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Theoretical and Applied Fracture Mechanics 124 (2023) 103750

Contents lists available at ScienceDirect

Theoretical and Applied Fracture Mechanics


journal homepage: www.elsevier.com/locate/tafmec

Experimental study on shear failure modes and acoustic emission


characteristics of rock-like materials containing embedded 3D flaw
Mingyang Teng, Jing Bi, Yu Zhao *, Chaolin Wang
College of Civil Engineering, Guizhou University, Guiyang, Guizhou, 550025, China
Guizhou Provincial Key Laboratory of Rock and Soil Mechanics and Engineering Safety, Guizhou University, Guiyang, Guizhou, 550025, China

A R T I C L E I N F O A B S T R A C T

Keywords: In nature, rock mass usually contains natural defects, which affect the mechanical properties of rock mass. At the
Fractured rock mass same time, the failure of rock mass is often accompanied by shear failure behavior. Therefore, it is great sig­
Shear strength nificance to monitor and predict the shear failure process of fractured rock mass in order to ensure the stability of
Crack propagation
structure and the safety of construction. In this study, a method for making rock-like samples containing
Acoustic emission characteristics
Kernel density estimation
embedded 3D flaw is proposed and a series of shear tests are carried out under different normal stresses. The test
results show that the complex shear stress-shear displacement curve can be divided into four stages. The shear
strength, residual strength and shear modulus of the specimens are affected by the flaw dip angle and normal
stress. The tensile failure mode is more likely to occur in low stress and small flaw angle specimens, while the
shear failure mode mainly occurs in high stress specimens. A sudden increase in AE counts, AE event rates, and a
sudden decrease in b-value to a minimum are usually precursors to rock failure. The RA/AF value can accurately
reflect the classification and development of rock tension shear cracks. Through the Kernel density estimation
(KDE) analysis on the distribution of AE events, the damage locations of rock-like in each stage are effectively
identified. The movement of the maximum density point is consistent with the rock crack propagation tendency,
almost following the uniform diffusion of the specimens from the middle to the end.

1. Introduction 3D pre-existing flaw is really difficult to be prefabricated in rock sam­


ples. Therefore, scholars at home and abroad spend a lot of time on the
With the increasingly exhausted of surface resources, deep under­ study of two-dimensional fractured rock mass and obtain lots of theo­
ground resources begin to attract the attention of researchers, so the retical basis [18-20]. From these articles, it is found that high pressure
study of rock mass is inevitable [1-3]. It is well known that most rock water jet and wire cutting technology are common methods to make
masses in nature have formed discontinuous structural planes of rock containing prefabricated fissures. The influences of different pre­
different types and scales under the joint action of complex environment fabricated fissures distribution, scale effect, number, size, shape and
and geological structure. These discontinuous structural planes usually crack angle on rock mass are studied [21-27]. However, the propagation
include faults, bedding, joints and fissures [4-10]. In practical engi­ of rocks containing embedded flaws has always been the focus of
neering, joint fissures usually exist in the rock slope and underground attention. There are non-penetrating flaws in most natural rock masses,
rock caverns (Fig. 1). When the fractured rock mass is subjected to which are generally defined as three-dimensional fissures. As early as
various external forces, shear failure behavior may occur, which seri­ 1963, Erdogan and Sih G.C. [28] made pioneering tests on three-
ously affects the stability of the rock slope and the surrounding rock dimensional cracks and put forward the hypothesis that the failure of
structure of the cave [11-13]. Therefore, it is great significance to study rock mass expanded along the direction of maximum stress action. It is
the mechanical characteristics and deformation characteristics of not convenient for the test and research because the on-site sampling
jointed and fractured rock mass, which can provide important reference cannot guarantee that there are flaws in the samples. Scholars use ce­
value for actual engineering construction [14,16,17]. ramics, gypsum, epoxy resin, cement mortar and other materials to
In the existing studies, perforating and semi-perforating pre­ make samples containing three-dimensional flaws, and research the
fabricated flaw are usually defined as two-dimensional flaw because the influence of fissure angle, number, rock bridge angle and spacing on the

* Corresponding author at: College of Civil Engineering, Guizhou University, Guiyang, Guizhou 550025, China.
E-mail address: zhaoyucivil@126.com (Y. Zhao).

https://doi.org/10.1016/j.tafmec.2023.103750
Received 23 September 2022; Received in revised form 9 December 2022; Accepted 2 January 2023
Available online 5 January 2023
0167-8442/© 2023 Elsevier Ltd. All rights reserved.
M. Teng et al. Theoretical and Applied Fracture Mechanics 124 (2023) 103750

deformation law and strength characteristics of rock mass under uni­ 2. Materials and methods
axial and triaxial test conditions [29-31]. Dyskin et al. [32] carried out
uniaxial compression tests on specimens containing three-dimensional 2.1. Specimens preparation
prefabrication fissure, and studied the influence of three-dimensional
fissure location and shape on crack propagation of the specimens. This study mainly carries out a series of shear tests on rock-like
Zhou et al. [33] studied the process of crack initiation, propagation and samples containing three-dimensional flaw, thus it is particularly
through failure of PMMA samples with three-dimensional cross fissures important to make the samples with flaw in this test. First, the prepared
under uniaxial compression. camphor pellet (C10H16O) is fixed inside the cube plastic mold with thin
In recent years, with the development of test monitoring technology, cotton thread, then the inside of the mold is coated with a release agent,
many scholars at home and abroad use acoustic emission (AE) tech­ and after the cement mortar formed by mixing standard sand, reference
nology to monitor the process of rock failure in real time [34-37]. Rock cement and water in a certain proportion (water: sand: cement =
in the shear process will occur up, convex shear, abrasion and other 1:3:0.48) is poured into the cube plastic mold. The poured molds are
phenomena. Acoustic emission real-time monitoring technology is placed in the room temperature for 24 h. Then the samples are placed in
similar to seismic monitoring, but much smaller in scale and higher in the constant temperature and humidity box (temperature 20 ± 1 ◦ C,
frequency. It is an effective means to study the formation of micro cracks relative humidity is 98 %) for 28 days after removing the molds, and
or the opening and closing movement of existing cracks [38-41]. When finally bake in the drying box at 50 ◦ C for 3 h, so as to remove the
studying the shear failure behavior of non-persistent jointed rocks, camphor pellet inside the test block. It is noted that the camphor pellet
Zhang et al. [19] used energy rate and b-value to evaluate the acoustic used in the test is solid at room temperature and easily sublimate when
emission characteristics of jointed rocks, and found that the acoustic heated. We take advantage of this property of the camphor pellet by
emission parameters could well reflect the failure mechanism of sam­ heating them to form gas that is then emitted through the pores of the
ples. Liu et al. [42] systematically analyzed the influence of strain rate sample, forming a complete three-dimensional flaw inside the sample.
on AE characteristic parameters, rock fracture characteristics and failure As shown in Fig. 2, after the sample containing flaw is cut by wire cut­
evolution. However, the acoustic emission characteristics of rock con­ ting, it is observed that the mothball inside the sample has been
taining embedded three-dimensional flaws in the process of completely volatilized, and a complete prefabricated flaw has been
compression-shear fracture are still unclear, which makes it difficult to formed, which has no impact on the periphery of the flaw.
determine and characterize the micro fracture type. In this paper, the term “flaw” is used to describe the artificial defect
To sum up, most of the existing studies focus on the through-joints, or fracture, while the term “crack” is used to describe new crack under
while the researches of rock masses containing 3D flaws mainly focus external load [43]. Fig. 3 shows the size of the sample (70 mm × 70 mm
on the mechanical properties of the specimens under uniaxial and × 70 mm) designed in this experiment, and the dimension of the pre-
triaxial compression tests. There are few researches on the failure of rock existing flaw is defined as follow: the length is 15 mm, the width is
mass containing three-dimensional embedded flaw under shear. It is about 10 mm, and the thickness is 2 mm. The design structural plane
inconsistent with the actual engineering, leading to inaccurate estima­ flaw dip angle θ is 0◦ , 30◦ , 45◦ , 60◦ , and 90◦ . A total of 24 samples are
tion of the actual rock strength, deformation and other characteristics,
and causing some hidden dangers of engineering safety. In this study, a
new method for making rock-like specimens containing three-
dimensional embedded flaw is presented. Cement mortar is used to
make samples with built-in three-dimensional flaw at different angles.
With the help of acoustic emission (AE) technology, the shear failure
characteristics of rock-like specimens under different flaw inclination
angles and different normal stresses are studied.

Fig. 2. Internal flaw of the sample.

Fig. 1. Fractured rock mass under two different working conditions. (a) High rocky slope; (b) Underground rock caverns.

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M. Teng et al. Theoretical and Applied Fracture Mechanics 124 (2023) 103750

Fig. 3. Geometric dimension of flaw angle and loading parameters.

prepared, including intact samples and 4 samples for each type of


inclination, and another group of samples are prepared under the same
conditions as backup.
It is found that the anisotropy of cement mortar samples is better
than that of other rock materials (gypsum, epoxy resin, PMMA, etc.), and
the physical and mechanical parameters are similar to those of sand­
stone (Table 1). At the same time, the shear stress-shear displacement
curve obtained by shear test under normal stress of 3 MPa (Fig. 4) is
consistent with the traditional curve, which can better represent the
mechanical properties of real sandstone. It is proved that the specimens
made of similar materials can further simulate the mechanical proper­
ties of the rocks with built-in flaws.

2.2. Test equipment and procedure

In this test, WDAJ-600 electro-hydraulic servo rock shear rheological


tester is used for mechanical loading (Fig. 5a). The testing machine is
composed of power system, loading system and servo control system. 0
The axial and tangential loading capacity is 600kN, and the loading
accuracy is 1 %. The maximum vertical and horizontal displacement is Fig. 4. Shear stress-shear displacement curve of intact rock-like sample (σ =
30 mm, and the loading accuracy is 0.001 m. To reduce the influence of 3 MPa).
the samples end, we use steel ball antifriction plate and petroleum jelly
to reduce friction, as shown in Fig. 5(c)-(d). The three-dimensional flaw
kHz. The positions of four Nano30 sensors on both sides of the sample
dip angle and normal stress are considered in the test. As shown in Fig. 3,
are shown in Fig. 6. ① and ③ are located at the coplanar diagonal, and
we consider the flaw dip angle of 0◦ , 30◦ , 45◦ , 60◦ , and 90◦ , and the
② and ④ are located at the opposite diagonal. The distance between the
normal stress σ is 1 MPa, 3 MPa, 5 MPa, and 7MP. In the shear test, the
probe and the sample boundary is 10 mm. When fixing the probe, the
axial load is first applied at the rate of 0.02kN/s, which remains un­
coupling agent is usually used to reduce the gap between the probe and
changed after loading to the target value σ and then horizontal load is
the contact surface, and has a transition effect to reduce the acoustic
started at the shear rate of 0.2 mm/min. According to the latest rec­
resistance difference between the sensor and the monitoring surface. At
ommended method of ISRM, the test is stopped when the shear
the same time, the shear cracking behavior of each sample is recorded by
displacement reaches about 10 % of the specimen length (70 mm) [45],
a high-speed high-definition camera with a resolution of 1920 × 1080
that is, the loading stops when the shear displacement reaches 7 mm.
and a frame rate of 100 fps.
An 8-channel PAC-AE win system is used to monitor the loading
failure process (Fig. 5b). The sampling frequency of AE system is set at 1
3. Experiment results
MHz and the preamplifier threshold is 40 dB. The acquisition parameters
HLT, HDT and PDT in the acoustic emission system are 300 µs, 200 µs
3.1. Shear stress-shear displacement curve
and 100 µs respectively. In order to reduce the impact of environment
and machine noise on AE system collection, the channel threshold is set
The shear stress-shear displacement curves of rock-like samples with
at 45 dB. The Nano30 sensor has a resonant frequency of 140 kHz and a
different 3D flaw dip angles under different normal stresses are shown in
sensitivity of 62 dB, and able to capture signal frequencies of 125–750

Table 1
Physical and mechanical parameters of the rock-like material and sandstone.
Density (g/cm3) Uniaxial compressive strength (MPa) Poisson’s ratio Cohesion Friction angle (◦ ) Wave Velocity
(MPa) (m/s)

Rock-like material 2.33 29.64 0.23 8.06 47.8 4060


Sandstone (zhuang 2.2–2.7 20–170 0.02–0.2 4–40 25–60 5500–3100
et al. [44])

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M. Teng et al. Theoretical and Applied Fracture Mechanics 124 (2023) 103750

Fig. 5. Test equipment. (a) Mechanical loading device and high-speed camera; (b) Control system; (c) Sample loading; (d) Anti-friction plate with steel balls.

sudden stress decrease at this stage, indicating that cracks may first
appear in samples with inclination angle θ = 45◦ at this phase. With
the continuous increase of shear stress, local cracks, called initial
cracks, appear on the sample surface, and the secondary cracks also
begin to expand rapidly (as shown in the BC section of Fig. 8). At this
stage, due to the initiation of secondary cracks inside the sample, the
energy at the flaw tip is released and the shear stress begins to
transfer to the rock element with relatively low strength. Macro­
scopically, the shear strength of specimen does not decrease with the
expansion of initial cracks and secondary cracks, but continues to
increase.
Unstable crack propagation stage before peak (BC): After the loading
Fig. 6. AE sensor placement. of AB segment, the shear strength enters the pre-peak unstable stage.
During this time, the strain has accumulated to a certain extent. With
Fig. 7. As can be seen from Fig. 7, the overall characteristics of the test the increase of shear stress, the crack expands and penetrates rapidly
result curves are similar, but they are different at each stage. Before at this stage and reaches the end of BC segment, which is the peak of
reaching the peak shear strength, the shear strength increases with the shear strength. In this stage, the curve can be divided into three
increasing shear displacement. After reaching the peak shear strength, types: (1) As shown in Fig. 7(a) (θ = 0◦ ), the stress curve is steep
the sudden decline mode of each sample is different. According to the before the peak value, and then the stress drops sharply, reflecting
test results and testing data, the shear displacement of the specimen that the crack of the sample expands rapidly and enters the next
when reaching the peak shear strength is generally 1–2.5 mm. However, stage; (2) Before the stress peak, it shows a downward concave
when θ = 45◦ , the shear displacement is in the range of 2.5–3 mm, and shape, and the stress drop is not obvious, as shown in Fig. 7(c)-(d),
these curves rise and fall steadily.7720965672465. reflecting the continuous crack propagation process of the sample;
As can be seen from Fig. 7, each stage of the shear stress-shear (3) The fracture of the curve before the stress peak indicates that the
displacement curve is very complex. Therefore, in order to reveal the sample has local fracture, resulting in the change of the direction or
complex shear fracture mechanism of the sample, taking the shear position of crack propagation and the change of failure mode.
stress-shear stress curve of the sample (θ = 30◦ ) in Fig. 7(a) as an Post peak residual stress stage (CD): In the samples with small
example, the curve and crack propagation characteristics of each phase normal stress (σ = 1 MPa and σ = 3 MPa), the energy of the samples
are as follows (as shown in Fig. 8): is released suddenly and the cracks spread through rapidly, resulting
in a sharp decrease of the peak stress. However, in the samples with
Pore compaction stage inside the sample (OA): At the initial stage of high normal stress (σ = 5 MPa and σ = 7 MPa), the peak stress de­
loading, the shear stress increases slowly and the curve shows an creases slowly and eventually trend to be stable due to the friction
inconspicuous concave shape. The micro pores between the coarse and occlusion of the section, and the hysteretic curve may appear, as
and fine aggregates inside the sample are compacted, and the in­ shown in the θ = 0◦ curve in Fig. 7(b).
ternal prefabricated flaw begins to be deformed and produce primary
cracks.
3.2. Variation law of mechanical parameters of rock-like specimens
Approximate linear elastic stage (AB): In this test, constant
displacement loading is adopted in shear direction. With the increase
It can be seen from Fig. 9(a) that under the action of different normal
of shear displacement, the shear stress increases rapidly and the
stresses, the variation characteristics of shear strength with flaw incli­
slope of curve reaches the maximum. However, unlike other com­
nation are basically similar. Generally, the shear strength of the same
plete rock curves, it is not completely linear deformation. In partic­
normal stress specimens minish first and then increase with the increase
ular, it can be found from Fig. 7 that all the curves for θ = 45◦ show a
of flaw inclination. Especially when σ = 5 MPa, the shear strength of the

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M. Teng et al. Theoretical and Applied Fracture Mechanics 124 (2023) 103750

Fig. 7. Shear stress-shear displacement curves of rocks containing flaw under different normal stresses. (a) σ = 1 MPa; (b) σ = 3 MPa; (c) σ = 5 MPa; (d) σ = 7 MPa.

strength with flaw angle and normal stress is shown in Fig. 9(b). It can be
seen from Fig. 9(b) that when σ = 1 MPa, the flaw angle varies from 0◦ to
90◦ , and the residual shear strength changes little and can be ignored.
When σ = 7 MPa, the residual shear strength firstly increases, then de­
creases and then increases with the increase of inclination angle, and
reaches the maximum at θ = 90◦ . That is to say, when the sample is
subjected to high normal stress, dip angle has a great influence on the
residual shear strength. Through the observation of Table 2, it is found
that the residual shear strength increases with the increase of normal
stress. When θ = 0◦ , the increase of residual shear strength is the min­
imum with the increase of normal stress; when θ = 90◦ , the increase of
residual shear strength from 1 MPa to 7 MPa is the maximum; and
compared with other conditions, θ = 90◦ , the fluctuation of each stage is
the maximum. Based on the analysis of Fig. 9(a)-(b) and Table 2, under
low stress condition, the residual shear stress of rock-like samples after
failure are also larger because the internal friction force and bite force of
rocks are larger than those under low stress, which can be visually
characterized by the percentage of residual shear strength. At the same
time, under the action of the same normal stress, the residual shear
strength of rock-like samples is different with the influence of different
angles, and the gradient of residual shear strength is relatively large at
Fig. 8. Shear stress-shear displacement curve division and crack propagation.
different angles.
The corresponding shear displacement when the specimen reaches
sample first increases, then decreases and then increases with the the peak shear strength is called the peak shear displacement. Fig. 9(c)
increasing flaw inclination angle. When the flaw inclination angle in­ shows the variation law of the peak shear displacement of fissured rock
creases from 0◦ to 90◦ , the overall shear strength under the same normal samples under different constant normal stresses. There are two laws of
force is basically the same. Interestingly when σ = 1 MPa, the shear peak shear displacement between different normal stress with the
strength reaches the minimum at θ = 60◦ , and the shear strength reaches change of flaw inclination angle. When σ = 1 MPa and σ = 5 MPa, there
the minimum at θ = 45◦ under other normal stress conditions. is a “Λ” type change law; When σ = 3 MPa and σ = 7 MPa, the “W” type
In general, once the rock is failure, its shear strength will change change law appears. The peak shear strength of all rock-like specimens
significantly, so it is of great significance to study the mechanical under normal stress reaches the maximum when the flaw dip angle is
behavior of the rock after the failure. The variation law of residual shear 45◦ , and reaches the maximum when σ = 5 MPa, with the maximum

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M. Teng et al. Theoretical and Applied Fracture Mechanics 124 (2023) 103750

Fig. 9. Mechanical parameters of samples containing embedded flaw. (a) Peak shear strength; (b) residual shear strength; (c) The displacement at peak shear
strength; (d) Shear stiffness.

Table 2
Partial mechanical parameters of rock containing three-dimensional flaw under different normal stresses.
Group Flaw angle Sample Shear stress peak Residual shear stress The displacement at peak shear Percentage of residual
(Normal stress/ (◦ ) number (MPa) (MPa) strength (mm) strength (%)
MPa)

1 0 T-0-1 4.92 0.72 0.994 14.6


30 T-30-1 4.75 0.79 1.736 16.6
45 T-45-1 3.59 0.93 2.772 25.9
60 T-60-1 2.99 0.59 1.603 19.7
90 T-90-1 4.58 0.85 1.687 18.6
3 0 T-0-3 8.23 1.84 2.135 22.4
30 T-30-3 7.79 2.54 1.645 32.6
45 T-45-3 5.49 2.29 2.504 41.7
60 T-60-3 6.89 1.99 1.414 28.9
90 T-90-3 7.19 2.49 1.995 34.6
5 0 T-0-5 9.68 3.90 1.694 40.3
30 T-30-5 10.84 3.98 1.96 36.7
45 T-45-5 7.03 4.14 2.842 58.9
60 T-60-5 9.17 3.99 1.855 43.5
90 T-90-5 9.43 3.06 1.442 32.4
7 0 T-0-7 12.22 4.46 2.17 36.5
30 T-30-7 11.74 5.08 1.722 43.3
45 T-45-7 10.24 5.34 2.611 52.1
60 T-60-7 11.96 4.94 1.89 41.3
90 T-90-7 11.84 5.86 1.834 49.5

Note: The second digit represents the flaw inclination, and the third digit represents the applied normal stress.

value of 2.84 mm; The minimum value is 0.994 mm at σ = 5 MPa and θ shear stiffness is the smallest when the flaw inclination angle is 45◦ . The
= 0◦ . shear stiffness of all rocks with different inclination angles is in the range
The variation of shear stiffness of fissured rock under different con­ of 15–68 MN/m. The minimum shear stiffness appears in the sample of
stant normal stresses is shown in Fig. 9(d). We usually use shear stiffness σ = 1 MPa and θ = 45◦ , and the maximum shear stiffness appears in the
“KS” to express the deformation characteristics of rock. It can be seen sample of σ = 7 MPa and θ = 30◦ . It can be seen from the comparison of
from Fig. 9(d) that the shear stiffness changes of rock-like specimens Fig. 9(c) and (d) that the peak shear displacement is just opposite to the
under constant normal stress are “V” and “M”, respectively, and the corresponding shear stiffness, that is, the shear stiffness can well reflect

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M. Teng et al. Theoretical and Applied Fracture Mechanics 124 (2023) 103750

the shear displacement characteristics of fissured rocks. time, there is an obvious angle between the crack propagation direction
and the flaw direction, such as samples with σ = 7 MPa, θ = 30◦ (as
3.3. Failure patterns with different conditions shown in Fig. 12), so this failure is called shear failure mode (S).
The failure modes of all samples are shown in Fig. 10. It can be seen
The whole failure process of all samples is recorded by a high-speed from the figure that the tensile failure mode is mainly concentrated on
camera. Through reading previous studies, we know that the tensile samples with σ = 1 MPa, θ = 0◦ , while the shear failure modes are
fracture is characterized by the opening of particles inside the sample, mainly concentrated on samples with σ = 7 MPa, θ = 30◦ and σ = 7 MPa,
and the shear fracture is characterized by the shear displacement be­ θ = 60◦ , and the rest of the samples are mixed tension-shear failure
tween the particles and the exfoliation of the rock surface. At the same modes. Through the analysis of the failure process of all samples, it is
time, the characteristics of the cross-section have obvious differences. found that the section characteristics and failure modes of rock-like
The tensile fracture surface is rough and there is no obvious scratch. samples have obvious regularity with the different normal stress and
Shear fracture surface is often accompanied by the appearance of white crack angle, which need to be discussed separately.
scratches, shear fragments or shear fracture zones. Three failure modes In order to have a more detailed understanding of the failure pro­
are summarized by analyzing all photos, namely tensile failure mode, cesses and failure modes of rock-like samples under different normal
tension-shear mixed failure mode and shear failure mode. stresses and flaw dip angles, samples with σ = 1 MPa (Fig. 11) and θ =
30◦ (Fig. 12) are taken as examples for analysis. “S” represents shear
3.3.1. Tensile failure mode failure and “T” represents tensile failure. The sample images in column
The initial crack appears from the edge and rapidly expands to both (a) represent the crack initiation position and propagation trend of the
sides until the specimen is completely destroyed, such as σ = 1 MPa, θ = samples during the initial loading stage, the sample images in column
0◦ (as shown in Fig. 11). The flaws inside the sample start to be subjected (b) represent the crack morphology when the samples reach the peak
to force at the initial stage of loading. With the continuous increase of shear strength. The sample images in column (c) represent the failure
load, the flaw tip generates secondary cracks in different directions in mode of the samples when the shear displacement reach 7 mm after the
the AB section of Fig. 8. When the specimen is under low normal stress peak shear strength and the sample pictures in column (d) represent the
and θ = 0◦ , the surface crack of the specimen will rapidly expand the rough characteristics of the sample section.
direction parallel to the flaw. When the peak shear strength is reached,
the whole specimen is broken through the shear plane and almost no 3.3.4. Influence of flaw angle
shear failure occurs during the failure process. The failure mode is Under the normal stress of 1 MPa, the crack growth and failure
abbreviated as tensile failure mode (T). modes of samples with different flaw angles are shown in Fig. 11. As can
be seen from Fig. 11(a), there are three ways of crack initiation: (1)
3.3.2. Tension-shear mixed failure mode Cracks begin to initiate from one side of the two edges (usually on the
The cracks of the sample first begin to initiates from the two edges or left side) and rapidly expands to the other side, such as samples with
the middle, and rapidly expands to the other side until the sample fails, flaw θ = 0◦ . (2) The sample begins to crack from both sides and rapidly
such as σ = 3 MPa, θ = 30◦ (as shown in Fig. 12). Similar to the crack expands to the middle until fracture. This initiation mode is often
propagation mechanism in tensile failure mode, under the action of accompanied by a large oblique pulling trend, such as sample with flaw
initial load, secondary cracks will first initiate at the internal flaw tip, θ = 60◦ . (3) The fracture starts from the middle part of the sample, ex­
and then crack will appear on the sample surface. Shear cracks are easy pands rapidly to the two edges, and finally breaks, accompanied by
to initiate when the flaw angle is between 30◦ and 90◦ . In addition, minor tensile failure when θ = 90◦ .
under the action of high normal stress, the friction and bite force of the In Fig. 11(b), it can be seen that when the normal stress is 1 MPa, the
rock structural plane increase, and secondary cracks may also be pro­ shear cracks gradually increase with the increase of flaw inclination, and
duced outward along both sides of the edge of the flaw, which is finally reach the maximum when θ = 60◦ . The failure process of all
accompanied by tensile cracks. This situation is more likely to occur samples corresponding to the final failure mode are shown in Fig. 11(c).
when the flaw angle is θ = 90◦ . The shear section of the sample is rough From the shear bands shown in Fig. 11(c), we find that the exfoliation
and both edges are accompanied by tensile failure. Therefore, this fail­ area of the samples surface increase with the increase of the inclination
ure is abbreviated as tension-shear mixed failure mode (T-S). angle, reaching the maximum at θ = 60◦ , and a large number of shear
fragments appear at this time. At the same time, a white shear scratch
3.3.3. Shear failure mode appears at the shear failure in Fig. 11(d).
Due to the action of normal stress, the crack of the sample initiates
from both ends and rapidly expands to edges. The continuous increase of 3.3.5. Influence of normal stresses
shear load eventually leads to the through failure of the sample, and the The crack growth and failure modes of rock with flaw angle of 30◦
crack propagation mechanism is consistent with the previous failure under different normal stresses are shown in Fig. 12. It can be seen from
mode. The sample section is smooth with obvious white scratches, and Fig. 12(a) that the crack initiation modes are included in the crack
there are broken powdery coarse particles in the middle. At the same initiation modes of the previous section and will not be repeated here. As
can be seen from Fig. 12(b), with the increase of normal stress in rocks
under the same flaw angle, shear cracks become more and more, and the
crack width becomes larger and larger. The increase of the normal stress
also leads to the gradual increase of the surface peeling area of the
specimens shown in Fig. 12(c). Meanwhile, it can be seen from Fig. 12(d)
that more and more shear segments and white scratches appear in the
section under high normal stress, and the failure mode is closer to the
shear failure.

4. Acoustic emission characteristic parameters


° ° ° ° °
° 4.1. Effect of flaw dip angle and normal stress on acoustic emission counts

Fig. 10. Failure modes of rock samples under normal stress and flaw tendency. Before the test loading, the acoustic emission probe should be

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M. Teng et al. Theoretical and Applied Fracture Mechanics 124 (2023) 103750

Fig. 11. Failure process and section characteristics of specimens with different flaw inclination angles under the same normal stress (σ = 1 MPa).

directly close to the sample surface, so as to receive the acoustic emis­ first and then increase. This characteristic is consistent with the previous
sion signal more accurately during the sample loading process. Fig. 13 analysis of the influence of flaw inclination angle on shear strength
defines the characteristic parameters of acoustic emission waveform under the same conditions (Fig. 9a).
signal in detail. In this study, four signal channels are used to monitor When the principal stresses are lower (σ = 1 MPa and σ = 3 MPa), the
the shear failure process of samples. The evolution curves of shear stress, inner convex body is completely sheared and the bite force decreases
acoustic emission counts and cumulative counts of samples under with the increase of the shear stress peak. At this point, AE counts in­
different shear stresses and flaw inclination angles are obtained by creases sharply, and the slope of cumulative counts reaches the
analyzing the acoustic emission generated by micro-cracks during rock- maximum value. The macro surface cracks of the sample propagate
like shear process (as shown in Fig. 14). At the same time, the evolution rapidly and penetrates through the whole sample, eventually leading to
law of cracks can be obtained by analyzing the variation law of AE rock fracture and failure (Fig. 14b and Fig. 14f). Under the condition of
counts under different loading times. high stress (σ = 5 MPa and σ = 7 MPa), the convex body inside the
By analyzing Fig. 14(a)-(e), except for Fig. 14(c), AE counts under sample is cut slowly due to the increase of bite force and friction force,
other conditions are less before the shear peak, indicating that AE ac­ resulting in relatively stable AE activity. The distribution trends of AE
tivities are in a static state. In Fig. 14(c), the pre-peak acoustic emission characteristic parameters are shown in Fig. 14(g)-(h). When the flaw
count increases sharply, which is consistent with the sudden decrease of angle is the same (θ = 30◦ ), the cumulative counts of AE under different
shear strength in the shear stress-displacement curve, indicating that the normal stresses are compared. It can be seen that the cumulative counts
sample under such conditions appears large micro-cracks at this time. increase with the increase of normal stress, which is consistent with the
Under the same normal stress conditions, the maximum value of the AE change of the corresponding shear strength. In all normal stress condi­
counts remains at the 104 orders of magnitude, while the maximum tions, the post-peak residual stage is almost similar, that is, the convex
value of the cumulative counts remains at the 106 orders of magnitude. body inside the specimen is completely cut off, and the force between
Comparing the cumulative counts under different flaw inclination an­ the two sections of the specimen decreases and slips. At this time, AE
gles, it can be concluded that with the increase of the inclination angle of activities are also in a stable stage. As we can be seen, the change of AE
the pre-existing flaw, the cumulative acoustic emission counts decrease counts and cumulative count can reflect the evolution process of internal

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M. Teng et al. Theoretical and Applied Fracture Mechanics 124 (2023) 103750

Fig. 12. Failure process and section characteristics of specimens with different normal stresses under the same flaw dip angle (θ = 30◦ ).

and the tensile crack and shear crack are distinguished by the diagonal
of the scatter diagram. The data points on the upper side of the dotted
line are the points generated by tensile failure, and the data points on the
lower side are the points generated by shear crack failure. Based on this
theory, domestic and foreign scholars have conducted more in-depth
research on the relationship between RA and AF. In this paper, the
linear relationship between RA and AF (AF = 3RA + 75) obtained by
Kun et al. [47] is used as the transition line of tensile-shear crack. Fig. 16
shows the evolution process of tensile-shear crack classification ob­
tained by AE feature parameters. The black dotted line represents the
transition line of the tensile-shear crack, and the red dotted line area
corresponds to the violent active period of acoustic emission. The data in
the scatter plot are colored over time, with a time interval of 100 s.
Fig. 16(a)-(e) show the evolution law of tensile-shear crack with time
Fig. 13. Definition of AE waveform signal parameters.
for rock-like samples under different inclination angles (σ = 1 MPa). It
can be seen from the scatter color and tensile-shear crack curve in the
micro-cracks in the shear process of the specimens. figure that the AE signals of all samples are in a “quiet period” at the
early stage of loading. When θ = 0◦ , the cumulative curve of cracks starts
to increase slowly at 300 s, and at this time, the AE signals are in the
4.2. Analysis of RA/AF characteristics “active period”. In the whole process after that, the cumulative number
of tensile cracks is always greater than that of shear cracks. When θ =
JCMS-IIIB 5706(2003) [46] first proposed a method to detect and 30◦ , the cumulative number of cracks starts to increase rapidly at 400 s,
classify concrete crack growth by using acoustic emission characteristic and the shear cracks are always larger than the tensile cracks throughout
parameters. The key parameters in identifying crack types are RA and the whole process. At θ = 45◦ , the crack curve develops slowly in 200 s-
AF. RA is obtained by the ratio of rising time to maximum amplitude in 500 s, while the crack accumulation increases rapidly after 500 s. The
AE parameters, AF is obtained by the ratio of AE counts to duration [47]. whole process is dominated by shear cracks. At θ = 60◦ , the crack
The equation is as follows: development trend is similar to that at θ = 45◦ . When θ = 90◦ , the
Rise time tensile-shear crack increases rapidly at 370 s, and the tensile crack is
RA = (1) always smaller than the shear crack in the whole process. Fig. 16(b) and
Amplitude
(f)-(g) show the evolution law of tensile-shear cracks of rock-like sam­
Count ples with time under different normal stresses (θ = 45◦ ). Except for σ = 7
AF = (2)
Duration MPa, the other three stress states are roughly the same, that is, the
As shown in Fig. 15, the RA and AF data are used as scatter diagrams, acoustic emission signal is relatively calm in the early stage of loading.

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M. Teng et al. Theoretical and Applied Fracture Mechanics 124 (2023) 103750

Fig. 14. Variation of shear strength, AE counts and cumulative counts with loading time. (a) σ = 1 MPa, θ = 0◦ ; (b) σ = 1 MPa, θ = 30◦ ; (c) σ = 1 MPa, θ = 45◦ ; (d) σ
= 1 MPa,θ = 60◦ ; (e) σ = 1 MPa,θ = 90◦ ; (f) σ = 3 MPa, θ = 30◦ ; (g) σ = 5 MPa,θ = 30◦ ; (h) σ = 7 MPa, θ = 30◦ .

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M. Teng et al. Theoretical and Applied Fracture Mechanics 124 (2023) 103750

mainly used to describe the relative relationship between seismic fre­


quency and magnitude, that is, the logarithm of the cumulative number
(N) greater than magnitude (M) is linearly related to magnitude (M)
[49]. In recent years, b-value has been widely used to analyze and
predict the failure precursors of rocks. When the b-value is small, it in­
dicates that the sample has a violent fracture behavior. On the contrary,
it indicates that there are a lot of micro-cracks in the sample. Based on
this theoretical basis [50,51], this paper statistically calculates the b-
value based on the amplitude, and the specific relationship is expressed
as:
LgN = a − b(AdB /20) (4)
Where a and b are constants, AdB is the maximum amplitude (dB) of
the AE signal, AdB = 20lgAmax, and Amax is the maximum amplitude
(microvolt) of the signal.
Fig. 17 shows the evolution characteristics of AE event rate, b-value
and shear stress-time curve. The pink dashed box in the figure shows the
b-value mutation of the sample, and the small diagram is a local
enlarged view of the b-value dense area. In Fig. 17(a), the b-value in the
early stage of AE has been in a high state, and the AE event rate is small,
reflecting that the AE activity is relatively stable. The AE event rate
increases abruptly at 380 s, and the corresponding b-value decreases for
the first time, indicating that a large number of micro-cracks begin to
Fig. 15. Crack classification based on acoustic emission parameters.
appear and rapidly expand in the specimen, which is the precursor point
of specimen failure. The AE b-value drops for the second time at 400 s,
With the gradual increase in horizontal load, the acoustic emission reaching the minimum value (0.49), at which time the sample is
signal is in an “active period”, and the cumulative number of cracks completely broken. In Fig. 17(b), the AE b-value suddenly drops for the
mainly dominated by shear cracks increases rapidly. first time at 350 s, and the AE event rate increases sharply. With the
It can be concluded from Fig. 16 that the number of shear cracks is progress of the test, the number of AE hits increase, and the b-value
greater than that of tensile cracks at all dip angles except θ = 0◦ . With the decreases for the second time, reaching the minimum value (0.89) at
increase of flaw inclination, the proportion of shear cracks increases and 610 s, at which time the sample is completely fractured. The variation
gradually becomes the main failure mode. At θ = 60◦ , the proportion of pattern of AE b-value in Fig. 17(c) and (b) are roughly similar, with two
shear crack is the largest, and the shear failure is the most obvious. These sudden drops, and the minimum value is 0.93 at 970 s.
phenomena are consistent with the failure patterns observed during the From the AE event rate, b-value and shear stress curve coupling in
test. Under the same flaw inclination angle, the proportion of shear Fig. 17, it can be seen that the rapid propagation of cracks and the
crack increases gradually with the increase of normal stress, reaching complete failure of specimen generally occur at the sudden drop of b-
the maximum at σ = 7 MPa. It can be seen from the above analysis that value. In particular, when the dip angle is 60◦ (Fig. 17b), the b-value has
the RA/AF value can reflect the classification and development of multiple mutations, which matches the complexity of the section in
tensile-shear cracks in specimens. 3.3.1. It can be seen from the above that the analysis of AE b-value can
further explore the failure time domain and failure precursor charac­
4.3. Evolution characteristics of AE b value teristics of rock-like samples, and provide a reliable test basis for the
wider application of AE technology in the future.
The parameters obtained in the AE monitoring process may be
accidental, therefore, this section will comprehensively evaluate the 4.4. AE event distribution (localization) and crack propagation
precursory characteristics of rock-like failure through acoustic emission
event rate and b-value. F(γ i) (AE rate) represents the average frequency The acoustic emission positioning technology used in this study is the
of acoustic emission hits in the “sliding time window” for n consecutive PCI-II three-dimensional positioning real-time monitoring technology of
events [48]. The value of n mainly depends on the total number of the American Physical Acoustics Corporation (PAC). Before each test
monitored AE events. The calculation steps of F(γ i) are as follows: loading, the P-wave prediction of rock-like samples is completed, and
First of all, in this paper, the value of each group of continuous events the P-wave velocity (3470 m/s) is measured by the active source method
(n) is 100, and the mean value (γii) between consecutive events (Δti) in (one sensor is set in the active mode and the other sensor is working on
the same group is calculated as follows: the receiver) of the acoustic emission system. The p-wave is automati­
γ i = Δti /n = (tn+i− 1 − ti− 1 )/n i = 2, 3, … (1). cally captured by the root mean square (RMS) automatic selection al­
Where tn+i-1 and ti-1 represent the number of acoustic emission events gorithm. The RMS auto-selection algorithm first calculates the auto-
occurring at n + i-1 and i-1, respectively. When i = 1, γ1 can be expressed selection function using the moving window method, amplitude peaks
as: appear in the function, and these peaks can be used to estimate the
γ 1 = (tn − t1 )/n (2) arrival time. The AE system uses the time difference positioning method
to determine the acoustic emission source, that is, according to the time-
Finally, F(γi) in a given time can be expressed as: difference of the AE signal emitted by the same acoustic emission source
1 to different sensors and the spatial position of the sensor arrangement,
F(γi ) = γ−i i = 1, 2, 3…
the equation is listed and solved by their geometric relationship, and the
In particular, since each specimen will generate a large number of AE accurate position of the acoustic emission source can be obtained. The
events at the time of critical failure and the time interval between each time-difference method assumes that the acoustic propagation of the
event is very small, equations (2) and (3) do not define n-1 AE events, material is isotropic and the wave velocity is constant. If at least three
which will not affect the accuracy of the overall test results. channels record a waveform with amplitudes above a preset threshold
The AE b-value, proposed by Gutenberg and Richter in 1944, is within a 25 µs time window, an acoustic emission event will be

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M. Teng et al. Theoretical and Applied Fracture Mechanics 124 (2023) 103750

Fig. 16. Evolution trend of RA/AF of rock-like specimens with time under different conditions. (a) σ = 1 MPa, θ = 0◦ ; (b) σ = 1 MPa, θ = 30◦ ; (c) σ = 1 MPa, θ = 45◦ ;
(d) σ = 1 MPa,θ = 60◦ ; (e) σ = 1 MPa,θ = 90◦ ; (f) σ = 3 MPa, θ = 30◦ ; (g) σ = 5 MPa,θ = 30◦ ; (h) σ = 7 MPa, θ = 30◦ .

identified. with two different flaw dip angles in four periods, as shown in Fig. 18.
This section will explore the internal damage process of fractured From Fig. 18(a) (θ = 30◦ ), it can be seen that the AE fracture source is
rock mass by analyzing the time domain characteristics of AE event less and the amplitude is smaller in the early stage (0–200 s) of hori­
distribution. We analyze the distribution of AE fracture sources in rocks zontal load loading. With the continuous application of horizontal load

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M. Teng et al. Theoretical and Applied Fracture Mechanics 124 (2023) 103750

Fig. 17. The evolution characteristics of b value and AE rate with time under different conditions. (a) σ = 1 MPa, θ = 30◦ ; (b) σ = 1 MPa, θ = 60◦ ; (c) σ = 5 MPa, θ
= 30◦ .

(200–400 s), a large number of AE fracture sources appear around the concentrated in the middle part of the sample. However, when the
3D flaw in the middle of the sample, and the shear fracture sources inclination angle is 60◦ (Fig. 18b), the AE starts to produce more fracture
account for a large proportion, which is the precursor of the sample sources at the early stage of load loading, and they are mainly concen­
fracture. The number of AE events increase sharply between 400 and trated at the 3D flaw tip, with a large amplitude. In the rapid crack
600 s. The AE sources are mainly concentrated in the middle and upper development stage, AE events are mainly concentrated in the middle and
right corner. At this time, the sample is completely fractured. During the upper parts, and the amplitude is large. During the fracture of the sample
residual strength period (600–800 s), AE fracture sources are mainly (400–600 s), the distribution of acoustic emission fracture sources is

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M. Teng et al. Theoretical and Applied Fracture Mechanics 124 (2023) 103750

Fig. 18. Distribution of AE fracture sources in different time periods. (a) σ = 1 MPa, θ = 30◦ ; (b) σ = 1 MPa, θ = 60◦ . The size of the sphere represents the amplitude,
the red sphere represents the shear fracture source, and the blue sphere represents the tensile fracture source. (For interpretation of the references to color in this
figure legend, the reader is referred to the web version of this article.)

relatively loose. expressed as:


From the above analysis, we can see that the distribution of AE
1 ∑ n
x − Xi
events in the fracture process of samples with different flaw dip angles is p(x) = K( ) (5)
quite different. The fractured rock mass has obvious aggregation during nh i=1 h
the fracture process (200–600 s). The high-density aggregation area of Where h is the width of kernel function, n is the total number of
these fracture sources can be regarded as a high-risk area. In order to acoustic emission events, and K(x) is a kernel function. In this study, we
further identify and visualize the AE gathering area, we will use another choose multivariate Gaussian function as the kernel function, and its
method to study the high-risk area of rock-like samples. Kernel density function satisfies Eq. (6):
estimation (KDE), as a non-parametric method, can calculate the prob­
ability density estimation of AE event features [52]. The “true” density K(x) =
1
exp(−
1 2
‖x‖ ) (6)
estimates for any set of AE event data (X1, X2, X3, …, Xn) at X can be (2π)d/2 2

K
K

Fig. 19. The cloud map of kernel density estimation and maximum point for fractured rocks at different times. (a) σ = 1 MPa, θ = 30◦ ; (b) σ = 1 MPa, θ = 60◦ .

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M. Teng et al. Theoretical and Applied Fracture Mechanics 124 (2023) 103750

According to the principle of kernel density estimation, the distri­ samples with σ = 7 MPa, θ = 30◦ and σ = 7 MPa, θ = 60◦ . The rest
bution cloud diagram of AE events is obtained (as shown in Fig. 19). It of the specimens are in tension-shear mixed failure mode.
can be seen from Fig. 18 that the distribution of AE events has certain (3) By comparing the AE characteristic parameters and the shear
aggregation and regularity, so the maximum density point obtained by stress-time curve of the sample, it is found that the acoustic
KDE is generally considered to be the fastest growing position of cracks. emission activity can be divided into three stages: the quiet stage
When the flaw dip angle is 30◦ (Fig. 19a), the maximum density point in the early stage of loading, the active stage, and the residual
first appears at the edge of the sample. As the horizontal load continues strength quiet stage. The sudden increase point of AE count can
to be applied, the maximum density point of the sample moves to the tip be used to predict the precursor point of rock fracture. It is
of the flaw before failure, and the shear micro-cracks mainly occur in the observed in the RA-AF scatter plot and the tension-shear crack
sample. When the sample is damaged, the maximum density point still accumulation curve that when θ = 0◦ , the number of tensile
appears at the tip of the flaw, and a small amount of tensile micro-cracks cracks is obviously larger than the number of shear cracks, and
appear at this time. Therefore, the failure mode of the sample is a tensile- shear cracks are smaller than tensile cracks at other inclinations,
shear failure mode dominated by shear failure. When the flaw dip angle which is consistent with the failure mode observed in the test.
is 60◦ , the maximum density value appears at the flaw tip at the initial (4) The rapid propagation of cracks and the complete failure of
stage of horizontal load. With the continuous application of horizontal specimens generally occur when the b-value drops suddenly, and
load, the maximum density point moves towards the end of sample, and the minimum b-value point can be used as the precursor char­
a large number of shear cracks appear inside the sample. When the acteristic point of specimen failure. Through the KDE analysis on
sample is damaged, the maximum density point moves to the lower the distribution of acoustic emission events, the damage location
middle corner. of rock in each stage is effectively identified. The position change
Through the distribution characteristics of AE events, it is found that of the maximum density point is consistent with the crack prop­
the flaw inclination angle has a significant influence on the space–time agation trend of the sample, almost following the uniform diffu­
characteristics of AE events. Since the failure of the sample is caused by sion from the middle to the end of the specimen.
the accumulation of damage inside the rock, most AE events occur at the
main crack position, that is, the middle position of the sample. Inter­
estingly, AE events accumulate rapidly near the shear zone before Declaration of Competing Interest
specimen failure, but decrease rapidly after specimen failure, which can
be used as a precursor of rock failure. According to the kernel density The authors declare that they have no known competing financial
cloud map and the movement of the maximum density point, it can be interests or personal relationships that could have appeared to influence
found that the nuclear density distribution is different with different the work reported in this paper.
flaw inclination angles, but the maximum density point always moves
from the tip to the end of the sample. Data availability

5. Conclusion Data will be made available on request.

In this study, a method for making rock-like specimens containing Acknowledgments


embedded 3D flaw from cement mortar is proposed, and a series of shear
tests are carried out on specimens with different flaw inclinations. The This work was supported by National Natural Science Foundation of
effects of three-dimensional flaw angle and different normal stresses on China (52164001, 52064006, 52004072), Talents of Guizhou University
the mechanical properties of the specimens are studied. In addition, the (Grant No. 201901), the Special Research Funds of Guizhou University
AE characteristic parameters during the failure process of rock-like (Grant No. 201903, 202011, 202012), Science and Technology Support
specimens are comprehensively analyzed, and the relationship be­ Project of Guizhou (No. [2020]4Y044) and No. [2018]2787), Guizhou
tween the kernel density estimation results and crack evolution under University Cultivation Program ([2020] No. 1), Higher Education
two different flaw dip angles is analyzed. The conclusions can be sum­ research project of Guizhou University (GDGJYJ2021009).
marized as follows:
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