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01/21/2004 09:48 8153511974

Where xx is the line number in the injector program. To

select one of the other commands, press (Tab I to position
the cursor on the D of DRAW, then press ®
or (I).
To delete a line from the injector program, display the
line to be deleted and press (Shift) (Delet0. Now press
(Ent.r) to del(Jf,e line or ~ to retain line.
T{) delete the complete injector program, press (Shift)
@elet.) (Inj voll. Now press (Enter) to delete injector
program or ~ to retain it.
,
I!
Injector Program YOIlcan use the followi ng commands in an injector
Commands program.
n<DRAW ... ,---JIFRoM VIAU --
Draws specified volume fronl specified vi ,11 llumber.
Limits: 0,1 ttl through MAXINJVOLUM (for volume) and a
through 100 (for vi,d nurnher),
x.:.1:DRAW """'C.-:-1l1 FROM· SAMPLE + n
Dl'a,ws specified voillme from actnal vial nurnher pIll';
specified llumher (defn.ldt no:=O).
Limits: 0,1 pl throllgh MAXINJVOLUM (for volllme) a.Tld °
I.hwugh IOn (for vial number).
xx DRAW ---ul FROM WASTE
Draws Specified volume from waAe--injection needle is
seated and rot.My val ve connects syri ngc to wast.e. -
r
Limits: 0.1 pI through MAXINJVOLUM (for volume).
xxDRAW..: ......C,tiIFROMAIR
Draws specifted vohune from air-injection needle is up
(not sca.t.ed) and rotary val ve connects syringe to open
end (air).
-
"---.

xxEjEg'I'i-7t"~iINTD. SAMPLE. + n·
Ejects specified vohime into a.ctu~l vial number pIns
specified nnmber (default n:::O).

4-22 Parameter Keys

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01/21/2004 09:48 8153511974

Limits: 0.1 pI through MAXINJVDLUM (for volume) and 0

through 100 (for vial number).

;i'··E:.J~S]W·[~f.tf~~d¥'NT5"'"'9A~T§!:ii";:';···'·
EJects speCifi~d ~o'lum~into;a,ste--=i~~jection needle is
seated and rotary valve connects syringe to waste.
Limits: 0.1 pI through MAX!NJVDLUM (for volume).
·'k:k:'.EjE:C±i;HgffGl••·.·. iNTb".AI~.i··· .,
Ejects specified volume into air·-injection needle is up
(not sea,ted) a,nd rotary valve connects syringe to open
cnd (air).
Limits: 0.1 t'J through MAXINJVOLUM (for volume).

~~'M±XJ..22--ul CYCLES.. 1
Moves specified volume back and furth in sample loop.
Mixing is done with injector needle up (mix in loop).
This mixing is repea,ted according to the number of
cycles you specify.
Limits: 0.1 pI through MAXINJVDLUM (for volume) and 1
through 999 ([or r.yc1es).
XiMIXV'::::'::'~ul CYCLES 1
Moves specified volume back and forth in sample loop.
Mixing is done with injector needJr in the vial la.st
ilt specj·rted in injector program (mix in vial). This nlixing
is repeated a.ccordi ng to the number of cycles YOll
specify.
Limits: 0.1 ,ul through MAXINJVDLUM (for volume) and 1
through 999 (for cycles).
£xWA 11'9.0 mih
;," .. "".. ,.... ,:,,',,
"" ",,""""'." ',.",,, ,,'.' '"
.
Waits specified time and then continues with next lille ,in
injector program.
xJC.Jin5~;S12;·.~~11i~t··d·····.··MAIrJPASS····.····
Moves rotary va.lve to injector loop (needle is seated a.,nd
solvent flows through needle).

Parameter Keys 4-23

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~~::1~~~~i~$~~~yt~~~~~:~"g¥t~~~~~§~i0&,£,i,i:,~\i
Moves rotary valve to bypass position, isolating the
reaction capilla.ry. This command is used as a last entry,
following INJECT a.nd is used when a micro-oven is
installed. This command must follow INJECT if injector
program contains further lines.

'g¥,j~'~~~ii~~~~lJi,§~~~:i;~1~@1£~;~~)':ii!'U;;:l%i
Controls the EVENT contacts El through E4 on the re<'l,r
panel of the HP 1090 and the column switching valve cs.
.--
Limits: 0 for open or inactive; 1 for closed or activej '2
for leave in current setting.
See "( E.t Cont )" a,ud "( Column Switch 1" for detail5.

U~'Cq,,~
down moves rotary valve
to injection mode: sample loop is reconnected to the
solven,t flow; the sample is flushed out of the injector and
.-'--
into the col umn.
After injection, the HP 1090:
• Creates start signal at REMOTE CONTROL
connector;
• Starts time program;
• Creates signal at DCD connector according to vial
number.

•
'-

,.,-
4-24 ' Parameter Keys
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7
Auxiliary Functions

The a.uxiliary functions are for configuration and

trou bleshooting and are not part of the cnrrent method.
You access the auxiliary funcl,ions by pressing: (Shift!
(§ill (Ent.r J, then moving to the desired function with
the 0 and fIl keys. The following exa.mple shows the
auxilia.fY functions of an HI' 1090 with: •
• DR5 or PV5 solvent delivery sy:;tem .
• Auto-injector.
RESEt.<I~JE2ToRi'. .
MAXFLOW©P = 0
MAXINJVOLUM= 25
TIME = HH:MM:SS ; 00:00:00
ABORT
RESET (will delete all methods!)
If your UP 1090 has a built-in filter photometric
detector, you will see an additional auxiliary function:
DETSIGNAL = 0

If your fIP 1090 has a built-in or stand-alone diode-arra,y

detector (connected through the Hp·IB commun.ication
interface), you will see a.n additional auxiliary function:
DAD TEST

Auxiliary Functions 7-1

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',---
.'~
., ,"'.

~4
RESET INJECTOR
RESET INJE:CTOR sets auto-injector and auto-sampler in ~
correct starting position. -'
Limits: None-to reset, press (Ente,). ~'
~ -
Use RESET INJECTOR after an injector error has occurred.
I
']
.~
...-

MAXFLOW@P
.-_H :I .... I

I
MAXFLOWlOP sets a pressure limit for solvent delivery
i;ystem when troublcshootin"g, see your III' 1090 guide
books. If li mit reached, solvent delivery system continues
to pump solvent but reduces flow.
-.- .....-

I
'
I

-- I

--- I
-.- I
Limits: 0 for function not used or 1 through 400 bar.
I

I
MAXINJVOLUM MAXINJVOLUM"'25

MAXINJVOLUM sets the maximl.tm injection volume of

metering device. •
I I

Li rni ts: 2.5 or 250 /ll

A 25 I'll syringe is fitted as standard, 250 Ii,] syringp is
-I
.," I

-, !,
;,I,

avaoila,ble as an accessory.

- , ,

-- I.
•-
. ...... ,

7-2 Auxiliary Functions

• -- , I
, 01/21/2004 09:48 8153511974 PRIMUS PAGE 50

TIME
Time sets the current time (24-hour clock!).
Limits: Time in hours (HH), minutes (MM), and seconds
(33). Setting time clears status logbook, see Cha.pter 8.

ABORT
ABORT resets the HP 1090 for operation.

Limits: None-to reset, press [Enter ). The current

anaJysis is sl:opped, auto-injector and a,uto-sampler are
reset. All methods a.re retained. The solvent delivery
system, column-compartment and filter-photometric
detector and./or diode-ana.y detector reta,in their status.
Any diode-array detector spectrum plots in progress are
aborted.
If your HP 1090 has an TNET communication interface
.'" and is connected through HP-IL to a,n HF :3392A
Integra.tor, the messa,ges LOOP DOWN and LOOP UP may be
printed on the integrator.
•,
,I
RESET R.ESET,{wiiIdei~1:eali methods l)
I, RE3ET resets the HP 1090 for operation.

Limits: None-to reset, press (Ente?). The current

•
, analysis is stopped, auto-injector and auto-sampler
are reset. All methods, sequence table a.nd logbook
are cleared.. The time is changed to 00:00:00. The
I solvent delivery system is turned off and initialized. The
column-compartment and filter-photometric detector
I

Auxiliary Functions 7-3