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SM-Grain Size Distribution of Soil
SM-Grain Size Distribution of Soil
SM-Grain Size Distribution of Soil
The sieve analysis is used for grain size distribution of the soil portion
that is cohesionless and grain size larger than 75μm (0.075 mm).
a. Sieve analysis:
1. Set of sieve (from 80 mm to 0.075 mm)
2. Sieve shaker
3. Balance of 0.1 gm accuracy
4. Drying oven
5. Porcelain dishes for drying sample
6. Wash bottles
Lid Lid
19 mm 2.36 mm
16 mm 1.12 mm
13.2 mm
0.6 mm
10 mm
9.5 mm 0.425 mm
6.7 mm 0.212 mm
4.75 mm 0.125 mm
Pan 0.075 mm
Pan
Set of sieve
Sieve shaker
Wash
bottles
Porcelain dish
Weighing balance sieve
Scoop Wooden mallet
Soil tray
spatula
Fully representative soil sample as received from the field is first air/ oven dried.
Take raw dry soil to a big sized Galvanized iron tray. Pound the soil with the
rubber/wooden mallet until all the big soil clods and lumps are properly broken.
After pounding, the overall soil is thoroughly mixed with a scoop so that proper
representative soil sample can be taken.
Place 1000 or 500 gm of this representative sample in a small enameled tray.
This is required for gravel analysis. The hygroscopic moisture content should be
known, if the soil is air dried or kept outside oven for a long duration.
Gravel analysis (Wet Sieving):
1. The first stage is meant for gravelly soils. Soak 500 g of air-dry soil
in the tray. The hygroscopic moisture content must be known to
calculate mass of completely (oven) dry soil.
2. Add a pinch of Na2CO3 to aid dispersion (or, 2 gm/lt water solution
of Sodium hexametaphosphate (NaPO3)6] and mix the mixture
thoroughly.
3. Leave the mixture for soaking for at least an hour.
4. Wash the mixture on 4.75 mm sieve under the current of water and
collect the fraction retained on the sieve.
5. Transfer the fraction retained on the sieve to a porcelain dish and
keep for drying in oven for 24 hrs.
6. Pass the dried soil through the set of sieves from 38.0 mm to 4.75
mm and record the mass of soil retained on each sieve in the record
sheet.
7. Calculate the percent soil finer than various sieve sizes.
Sand analysis (Wet Sieving):
1. The soil passing through 4.75 mm sieve is subjected to sand
analysis.
2. Take 100 g of air dry soil (soil sieved from 4.75 mm sieve)
with known hygroscopic moisture content.
3. Soak the sample for an hour in water.
4. Wash the soaked sample on 75μ sieve till almost clean water
passes.
5. Keep the soil retained on the 75μ sieve in oven for 24 hrs.
6. Sieve the dried soil through the set of sieves from 2.39 mm to
75μ and record the mass of the soil retained on each sieve in
the record sheet.
Calculation Steps:
1. In order to combine results of the gravel sieve analysis
with that of sand sieve analysis, percent finer (N%)
calculated from sand sieve analysis is modified as follows:
N N 'g
Modified percent finer, N': N '
100
N'g = last value of percent finer in gravel analysis
D30 2
3. Coefficient of curvature, Cc : Cc
D10 D60
NOTE:
• For Dry sieving, the total soil must be oven dried before performing
the sieve analysis.
• For Wet sieving, air dry soil can be taken to wash the soil through
4.75 mm and 75μ sieves. Then the retained soil mass over 4.75 mm
and 75μ sieves are oven dried to perform gravel and sand analysis,
respectively.
The mass of initial total dry soil is calculated using
hygroscopic moisture content and that mass is used to calculate
percent finer.
Specimen calculation of Gravel analysis:
Sr. No. Sieve Mass of soil Percent Cumulative Percent
opening, retained, gm retained, percent finer, N,
mm % retained, % %
1 19 131.46 28.96 28.96 71.04
2 16 9.09 2.00 30.96 69.04
3 13.2 45.96 10.12 41.08 58.92
4 10 30.60 6.74 47.82 52.92
5 9.5 2.3 0.51 48.33 51.67
6 6.7 20.1 4.43 52.76 47.24
7 4.75 6.98 1.54 54.30 45.70
• Percent retained,% • Cumulative percent • Percent Finer, N:
= (9.09/454)×100 retained,%: = 100-30.96
= 2.00% = 28.96+2.00 = 69.04%
= 30.96%
**It should be noted from the record sheet that the last value of percent
finer in gravel analysis (N'g) is 45.70%.
Specimen calculation of sand analysis (Wet/ Dry Sieving):
1. From passing 4.75 mm sieve, taken mass of air dry soil = 100 g
2. Hygroscopic moisture content = 10.10%
3. Mass of oven dry soil = 90.83 g
Sr. Sieve Mass of soil Percent Cumulative Percent Corrected
No. opening, retained, gm retained, percent finer, N, Percent
mm % retained, % % finer, N', %
1 2.36 1.656 1.82 1.82 98.18 44.87
2 1.18 6.397 7.04 8.86 91.14 41.65
3 0.600 2.624 2.89 11.75 88.25 40.33
4 0.425 3.693 4.07 15.82 84.18 38.47
5 0.212 5.686 6.26 22.08 77.92 35.61
6 0.125 5.343 5.88 27.96 72.04 32.92
7 0.075 3.099 3.41 31.37 68.63 31.36
**N's = last value of percent finer in sand
Corrected Percent finer, analysis = 31.36%
N N 'g
N' = (98.18× 45.70)/100 = 44.87%
100
44.87
Theory of Sedimentation
- After a time t, within a depth He, mass of solid particles finer than D is MD in
suspension volume VD up to that depth. All particles larger than D settled
below that depth.
Concentration of soil solids up to depth He = mD = MD/VD
M Mw ρ w Vw ρ w VD Vs
ρ D ρ mD ρ mD
VD VD VD
MD MD
ρ mD ρ w 1 ρ mD ρ w 1
VDρ s VDGsρ w
MD mD
ρ mD ρ w ρ mD ρ w
VDGs Gs
1 Gs
mD 1 ρ - ρ w mD ρ - ρ w
Gs Gs 1
mD
N(%) 100
ms
Gs 1
N(%) ρ - ρ w 100
Gs 1 ms
Gs V
N(%) ρ - ρ w 100
G s 1 Ms
R Gs V
N(%) 100
1000 Gs 1 Ms
The readings on
the Hydrometer stem
give the density (ρ) of
the soil suspension
situated at the centre
of the bulb at any
time.
For convenience
Hydrometer reading
is recorded as,
R = (ρ- ρw) x 1000
R = (ρ-1) x 1000
Sedimentation Analysis
W = U + FD
W U FD
4 3 4 3
r s r w 6πηrv
3 3
2 r2
v ( s w )
9
2
1 D D = diameter of the sphere
v (s w )g Gs = sp. gravity of the material of sphere
18 g = acceleration due to gravity
gD 2 (G s 1) w 18v
v D
18 gG s 1 w
If a spherical material settles a depth ‘He’ cm in ‘t’ mint
with a constant terminal velocity ‘v’,
He
v cm/sec v in cm/sec,
60t
He in cm,
18v t in mint,
D
g G s 1 w
η in poise (Dyne-sec/cm2),
g = 981 cm/sec2,
18 He
D in cm ρ =in gm/cm3
981 60 G s 1 w t w
18 He
D 10 in mm **Assuming soil particles
981 60 G s 1 w t as sphere, D is calculated
Preparation of Soil Suspension:
1. 50 gm oven dried soil passing 75μ IS sieve is taken in a porcelain dish.
2. 33 gm Sodium hexameta-phosphate and 7 gm Sodium Carbonate are
mixed in required quantity of distilled water to make 1000 ml solution. 100
ml of that dispersing solution is added to the oven dried soil.
3. The mixture is warmed gently for about 10 mints.
4. The mix is transferred to a mechanical mixture and distilled water is
added to make the cup of mixture about three-fourth filled.
5. The suspension is stirred for about 15 mints.
6. After that transfer the entire mix into a 1000 ml measuring cylinder and fill
the remaining volume with distilled water to make volume of suspension
1000 mm.
7. Turn the measuring cylinder upside-down 3-4 times keeping palm of hand
firmly on the top of cylinder to make a uniform density initial suspension
and put the measuring cylinder immediately on the test table and start the
stop watch.
8. The dispersing agent was added to neutralise the charges on the smaller
grains and the soil solids do not form soil clods/lumps in the suspension.
Note:
Take the hydrometer reading at total elapsed times
of ½, 1 and 2 minutes without removing the
hydrometer.
After the 2 minute reading, remove the hydrometer
gently without disturbing the suspension and place it
in the neighbouring cylinder containing only distilled
water, rinse it by a twisting motion to remove any soil
particle that may have settled on it. After taking each
reading hereafter, the same needs to be followed.
Just before taking readings, the hydrometer is
gently inserted into the soil suspension.
After first 2 minutes, readings are usually taken at
5, 15, 30, 60, 90, 120, 150, 180, 1440 minutes.
Determine the meniscus correction (Cm),
dispersing agent correction (Cd), and temperature
correction (Ct).
h V V
He H h h
h Vh
He H
2 2A A 2 2A
Immersion correction:
Immersion correction = -Vh/2A
Vh = volume of hydrometer
A = cross sectional area of jar containing
suspension
Corrections to hydrometer reading:
1. Meniscus correction, Cm:
Since the soil suspension is not
transparent enough, the scale has to be R
read at the upper rim of meniscus. Rh
This correction is always additive to the
reading because density readings on the
hydrometer stem increases downwards.
If at the upper rim of meniscus, the
hydrometer reading is R, the actual reading
after applying meniscus correction (Rh),
Rh = R + Cm
This ‘Rh’ value is used to calculate the
effective height (He) of fall at time t.
Calibration of hydrometer:
16.6 72
He H
2 2 30
He H 7.1 cm
Rh ρh
24
22
20
18
Ehhective depth (He), cm
16
14
12
10
8
6
4
2
0
Rh: -5 0 5 10 15 20 25 30
ρh: 0.995 1 1.005 1.010 1.015 1.020 1.025 1.030
Hydrometer reading (Rh)/ or, (ρh)
Calibration curve for the hydrometer
Note: The calibration curve for hydrometer always plots a straight line.
Other Corrections to Hydrometer reading:
2. Dispersion correction, Cd:
The addition of dispersing agent results in the
density of liquid in which sedimentation takes
place, being greater than that of water.
To obtain the dispersion correction, 100 cc of
dispersing agent solution is taken in standard
measuring cylinder and the volume is made
equal to 1000 cc by adding distilled water.
Hydrometer is inserted and reading is taken.
Similarly hydrometer is inserted in standard
measuring jar filled with water and reading is
taken. The difference between the two readings
gives the dispersing agent correction
‘Cd’ is always subtracted from the hydrometer
reading, already corrected for meniscus.
The corrected hydrometer reading after applying
meniscus and dispersion correction (Rc'),
Rc' = Rh - Cd
3. Temperature correction, Ct:
Hydrometer is calibrated at 27⁰C.
To apply temperature correction, take cool water and
note the hydrometer reading corresponding to
temperature at interval of 2⁰C up to 33⁰C.
If the temperature is more than 27⁰C, the suspension is
lighter, and the correction is positive.
If the temperature is less than 27⁰C, the suspension is
denser and the correction is negative.
‘Ct’ is always applied to the hydrometer reading,
already corrected for meniscus and dispersion agent.
The corrected hydrometer reading after applying meniscus,
dispersion agent and temperature correction (Rc),
Rc R'c Ct
Rc Rh - Cd Ct Rc R Cm - Cd Ct
Composite correction, C = Cm - Cd ± Ct
Rc R C
The percent finer (N) is calculated using the corrected
hydrometer reading (Rc) value as follows:
R c Gs V
N(%) 100
1000 Gs 1 Ms
Gs V
N(%) ρ c - ρ w 100
G s 1 Ms
ρc ρ Cm - Cd Ct
Sample Calculations:
Hydrometer analysis:
1. Particle diameter, D
18 He
D 10 in mm
981 60 G s 1 w t
He in cm,
t in mint,
η in poise (Dyne-sec/cm2) = 0.00836 poise at test temperature,
ρw in gm/cm3 = 0.996 gm/cm3 at test temperature
Gs = specific gravity of soil solids = 2.6
2. Percent finer, N (%)
Gs V
N(%) ρ c - ρ w 100 ρc ρ Cm - Cd Ct
G s 1 Ms
Where,
Gs = specific gravity of soil solids = 2.6
V = volume of soil suspension = 1000 ml
Ms = mass of oven dry soil taken = 50 gm
ρc = corrected hydrometer density reading
ρw = density of clean water at test temperature = 0.996 gm/cm3
16
14
12
10
8
6
4
2
0
Rh: -5 0 5 10 15 20 25 30
ρh: 0.995 1 1.005 1.010 1.015 1.020 1.025 1.030
Hydrometer reading (Rh)/ or, (ρh)
Particle diameter, D
18 He
D 10 in mm
981 60 G s 1 w t
18 0.00836 16.25
D 10 0.013 mm
981 60 2.6 1 0.996 15
Viscosity of Relative
Temperature
water ‘η’ in density
η = 0.008360 (from table ᵒC
poise of water (Rw)
for viscosity of water at
26 0.008737 0.9968
28ᵒC temperature) 27 0.008545 0.9965
28 0.008360 0.996
29 0.008139 0.99597
30 0.008007 0.99567
Percent finer (N %),
Gs V
N(%) ρ c - ρ w 100
G s 1 Ms
2.6 1000
N (1.007 0.996) 100
2.6 1 50
35.75%
Combined 19 71.04
16 69.04
results from 13.2 58.92
Sieve and 10 52.92
Coefficient of curvature, Cc : Cc
D30 2
D10 D60
Where, D represents the apparent diameter of soil particle and
subscripts denote percent finer than D. D10 = 0.01 mm means 10%
of sample grains are smaller than 0.01 mm
D10 size is also known as the effective size.
Cu
D 60
14
1400 Cc
D30 2
0.075
2
0.04
D10 0.01 D10 D60 0.0114
Gradation characteristics based on Cu and Cc
If %finer 75μ > 12% for gravel and sand, the soil is clayey
or silty gravel and sand.
Grading of Soils (After Arora 2004)
Example 3.2: A dry soil sample of mass 50 gm is mixed with distilled
water to prepare a soil suspension 1000 mm for hydrometer analysis.
The reading of the hydrometer taken after 5 minutes was 28 and the
depth of the centre of the bulb below the surface with meniscus
correction was 150 mm. Volume of the hydrometer was 62 ml. Cross-
sectional area of the jar was 55 cm2. G = 2.68, η = 9.81 millipoise, Cm
= 0.4, Cd = 3.4. Determine the coordinates of the point corresponding
to above observation.
Solution:
1. Meniscus correction, Cm = 0.4 4. Gs = 2.68
2. Dispersion correction, Cd = 3.4 5. Ms = 50 gm
3. Viscosity of water (η) = 0.00981 poise 6. V = 1000 ml
h Vh 62
He H 15 14.436 cm
2 2A 2 55
Rc = 28 + 0.4 - 3.4 = 25
Particle diameter, D
18 He
D 10 in mm
981 60 G s 1 w t
18 0.00981 14.436
D 10 0.023 mm
981 60 2.68 11 5
Percent finer (N %),
R c Gs V
N(%) 100
1000 Gs 1 Ms
25 2.68 1000
N 100 79.76%
1000 2.68 1 50
The coordinate of the point on particle size distribution curve
is (0.023 mm, 79.76%).