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a r t i c l e i n f o a b s t r a c t
Article history: In this study, uniaxial and triaxial compression acoustic emission (AE) tests were implemented to inves-
Received 8 April 2021 tigate the AE effect and failure characteristics of sandstone under different confining pressures (r3). The
Received in revised form 23 June 2021 evolution of AE parameters in the rock failure process and fracture fractal dimension characteristics after
Accepted 20 August 2021
failure were analyzed. The results revealed that the activity of the AE signal is strongly related to r3. The
Available online 30 August 2021
evolution of the Ib value can be divided into the I-fluctuation, II-stability, and III-decrease stages. In the
first stage, the Ib value of the AE was relatively high, and the AE energy was low. Then, the Ib value tended
Keywords:
to be stable; however, the fluctuation amplitude decreased, and the AE energy rapidly increased. In the
Sandstone
Acoustic emission
stage of decrease, the AE energy sharply increased before the load approached the peak value, and the Ib
Ib value value significantly decreased and dropped to the lowest point before the peak value. As r3 increased, the
Failure mode rock’s failure mode changed from tensile failure to shear failure and became more coordinated. As the
Fractal dimension confining pressure increased, the shape dimension decreased, and the order degree of rock failure
increased. The confining pressure exerted a certain control effect on the rock failure.
Ó 2021 Published by Elsevier B.V. on behalf of China University of Mining & Technology. This is an open
access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).
https://doi.org/10.1016/j.ijmst.2021.08.003
2095-2686/Ó 2021 Published by Elsevier B.V. on behalf of China University of Mining & Technology.
This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).
Z. Huang, Q. Gu, Y. Wu et al. International Journal of Mining Science and Technology 31 (2021) 963–974
Table 1
Physical and mechanical properties of the sandstones.
Specimen Diameter Height Mass Density P-wave Confining pressure, Elastic Deformation Peak Peak stress
No. (mm) (mm) (g) (g/cm3) velocity (m/s) r3 (MPa) modulus (GPa) modulus (GPa) strain (%) (MPa)
S-1 49.92 100.20 439.68 2.24 1996 2 80.60 61.80 1.72 106.12
S-2 50.20 100.20 436.62 2.22 2861 71.37 69.47 1.55 107.46
S-3 50.38 100.18 440.12 2.24 2457 77.35 55.67 1.48 82.28
S-4 49.90 100.20 436.88 2.22 2611 75.16 59.61 1.39 82.61
S-5 50.00 98.02 430.11 2.19 2346 4 84.87 73.92 1.49 110.29
S-6 50.06 97.66 427.98 2.18 2681 86.35 72.42 1.75 126.89
S-7 50.02 98.00 434.60 2.21 2466 84.15 73.20 1.77 129.70
S-8 49.82 98.40 437.83 2.23 2096 76.27 67.57 1.86 125.40
S-9 50.08 100.04 440.47 2.24 1955 6 85.60 73.98 1.74 128.40
S-10 50.40 100.20 438.27 2.23 2361
S-11 50.20 100.00 437.64 2.23 1990 89.19 74.04 1.97 145.94
S-12 49.90 100.30 439.18 2.23 2558 78.90 69.74 2.17 151.06
S-13 50.00 100.20 440.25 2.24 2378 8 86.33 84.57 1.86 157.18
S-14 50.10 100.20 440.43 2.24 2469 88.67 71.49 2.08 148.43
S-15 49.34 100.10 429.60 2.18 2381 79.83 72.14 2.28 164.23
S-16 49.36 100.02 427.50 2.17 1927
S-17 50.00 100.04 440.41 2.24 1903 0 122.00 72.90 0.82 59.95
S-18 49.16 99.48 434.16 2.21 2004 173.67 107.04 0.77 82.87
S-19 49.70 100.30 437.28 2.22 2463 164.88 93.80 0.81 76.35
S-20 50.00 100.00 433.51 2.20 2016 182.13 85.05 0.92 78.49
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Fig. 4. Stress–strain curves of rock specimens under triaxial compression (r1 is the peak stress of the rock under differentconfining pressures, and r3 is the test confining
pressure of rock).
Fig. 5. Relationships between elastic and deformation moduli and confining pressure.
coefficient exceeding 0.99. The fitted equation for the elastic mod- the elastic modulus. The increase of the confining pressure densi-
ulus is Et = 1.9064r3 + 72.6556 Et ¼ 19064r3 þ 72:6556and the fit- fied the internal fracture and pore structure of the rock, which
ted correlation coefficient R2 = 0.9959. The mean elastic modulus of made the preliminary densification stage increasingly unobvious
the yellow sandstone increased from 76.5 to 87.6 GPa with the and thus caused the increase of the deformation modulus. The test
increase of the test confining pressure from 2 to 8 MPa. Impor- results are essentially consistent with the test results obtained by
tantly, the effect of r3 on Et is related to the internal structure of Zhao et al. [30].
the rock. For the yellow sandstone, the increase of the confining The peak strain is the strain value corresponding to the time at
pressure contributed to the densification of internal defects, such which the rock stress reached its peak. Fig. 6 shows the relation-
as pores and fissures inside the rock sample, to a certain extent, ship between the peak strain of the sandstone and r3. As shown
and the limiting effect of the confining pressure increased the stiff- in Fig. 6, the law of peak strain variation is essentially consistent
ness of the rock to a certain extent. Thus, the elastic modulus of the with the law governing the variation of the modulus of elasticity
rock increased accordingly. and deformation modulus with the variation of the confining pres-
Fig. 5b shows the relationship between Es and r3. Similar to the sure. As the confining pressure increased, the peak strain exhibited
relationship between Et and r3, as r3 increased, the rock’s Es exhib- an increasing trend, the peak strain of the rock under the uniaxial
ited an increasing trend, with a faster increase occurring in the 2-MPa condition was elevated, and the average peak strain value
range of 2–4 MPa and a slower increase was occurring in the range ranged from 0.83 under the uniaxial condition to 1.53 under the
of 4–8 MPa, which indicates a tendency toward stabilization. 2-MPa condition. Then, as the test confining pressure increased
The fitting equation of the deformation modulus is Es = 0. (0–8 MPa), the peak strain slowed down as the test envelope pres-
2614r23 + 4.8728r3 + 53.3732 and the fitting correlation coefficient sure increased (0–8 MPa) and the peak strain only increased by
R2 = 0.9257. The average deformation modulus of the yellow sand- 0.05, from 6 to 8 MPa. The fitting formula of the yellow sandstone
stone increased from 62.5 to 75.6 GPa when r3 increased from 2 to peak strain and confining pressure is e1 = 0.02r23 +
8 MPa. The effect of r3 on Es is essentially consistent with that of 0.3059r3 + 0.8796, and the fitting correlation coefficient
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Fig. 6. Relationship between the peak strain and confining pressure of sandstones. 3.2.1. Acoustic emission event rate
The AE frequency, amplitude, and other related parameters of
crack development and expansion in rocks at different stages of
stress damage have obvious differences, and the AE characteristics
at different stages contain important information on the rock dam-
age process. In this study, the AE characteristics during the damage
of rocks under different confining pressures were analyzed using
the AE event rate and cumulative AE event number, which reflect
the frequency and total amount of AE signals, respectively. The
evolution of the AE event rate and cumulative AE events in sand-
stone under different confining pressures is shown in Fig. 8.
It can be found from Fig. 8 that the stress curves and AE counts
of the rocks under different confining pressures exhibit similar
variation characteristics. At the early stage of loading, only a few
of AE events occurred in the initial densification stage of the rocks
under different confining pressures, because the AE signal at the
early stage of loading was mainly generated by the closure and
densification process of the initial cracks inside the rocks, which
released a small amount of transient elastic waves under the action
of compression and friction. However, the overall decreasing trend
of the AE event rate with the increase of r3 indicates the direct
Fig. 7. Relationship between peak strength of sandstones and confining pressure.
relationship of the AE event rate with r3. As the axial load
increased, the compaction stage ended and the linear elastic stage
began to form. At this stage, the stress–strain curve was approxi-
R2 = 0.9758. This indicates that the confining pressure had an obvi-
mately linear, and the rock specimen mainly underwent elastic
ous controlling effect on the deformation damage. As the confining
deformation. The external load was not sufficient for forming
pressure increased, the rock deformation exhibited the characteris-
new microcracks in the rock specimen, the AE event rate and the
tics of transformation from the brittle state to plastic failure, and
cumulative number of AE events were in a relatively stable state,
the rock damage is strongly influenced by the stress state of the
and the cumulative number of AE events exhibited a relatively
rock.
stable period of increase. After the end of the linear elastic stage,
Nowadays, the Mohr-Coulomb (MC) strength criterion is one of
the yellow sandstone began to enter the plastic deformation stage.
the most widely used strength criteria. According to the MC, the
At this stage, the new microcracks inside the sample began to
rock damage process is the result of the joint action of normal
increase and eventually penetrated and connected to each other
stress and shear stresses. Thus, the MC can describe the damage
to form macroscopic cracks as the number and size of microcracks
characteristics of brittle, plastic materials based on the assumption
increased. Additionally, the overall rock rupture exhibited an
that the intermediate principal stress does not affect the strength
unstable development stage wherein the AE activity entered the
of the rock, depending on whether the rock damage occurs when
active stage, and the AE event rate and cumulative AE events
the normal stress and shear stresses reach their ultimate value at
appeared to surge (Fig. 8). Before the axial load approached the
an interface within the rock [31]. The maximum shear force carried
peak, the AE event rate surged to the peak, as shown in Fig. 8. By
by the rock can be determined by the cohesion and internal friction
the time that the axial load peaked, the rock sample had com-
angle; the MC criterion is expressed as follows:
pletely lost its bearing capacity, and the AE event rate appeared
sm ¼ c þ rtanu ð1Þ to increase to a certain extent. Overall, the AE activity of rocks in
the initial pressure-density stage and the elastic stage was rela-
where sm is the shear stress of rock material; c the cohesive force of tively calm, and the AE signal was mainly generated by the closure
the rock material; r the normal stress at the breaking surface of the of the initial fissure and the sprouting of a small number of micro-
rock material; and u the internal friction angle of the rock material. cracks. The active degree of the AE signal in the initial pressure-
In this study, the strength characteristics of sandstone under density stage is strongly related to r3, and the increase in r3 sup-
different confining pressures were analyzed based on the MC, pressed the active degree of the AE signal in the initial pressure-
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Fig. 8. Variation of stress and AE events of sandstone under different confining pressures.
density stage to a certain extent. In the plastic stage, microfrac- and means that the rock material is in the macrofracture expansion
tures within the rock sprouted, developed, expanded, and con- state. When the b value stably changes with a small change ampli-
nected to produce macroscopic cracks [32–34]. Additionally, the tude, this shows that the specimen is in a more stable and progres-
AE activity entered the active stage, and the AE event rate and sive fracture expansion state. However, because the b value was
cumulative AE events appeared to surge. originally defined in seismology, various application problems
emerge when it is directly introduced into the AE signals of engi-
neering materials. Hence, Shiotani et al. [38] proposed an ‘‘im-
3.2.2. Analysis of Ib value of acoustic emission proved b value”, namely, the Ib value, which is more applicable
In 1944, Gutenberg et al. [35] analyzed the pattern between the to the analysis of the AE signals of rock and concrete materials.
earthquake frequency and the earthquake magnitude and pro- The formula for calculating the Ib value is expressed as follows:
posed the concept of using the value of the b parameter to describe
Z 1
the proportion of the focal dimension distribution. Since then, the b
nðaÞda ¼ b ð3Þ
value has been widely used as important prior information for 0
earthquakes by researchers in the field of seismic activity and haz-
ard assessment. The mechanism of the rock damage process under Z 1
stress is similar to that of earthquake occurrence, and the acoustic Nðw1 Þ ¼ Nðl a2 eÞ ¼ nðaÞda ð4Þ
la2 e
signal generated by rock damage is also defined as microseismic
activity. Therefore, Mogi [36] and Scholz [37] introduced b values Z 1
into the field of rock engineering based on AE monitoring technol- Nðw2 Þ ¼ Nðl þ a1 eÞ ¼ nðaÞda ð5Þ
ogy, and used the correlation between the magnitude of the AE sig- l þ a2 e
nal’s amplitude and the fracture scale to replace the earthquake
magnitude in the original calculation equation with the AE signal log10 Nðw1 Þ log10 Nðw2 Þ
Ib ¼ ð6Þ
amplitude. Thus, they investigated the change of the internal ða1 þ a2 Þe
microfracture scale during the force damage of rocks by consider-
ing the b value characteristics of AE. Generally, it is thought that where n(a) denotes the cumulative AE events about a; b a certain
the increase of the b value reflects an increase in the proportion number of AE events, where b in the range of 50–100 is considered
of small-scale events, which indicates the dominance of small- as a suitable value for fitting the Gutenburg-Richter formula [38];
scale fracture development and expansion within the rock material a1 and a2 the constants; l and e the statistical mean value and stan-
and means that the rock material is in the stable state of microfrac- dard deviation of amplitudes, respectively; w1 and w2 the sublayer
ture expansion. The decrease of the b value reflects an increase in and upper amplitudes, respectively; and N(w1) and N(w2) the cumu-
the proportion of large-scale events, which indicates the domi- lative number of the upper layer and sublayer amplitudes,
nance of large-scale fracture expansion within the rock material respectively.
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In this study, equal time intervals were used to calculate the AE to the calculation results obtained by Zhang et al. [39] for the AE b
Ib value of the damage process of the rock under different confin- value of rock under different confining pressures. The fluctuation of
ing pressures with 6 s as the time interval, according to the above the Ib value at the early stage of loading is strongly influenced by
Ib value calculation formula. The change law of the AE Ib value for the compaction effect of the confining pressure. Owing to the ini-
the damage process of yellow sandstone under different confining tial confining pressure, the microfractures inside the rock material
pressures is shown in Fig. 9. It can be seen from Fig. 9 that during appeared to undergo densification, and microfractures with a rela-
the stress damage of rock with r3, the Ib values exhibit a similar tively larger size were more likely to densify under the action of
variation law, which can be separated into three stages: I- the confining pressure. As the confining pressure increased, the
fluctuation, II-stability, and III-decrease. densification of the rock material by the confining pressure became
In the fluctuation stage (stage I), the AE Ib value fluctuated more significant, which in turn led to the larger fluctuation of the
upward and downward as the load increased. The range of upward Ib value at the early stage of loading as r3 increased.
and downward fluctuation was large, and the Ib maintained a rel- As the axial load increased, the Ib value entered the stable
atively high value mainly because the rock was in the crack com- stage (stage II) and gradually stabilized, the fluctuation range
pression and linear elastic stage at the beginning. Additionally, gradually decreased, and a relatively gentle stage appeared
the primary microcrack and pore structure inside the rock was in before the Ib value decreased. However, the AE energy appeared
the process of densification and closure, and the AE signal in this to rapidly increase, which reflects that the rock material was in a
stage was generated by the densification of the primary microcrack more stable progressive microfracture expansion state corre-
and pore structure, which corresponds to small-scale fracture sponding to the stage of stable crack expansion in the process
change. Hence, the Ib fluctuated upward and downward and had of rock force damage. At this stage, the internal fracture of the
a high value. In this stage, the AE energy was low, and had good rock was in the stable expansion state; therefore, the Ib value
synchronization with the fluctuation stage of the Ib value. The remained relatively stable and the AE energy was in the increas-
comparison of different confining pressure conditions reveals that ing stage.
there existed some variability in the change of the Ib value at the As the axial load kept increasing, the Ib value entered the
initial stage of loading. The stage without the Ib value appeared decreasing stage (stage III), and the AE energy exhibited an obvious
at the initial stage of loading under the 8-MPa condition, owing surge at this stage, which reflects the further development, connec-
to the effect of the higher r3. This produced the initial compression tion, and penetration of the small fissures that developed inside
density of the microfracture and pore structure inside the rock the rock toward forming larger fissures. At this stage, the AE signal
before loading, and resulted in the stage without the AE signal at was mainly generated by the expansion of larger fissures, which
the initial stage of loading, which was then used to obtain the cal- produced higher-energy AE, and the Ib value appeared to decrease.
culation results without the Ib value. As the confining pressure When the axial load approached closer to the peak intensity, the
increased, the AE Ib value exhibited more upward and downward fissures inside the rock material further expanded to form macro-
fluctuation, and the Ib value fluctuated in the range of 0.04–0.20 scopic penetration fissures, and the Ib value dropped to the
at 8 MPa, but remained within 0.04–0.12 at 2 MPa, which is similar minimum.
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After the test was completed, the rock specimens that had
deformed and became damaged under different confining pres-
sures were removed from the pressure chamber. The heat shrink
tube and sensors on the surface were removed, and the damaged
rock samples were processed and analyzed. To compare and inves-
tigate the differences in the rock rupture characteristics under con-
fining pressure and without confining pressure, a uniaxial
compression test (r3 of 0 MPa) was conducted on the yellow sand-
stone. The failure patterns of the rock specimens obtained under
different confining pressures are shown in Fig. 10. As can be seen,
when r3 was 0 MPa, the rock was mainly in the form of brittle ten-
sile damage, the rock surface exhibited multiple vertical penetra-
tion fissures, and the fissure surfaces at the middle of the
specimen were more densely distributed and intersected with each
other. The central fissure intersection exhibited a slight decrease,
the overall shape of the block was cut, the specimen fractured,
and the middle of the specimen exhibited certain dilatancy. When
r3 was 2 MPa, the crack density on the surface of the specimen was
significantly reduced, the cracks were mainly 3–5 through cracks,
and the specimen did not exhibit central dilation. When r3 was
4 MPa, the main fractures in the specimen consisted of a single
shear surface fracture and one vertical through the fracture, and
the middle of the vertical through fracture was connected to
several secondary fractures. When the confining pressure was Fig. 12. Grayscale image of the fracture surface of sandstones.
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Fig. 13. Relationship between lgN(A) and lgr of rocks under different confining pressures.
8 MPa, two single shear surfaces appeared on the surface of the shear surface further increased with respect to 6 MPa. As can be
specimen. The two shear surfaces penetrated each other, which seen, the uniaxial conditions of the sandstone were mainly domi-
divided the rock specimen into two parts, and the angle of the nated by brittle tensile damage. The main fractures were mainly
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Table 2
Summary of the value of the fitting parameters.
vertical through fractures, and the middle of the vertical fractures Table 2, it can be seen that the correlation coefficients calculated
was connected to several secondary fractures with an obvious cen- in the figure are higher than 0.98, which indicates that the fracture
tral dilation. As the confining pressure increased, the yellow sand- surfaces, which formed by the force damage of the sandstone
stone gradually exhibited typical shear damage, and the main under different surrounding pressures, have obvious fractal dimen-
fractures of the specimens formed gradually from single shear frac- sion characteristics.
tures. Additionally, the number and density of the fractures exhib- Fig. 14 presents the variation of the surface fractal dimension
ited a decreasing trend with r3, and the dip angle of the single (D) of the fractured rock samples under different confining pres-
shear fractures exhibited a small increase as the confining pressure sures. As can be seen, the fractal dimension of the fracture surface
increased. This is consistent with the results obtained by scholars fluctuated in the range of 1.35–1.42 with an average value of
such as Mogi [40]. approximately 1.39 at 0 MPa. At 2 MPa, D exhibited an obvious
decreasing trend with an average value of approximately 1.30. At
4.2. Fractal dimension characteristics of post-failure rocks 4 MPa, D fluctuated in the range of 1.25–1.30 with an average value
of 1.26. Compared with D at 0, 2, and 4 MPa, D at 6 and 8 MPa
The box-counting dimension is gradually becoming one of the decreased further. Therefore, within a certain confining pressure
main methods for calculating the fractal dimension, owing to its range, the fractal dimension of the damaged rock sample’s surface
benefit of being able to accurately and easily measure the fractal tended to decrease as r3 increased, and the calculated fractal
dimension of self-similar images [22]. The method of calculating dimension is essentially consistent with the macroscopic damage
the box-counting dimension entails covering the curves with frac- results and similar to the findings of Zhou et al. [41]. Because the
tal dimension characteristics consisting of squares (shapes) or fractal dimension is a parameter used to characterize the degree
boxes with different side lengths r. The number of boxes N(A) with of order and disorder of a nonlinear system, as the fractal dimen-
different side length r covering the curves with the fractal dimen- sion increases, the system’s degree of disorder increases. Similarly,
sion is recorded, and the slope of the (lgr, lgN(A)) distribution a smaller fractal dimension value indicates a higher degree of order
points is calculated from the relationship between Nr(A) and its in the system. Hence, it is understood that as r3 increases, the
corresponding squares (shapes) or boxes. Thus, the corresponding orderly degree of rock damage exhibits an increasing trend. That
fractal dimension was estimated, and the calculation formula is is, the confining pressure exerts a certain controlling effect on
given as follows: the rock damage pattern.
lgNðAÞ
D ¼ lim ð7Þ
r!0 lgr
where N(A) is the number of boxes in the fractal dimension; and r
the side length of the box.
First, a translucent copy paper (with the same size as the sur-
face of the specimen) was wrapped around the surface of the dam-
aged specimen, and a sketch pencil was used for tracing along the
fracture surface of the rock sample. Subsequently, a scanner was
used to scan the finished copy paper and convert the image of
the fracture morphology of the copy paper into a picture file
(Fig. 11a). Fig. 12 shows the gray-level image of the fracture surface
morphology of a typical rock sample. The image file was imported
into a MATLAB binarization program that was developed to con-
vert the fracture surface morphology image from a gray-level
image to a binary image, as presented in Fig. 11b, and the logical
data from the binarization process were converted into binary data
to be used in the calculation of the fractal dimension. Thus, the bin-
ary data of the fracture surface morphology were extracted. The
lgN(A)-lgr curves of various typical rock samples and the fitting
equations are shown in Fig. 13 and Table 2. The slope of the curve
is the fractal dimension of the fracture surface. From Fig. 13 and Fig. 14. Relationship between fractal dimension and different confining pressures.
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