Calib

Method: Pb Std4 0-30

Result: AAS 18&19.05.2017 Pb

Pb 283,31

0,258
Absorbance

0,000
0,0 conc(mg/L) 30,0
Calib Eq'n: Lin, Calc Int
Corr Coeff: 0,998566

16/05/2017 15:56:26 Page 1 WinLab32

Method: Pb Std4 0-30 Page 1 Date: 16/05/2017 15:56:42

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Analysis Begun

Logged In Analyst: HP Technique: AA Flame

Spectrometer: PinAAcle 900F, S/N PFAS14091703 Autosampler:

Sample Information File: C:\Users\Public\PerkinElmer\AA\Data\Sample Information\

AAS 18&19.05.2017 Pb.sif
Batch ID:
Results Data Set: AAS 18&19.05.2017 Pb
Results Library: C:\Users\Public\PerkinElmer\AA\Data\Results\resultsV01.mdb

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Method Loaded
Method Name: Pb Std4 0-30 Method Last Saved: 29/05/2015 8:52:47
Method Description:
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Sequence No.: 1 Autosampler Location:
Sample ID: Calib Blank 1 Date Collected: 16/05/2017 15:50:44
Analyst: Data Type: Original
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Replicate Data: Calib Blank 1 Analyte: Pb 283,31
Repl SampleConc StndConc BlnkCorr Time Signal
# mg/L mg/L Signal Stored
1 [0,00] 0,5712 15:50:45 Yes
2 [0,00] 0,5711 15:50:48 Yes
3 [0,00] 0,5717 15:50:51 Yes
Mean: [0,00] 0,5713
SD: 0,0000 0,0003
%RSD: 0,00% 0,06
Auto-zero performed.
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Sequence No.: 2 Autosampler Location:
Sample ID: Calib Blank 1 Date Collected: 16/05/2017 15:50:56
Analyst: Data Type: Original
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Replicate Data: Calib Blank 1 Analyte: Pb 283,31
Repl SampleConc StndConc BlnkCorr Time Signal
# mg/L mg/L Signal Stored
1 [0,00] -0,0004 15:50:56 Yes
2 [0,00] -0,0001 15:50:59 Yes
3 [0,00] -0,0001 15:51:03 Yes
Mean: [0,00] -0,0002
SD: 0,0000 0,0001
%RSD: 0,00% 59,90
Auto-zero performed.
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Sequence No.: 3 Autosampler Location:
Sample ID: Calib Std 1 Date Collected: 16/05/2017 15:51:17
Analyst: Data Type: Original
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Replicate Data: Calib Std 1 Analyte: Pb 283,31
Repl SampleConc StndConc BlnkCorr Time Signal
# mg/L mg/L Signal Stored
1 [7,5] 0,0735 15:51:17 Yes
2 [7,5] 0,0737 15:51:20 Yes
3 [7,5] 0,0737 15:51:24 Yes
Mean: [7,5] 0,0737
SD: 0,000 0,0001
%RSD: 0,00% 0,17
Standard number 1 applied. [7,5]
Correlation Coef.: 1,000000 Slope: 0,00982 Intercept: 0,00000
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Sequence No.: 4 Autosampler Location:
Sample ID: Calib Std 2 Date Collected: 16/05/2017 15:51:37
Analyst: Data Type: Original
Method: Pb Std4 0-30 Page 2 Date: 16/05/2017 15:56:42

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Replicate Data: Calib Std 2 Analyte: Pb 283,31
Repl SampleConc StndConc BlnkCorr Time Signal
# mg/L mg/L Signal Stored
1 [15] 0,1392 15:51:37 Yes
2 [15] 0,1392 15:51:40 Yes
3 [15] 0,1392 15:51:43 Yes
Mean: [15] 0,1392
SD: 0,00 0,0000
%RSD: 0,00% 0,01
Standard number 2 applied. [15]
Correlation Coef.: 0,999435 Slope: 0,00928 Intercept: 0,00135
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Sequence No.: 5 Autosampler Location:
Sample ID: Calib Std 3 Date Collected: 16/05/2017 15:51:57
Analyst: Data Type: Original
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Replicate Data: Calib Std 3 Analyte: Pb 283,31
Repl SampleConc StndConc BlnkCorr Time Signal
# mg/L mg/L Signal Stored
1 [22,5] 0,2053 15:51:58 Yes
2 [22,5] 0,2036 15:52:01 Yes
3 [22,5] 0,2037 15:52:05 Yes
Mean: [22,5] 0,2042
SD: 0,000 0,0010
%RSD: 0,00% 0,48
Standard number 3 applied. [22,5]
Correlation Coef.: 0,999531 Slope: 0,00904 Intercept: 0,00254
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Sequence No.: 6 Autosampler Location:
Sample ID: Calib Std 4 Date Collected: 16/05/2017 15:52:19
Analyst: Data Type: Original
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Replicate Data: Calib Std 4 Analyte: Pb 283,31
Repl SampleConc StndConc BlnkCorr Time Signal
# mg/L mg/L Signal Stored
1 [30] 0,2613 15:52:19 Yes
2 [30] 0,2569 15:52:22 Yes
3 [30] 0,2562 15:52:26 Yes
Mean: [30] 0,2581
SD: 0,00 0,0028
%RSD: 0,00% 1,07
Standard number 4 applied. [30]
Correlation Coef.: 0,998566 Slope: 0,00862 Intercept: 0,00568

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Calibration data for Pb 283,31 Equation: Linear, Calculated Intercept
Entered Calculated
Mean Signal Conc. Conc. Standard
ID (Abs) mg/L mg/L Deviation %RSD
Calib Blank 1 0,0000 0 -0,659 0,00 59,90
Calib Std 1 0,0737 7,5 7,882 0,00 0,17
Calib Std 2 0,1392 15,0 15,484 0,00 0,01
Calib Std 3 0,2042 22,5 23,021 0,00 0,48
Calib Std 4 0,2581 30,0 29,272 0,00 1,07
Correlation Coef.: 0,998566 Slope: 0,00862 Intercept: 0,00568
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Sequence No.: 7 Autosampler Location:
Sample ID: N1 Date Collected: 16/05/2017 15:52:46
Analyst: Data Type: Original
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Replicate Data: N1 Analyte: Pb 283,31
Repl SampleConc StndConc BlnkCorr Time Signal
# mg/L mg/L Signal Stored
1 0,871 0,871 0,0132 15:52:47 Yes
2 0,861 0,861 0,0131 15:52:50 Yes
Method: Pb Std4 0-30 Page 3 Date: 16/05/2017 15:56:42

3 0,893 0,893 0,0134 15:52:54 Yes

Mean: 0,875 0,875 0,0132
SD: 0,0162 0,0162 0,0001
%RSD: 1,86% 1,86% 1,06
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Sequence No.: 8 Autosampler Location:
Sample ID: N2 Date Collected: 16/05/2017 15:53:07
Analyst: Data Type: Original
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Replicate Data: N2 Analyte: Pb 283,31
Repl SampleConc StndConc BlnkCorr Time Signal
# mg/L mg/L Signal Stored
1 1,264 1,264 0,0166 15:53:07 Yes
2 1,144 1,144 0,0156 15:53:11 Yes
3 1,201 1,201 0,0160 15:53:14 Yes
Mean: 1,203 1,203 0,0161
SD: 0,0598 0,0598 0,0005
%RSD: 4,97% 4,97% 3,21
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=
Sequence No.: 9 Autosampler Location:
Sample ID: N3 Date Collected: 16/05/2017 15:53:25
Analyst: Data Type: Original
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Replicate Data: N3 Analyte: Pb 283,31
Repl SampleConc StndConc BlnkCorr Time Signal
# mg/L mg/L Signal Stored
1 0,912 0,912 0,0134 15:53:26 Yes
2 0,941 0,941 0,0131 15:53:29 Yes
3 0,926 0,926 0,0133 15:53:33 Yes
Mean: 0,926 0,926 0,0133
SD: 0,0145 0,0145 0,0002
%RSD: 1,57% 1,57% 1,34
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