tests and FE analysis for UC-2 and UC-3.

UC Peak Cycle Force (N), Exp. Force (N), FEM Err. (%)

UC-2 Peak 1 First cycle 138 127 7.9


Second cycle 78 72.7 6.8
Peak 2 First cycle 127 117 7.8
Second cycle 111 99 10.8

UC-3 Peak 1 First cycle 122.8 119 3.1


Second cycle 81 88 8.6
Peak 2 First cycle 134.4 124 7.8
Second cycle 114 100 12.2

according to figure 18(c) for α = 12.5◦ at dmax = 12 mm, the α = 5◦ and 8◦ . That is due to the fact that cross beams already
frames, plates, and cross beams remain in the elastic region, absorbed some energy, and a lower level of the energy is trans-
and the overall PE value of DNA member is lower than that of formed to the DNA member reducing the plastic defamation

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Smart Mater. Struct. 32 (2023) 034006 M Hosseinabadi et al

Figure 15. Stress–strain response of (a) UC-1, (b) UC-2, (c) UC-3, (d) UC-4, and (e) UC-5 during two cyclic loadings.

growth. By considering the force-displacement response of unstable snap-through-like deformation with a higher anergy
UC-5 with α = 15◦ in figure 17, it is seen that the force starts to absorption for α = 15◦ is clearly seen.
decrease significantly at d = 5.5 mm owing to the activation Figures 19(a)–(d) displays the stress–strain behaviors of
of the first snap-through mechanism in the top cross beams, UC-5 with different α angles under three cyclic loadings for
and UC-5 with α = 15◦ exhibits an NS behavior. The second dmax = 12 mm and tD = 2 mm. Furthermore, table 5 lists
snap-through instability occurs at d = 10 mm and the bottom the values of E, Em and ψ for each cycle. The results presen-
cross beams buckle. Figure 18(d) shows the plastic contour ted in figure 19 and table 5 reveal that UC-5 with α = 15◦
of UC-5 with α = 15◦ at dmax = 12 mm. By comparing PE has the highest values of E and Em in all three cyclic load-
value and UC-5’s response for different α’s, it is found that ings. Also, in a comparison between α = 5◦ and 8◦ , the val-
the case of α = 15◦ experiences maximum snap-through-like ues of E and Em in all the three cyclic loadings for α = 5◦
mechanical instability and its DNA member undergoes min- are larger than those for α = 8◦ . In fact, the stable harden-
imum plastic deformation at hinges. Finally, from an energy ing behavior of UC-5 with α = 5◦ leads to absorbing more
absorption and stability points of view, a transient behavior energy compared to α = 8◦ that tends to have a nearly flat
from overall stable bending defamation from α = 5◦ to an plateau.

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Smart Mater. Struct. 32 (2023) 034006 M Hosseinabadi et al

Table 4. Values of E, M, Em , ∆E, and ψ for different loading cycles.


( ) ( ) ( ) ( )
E J mm−3 Em J mm−3 × kg E ′ J mm−3 ∆E mJ mm−3
UC Cycle ×10−6 M (kg) ×10−6 ×10−6 ×10−6 ψ

UC-1 First cycle 0.0794 0.0280 2.84 0.0765 0.003 0.036


Second cycle 0.0762 1.72 0.0762 0 0

UC-2 First cycle 0.0900 0.0306 2.94 0.0484 0.0416 0.422


Second cycle 0.0604 1.97 0.0394 0.021 0.301

UC-3 First cycle 0.0929 0.0324 2.87 0.0504 0.0425 0.457


Second cycle 0.0589 1.82 0.041 0.0179 0.303

UC-4 First cycle 0.1050 0.0318 3.30 0.0754 0.0296 0.281


Second cycle 0.0849 2.52 0.0767 0.0082 0.096

UC-5 First cycle 0.1351 0.0319 4.23 0.0727 0.0624 0.461


Second cycle 0.0821 2.5455 0.0706 0.0115 0.14
Third cycle 0.0812 2.5454 0.0703 0.0110 0.136

Figure 16. Stress–strain response for UC-5 during three cyclic loadings.

Before a discussion about ψ values, it is necessary to dis- Because the values of a = 18.46 mm and Ls = 2.4 mm are
cuss the maximum allowed applied displacement, da , for a UC. constant in this paper, according to equation (8), da depends
For d > da during compressive loading, the frame of the UC on α. Therefore, for UC-5 with α = 5◦ , 8◦ , 12.5◦ , and 15◦ ,
is subjected to undesirable buckling which results in the UC da values are 8.02 mm, 9.98 mm, 12.90 mm, and 14.68 mm,
instability. According to figure 20, the maximum allowable respectively. It can be concluded that for α = 12.5◦ and 15◦ ,
displacement of the cross beams is 2b. In addition, the follow- it is possible to maximize the applied compressive displace-
ing relationship should be satisfied to maintain the stability of ments (dmax ) to more than 12 mm. Therefore, for optimiz-
the UCs: ing UC-5 with α = 12.5◦ and 15◦ , it is possible to increase
dmax value, however, to compare the results in an equal com-
da ⩽ 2 (Ls + b) . (7) pressive displacement, dmax = 12 mm is considered here. Also,
among allowed applied displacements for different angles, da
Considering b = a tan α. in figure 19 leads to: for α = 12.5◦ is the closest to dmax = 12 mm.
As per energy dissipation, ψ values in table 5 show that
da ⩽ 2 (Ls + a tan α) . (8) α = 12.5◦ has the highest value and its value is greater

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Smart Mater. Struct. 32 (2023) 034006 M Hosseinabadi et al

Figure 17. Force–displacement response of UC-5 for the first compressive loading for tD = 2 mm.

Figure 18. Plastic strain (PE) contour of UC-5: (a) α = 5◦ , (b) α = 8◦ , (c) α = 12.5◦ and (d) α = 15◦ for tD = 2 mm at dmax = 12 mm.

than the one for 15◦ in all three cycles. The reason is that and therefore, UC-5 with α = 15◦ cannot present its max-
da = 12.90 mm for α = 12.5◦ is closer than da = 14.68 mm for imum efficiency. Therefore, it is concluded that the highest
α = 15◦ to the maximum applied displacement (d = 12 mm), performance of the NSSs can be achieved by applying

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Smart Mater. Struct. 32 (2023) 034006 M Hosseinabadi et al

Figure 19. Stress–strain behavior of UC-5 during three cyclic loadings for with tD = 2 mm and (a) α = 5◦ , (b) α = 8◦ , (c) α = 12.5◦ and,
(d) α = 15◦ .

Table 5. E,Em , and ψ for first, second and third loading cycles of UC-5 for a given α.
( ) ( )
α Cycle E J mm−3 Em J mm−3 × kg ψ

α = 5◦ First cycle 0.112 3.1728 0.454


Second cycle 0.0631 1.7875 0
Third cycle 0.063 1.7847 0

α=8 First cycle 0.0813 2.3911 0.358
Second cycle 0.0549 1.6147 0.049
Third cycle 0.0549 1.6147 0.049

α = 12.5 First cycle 0.0981 2.9283 0.463
Second cycle 0.0631 1.8835 0.164
Third cycle 0.0631 1.8835 0.164

α = 15◦ First cycle 0.1351 4.2351 0.461


Second cycle 0.0821 2.5455 0.14
Third cycle 0.0812 2.5454 0.136

displacements near to their maximum allowable displace- UC-5 with α = 5◦ shows a non-linear super-elastic behavior
ments. In the comparison between α = 5◦ and other angles, with no energy dissipation over cycles two and three, other
ψ value for the first cycle at α = 5◦ is lower than others. α cases experience a non-linear super-elastic behavior with
Besides, ψ value for α = 5◦ becomes zero for the second energy dissipation due to the non-linear mechanical instabil-
and third load cycles but it remains constant and non-zero for ity. A decreasing–increasing trend of the specific absorbed
other cases. As the stress–strain graphs get back to the origin energy is seen when α value is increased. In a converse man-
at the end of the second and third unloading cycles, it implies ner, an increasing-decreasing trend of the loss factor can be
that the plastic hinges do not growth over these cycles. While observed as α value is increased. These transient trends can be

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Smart Mater. Struct. 32 (2023) 034006 M Hosseinabadi et al

Figure 20. Front view of stalk, plate, and cross beams.

Figure 21. Stress–strain response of UC-5 with different tD : (a) tD = 1 mm, (b) tD = 2 mm, (c) tD = 3 mm for α = 15◦ .

associated to the switch in energy absorption and dissipation tD = 3 mm has the maximum value of ψ for the first cycle.
mechanisms. Our investigation of the further cycles shows that From table 6 it is found that, for tD = 1 mm, ψ value becomes
E, Em and ψ remain unchanged for the fourth and fifth cycles zero for the second and third cycles resulting in zero energy
results of which are not presented here for keeping the report dissipation. By following figures 21(b) and (c) and table 6 for
brief. the second and third cyclic loadings, it is found that ψ val-
ues of tD = 2 mm are a bit greater than those of tD = 3 mm,
and tD = 2 mm case results in a higher energy dissipation.
4.3.2. Effect of DNA member thickness. Figures 21(a)–(c) In fact, a lower level of the plastic deformation in the case of
shows the stress–strain response of UC-5 under three cyc- tD = 2 mm compared to tD = 3 mm lets the meta-structure
lic loadings for tD = 1 mm, 2 mm, and 3 mm, respectively experience stiffer mechanical instability and consequently res-
(α = 15◦ for all NSSs). Also, table 6 presents the values ults in more energy dissipation.
of E, Em and ψ for each cycle. According to figure 21 and Next, the effects of both α and tD on Em are investig-
table 6, with an increase in the DNA member thickness, the ated. Figures 22(a)–(c) shows Em values for the first, second
stiffness of DNA part increases and the values of E and Em and third loading cycles, respectively. With an increase in α,
increase for the first cycle. The stiffer the system, the higher except for α = 5◦ , Em values increase for constant thicknesses.
the absorbed energy. Also, with an increase in tD , the hyster- In addition, Em for α = 5◦ is greater than that for α = 8◦ for
esis loop area increases in the first cycle, and the energy dis- all thicknesses in each cyclic loading because as mentioned
sipation capability of UC-5 improves in this cycle. Therefore earlier in section 4.3.2, the DNA member in UC-5 with α = 5◦

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Smart Mater. Struct. 32 (2023) 034006 M Hosseinabadi et al

Table 6. Values of E and ψ for the first, second and third load cycles of UC-5 for different energy absorber thicknesses and α = 15◦ .
( ) ( )
tD Cycle E J mm−3 Em J mm−3 × kg ψ

tD = 1 mm First cycle 0.0938 2.9968 0.154


Second cycle 0.0793 2.5335 0
Third cycle 0.0793 2.5335 0

tD = 2 mm First cycle 0.1351 4.2351 0.461


Second cycle 0.0821 2.5455 0.14
Third cycle 0.0812 2.5454 0.136

tD = 3 mm First cycle 0.1836 5.6842 0.624


Second cycle 0.0807 2.498 0.137
Third cycle 0.0804 2.489 0.135

Figure 22. Specific energy absorption, Em , versus inclined angles for different energy absorber thicknesses of UC-5: (a) first cycle,
(b) second cycle, and (c) third cycle.

absorbs energy in the elastic region. In addition, according Finally, figures 23(a)–(c) shows the ψ values for the first,
to figure 22(a), in the first loading cycle with the increase second and third loading cycles, respectively. According to
in the thickness, the Em values increase for all the inclined figure 23(a) for the first cycle, with the increase in tD at a con-
angles. Also, considering figures 22(b) and (c), the thickness stant α, the ψ values increase significantly. Also, for a con-
parameter does not have a significant effect on Em values for stant tD , ψ values become maximum for α = 12.5◦ , because, as
second and third loading cycles. Em has a maximum value for mentioned earlier, at this angle, da is closer than other angles
tD = 2 mm and α = 15◦ for both second and third loading to dmax . By focusing on figures 23(b) and (c) for the second
cycles. and third loading cycles, it is seen that the difference between

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Smart Mater. Struct. 32 (2023) 034006 M Hosseinabadi et al

Figure 23. The loss factor, ψ, versus inclined angles for different energy absorber thicknesses of UC-5: (a) first cycle, (b) second cycle, and
(c) third cycle.

ψ values become considerable for different thicknesses. From material, and energy consumption. SLS 3D printer was used to
these figures, it is seen that loss factors are zero for tD = 1 mm fabricate material and structural samples. Dog-bone samples
at all inclined cross beam angles. In addition, in the second and were tested and shown that mechanical properties are almost
third cycles, DNA member with tD = 2 mm and α = 12.5◦ independent of printing direction. The high accuracy of the FE
results in the maximum loss factor values. Furthermore, for model was verified via the mechanical testing of 3D printed
tD = 3 mm, the structure is subjected to a considerable plastic NSSs. The computational model was then employed to further
deformation in its first load cycle that affects its energy dissip- investigate the mechanical behaviors of NSSs. The implica-
ation performance in the following load cycles. tions of the effect of inclined cross beam angle, and energy
absorbing member thickness on the mechanical response of
NSSs were put into evidence via a parametric study, and
5. Conclusion related conclusions were drawn. It was observed that all NSSs
have a high capability of energy absorption and dissipation in
The aim of this paper was to propose a new class of 3D cubic the first cycle via plasticity and instability mechanisms. In the
NSSs that can offer high energy absorption, superior energy further loading/unloading cycles, depending on the geomet-
dissipation, full/partial shape recovery, super-elasticity, and rical parameters and configurations, NSSs show super-elastic
reversibility in cyclic loadings. The NSSs include stalks, stability/instability with high energy absorption and full/
plates, cross beams and a frame. To prevent undesirable buck- partial shape recovery. The presented conceptual design and
ling of the frames, the thickness of the frames was higher results are expected to contribute to a better understanding of
than those of the cross beams. In addition, to absorb high val- the behavior of NSSs and to be instrumental towards an effi-
ues of energy, energy absorber members with different con- cient design of NSS for various applications.
figurations were designed and assembled inside the UC. Dif- The ways to activate snap-through mechanisms simultan-
ferent NSSs were designed exploiting geometrical influences, eously in the top and bottom curved beams in the designed
snap-through instability mechanism, elasto-plastic deforma- NSSs could be investigated in the future research effort.
tion growth and plastic hinges. A FE modeling via ABAQUS Also, 2 × 2 and 3 × 3 cellular NSSs based on the foresaid
software package assuming an elasto-plastic material behavior designed NSSs could be further investigated to explore new
was implemented to design and analyze NSSs saving time, futures.

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Smart Mater. Struct. 32 (2023) 034006 M Hosseinabadi et al

Data availability statement [14] Drugan W J 2017 Wave propagation in elastic and damped
structures with stabilized negative-stiffness components J.
All data that support the findings of this study are included Mech. Phys. Solids 106 34–45
[15] Zhang L-Y and Xu G-K 2015 Negative stiffness behaviors
within the article (and any supplementary files).
emerging in elastic instabilities of prismatic tensegrities
under torsional loading Int. J. Mech. Sci. 103 189–98
[16] Chen B, Chen L, Du B, Liu H, Li W and Fang D 2021 Novel
Acknowledgments multifunctional negative stiffness mechanical metamaterial
structure: tailored functions of multi-stable and compressive
The authors would like to thank the 4D Materials and Print- mono-stable Composites B 204 108501
ing Lab at Nottingham Trent University for providing software [17] Chen T, Bilal O R, Shea K and Daraio C 2018 Harnessing
and hardware facilities for conducting this research. bistability for directional propulsion of soft, untethered
robots Proc. Natl Acad. Sci. 115 5698–702
[18] Chen L, Nagarajaiah S and Sun L 2021 A unified analysis of
negative stiffness dampers and inerter-based absorbers
ORCID iD
for multimode cable vibration control J. Sound Vib.
494 115814
M Bodaghi  https://orcid.org/0000-0002-0707-944X [19] Lin S, Zhang Y, Liang Y, Liu Y, Liu C and Yang Z 2021
Bandgap characteristics and wave attenuation of
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