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Environ Earth Sci (2016) 75:828

DOI 10.1007/s12665-016-5649-7

ORIGINAL ARTICLE

Spatial evolution and fractal characteristics of natural fractures


in marbles under uniaxial compression loading based
on the source location technology of acoustic emission
Jianliang Pei1 • Wenping Fei1 • Jianfeng Liu1

Received: 17 November 2015 / Accepted: 16 April 2016 / Published online: 5 May 2016
Ó Springer-Verlag Berlin Heidelberg 2016

Abstract Natural fractures are widely distributed in rocks. concentrate around the intersection points of fractures. The
Generally, there are four types of natural fractures, i.e., case with mixed natural fractures has the most complex AE
single, parallel, intersected and mixed. Uniaxial compres- event distribution than those of the others. However, it is
sion tests on naturally fractured marble samples, taken still not difficult to determine the internal weakness parts
from the transportation tunnels of Jinpin II hydropower and stress field based on the spatial AE event distribution.
station in southwestern China, are conducted with a The fractal dimension of the spatial AE event distribution,
MTS815 rock mechanics testing system. The acoustic capable of describing the mechanical behavior and struc-
emission (AE) events are monitored by PCI-II AE system. tural damage of rock materials, is estimated by a newly
The spatial evolutions of different natural fractures have developed analysis method. The parameters of AE events
been successfully located and tracked according to the AE for different types of natural fractures, such as AE accu-
ringing number. Experimental results indicate that the mulative value, amplitude and absolute energy, are statis-
failure process of fractured marble is locally progressive. tically analyzed. The present testing scheme can be an
The AE event accumulation is strongly related to the initial step toward further development of in situ micro-
loading process and stress redistribution in rock. For the seismic monitoring techniques for complex fractures.
former two types, i.e., single and parallel natural fractures, Moreover, the obtained experimental and analytical results
the spatial AE event distributions in marbles are relatively can facilitate the investigation on rock mass failure and
simpler than those of the other two. The corresponding instability mechanism.
strong AE event numbers (with ringing number greater
than 20) increase with the compressive stress along the Keywords Rock mechanics  Acoustic emission  Natural
naturally fractured surfaces when the stress is low. When fracture  Rock failure  Crack propagation process
the compressive stress is close to the failure strength of the
rock, AE events first appear around the natural fracture tip,
then spread along the final rupture direction. For the marble Introduction
containing intersected natural fractures, strong AE events
are approximately uniformly distributed at the initial stage Acoustic emission (AE) is a kind of physical phenomenon
of the compression test. Later, the AE events increase when which often happens among brittle materials, such as rocks,
the compressive stress gets higher continuously, and then under internal or external forces. The elastic energies of
such materials will be released immediately, causing
transient elastic waves due to the internal deformation and
& Wenping Fei crack propagation. As an accompanying phenomenon of a
wpfei@scu.edu.cn rock failure process, AE contains full information about
1
internal deformation characters and mechanical behaviors
State Key Laboratory of Hydraulics and Mountain River
of the material (Kranz 1983; Lockner 1993).
Engineering, School of Water Resources and Hydropower,
Sichuan University, No. 24, South Section 1, Yihuan Road, AE technique is one of the nondestructive testing tech-
Chengdu 610065, China niques which can obtain information about the crack

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828 Page 2 of 15 Environ Earth Sci (2016) 75:828

propagation and abrupt failure of the structure. Thus, AE in granite samples with different prefabricated cracks.
technique is helpful in identifying crack development in Vidya Sagar and Raghu Prasad (2013) presented an
rocks, predicting the failure process of rock and the experimental study on variation in acoustic emission
occurrence of earthquake. Since the AE events exist in the parameters during cracking in reinforced concrete beams
internal structure of compressed rocks, the corresponding subjected to incremental cyclic loading in laboratory con-
AE monitoring technologies have been widely applied in ditions. Haeri et al. (2013) carried out the uniaxial com-
evaluations of original ground stress, earthquake sequence, pression experiments on rock-like Brazilian disk samples
microcracking mechanism and stability of rock mass containing a single flaw, and identified different crack
(Hardy 1972; Katsuyama 1997). types, which can be applied to further study crack coales-
Researches on the AE spatial source location started cence and failure mode. Zhou et al. (2014) conducted
from late 1960s. Mogi (1968) first investigated the two- experiments on rock-like materials containing multiple
dimensional (2D) AE source location of granite with man-made flaws and demonstrated different crack propa-
bending deformations. Scholz (1968) obtained the spatial gation types in detail. Liu et al. (2015) studied the rect-
locations of the AE events of brittle rocks under uniaxial angular rock-like samples containing two parallel
compression through six AE monitoring sensors. Taking preexisting flaws under uniaxial compression experimen-
the benefits of multi-channel and high-speed data acquisi- tally and evaluated the influence of the flaws on crack
tion systems and the improvement of AE monitoring growth.
equipments, researches on spatial source location of AE Fractal method is a kind of useful mathematical tool to
events have been widely conducted. Using an AE moni- explain some natural phenomena and describe microseismic
toring method, Jansen et al. (1999) studied the full process activities in rock engineering (Nanjo and Nagahama 2004;
of a rock failure, including three-dimensional (3D) Wang et al. 2009). Hirata et al. (1987) studied the AE events
microcrack damage accumulation, crack nucleation and of fine-grained Oshima granodiorites under creep deforma-
macrocrack propagation. Lei et al. (2004) quantified the tions (the surrounding pressure was 40 MPa) and obtained
AE temporal–spatial distributions of the rocks containing the fractal characteristics of the spatial distribution of the AE
fractured surfaces or joints under triaxial compression by sources. Yuan and Li (2009) analyzed the fractal properties
using a 32-channel waveform recording system. In order to of the spatial AE event distributions during the failure pro-
investigate the fractural instability mechanism, Zhao et al. cess of rock specimens. Experiments on bedded rock salt
(2008a, b) conducted experiments to study the spatial AE specimens under uniaxial compression and indirect tension
event distributions during the rock failure processes with were conducted by our recent work (Xie et al. 2011), and a
different rock samples based on AE monitoring and column covering method was proposed to analyze the fractal
locating technologies. Li et al. (2010) acquired the changes property of the spatial AE event distribution during the rock
in spatial correction length of AE events during fracture damage and failure process. Based on the newly developed
process of granite and marble specimens subjected to method (Xie et al. 2011), Pei et al. (2010) studied the fractal
uniaxial compression, which showed that 3D source dimension of the spatial AE event distribution in granites
locating of AE events can directly reflect the process of under uniaxial compression.
initiation, propagation and evolution of microcracks and Fractured rock mass widely exists in geotechnical
the stress redistribution in the specimens. Georg et al. engineering. AE technique has been widely applied to
(2010) observed the formation of borehole breakouts in study the behaviors of cracks in recent years. It plays an
tests performed on sandstone samples using advanced important role in monitoring the propagation and evolution
acoustic emission analysis and microstructure of cracks in materials. Existing research works focus more
observations. on samples with precut and man-made flaws. However,
Considering that the rock is a kind of complex and natural fractures in original rock are much more complex
multi-phase composite materials, Sobolev et al. (1987) than precut or man-made ones. Very few experimental
proposed a concrete fault model to study the spatial AE studies have been performed on naturally fractured rocks,
event distribution in rock samples containing geological especially those containing different fracturing combina-
discontinuities. Jiang et al. (2003) designed a collinear tions. The present work explores the dynamic spatial
disconnected faults physical model by a prefabricating evolution process of natural fractures with various spatial
crack technique and preliminarily studied the temporal– combination modes in fractured marble samples under
spatial evolution of fracture events on mesoscale gabbro uniaxial compression by using the AE locating technology.
samples under a biaxial compression. Based on an AE The newly developed column covering method is used to
locating technology, Zhao et al. (2007) studied the 3D analyze the fractal characteristics of the spatial AE event
spatial evolution process of inner microcracks (from ges- distributions of marble samples. The natural fractures and
tation, growing, propagation and nucleation to perforation) their propagation processes are characterized exactly based

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Environ Earth Sci (2016) 75:828 Page 3 of 15 828

on the collected AE ringing numbers. The research results Step 5: Calculating the coordinates of AE source (xs, ys,
are helpful for further investigation on the fracture mech- zs) when X2 reaches its minimum.
anism of rock mass and improvement of monitoring
accuracy of rock mass instability.
According to the above method, only one set of rea-
Column covering fractal model of AE
sonable coordinates of AE source will be obtained if
enough sensors are introduced and uniformly arranged. In
Rupture occurs in loaded rocks. During a rupture process,
this test, 8 sensors are settled uniformly around each
each AE event corresponds to a rupture surface or volume.
sample, in order to improve the accuracy of AE spatial
Proved by experiments, AE sequence of rock material
location estimation and to a certain extent reduce the effect
follows a fractal distribution not only in time domain, but
of AE amplitude attenuation.
also in spatial domain.
For the cylindrical rock specimens, column covering
The source location theory of AE events method is more appropriate. With the method, the spatial
distribution characteristics of AE events are apt to be
Spatial fractal dimension of AE research can be used to described exactly. Due to the shape of rock specimens, it is
determine the spatial locations of AE events. Several AE very convenient for the method to calculate the fractal
sensors, usually exhibited as an array, are arranged on dimension of the spatial AE event distribution according to
some certain fixed points. Through measuring the arrival the coordinates of AE events. Therefore, the method can be
time difference of an event to sensors, the locations of AE used to determine the critical value of rock failure, predict
events are determined by the following formula: the rock bursts and evaluate the stability of rock mass.
qffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffi When spatially distributed AE events are covered by a
ðxi  xs Þ2 þ ðyi  ys Þ2 þ ðzi  zs Þ2 ¼ vðti  tÞ ð1Þ small sphere with radius r (Fig. 1), the relationship
between the AE event number within the sphere and the
where (xi, yi, zi) is the coordinates of the i th sensor to
radius is Xie (1996):
receive the P-wave; (xs, ys, zs) is coordinates of AE source;
v is the velocity of P-wave; t is the exact time when an MðrÞ / r 3 ð5Þ
event originated; ti is the receiving time of the i th sensor.
According to the basic fractal theory, the relationship
There are four unknown variables in formula (1) for a
between the AE event number and the radius can be
single sensor. Therefore, the spatial location of AE source
expressed as:
can be determined by four noncoplanar sensors.
Defining the relative time difference between the i th MðrÞ / Cr D ð6Þ
and the first sensors to receive the P-wave.
where C is a material constant. Equation (6) can be further
Dti ¼ ti  t1 ð2Þ expressed as:
qffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffi
Dti ¼ ðxi  xs Þ2 þ ðyi  ys Þ2 þ ðzi  zs Þ2
qffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffi
 ðx1  xs Þ2 þ ðy1  ys Þ2 þ ðz1  zs Þ2 =v ð3Þ

If there have more than 4 sensors, the final location


coordinates of AE source is determined by the following
steps:
Step 1: Calculating the actual observed time difference
Dti,obs by the actual arrival time of the receiving sensors
according to formula (2).
Step 2: Calculating the coordinates of AE source (xs, ys,
zs) by four noncoplanar sensors according to formula (1).
Step 3: Calculating the calculated time difference Dti,calc
according to formula (3).
Step 4: For each potential AE source coordinates,
P
calculating X2 = (Dti,obs - Dti,calc)2.
Fig. 1 Spherical and column covering methods. a Spherical cover-
ing. b Column covering

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log MðrÞ ¼ log C þ D log r ð7Þ Experimental techniques


Similarly, when the AE events are covered by a column Rock sample preparation
with radius r and height h, the relationship between the AE
event number and the radius of the column is: Rock samples used in experiment are naturally fractured
MðrÞ / r 2 h ð8Þ marble samples taken from the transportation tunnels of
Jinpin II hydropower station in southwestern China. The
Note that the height–radius ratio C1 is a constant, Eq. (8) buried depth of the rock samples is about 2010 m.
can be expressed as: Interbedding marbles from Yantang Formation are taken
MðrÞ / C1 r 3 ð9Þ from transportation tunnel A, and the stake number is
AK12?621, while marbles from Baishan Formation are
Therefore, the fractal expression of the spatial AE event taken from transportation tunnel B, and the stake
distribution by column covering method is: number is BK12?028.7. The rock sample preparation
log MðrÞ ¼ log C þ log C1 þ D log r ð10Þ strictly follows related standards and regulations. The
size of sample is /50 mm 9 100 mm
For a given radius r, a value of M(r) can be obtained through
(diameter 9 height).
Eq. (10). In a double logarithmic coordinate system, point
According to the spatial geometrical distribution of
series (log r, log M(r)) corresponding to given radii can be
natural fractures in rock samples, these natural fractures are
portrayed. The spatial AE event distribution has fractal char-
statistically divided into four basic types, i.e., single, par-
acteristic in the range of a given scale if those points approx-
allel, intersected and mixed types. The interface of each
imately distribute along a straight line. The slope of the line is
naturally fractured surface in marble samples is closed
the exact fractal dimension of the spatial AE event distribution.
tightly and filled with calcite crystal. Representative frac-
tured marble samples of the four types chosen in the
experiment are demonstrated in Fig. 2. The corresponding
structural characteristics of naturally fractured marble
samples are illustrated in Table 1. The series number of the
samples consists of two parts. The first part represents the
group number of the interbedding marble, i.e., group A
from Yantang Formation and B from Baishan Formation.
Group A can be further divided into two subgroups. They
are Group A1 under axial compression with direction
parallel to the bedding surface and A2 with that vertical to
the bedding surface. The letter of the second part is
abbreviation of the basic type of fractured samples, i.e., S
for simple, P for parallel, I for intersected and M for mixed.
The number of the second part represents experiment
Fig. 2 Basic type of naturally fractured rock samples. a Single. number of each group.
b Parallel. c Intersected. d Mixed

Table 1 Structural
No. b Dip g Connection t Volume Type Formation
characteristics of naturally
angle/° rate/% density/(10-2 mm-1)
fractured rock samples
B-S2 69.9 88.0 1.22 Single Baishan
A1-P2 71.5 100.0 0.87 Parallel Yantang
71.1 54.0 1.22
51.0 59.9 0.70
A2-I3 67.6 62.2 1.17 Intersected Yantang
44.7 17.3 0.24
A1-M2 80.1 55.4 1.44 Mixed Yantang
80.0 46.4 1.14
22.3 59.4 0.65
For mixed type of fractured rock, only three main cracks are listed

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Environ Earth Sci (2016) 75:828 Page 5 of 15 828

According to the results of X-ray diffraction on min-


eral components, the main components of interbedding
marbles from Yantang Formation are 54.7 % of calcite
and 45.3 % of dolomite. The lithology of marbles from
Baishan Formation is more homogeneous, mainly con-
sisting 91 % of dolomite, only 8.6 % of calcite and 0.4 %
of mica.

Test procedure and method

The uniaxial compression experiments with AE measure-


ment are carried out by a MTS815 rock testing system in
Fig. 3 Layout of probes and AE sensors. (1) Circumferential
Sichuan University. The maximum axial load is 4600 kN. extensometer. (2) Axial extensometer. (3) AE sensor. (4) Strain
The axial measuring range of uniaxial extensometer is meter. (5) PTFE slice
-2.5 to 12.5 mm, while the transverse travelling range is
-4 to ?4 mm, and that along the axial direction is A group of 8 probes is introduced to collect data to
0–100 mm (±50 mm). Measuring accuracy of each testing obtain higher test accuracy for 3D source locating of AE
sensor is 0.5 % of the indicating value. More details about events in naturally fractured samples. PTFE slices are
the testing system can be found in Refs. Yuan and Li placed on both sides of the sample to eliminate the friction
(2009), Xie et al. (2011). effects. Vaseline is used between AE sensor and sample for
Considering that marble samples selected for the better contacting. Both the sample and AE sensors are fixed
experiments are hard and brittle, sudden failure of the rock by clamps. The sensors are calibrated before the experi-
samples may damage the sensor. The loading rate is set as ments. Installation of AE probes and arrangement of sen-
20 kN/min and controlled by axial load and circumferential sors are shown in Fig. 3.
deformation when the samples are under elastic and plastic Many factors affect the accurate location of AE source,
deformations, respectively. The circumferential deforma- such as identification error of arrival time, nonuniformity
tion rate is controlled as 0.02 and 0.04 mm/min before and of wave velocity, nonpoint source characteristic of AE,
after the compressive strength, respectively. accuracy of observation system. Therefore, it is difficult to
At the same time, because the rock sample is selected determine the exact location of AE source and estimate the
from a deep underground tunnel, the characteristic of rock source location error. For this reason, manual trigger tests
burst during excavation is obvious. In order to obtain the by breaking pencil leads on the surface of the samples are
rock burst proneness index of the rock sample [the corre- executed before actual tests. The manual trigger testing
sponding results can be found in Ref. Xie et al. (2011)], an results on the rock sample A1-M2 are listed in Table 2,
unloading process is included in the whole testing process, which show us that the absolute errors of AE source
i.e., when the loading stress is about 0.8 rc, the testing location are all within 5 mm.
force will be unloaded to 0.05 rc, then reloaded to the end
of the test.
Test results and discussion
AE system
Marble sample containing a single fracture
A 3D source locating and real-time monitoring AE system
with twelve channels made by PAC can work together with The testing results by AE technology on marble sample
the loading system. Due to the advantages of high pro- containing a single fracture are shown in Fig. 4. The
cessing speed, low noise, low threshold value and reliable relationship curves between axial compression stress and
stability, noise can be minimized by using PCI-II board. In time, AE event cumulative counts and time are shown in
addition, the system can count and store AE events auto- Fig. 4a. The spatial AE event distributions under different
matically to realize real-time monitoring and 3D source stresses are shown in Fig. 4b. Considering that AE ringing
locating by using 18-bit A/D conversion technology. number can reflect the strength and frequency of AE events
External parameters, such as load, temperature, stress, to some extent, energy of AE events with higher ringing
strain, can be processed synchronously. For the AE system, number is generally higher. In this paper, AE events with
its main amplifier is set as 40 dB, the threshold value is ringing number more than the average (default value = 20)
45 dB, the frequency of sensor is 200 kHz, and sampling are thus defined as strong AE events. Failure characteristics
frequency is 40 MHz.

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Table 2 AE location results by manual trigger testing on the rock sample A1-M2
No. Actual location of AE source (x, y, z)/mm Location of AE source obtained by sensors (x0 , y0 , z0 )/mm Absolute errors
Dx/mm Dy/mm Dz/mm

1 (17.96, 17.96, 25) (17.74, 17.35, 26.04) -0.22 -0.61 1.04


2 (-17.96, 17.96, 25) (-18.98, 18.71, 24.07) -1.02 0.75 -0.93
3 (-17.96, -17.96, 25) (-16.73, -19.02, 23.27) 1.23 -1.06 -1.73
4 (17.96, -17.96, 25) (15.25, -15.83, 21.50) -2.71 2.13 -3.50
5 (25.40, 0, 50) (22.96, 2.95, 53.42) -2.44 2.95 3.42
6 (0, 25.40, 50) (1.69, 22.93, 54.47) 1.69 -2.47 4.47
7 (-25.40, 0, 50) (-23.37, -2.24, 47.32) 2.03 -2.24 -2.68
8 (0, -25.40, 50) (-1.48, -23.29, 52.42) -1.48 2.11 2.42
9 (17.96, 17.96, 75) (18.67, 20.63, 78.30) 0.71 2.67 3.30
10 (-17.96, 17.96, 75) (-15.86, 17.25, 77.13) 2.10 -0.71 2.13
11 (-17.96, -17.96, 75) (-19.70, -15.75, 71.18) -1.74 2.21 -3.82
12 (17.96, -17.96, 75) (19.66, -16.14, 77.39) 1.70 1.82 2.39
The origin of Cartesian coordinate system is the bottom center of the cylindrical sample, and z-axis is vertical upward

Fig. 5 AE spatial evolutions in a typical sample with a single natural


fracture using a constant stress increment (Dr = 0.2rc). a AE events.
b Strong AE events

Fig. 4 Testing results of typical sample with single natural fracture Naturally fractured surface and final failure surface are
under uniaxial compression. a Relationships between axial stress, AE
cumulative events and time. b Spatial AE event distributions under depicted in red lines, as shown in Figs. 4 and 5. Turning
various stress level points exist in naturally fractured surface with average dip
angle of 69.9°. The maximum connection rate reaches
of a sample cannot be fully captured by cumulative AE 88.0 % along final failure surface in those cases. Therefore, a
events. Therefore, AE events should be divided into several large number of AE events happen in sample B-S2 at the
stages according to a specific stress increment (in the initial compacting stage under a low stress, as demonstrated
present work, the increment Dr = 0.2 rc, where rc is the in Fig. 4a. At this stage, the relationship curve between the
compressive strength of rock). accumulative ringing number and time rises sharply. When

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Environ Earth Sci (2016) 75:828 Page 7 of 15 828

the loading stress reaches 0.2 rc, the total amount of AE loaded large block with the fact that the strong AE events and
events is 2793, which is much larger than that of intact rock the periphery of defect are nearly in the same plane.
samples. The AE events of intact rock samples under the
same loading stress are approximately uniformly distributed. Marble sample containing parallel fractures
Although AE events in Fig. 4b are distributed in large area
within the rock sample, some AE events tend to centralize The marble sample A1-P2 contains three parallel naturally
around the naturally fractured surface due to the inconsistent fractured surfaces, which are numbered as , ` and ´.
deformation on both sides of the failure surface. After The geometric parameters of the sample are shown in
ignoring the AE events with ringing number less than 20, it is Table 1. Testing results and the spatial evolutions of AE
found that strong AE events (totally 353) are mainly con- events with a fixed stress increment Dr = 0.2 rc are shown
centrated around the turning point of the failure surface, as in Figs. 6 and 7, respectively.
shown in Fig. 5b. Densely distributed AE events represent The compressive strength of sample A1-P2 is relatively
significant stress concentration, squeezing and friction low (rc = 25.3 MPa). When the stress reaches 0.2 rc, a total
actions near the fracture. After the initial compacting stage, of 209 AE events are detected. The spatial AE event distri-
the natural fracture is nearly closed. The AE event number bution is more homogeneous than that of the marble sample
under applied load from 0.2 rc to 0.4 rc is decreased largely containing a single fracture. Sixty-six strong AE events are
(totally 964), especially the strong AE events (only 29), as distributed at the end of No. ` fractured surface, indicating
shown in Fig. 5b. that stress concentration appears even under a low stress level.
The strong AE events distribute almost along the fractured If the loading continues, AE events increase and mainly
surface. When the load is between 0.4 rc and 0.6 rc, the AE distribute between Nos.  and ` fractured surfaces on the
event number increases to 2483, forming an AE event gath- top of the rock sample, while strong AE events are still
ering area connecting both ends along the naturally fractured concentrated around No. ` fractured surface with a ten-
surface in rock sample (Fig. 5). The area is largely consistent dency of stretching downwards along the fractured surface.
with the final failure path of the rock sample. As shown in During the subsequent stage, when the stress is less than
Fig. 4a, the total lasting time is 521.5 s (from 460.7 to 982.2 s) the previous maximum stress, internal AE events increase
when the applied load increases from 0.55 rc to 0.6 rc. During significantly. The phenomenon is quite different from that
this time, the natural fracture begins to crack and propagate of a single fracture.
toward the end of the rock sample. Due to the propagation and
evolution of the crack, the stress redistribution occurs in the
rock sample, which results in several drops of axial com-
pression. During this stage, the AE event number is up to 1956,
with 193 strong AE events. Spatial evolution of AE events
shows that strong AE events are distributed homogeneously
along the both sides of naturally fractured surface, indicating a
relative sliding tendency between the both surfaces within the
rock sample. Due to the relatively simple spatial distribution
of single natural fracture, the number and spatial distribution
of AE events has a good corresponding relation with the ini-
tiation and propagation of the natural fracture.
As shown in Fig. 4a, stress decreases sharply after the
stress reaches 48.6 MPa (0.65 rc). The rock sample is then
further cut into two independent blocks by the failure surface
of the sample according to the spatial AE event evolution.
The failure of the compressing sample is locally progressive.
The small blocks are apt to slide under a continue load,
resulting in a zigzag-shaped cycled loading–unloading
curve. Due to the loading capacity of the large block (con-
taining defects), the curve is upward with oscillations. The
oscillating process can be well explained by that the spatial
location of AE events mainly concentrated in the top region
Fig. 6 Testing results on a typical sample with parallel natural
of the large block in the following stress stage. Moreover, AE fractures under uniaxial compression loading. a Relationships
events start to appear at the bottom of the rock sample as between axial stress, AE cumulative events and time. b Spatial AE
shown in Fig. 5. Vertical failure surface is expected in the event distributions under various stress level

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Fig. 7 AE spatial evolutions in a typical sample with parallel natural


fractures using a constant stress increment (Dr = 0.2rc). a AE
events. b Strong AE events Fig. 8 Testing results on a typical sample with intersected natural
fractures under uniaxial compression loading. a Relationships
between axial stress, AE cumulative events and time. b Spatial AE
Further analysis on spatial evolution of natural fractures event distributions under various stress level
shows that the spatial AE event distribution of rock sample
A1-P2 is roughly uniform in each stress stage among twisting and No. ` fractured surface has a moderate dip
0.2–0.8 rc. However, strong AE events are distributed angle. When stress reaches 0.2 rc (21.2 MPa), there are
around No. ` fractured surface during the whole process. 164 AE events distributed uniformly in rock sample.
When the stress increases continuously, AE events tend to Strong AE events have no concentration tendency, indi-
concentrate on the fractured surfaces, obviously revealing cating that the stress at this stage is too low to cause sliding
the progressive characteristic of local damages. During the or dislocation of the fractured surface.
stress stage of 0.8–1.0 rc, strong AE events increase During the stress stage of 0.2–0.4 rc, AE events are
rapidly and concentrate at the bottom of the rock sample influenced by unloading. At other stages, increasing speed
with complex stress field. Axial splitting failure is found on of AE events keeps unaltered approximately. The spatial
the rock sample along the end of No. ` fractured surface. AE event distribution is relatively uniform. There are sel-
At the same time, a vertical splitting crack appears along dom large cracks caused by sliding and dislocation of
the outcropping trace of No. ´ fractured surface at the naturally fractured surfaces. During the stress stage of
bottom of the rock sample. 0.4–0.6 rc, most AE events appear around both the ends of
the rock sample. Strong AE events concentrate along No.
Marble sample containing intersected fractures ` fractured surface, indicating that this fractured surface
tends to be dislocated gradually.
Two intersected naturally fractured surfaces are contained Influenced by independent tiny blocks cut by two frac-
in the rock sample A2-I3, which are defined as No.  tured surfaces along the lateral surface of the rock sample,
(upper) and No. ` (lower) fractured surfaces, respectively. strong AE events around crossing area of both the fractured
The average dip angle of No.  fractured surface is rather surfaces increase several times during the stress stage of
steep (67.6°), while that for No. ` fractured surface is 0.6–0.8 rc. Then AE events spread toward the bottom of
moderate (44.7°). The corresponding testing results and the rock sample, which indicates an obvious stress con-
spatial evolutions of AE events are shown in Figs. 8 and 9, centration in this area and a probability of vertical failure.
respectively. Within the stress stage of 0.8–1.0 rc, cracks continue to
Only few AE events happen in rock sample A2-I3 at the propagate toward both the ends of the rock sample, forming
initial compacting stage since No.  fractured surface is a large failure surface. Due to the energy absorption by the

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Environ Earth Sci (2016) 75:828 Page 9 of 15 828

Fig. 9 AE spatial evolutions in a typical sample with intersected


natural fractures using constant stress increment (Dr = 0.2rc). a AE
events. b Strong AE events Fig. 10 Testing results on a typical sample with mixed natural
fractures under uniaxial compression loading. a Relationships
between axial stress, AE cumulative events and time. b Spatial AE
event distributions under various stress level
rock sample and intensive distribution of cracks around the
defected side surface, several vertical splitting failure sur-
faces are observed until final sudden failure happens. There stress stage of 0.2–0.4 rc, strong AE events begin to con-
is a strong correlation between the location of failure sur- centrate within the transition region of naturally fractured
face and the spatial AE event distribution. surfaces with high connectivity rate. In other words, stress
At the post-peak stage, the tiny blocks cut by Nos.  and concentration in this area is remarkable.
` fractured surfaces are extruded out, causing sudden Due to the complex mechanical behaviors in rock
increase of circumferential deformation. Therefore, the sample containing mixed fractures during the stress stage
circumferential deformation sensors placed in the middle of 0.4–0.8 rc, AE events do not appear along one of the
part of rock sample are directly influenced. The test naturally fractured surfaces. On the contrary, the AE event
machine is then protected automatically. When the axial distribution regions overlap mutually and spread all
stress declines linearly to 0 MPa, the test is over, as shown around. Moreover, strong AE events distribute uniformly,
in Fig. 8a. indicating that stress field becomes more uniform in rock
sample with the increase in the stress. When the rock
Marble sample containing mixed fractures sample is close to failure (0.8–1.0 rc), AE events distribute
in all locations of the entire rock sample. Strong AE events
Marble sample A1-M3 contains several crisscrossing nat- increase sharply to 749, which is 4.43 times of that during
urally fractured surfaces. The corresponding testing results the stress stage of 0.6–0.8 rc.
and spatial evolutions of AE events under uniaxial com-
pression are shown in Figs. 10 and 11, respectively. Failure mode and propagation of natural fractures
The uniaxial compressive strength of rock sample A1-
M2 is 31.85 MPa. AE events increase continuously during The final failure modes of rock samples containing dif-
the whole loading stages. Moreover, ascending gradient of ferent types of natural fractures are shown in Fig. 12.
the AE event curve remains unchanged approximately. Vertical rupture planes appear on the external surface of
When the loading stress reaches 0.2 rc, AE events (to- rock sample, indicating that the failure of marble samples
tally 321) are mainly distributed within two local regions in is exhibited as axial splitting.
the rock sample. But strong AE events (totally 59) mainly As shown in Fig. 4, the crack of rock sample B-S2
distribute along the weakest fractured surface. Within the propagates along the rupture plane and marches toward the

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828 Page 10 of 15 Environ Earth Sci (2016) 75:828

an obvious twist plane, while that of No. ` is clearly in a


stepwise shape. As shown in Fig. 8, lots of AE events are
triggered by the dislocation and sliding of No. ` fracture
surface during the stress stage of 0.2–0.8 rc. Then AE
events gradually concentrate around the intersecting line of
the both fracture surfaces, where the corresponding
cracking plane starts and propagates toward both the ends
of the rock sample. The final failure mode of the rock
sample is: Firstly, a tiny block is cut by the two fracture
surfaces; crack then happens along the intersecting line and
propagates toward the top of rock sample; finally, the axial
tensile-shear cracking through the sample appears due to
the sliding of No. ` fracture surface.
Rock sample A1-M3 is cut vertically and horizontally
by several naturally fractured surfaces with irregular
shapes. The final failure modes include the tensile-shear
failure caused by fracture propagation and opening failure
of fracture plane caused by tension and compression.
Several opening cracks even appear on the top of rock
sample during the stress adjustment.
Fig. 11 AE spatial evolutions in a typical sample with mixed natural AE event ringing number can roughly represent the
fractures using a constant stress increment (Dr = 0.2rc). a AE
events. b Strong AE events
energy of AE signal. According to the spatial evolutions of
strong AE events in the single and parallel types of rock
samples, AE event ringing number agrees well with the
sample bottom due to the tensile shear induced by the location and spatial evolutions of naturally fractured sur-
dislocation of curved natural fracture surface. faces. For intersected type of rock samples, AE event
Though there are three parallel natural fractures in rock ringing number is still relevant to naturally fractured sur-
sample A1-P2, its fractures distribution is still rather sim- faces. Although mixed type of rock samples are much
ple. As shown in Fig. 6, No. ` fracture surface is preferred. complex, the weak parts and corresponding stress field
Stress concentration occurs around both the ends of the variation can also be easily determined.
sample after the dislocation of the fracture surface. Despite
of the final convergence occurring between No. ` fracture Fractal characteristics of the spatial AE event
surface and No. ´, the fracture propagates along axial distributions in naturally fractured marbles
direction and breaks through the sample due to the tensile
shear. Nevertheless, the final rupture trace of No. ´ frac- According to the column covering method, for a given
ture surface has a tendency of closing to No. `, as shown radius r of a column within the rock sample, the AE event
in Figs. 6 and 7. Unfortunately, limited to the number and value M(r) covered by the column can be obtained, as
size of the rock samples, merging of parallel natural frac- shown in Fig. 1b. The logarithmic relation curve between
tures is not found in this test. M(r) and r can be plotted and fitted by a straight line.
Marble sample A2-I2 contains two coarse naturally According to Eq. (10), the fractal dimension Ds of the
fractured surfaces. The surface trace of No.  is shown as spatial AE event distribution is the slope of the fitted line.

Fig. 12 Uniaxial compression


failure mode of marble samples
with different natural fractures.
a Single sample. b Parallel
sample. c Intersected sample.
d Mixed sample

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Environ Earth Sci (2016) 75:828 Page 11 of 15 828

4 closure of microcracks and the dislocation of microstruc-


tural planes is also relatively uniform. The fractal dimen-
sion Ds of the spatial AE event distribution is relatively
3.5 large (nearly 3.0), with little change. When the test con-
tinues, new microcracks emerge gradually in the rock
sample if the axial compressive stress reaches about
y axis / lg M (r )

3 0.6–0.7 rc. At the same time, the spatial fractal dimension


y =2.214x +0.917, R ²=0.983
y =2.274x +0.765, R ²=0.984
y =2.230x +0.776, R ²=0.981
decreases obviously. New cracks then propagate and con-
y =2.164x +0.800, R ²=0.977
y =2.241x +0.665, R ²=0.973 centrate. Microcracks also gradually gather together around
2.5 y =2.337x +0.455, R ²=0.965 0.1σc
0.2σc
the initial defects. Ds steadily drops and reaches the min-
y =2.600x +0.064, R ²=0.967
0.3σc
y= 2.551x +0.086, R ²=0.954
0.4σc
imum, while the loading stress reaches the maximum. For
y =2.519x +0.052, R ²=0.965
0.5σc
0.6σc
intact loaded rock sample, both the deformation and spatial
2 0.7σc
0.8σc
distribution of microcracks are uniform at the preliminary
0.9σc
y =2.537x -0.463, R ²=0.972
1.0σc
stage. When deformation is large enough, the evolution of
inner microcracks is self similar.
1.5
0.7 0.8 0.9 1 1.1 1.2 1.3 1.4 Comparing with intact rock, the evolution of the spatial
x axis / lg r AE event distribution in naturally fractured rock is differ-
ent, which is related to the rock material damaged by
Fig. 13 Fitting lines between log M(r) and lg r of the rock sample
B-S2 under various alternative stress levels fractures. As shown in Fig. 14, AE events emerge around
the naturally fractured surfaces at the stress stage of
0–20 % rc. At the same time, Ds in fractured sample are
obviously smaller than that in the intact one, which is
related to the irregular stress distribution caused by the
fractures. Moreover, Ds in single and parallel fractured
samples are smaller than those in the intersected and mixed
fractured samples. It indicates that the inner stress fields of
the two former samples are more heterogeneous than those
of the latter ones. With the closure of naturally fractured
surfaces, the corresponding normal stress (about 0.2–0.5
rc) and friction induced by compacted fractured surfaces
increase. The deformation compatibility between the both
sides of the naturally fractured surface is improved. The
inner stress fields in fractured samples become more uni-
Fig. 14 Fractal dimension of rock samples under various alternative form. Therefore, Ds rise a little. When the shear stress
stress levels between the naturally fractured surfaces is large enough to
resist the friction, the inner stress of fractured samples is
relatively uniform. AE events concentrate around the tip or
The relation curve of log M(r) * log r and corresponding turning point of fractured surfaces. After that, Ds begin to
Ds of the rock sample B-S2 under different compressive decline continuously with the inner damage accumulation
stress levels are shown in Fig. 13. of each sample. Cracks with large scale distributed along
Similarly, the fractal dimension of the spatial AE event the main fracture surface gradually increases. When the
distribution in other naturally fractured rock samples under loading stress reaches the maximum, the main fracture
various alternative stress levels can also be determined, as surface propagates through the sample, and Ds decrease to
shown in Fig. 14. Considering that AE events are caused the minimum.
by microcracks propagation in the rock, the spatial evolu- Therefore, Ds can exactly represent the complexity of
tion of AE event distribution is related to various defects in the spatial AE event distribution. Ds can also reflect uni-
the rock material. formity of inner stress. So, it can be a new index to describe
As shown in Fig. 14, the fractal dimension of AE event the mechanical and damage behaviors of rock materials.
distribution in intact rock sample decreases continuously During the whole test, Ds of intact rock sample keep
during the whole test. At the preliminary loading stage decreasing, which means that the distribution of microc-
(with the stress level about 0–0.5 rc), the initial microde- racks in the rock sample is transferred from ‘‘scattered’’ to
fects distribute uniformly in the intact rock sample. ‘‘concentrated.’’ Nevertheless, Ds of fractured rock sample
Therefore, the spatial AE event distribution caused by the rise first and then fall, demonstrating the ability of self-

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organizing for the structure of fractured rock. A small lithology of Baishan Formation, a large number of AE
fractal dimension means the occurrence of a strong fracture events occur even under a low stress level (r \ 0.2 rc). At
event. Rising of Ds can be used to evaluate the integrity of the time of rock failure, the AE accumulative value,
rock structure. Declining of Ds can act as a simple but amplitude and absolute energy of sample form Baishan
valuable criterion to predict the cracking or rupture. Formation are 1.6–2.6, 2.1–3.3 and 9–20 times of that of
samples from Yantang Formation, respectively. When the
Statistical analysis of AE events for different types stress r is about 0.57 rc, the AE events increase steeply in
of natural fractures rock sample B-S2. Whether accumulative amplitude or
absolute energy curve presents an obvious step, which
For different spatial combination types of natural fractures, means the natural fracture begins to crack and propagate.
the spatial distributions and fractal characteristics of AE Under this stress level, crack propagation and stress
events are different. The parameters of AE events for adjustment result in a large number of AE events.
single, parallel, intersected and mixed natural fractures, Compared with the rock sample B-S2 from Baishan
such as AE accumulative value, amplitude and absolute Formation, less AE events occur under a low stress level
energy, are statistically analyzed as follows. (r \ 0.2 rc) in three rock samples from Yantang Forma-
The accumulative value and amplitude curves of AE tion. For the rock sample A1-M2 with mixed natural
events under different stress levels are shown in Fig. 15, fractures, due to its widespread natural fractures and poor
and the absolute energy curves of AE events under dif- integrity, the AE accumulative value, amplitude and
ferent stress levels are shown in Fig. 16. It is necessary to absolute energy are larger than that of rock samples with
point out that the AE event parameters after the failure of parallel or intersected fractures when r \ 0.8 rc. As shown
rock samples are not included in Figs. 15 and 16. in Fig. 5, the AE accumulative value and amplitude curves
As shown in Figs. 15 and 16, the AE event parameter increase gently with the stress level. Even during unload-
curves (accumulative value, amplitude and absolute ing–reloading test in order to obtain the rock burst prone-
energy) of naturally fractured rock samples under uniaxial ness index, the AE events increase only a little. As shown
compression loading are well consistent. For rock sample in Fig. 16, when the axial compression stress is up to 0.3
B-S2 with single natural fracture, influenced by the rc, the accumulative absolute energy curve of rock sample

Fig. 15 Accumulative value (a)


and amplitude curves of AE
events under different stress
levels. a AE accumulative
value. b AE accumulative Crack propagation and stress adjustment
amplitude

Unloading and reloading test

67% Crack propagation and stress adjustment

(b)

Crack propagation and stress adjustment

Unloading and reloading test

67% Crack propagation and stress adjustment

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Environ Earth Sci (2016) 75:828 Page 13 of 15 828

Fig. 16 Absolute energy curves (a)


of AE events under different
stress levels. a Sample from
Baishan Formation. b Samples
from Yantang Formation

Crack propagation and stress adjustment

(b)

Unloading and reloading test

67% Crack propagation and stress adjustment

A1-M2 with mixed natural fractures appears several step- As shown in Fig. 15, the AE accumulative value and
like slight increases. The unaxial compression test on rock amplitude curves of the rock sample A2-I3 with intersected
sample with poor integrity shows that the stress adjustment natural fractures can be divided into two parts. When
is not obvious due to their interaction among several nat- r \ 0.67 rc, the AE accumulative value and amplitude
ural fractures. Therefore, the AE accumulative value, curves increase slowly. But when r [ 0.67 rc, these curves
amplitude and absolute energy of rock sample A1-M2 with increase steeply with the increase of axial compressive
mixed natural fractures are hardly affected by the axial stress. As shown in Fig. 16, when r [ 0.67 rc, the AE
compression stress level. accumulative absolute energy curve appears several step-
Compared with the rock samples with mixed and like slight increase, whose gradient is steeper than that of
intersected natural fractures, the spatial distribution of the rock sample A1-M2 with mixed natural fractures. In
parallel natural fractures in rock sample A1-P2 is relatively general, the stress filed of the rock sample with intersected
simple. Also, the AE accumulative value, amplitude and natural fractures under uniaxial compression test is rela-
absolute energy curves present obvious steps. Because of a tively uniform, and its stress adjustment is more obvious
bit more natural fractures, the uniaxial compressive than that of rock sample with mixed natural fractures.
strength is the minimum among all the samples, only So, the AE accumulative value and corresponding sta-
25.3 MPa (as shown in Fig. 6). Therefore, when r \ 0.85 tistical parameters are different for rock samples with dif-
rc, the AE accumulative value and other parameters of ferent types of natural factures. Because the spatial
rock sample A1-P2 with parallel fractures are less than that distributions of natural fractures in the rock sample B-S2
of rock samples with mixed and intersected natural frac- with simple natural fracture and A1-P2 with parallel natural
tures. When r is about 0.85 rc, influenced by not only the fractures are relatively simple, stress concentration phe-
sharp stress adjustment around the end of the fractures, but nomenon around the ending of the natural fractures happens
also cracks initiation and propagation, the AE accumula- more obviously. Their AE accumulative value, amplitude
tive value, amplitude and absolute energy curves increase and absolute energy curves demonstrate prominent step-like
steeply. The parameters are 2.4, 3.3 and 5.4 times of that of characteristics. A large number of AE events will occur
the stage of r \ 0.85 rc, respectively. during the stage of crake initiation and propagation. The AE

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828 Page 14 of 15 Environ Earth Sci (2016) 75:828

accumulative value and amplitude curves of the rock sample compared with the other fractures with the increase of
A1-M2 with mixed natural fractures increase slowly or compressive stress.
remain unchanged, while the AE accumulative value and 5. Ds can exactly represent the complexity of the spatial
amplitude curves of the rock sample A2-I3 with intersected AE event distribution and further describe the mechan-
natural fractures present two parts with obviously different ical and damage behavior of rock materials. The
gradients before and after r = 0.67 rc. The gradient is gentle decline of Ds indicates the transformation of cracks
under a low stress level and steep under a high stress level. distribution from ‘‘scattered’’ to ‘‘concentrated’’ for
Furthermore, the stress fields in the rock sample A2-I3 with intact rock sample. The Ds rise first and then fall for all
intersected natural fractures and A1-M2 with mixed natural fractured rocks, demonstrating the self-organizing
fractures are relatively uniform. Although the AE accumu- ability of ‘‘concentrated–scattered–concentrated’’ dur-
lative absolute energy curves also demonstrate step-like ing the failure process.
characteristics, both the accumulative absolute energy under 6. The statistical laws are different for rock samples with
the maximum compression stress and the height of steps are different types of natural fractures. For the rock
less than those of other two types of rock samples. samples with single or parallel natural fractures, the
AE accumulative value, amplitude and absolute energy
curves present obvious step-like characteristics with
the increase of axial compression stress. These
Conclusions parameters are very large while failure. For the rock
samples with intersected or mixed natural fractures, the
Uniaxial compression experiments with AE monitoring on axial compression level has less impact on the AE
marble samples containing natural fractures were carried events and their corresponding parameters. The corre-
out. Comparison and analysis work was conducted to sponding accumulative curves of the rock sample with
investigate the characteristics of the AE events and fracture mixed natural fractures basically remain unchanged.
spatial evolution within marble samples containing various Compared with the stage of low stress level, the
types of natural fractures. The results revealed the crack corresponding accumulative curves of rock sample
propagation processes can be exactly described by the with intersected natural fractures at the stage of high
spatial evolutions of AE events. The main conclusions of stress level have steeper gradients.
this study are:
1. Failures of naturally fractured marble samples are Acknowledgments The work is supported by the China National
locally progressive under compression loads. Internal Natural Science Fund (CSNF) under Nos. 51120145001, 51374148,
natural fissures cause a large number of AE events 51379139 and 51409179. The authors wish to offer their gratitude and
regards to everyone who has been a part and support to this project in
even under a low stress level. According to the spatial all means.
location of strong AE events, the dynamic propagation
and evolution of natural fractures in rock samples can
be traced. References
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