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INVESTIGATION OF A HIGH-VOLUME FLY ASH WOOD FIBER MATERIAL


SUBJECTED TO LOW VELOCITY IMPACT AND BLAST LOADS

Technical Report · August 2007

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CENTER FOR INFRASTRUCTURE
ENGINEERING STUDIES

INVESTIGATION OF A HIGH-VOLUME FLY ASH-

WOOD FIBER MATERIAL SUBJECTED TO LOW-

VELOCITY IMPACT AND BLAST LOADS

by

Matthew Tinsley

Dr. John J. Myers

University of Missouri - Rolla

CIES
07-74
2

Disclaimer

The contents of this report reflect the views of the author(s), who are
responsible for the facts and the accuracy of information presented herein. This
document is disseminated under the sponsorship of the Center for Infrastructure
Engineering Studies (CIES), University of Missouri -Rolla, in the interest of
information exchange. CIES assumes no liability for the contents or use thereof.
The mission of CIES is to provide leadership in research and education for
solving society's problems affecting the nation's infrastructure systems. CIES is
the primary conduit for communication among those on the UMR campus
interested in infrastructure studies and provides coordination for collaborative
efforts. CIES activities include interdisciplinary research and development with
projects tailored to address needs of federal agencies, state agencies, and private
industry as well as technology transfer and continuing/distance education to the
engineering community and industry.

Center for Infrastructure Engineering Studies (CIES)


University of Missouri-Rolla
223 Engineering Research Lab
1870 Miner Circle
Rolla, MO 65409-0710
Tel: (573) 341-6223; fax -6215
E-mail: cies@umr.edu
www.cies.umr.edu
ii

REPORT OUTLINE

This report consists of the following two distinct investigations:

Pages 1-76: Low Velocity Impact Testing (Paper 1)

Pages 77-146: Blast Testing of Reinforced Panels (Paper 2)


iii

ABSTRACT

The report document consists of two technical papers, compiling the results of the

research done on a high-volume fly ash-wood fiber material. The two papers

independently examine the relative impact resistance and blast resistance of the material,

respectively. The objective of the study was to develop a composite material composed

of the two recyclables and investigate its use as a sacrificial liner in a blast barrier

application.

A modified version of the ACI drop-weight impact test for concrete was used to

relatively compare and quantify the impact resistance of seven various mix designs. The

mix designs included class C fly ash, Portland cement, and wood fibers. Two wood fiber

composite materials were selected for use in the blast barrier study based on the results

from the drop-weight impact test. Furthermore, the research findings proved the fly ash-

wood fiber composite had a relatively high impact resistance compared to plain concrete.

The blast resistance of the composite materials was assessed using real blast

loads. Ten test panels were fabricated from plain concrete and hybrid materials

incorporating wood fibers. A polyurea coating was also applied to five of the test panels

in the second phase of the blast study. The results validated an added benefit of using the

low density, low stiffness composite in a layered construction with reinforced concrete.

Polyurea also proved useful in containing debris when applied to the tension face of the

test panel.
iv

ACKNOWLEDGMENTS

The authors would like to acknowledge the Air Force Research Laboratory

(AFRL) for financial assistance in this study. Special thanks to Mr. Robert Dinan and

Ms. Jennifer Robertson, both of AFRL, at Tyndall AFB for their interest and assistance in

this work. The authors would like to thank Dr. Jason Baird and Mr. Jeff Bradshaw at the

University of Missouri-Rolla for their assistance in completing the blast testing phase of

the study. The field blast tests would not have been possible without their assistance.

The authors are also truly grateful to Mr. Steve Gabel for machining and constructing the

equipment necessary for the experimental tests and to Mr. Mike Lusher for his assistance

in fabricating and testing specimens. The assistance of students: Travis Hernandez, Amol

Sawant, Trevor Hrynyk, Jared Brewe, Dave Holdener, Yosuke Tanizawa, and Matt

Beyer, who played a vital role in specimen fabrication and testing is also acknowledged.
v

TABLE OF CONTENTS

Page
REPORT OUTLINE........................................................................................................... ii
ABSTRACT....................................................................................................................... iii
ACKNOWLEDGMENTS ................................................................................................. iv
LIST OF ILLUSTRATIONS........................................................................................... viii
LIST OF TABLES............................................................................................................. xi
NOMENCLATURE ........................................................................................................ xiii
PAPER I.............................................................................................................................. 1
IMPACT RESISTANCE OF BLAST MITIGATION MATERIAL USING A
MODIFIED ACI DROP-WEIGHT IMPACT TEST...................................................... 1
ABSTRACT............................................................................................................ 1
1. INTRODUCTION .............................................................................................. 2
1.1 Green materials ............................................................................................. 2
1.2 Uses of fiber-reinforced concrete .................................................................. 4
1.3 Importance of statistics.................................................................................. 4
2. RELATED WORK ............................................................................................. 7
2.1 Drop-weight impact test proposed by ACI Committee 544.......................... 7
2.2 Modified ACI drop-weight impact test for concrete ................................... 10
2.3 Impact resistance of steel fiber-reinforced concrete.................................... 17
3. STUDY OF OBJECTIVES .............................................................................. 20
3.1 Test setup..................................................................................................... 21
3.2 Materials and mix designs........................................................................... 24
3.2.1 Materials............................................................................................. 24
3.2.2 Mix proportions and processes........................................................... 29
3.3 Mechanical properties ................................................................................. 36
3.3.1 Compressive strength ......................................................................... 36
3.3.2 Splitting tensile strength..................................................................... 40
3.3.3 Modulus of elasticity.......................................................................... 41
3.4 Impact resistance ......................................................................................... 45
vi

3.4.1 Group 1 (FA-C-WF)........................................................................... 49


3.4.2 Group 2 (Concrete)............................................................................. 53
3.4.3 Group 3 (PFRC) ................................................................................. 56
3.4.4 Group 4 (FA-WF)............................................................................... 59
3.4.5 Group 5 (FA-WF-A) .......................................................................... 61
3.4.6 Group 6 (WF Concrete)...................................................................... 62
3.4.7 Group 7 (Bi-layered) .......................................................................... 64
3.4.8 Summary of impact resistance ........................................................... 67
3.5 Summary ..................................................................................................... 71
4. CONCLUSIONS............................................................................................... 73
5. ACKNOWLEDGEMENTS.............................................................................. 75
6. REFERENCES ................................................................................................. 75
PAPER II .......................................................................................................................... 77
INVESTIGATION OF A HIGH-VOLUME FLY ASH-WOOD FIBER MATERIAL
FOR MITIGATING BLAST PRESSURES ................................................................. 77
ABSTRACT.......................................................................................................... 77
1. INTRODUCTION ............................................................................................ 77
2. RELATED WORK ........................................................................................... 79
2.1. Nature of explosives................................................................................... 79
2.1.1 Dynamic strength of materials ........................................................... 85
2.1.2 Shock wave behavior in solids ........................................................... 87
2.2. Retrofitting reinforced concrete slabs with composites ............................. 88
2.2.1 Material properties ............................................................................. 89
2.2.2 Test results.......................................................................................... 89
3. EXPERIMENTAL PROGRAM ....................................................................... 90
3.1 Test setup..................................................................................................... 92
3.1.1 Materials............................................................................................. 93
3.1.2 Test specimen fabrication................................................................... 98
3.1.3 Spray-on polyurea application ......................................................... 105
3.2 Mechanical properties of the material ....................................................... 105
3.2.1 Compressive strength ....................................................................... 106
3.2.2 Modulus of elasticity........................................................................ 107
vii

3.2.3 Splitting tensile strength................................................................... 109


4. EXPERIMENTAL TEST RESULTS ............................................................. 109
4.1 Phase 1 blast testing .................................................................................. 109
4.1.1 Panel 1A (Bi-layered system, ρ = 0.2 percent) ................................ 110
4.1.2 Panel 2A (FA-C-WF) ....................................................................... 116
4.1.3 Panel 3A (wood fiber concrete) ....................................................... 118
4.1.4 Panel 4A (reinforced concrete; ρ = 0.5 percent) .............................. 120
4.1.5 Panel 5A (bi-layered system, ρ = 0.5 percent) ................................. 121
4.2 Phase 2 blast testing .................................................................................. 123
4.2.1 Panel 1B (bi-layered system with polyurea, ρ = 0.2 percent) .......... 124
4.2.2 Panel 2B (FA-C-WF and polyurea, ρ = 0.2 percent) ....................... 127
4.2.3 Panel 3B (WF concrete & polyurea, ρ = 0.2 percent) ...................... 129
4.2.4 Panel 4B (reinforced concrete with polyurea, ρ = 0.5 percent)........ 131
4.2.5 Panel 5B ........................................................................................... 133
4.3 Comparison of test results ......................................................................... 135
5. CONCLUSIONS............................................................................................. 140
6. FUTURE RECOMMENDATIONS ............................................................... 143
7. ACKNOWLEDGMENTS .............................................................................. 144
8. REFERENCES ............................................................................................... 144
DISTRIBUTIONS OF IMPACT RESULTS.................................................................. 147
ANALYTICAL PRESSURES........................................................................................ 160
viii

LIST OF ILLUSTRATIONS

Figure Page
PAPER I
1. Standardized normal distribution for drop-weight specimens ...................................... 6
2. Drop-weight test apparatus ........................................................................................... 9
3. Drop-weight impact mold preparation........................................................................ 22
4. Modified ACI drop-weight impact test fixture ........................................................... 23
5. Impact piston............................................................................................................... 24
6. Class C fly ash and Portland cement........................................................................... 26
7. Consitutents of drop-weight test mix designs............................................................. 27
8. Polypropylene fibers and capping compound............................................................. 29
9. Batching drop-weight impact specimens .................................................................... 32
10. Concrete drop-weight impact specimens .................................................................... 33
11. Comparison of wood fiber concrete to plain concrete ................................................ 35
12. Layered construction of Group 7 ................................................................................ 36
13. Determination of material strength ............................................................................. 38
14. Determination of tensile strength and material stiffness............................................. 42
15. Modulus of elasticity curve for Group 1..................................................................... 43
16. Modulus of elasticity comparison............................................................................... 44
17. Base plate modifications ............................................................................................. 46
18. Distribution of 28-day FC test results for Group 1 ..................................................... 48
19. Normal probability curve for Group 1 ........................................................................ 48
20. Standardized normal distribution for Group 1 ............................................................ 49
21. Group 1 impact specimens.......................................................................................... 50
22. Group 2 impact specimens.......................................................................................... 56
23. Group 7 impact specimens.......................................................................................... 65
24. Mean ultimate resistance to impact at 28 days of age ................................................ 68
25. Ratio of mean ultimate and first crack resistances...................................................... 69
26. First crack impact resistance with increasing age....................................................... 72
27. Ultimate impact resistance with increasing age.......................................................... 72
ix

PAPER II
1. Typical blast pressure profile...................................................................................... 81
2. Simplified triangular blast pressure profile................................................................. 81
3. Theoretical incident and reflected pressure curves..................................................... 86
4. Polyurea tensile test .................................................................................................... 97
5. Stress-strain relationship for polyurea undergoing tensile load.................................. 98
6. Tensile test on No. 3 rebar .......................................................................................... 99
7. Formwork for blast panel fabrication ....................................................................... 100
8. Batching procedures.................................................................................................. 102
9. Fabrication of Panels 1A and 1B .............................................................................. 104
10. Fabrication phases for Panel 5A ............................................................................... 104
11. Polyurea application.................................................................................................. 105
12. Modulus of elasticity curves for blast panels............................................................ 108
13. Test setup of Panel 1A .............................................................................................. 110
14. Accelerometer location ............................................................................................. 111
15. Representative acceleration curve............................................................................. 112
16. Acceleration impulse ................................................................................................ 113
17. Panel 1A (bi-layered system, ρ = 0.2 percent).......................................................... 114
18. Panel 2A (FA-C-WF)................................................................................................ 117
19. Panel 3A (wood fiber concrete) ................................................................................ 119
20. Panel 4A (reinforced concrete, ρ = 0.5%)................................................................. 121
21. Panel 5A (bi-layered system, ρ = 0.5 percent).......................................................... 123
22. Panel 1B (bi-layered system with polyurea)............................................................. 125
23. Panel 1B after Event 4 .............................................................................................. 126
24. Panel 2B (FA-C-WF coated with polyurea) ............................................................. 128
25. Panel 3B (WF Concrete and polyurea) ..................................................................... 130
26. Panel 4B (reinforced concrete with polyurea, ρ = 0.5 percent) ................................ 132
27. Panel 4B following Event 3 ...................................................................................... 133
28. Panel 5B (panels separated by air gap) ..................................................................... 135
29. Crack patterns for panel system 5B .......................................................................... 136
x

30. Failure modes of the test panels................................................................................ 139


31. Benefits of polyurea.................................................................................................. 139
32. Polyurea delamination and fracture .......................................................................... 140
xi

LIST OF TABLES

Table Page
PAPER I
1. Mixture proportions for PFRC specimens .................................................................. 11
2. Physical properties of polypropylene fiber ................................................................. 12
3. Compressive strength results ...................................................................................... 13
4. Drop-weight impact test results .................................................................................. 14
5. Comparison of the drop-weight test methods ............................................................. 15
6. Number of specimens required for given percent error .............................................. 16
7. Mix proportions for SFRC .......................................................................................... 18
8. Test results of SFRC ................................................................................................... 19
9. Test results of plain concrete ...................................................................................... 20
10. Chemical composition of fly ash ................................................................................ 25
11. Mechanical properties of oak...................................................................................... 26
12. Specification data for polypropylene fibers................................................................ 28
13. Mix proportions by weight.......................................................................................... 30
14. Compressive strengths of drop-weight impact groups................................................ 39
15. Tensile strengths of fiber-reinforced materials ........................................................... 41
16. Summary of properties of base mix designs ............................................................... 44
17. Group 1 impact test results ......................................................................................... 51
18. Statistical comparison of impact test results............................................................... 52
19. Group 2 impact test results ......................................................................................... 54
20. Comparison of plain concrete ..................................................................................... 55
21. Group 3 impact test results ......................................................................................... 57
22. Comparison of PFRC.................................................................................................. 59
23. Group 4 impact test results ......................................................................................... 61
24. Group 5 impact test results ......................................................................................... 62
25. Group 6 impact test results ......................................................................................... 63
26. Group 7 impact test results ......................................................................................... 66
27. Mean percent increase in the number of blows from FC to UR ................................. 70
xii

28. Minimum number of tests required for 10% error...................................................... 71


PAPER II
1. TNT equivalence values for common explosives....................................................... 83
2. Dynamic increase factors............................................................................................ 86
3. Phase 1 test matrix ...................................................................................................... 91
4. Phase 2 test matrix ...................................................................................................... 92
5. Chemical composition of fly ash ................................................................................ 94
6. Mechanical properties of oak...................................................................................... 95
7. Mixture proportions for blast panel fabrication ........................................................ 101
8. Mechanical properties summary for blast panels...................................................... 107
9. Results for Panel 1A ................................................................................................. 112
10. Results for Panel 2A ................................................................................................. 116
11. Results for Panel 3A ................................................................................................. 118
12. Results for Panel 4A ................................................................................................. 120
13. Results for Panel 5A ................................................................................................. 122
14. Results for Panel 1B.................................................................................................. 124
15. Results for Panel 2B.................................................................................................. 127
16. Results for Panel 3B.................................................................................................. 129
17. Results for Panel 4B.................................................................................................. 131
18. Results for Panel 5B.................................................................................................. 134
19. Summary of results for 680 gram charge at 610 mm (Z = 0.69 m/kg1/3).................. 137
xiii

NOMENCLATURE

Symbol Description
b decay coefficient
d diameter of specimen
e specified error
L length of specimen
n minimum number of tests
N total number of specimens
P load at failure
Pi incident pressure
Po ambient atmospheric pressure
Pr reflected pressure
Ps peak overpressure
p(t) pressure as a function of time
R standoff distance
S standardized variable
t value from t-student distribution
T tensile strength
T+ positive phase duration
v coefficient of variation
W charge weight
X original variable
y number of blows
Z scaled distance
η mean
σ standard deviation
PAPER I

IMPACT RESISTANCE OF BLAST MITIGATION MATERIAL USING A


MODIFIED ACI DROP-WEIGHT IMPACT TEST

ABSTRACT

This experimental program was conducted to evaluate the effectiveness of a high

volume fly ash-wood fiber material at resisting repeated low velocity drop-weight impact.

A modified version of the ACI drop-weight test proposed by ACI Committee 544 was

conducted on seven groups of specimens. Each group was unique, consisting of various

quantities of materials including cement, fly ash, and wood fibers. Testing procedures for

the drop-weight test were consistent with test procedures listed in a previous research

study on drop-weight impact testing of polypropylene fiber-reinforced concrete (Badr and

Ashour, 2005). However, a few modifications were made to the previous test setup to

better accommodate this study.

Test results revealed that the fly ash-wood fiber specimens have a significant

resistance to drop-weight impact as compared to unreinforced concrete specimens.

Although results show that polypropylene fiber-reinforced concrete has the highest drop-

weight impact resistance, the fly ash-wood fiber material is a likely candidate for use in a

barrier system due to its low stiffness and ductile failure mode. Impact test results also

coincided with results from previous drop-weight impact tests.


2

1. INTRODUCTION

Due to the lack of a standard impact test for concrete, designers are not yet able to

use impact resistance as a design parameter. The lack of a standard impact test is due to

high variations in the results. However, ACI Committee 544 proposed a drop-weight

impact test that is becoming a common method to determine the relative brittleness and

impact resistance of fiber-reinforced concrete. In this regard, this study uses a modified

version of the ACI drop-weight test proposed by Badr and Ashour in 2005. The results

produced from their modified version of the ACI test proved to be much more

statistically accurate. Therefore, procedures documented by Badr and Ashour were

followed closely with very few modifications.

Various materials were used to produce seven distinctly different groups of drop-

weight impact test specimens. The types of materials investigated in this study include

plain concrete, polypropylene fiber-reinforced concrete (PFRC), and a high-volume fly

ash-wood fiber material (FA-WF). Impact tests were conducted at three curing ages: 7,

14, and 28 days.

1.1 Green materials

Several mix designs investigated in this study consist of environmentally green

materials produced as by-products of other manufacturing processes. For example, fly

ash is a by-product of the combustion of pulverized coal. Its pozzolanic characteristics

make it a beneficial ingredient in concrete, and its use has increased with increasing

energy costs in cement production. Recent studies show that nearly 90 million tons of fly

ash is produced in the United States alone, and approximately 18 to 20 percent of that

total is used in the production of concrete and concrete products (Joshi and Myers, 2005).
3

Fly ash became readily available in the 1930s and was initially used as a volume

replacement of hydraulic cement. Researchers now know that fly ash provides several

benefits to concrete including improved resistance to deterioration from sulfates,

improved workability of fresh concrete, higher strengths at later ages of hardened

concrete, and reductions in temperature rise during initial hydration in large masses of

concrete (ACI 232.2R-03).

Another main ingredient in several mix designs was wood fiber. The United

States is currently facing the serious challenge of disposing of wood-based waste in many

landfills throughout the country that are already near capacity. In 1994, 13.2 million

metric tons of solid wood waste was generated, and only 1.3 million tons were used for

recycling or compositing. The discarded wood was either burned or placed in landfills.

Examples of compositing include oriented strandboard (OSB), particleboard, and

Spaceboard. These composites are lightweight, tough, easy to use, and are excellent

insulators (Joshi and Myers, 2005).

Solid wood waste includes wooden pallets and containers, full-sized lumber

salvaged from building demolition, old wooden utility poles and railroad ties, furniture,

and miscellaneous products made from wood. This waste has great potential for use in

many types of building products. Recycled wood fibers held together with an inorganic

matrix, such as gypsum and Portland cement, form a composite that can be used in

various structural and architectural applications (Falk, 1994). The recycled wood waste

material used in this study was milled oak wood fibers, which were milled from old

loading pallets. The wood fibers were provided by Encore Building Solutions in St.

Louis, Missouri.
4

1.2 Uses of fiber-reinforced concrete

Several types of fibers are used to reinforce concrete. The basic fiber categories

are steel, glass, synthetic, and natural fibers. Fiber-reinforced concrete (FRC) is currently

used in hydraulic structures, airport and highway paving, industrial floors, bridge decks,

thin-shell structures, and shotcrete linings and coverings. Steel and synthetic FRC has

also been used in place of welded wire fabric reinforcement. Many tests have proven that

the addition of fibers greatly improves energy absorption and cracking resistance of

concrete under dynamic loads. The energy absorption of the material is commonly

termed as toughness under impact. Sources of dynamic loads include impact from

missiles and projectiles, earthquakes, and machine dynamics (ACI 544.1R-96).

1.3 Importance of statistics

The design of FRC elements relies heavily on the statistical consideration of their

properties because of the significant influence of the fabrication method, sampling, and

testing. The orientation and concentration of fibers within the structural element, which

have a huge impact on the mechanical properties of the element, vary with the method of

placing and degree of compaction. The variations in mechanical properties should be

taken into account in deciding the minimum number of tests required to determine the

mechanical properties. Variations in results are higher for impact testing than for either

compressive or flexural testing. The observed coefficient of variation (COV) in impact

resistance is often greater than 50 percent. Therefore, many specimens are needed to

develop reliable conclusions about the normality of the distribution of impact resistance

test results (Nataraja et al., 1999).


5

The normality of a distribution is a measure of how well the results follow a

normal distribution curve. A normal distribution curve is a symmetric, single-peaked,

bell-shaped density curve based on a mathematical model that can be used to describe a

set of single-variable data. The curve is idealized and not completely accurate. The

normal distribution curve for a set of data is described using the mean (η) and standard

deviation (s) of the data. The mean controls the location of the peak of the curve, and

the standard deviation controls the spread of the normal curve. The standard deviation is

located at the point at which the curve changes curvature on either side of the mean. The

function for the normal density curve is listed in equation (1).


2
−1⎛ x − η ⎞
1 ⎜ ⎟
F(x) = e2⎝ σ ⎠
Eq. (1)
σ 2π

The 68-95-99.7 rule states that for any normal distribution, 68 percent of the

observations fall within a standard deviation of the mean, 95 percent of the observations

fall within two standard deviations of the mean, and 99.7 percent of the observations fall

within three standard deviations of the mean. The vertical scale for a frequency

histogram depends on the total number of observations (Moore et al., 1989). A

maximum of 18 specimens were tested for each group in the drop-weight test, so the

actual distribution of the impact data is skewed, and the normal distribution curve does

not fit the distribution well.

All normal distributions are equivalent when measurements are made in standard

deviations in relation to the mean as the origin. This occurrence is known as the standard

normal distribution. The equation used to standardize variables in a data set is listed in
6

equation (2). The standardized variable (S) is a function of the mean (η) and standard

deviation (σ).

X-η
S= Eq. (2)
σ

A standardized normal distribution plot shows how many standard deviations the

original observation falls away from the mean. Standardization changes the mean to zero

and the standard deviation of the standardized data to one. An example of a standardized

normal distribution plot is shown in Figure 1.

3
Standardized normal distribution

-1 First crack
Ultimate
resistance
-2

-3
0 5 10 15 20 25 30 35 40
Impact resistance in blows

Figure 1. Standardized normal distribution for drop-weight specimens


7

2. RELATED WORK

This experimental program was conducted mainly to evaluate the effectiveness of

a high-volume FA-WF material at resisting repeated low velocity drop-weight impact.

No experimentation on the impact resistance of this material has taken place in the past.

However, numerous studies have been carried out to analyze the drop-weight impact

resistance of other types of FRCs. Other types of fiber reinforcement include synthetic

fibers and steel fibers. In two previous studies referenced herein, the drop-weight impact

resistances of PFRC and steel fiber reinforced concrete (SFRC) were measured. The

PFRC was tested according to modified ACI impact testing procedures (Badr and

Ashour, 2005), and the SFRC was tested in accordance with current ACI drop-weight

impact testing procedures (Nataraja et al., 1999).

2.1 Drop-weight impact test proposed by ACI Committee 544

Several types of tests have been used to measure the impact resistance of FRC.

ACI classifies these tests in the following categories: (a) weighted pendulum Charpy-type

test; (b) drop-weight test; (c) constant strain-rate test; (d) projectile impact test; (e) split-

Hopkinson bar test; (f) explosive test; and (g) instrumented pendulum impact test (ACI

544.2R-89).

The repeated impact drop-weight test is the simplest of all the impact tests, and

therefore is widely used to quantify impact resistance of FRC. This test yields the

number of blows necessary to cause prescribed levels of damage in the test specimen.

The number of blows recorded serves as a qualitative estimate of the energy absorbed by

the specimen at the levels of distress specified. The relative impact resistances of various

materials can easily be established using the repeated drop-weight impact test. The
8

impact test equipment and procedure are outlined by ACI Committee 544 (ACI 544.2R-

89). Data from the impact test is usually exceedingly scattered due to the nature of the

test and nonhomogeneous condition of the concrete. Also, the fabrication and testing

processes strongly influence the impact strength of FRC. Therefore, statistical

considerations must be taken into account when designing FRC systems.

The equipment for the ACI drop-weight impact test consists of the following: (1)

a standard, manually operated 4.54 kg (10 lb) compaction hammer with a 457 mm (18

in.) drop (ASTM D 1557), (2) a 63.5 mm (2.5 in.) diameter hardened steel ball, and (3) a

flat baseplate with a positioning bracket. In addition to this equipment, a mold to cast

152 mm (6 in.) diameter by 63.5 mm (2.5 in.) [±3 mm ±(.125 in.)] concrete specimens

is needed. This task can be accomplished by using standard ASTM C 31 or C 470 molds.

Specimens are made in 152 mm (6 in.) diameter cylinder molds according to

procedures recommended for compressive cylinders. The molds can be filled partially to

the 63.5 mm (2.5 in.) depth and float finished, or specimens may be sawn from full-sized

cylinders to yield a specimen with the proper thickness. ACI Committee 544

recommends that specimens be tested at 7 and 28 days of age. Specimens may also be

tested at 90 days of age if desired. Curing and handling of the specimens should be

similar to that used for compressive cylinders, but accelerated curing is not desirable.

The thickness of each specimen should be recorded to the nearest 2 mm (0.0625

in.). The reported thickness is determined by averaging the measured thickness at the

center and each edge of the specimen along any diameter across the top surface. After

the thickness of the specimen is recorded, the bottom of the specimen should be coated

with a thin layer of petroleum jelly or grease. The specimen is then placed on the base
9

plate within the positioning lugs with the finished side face up. The positioning bracket

is bolted in place, and the hardened steel ball is placed on top of the specimen within the

bracket. Before testing, pieces of foam are placed between the positioning lugs and the

specimen to prevent movement of the specimen during testing to the first visible crack.

Once the specimen and steel ball are in position, the drop hammer is placed with

its base upon the steel ball and held there with just enough down pressure to keep it from

bouncing off the ball during the test. The steel ball transfers a single-point impact to the

surface of the specimen. ACI recommends that the base plate be fastened to a rigid base

during the test. An automated system with an automatic counter may also be used if the

equipment is available. Figure 2 displays the testing device for the repeated drop weight

impact test proposed by ACI Committee 544 (ACI 544.2R-89).

Figure 2. Drop-weight test apparatus (ACI 544.2R-89)


10

The hammer is dropped repeatedly, and the number of blows required to cause the

first visible crack on the top and to cause ultimate failure are both recorded. ACI

Committee 544 defines the ultimate failure as the opening of cracks in the specimen so

that the pieces of concrete are touching three of four positioning lugs on the base plate.

ACI Committee 544 reports that results of these tests exhibit a high variability and may

vary considerably with different types of mixtures and fiber contents (ACI 544.2-89).

2.2 Modified ACI drop-weight impact test for concrete

A modified ACI drop-weight impact test for concrete was proposed by Badr and

Ashour in an effort to reduce the large variations in the existing ACI drop-weight impact

test proposed by ACI Committee 544. Large variations that occur in test results from the

existing ACI method suggest that the test is rather unreliable. Large variations are a

universal problem in impact testing, and it is very difficult to develop ways to reduce the

variations. There are several sources of error in the current ACI drop-weight test. First,

the likelihood of erroneous results is increased by using a single point of impact because

the impact is localized on such a small amount of material. Second, the subjectivity of

the test is increased when cracks are allowed to occur at any location on the specimen.

Furthermore, by declaring failure when the pieces of the specimen touch the lugs, more

impacts may be applied than necessary to break the specimen. Criteria for accepted

failure modes must be set in place. Lastly, specimens must all be prepared in the same

manner (Badr and Ashour, 2005).

The changes listed below were proposed by Badr and Ashour to reduce the

amount of variation in the results of the drop-weight impact test:

1. Notch the specimens to force cracks along a predefined path.


11

2. Use a 50 mm (2 in.) line of impact from a steel bar, rather than using a single point

of impact from a steel ball.

3. All the specimens should have similar faces. Either cast the specimens in identical

molds and slice them to the proper thickness with a wet saw or trowel the top

surface of each specimen.

4. Declare ultimate failure when the specimen is separated completely into halves, or

the specimen touches the two opposite lugs of the apparatus.

5. Only accept specimens that crack through the line of impact; reject any other

failure locations.

6. The specimen thickness should be reduced from 63.5 mm (2.5 in.) to 50 mm (2

in.) to reduce the time required to test a single specimen, especially if the testing

apparatus is manually operated.

In the previous work conducted by Badr and Ashour, 40 PFRC specimens were

tested using the modified technique. Also, 40 specimens of the same mix design were

tested according to the current ACI drop-weight impact test for comparison. The mixture

proportions used in the study are listed in Table 1, and the physical properties of the

polypropylene fibers are listed in Table 2.

Table 1. Mixture proportions for PFRC specimens (Badr and Ashour, 2005)

Component Contents per m3 of concrete


Cement 410 kg
Fine aggregate 800 kg
Coarse aggregate 1000 kg
Water 185 L
High-range water reducer 4.1 L
Polypropylene fiber 3 kg
Unit conversion: 1 kg = 2.205 lb; 1 L = 33.814 floz
12

Table 2. Physical properties of polypropylene fiber (Badr and Ashour, 2005)

Physical properties and dimensions


Specific gravity 0.91
Tensile modulus 4.1 Gpa
Tensile strength 560 MPa
Length 12 mm
Nominal diameter 18 µm
Unit conversion: 1 MPa = 145 psi; 1 mm = 0.0394 in.

A rotary drum mixer was used to batch each mix. The aggregates and cement

were mixed dry for approximately 1 minute. The aggregates consisted of quartzite gravel

of 10 mm (0.4 in.) nominal maximum size and quartzite sand. Approximately half the

water was added after 1 minute of mixing. The remainder of the water and high-range

water reducer was added after 2 minutes of mixing. The concrete was allowed to mix 3

minutes before the polypropylene fibers were added slowly by hand. Once the fibers

were added, the concrete mixed 5 minutes to reach a uniform distribution. The slump test

yielded values of 80 mm and 105 mm (3.15 in. and 4.14 in.) for the first and second

batches, respectively (Badr and Ashour, 2005).

Specimens were made from two identical batches of concrete. Each batch

produced enough cylinders to create 40 test specimens. Half of the specimens were

tested according to the current ACI test method and half according to the proposed

method. Standard cylinders with a diameter of 150 mm (6 in.) and a height of 300 mm

(12 in.) were cast and demolded after a 24 hour period. Then, the cylinders were cured in

a moisture room seven days, after which they were cut with a diamond blade to achieve a

specimen thickness required for each test method. The top and bottom portion of the
13

cylinders were discarded. The specimens were placed in an environmental chamber until

a testing age of 28 days (Badr and Ashour, 2005).

Compressive strengths were determined using ten 100 mm (4 in.) cubes from each

batch. The cubes were tested according to BS 1881: Part 108: 1983. A total of 20 cubes

were tested at 28 days of age. The compressive strength test results are shown in Table 3.

Table 3. Compressive strength results (Badr and Ashour, 2005)

Batch No. Batch 1 Batch 2 Overall


Mean, MPa 38.6 44.1 41.3
Standard deviation, MPa 2.80 3.46 4.17
Coefficient of variation, % 7.26 7.85 10.09
Unit conversion: 1 MPa = 145.04 psi

Impact testing was conducted using a standard soil compaction machine, which

applies and counts the number of blows automatically. A total of 40 specimens were

tested according to the current ACI drop-weight test proposed by ACI Committee 544.

For the modified version of the ACI drop-weight test, a steel bar of 13 mm (0.5 in.) in

diameter and 50 mm (2 in.) in length was welded to the bottom of a steel cylinder 50 mm

(2 in.) in diameter and length. The bar was allowed to rest on top of the specimen during

the test, so the impact was transferred through the bar as a line load on the top surface of

the specimen. A total of 40 specimens were tested using the modified technique as well.

The number of blows to achieve first crack (FC) and ultimate resistance (UR) were

recorded for each specimen.

Table 4 presents the impact resistances of the PFRC specimens using the current

ACI impact test and the modified test procedure proposed by Badr and Ashour.
14

Table 4. Drop-weight impact test results (Badr and Ashour, 2005)

Current ACI method Proposed modified technique


Batch 1 Batch 2 Batch 1 Batch 2
Specimen FC UR FC UR FC UR FC UR
1 11 18 9 16 12 23 13 15
2 12 27 12 20 20 29 19 24
3 17 30 14 25 22 34 23 29
4 26 38 15 28 27 38 26 33
5 28 40 24 43 32 41 29 38
6 32 41 33 52 34 43 32 40
7 34 65 43 74 39 48 34 43
8 43 73 47 63 40 53 37 47
9 46 60 55 79 43 54 39 50
10 53 89 56 73 45 57 42 52
11 54 100 58 89 45 58 42 55
12 65 95 64 95 48 61 43 56
13 67 89 66 81 49 63 44 58
14 77 121 68 101 52 68 47 64
15 79 121 70 85 54 72 52 65
16 81 104 76 98 59 73 55 68
17 97 135 76 103 62 78 57 70
18 99 127 90 141 66 81 64 73
19 108 141 109 129 74 87 73 82
20 148 173 118 134 77 96 79 86

As illustrated in Table 4, the results from the current ACI method are inconsistent.

For example, specimen 13 from the first group tested according to the current ACI drop-

weight test has a higher FC resistance than specimen 11 of that same group. However,

the UR of specimen 13 is lower than the UR of specimen 11. All specimens in both

groups tested according to the modified ACI method are consistent.

A summary of the results from the tests conducted by Badr and Ashour is

presented in Table 5. The table shows that the COVs for the current ACI method are

much higher than those using the modified technique.


15

Table 5. Comparison of the drop-weight test methods (Badr and Ashour, 2005)

Batch 1 Batch 2 Overall


Method Parameter FC UR FC UR FC UR
Current Mean (blow) 59 84 55 76 57 80
ACI Standard deviation (blow) 36.2 43.9 31.2 37.3 33.4 40.4
method Coefficient of variation, % 61.4 52.1 56.6 48.7 58.6 50.2
Mean (blow) 45 58 43 52 44 55
Modified
technique Standard deviation (blow) 17.6 19.8 17.3 19.1 17.3 19.4
Coefficient of variation, % 39.1 34.3 40.7 36.5 39.4 35.2

Due to the reduced thickness of the modified specimens, the number of blows to

achieve the FC and UR of the specimen is much less than that required for specimens

fabricated using the current ACI method. Overall, there was a 22 percent reduction in the

FC mean and 30 percent reduction in the UR mean by using the modified drop-weight

technique. Although using standard deviations to compare impact results is not suitable,

the standard deviations from the modified technique are about half of those obtained

using the current ACI method.

The COV, which is the standard deviation divided by the mean, is used more

commonly because it accounts for the mean and standard deviation. In fact, several ACI

committees have adopted the COV as a measure of inconsistency, rather than the

standard deviation. As shown in Table 5, the COV values for the modified technique are

much less than those of the current ACI method. There is nearly a 30 percent reduction

in the overall COV value when using the modified technique. Based on drop-weight test

results using other types of FRC, the reduction of the COV using the modified technique

should remain consistent for any type of FRC (Badr and Ashour, 2005).

The minimum number of tests required to keep the percent error of the measured

average below a specified limit at a specific level of confidence can be determined using
16

the COV in equation (3) below. In equation (3), n is the minimum number of tests, e is

the specified error, v is the COV value, and t is a value obtained from the t-student

distribution for the specified level of confidence (Nataraja et al., 1999).

n = (t2v2)/e2 Eq. (3)

Table 6 shows the number of specimens required to keep the error under a

specific limit for 95 percent and 90 percent confidence levels for both techniques. The

number of specimens required to keep the error under 10 percent on a 95 percent

confidence level is 42 for the modified technique and 93 for the current ACI method.

Obviously, a great improvement in results is seen when using the modified technique

proposed by Badr and Ashour.

Table 6. Number of specimens required for given percent error (Badr and Ashour, 2005)

Current ACI method Modified technique


Percent 95% 90% 95% 90%
error FC UR FC UR FC UR FC UR
10 93 68 56 41 42 34 26 20
15 41 30 25 18 19 15 11 9
20 23 17 14 10 11 8 6 5
25 15 11 9 7 7 5 4 3
30 10 8 6 5 5 4 3 2
40 6 4 4 3 3 2 2 1
50 4 3 2 2 2 1 1 1

The modified ACI drop-weight test described improved the consistency of the

results and reduced the time required for testing. If the current common practice of

testing five specimens is used to establish the impact resistance of concrete mixtures, the

error in the measured value obtained using the current ACI test could possibly fall
17

between 30 percent and 40 percent depending on the confidence level. The error from

testing only five specimens using the modified test would be reduced to 25 percent.

2.3 Impact resistance of steel fiber-reinforced concrete

The objective of the research conducted by Nataraja was to study the impact

resistance of SFRC by applying the ACI drop-weight test proposed by ACI Committee

544 (Nataraja et al., 1999). The goal was to assess the variations in the impact properties

of the SFRC.

The impact strength of concrete is greatly increased with the addition of steel

fibers, similar to concrete reinforced with polypropylene fibers. Although the impact

strength is clearly increased with the addition of steel fibers, the results from the ACI

drop-weight test are scattered. Several sources of error, as mentioned previously, include

the likelihood that concentrations and orientations of the steel fibers vary throughout the

specimen. Concentrations of fibers within the specimen depend on several factors

including the method of placement, workability of the mix, and degree of compaction.

Steel fibers detrimentally affect the workability of the concrete as well.

The test specimens were composed of the mix design presented in Table 7.

Granite aggregate with a maximum nominal diameter of 20 mm (0.75 in.) and river sand

conforming to zone IV of IS: 383-1970 were used for coarse and fine aggregates,

respectively. The water cement ratio was 0.49, which produced average 28-day

compressive strengths of 29.4 and 36.0 MPa (4264 and 5222 psi) for the plain concrete

and FRC, respectively. The round crimped steel fibers of 0.5 mm (0.02 in.) diameter had

a breaking strength of 550 Mpa (80 ksi) and an aspect ratio of 55.
18

Table 7. Mix proportions for SFRC (Nataraja et al., 1999)

Component Contents per m3 of concrete


Cement 397 kg
Fine aggregate 562 kg
Coarse aggregate 1152 kg
Water 195 kg
High-range water reducer None
Crimped steel fiber 0.5% by volume
Unit conversion: 1 kg = 2.205 lb

Mixing procedures used here were similar to those used by Badr and Ashour.

Twelve SFRC standard cylinders of 150 x 300 mm (6 x12 in.) were made in two batches

of six. Five cylinders of each group were cut into thicknesses of 64 mm (2.5 in.), so each

cylinder provided three specimens. Thirty specimens were tested overall. Similarly, 12

cylinders of plain concrete were batched, providing a total of 32 specimens. Test results

for the first batch of SFRC specimens are shown in Table 8. Nataraja also reported the

average transit time and pulse velocity, which are not shown in the table.

The COV for the number of blows to FC and to UR, 55.1 and 46.0, respectively,

are very similar to those recorded in Table 5; 58.6 and 50.2 for FC and UR, respectively.

Both tests were conducted using the current ACI drop-weight test. In this regard, the

type of fiber used causes no distinction in the statistical results. The average number of

blows needed for FC and UR for the SFRC specimens were 98 and 139, respectively.

However, the average number of blows to FC and UR were much lower for the PFRC

specimens presented in Table 5, which shows the average number of blows to reach the

FC and UR to be 57 and 80, respectively. Therefore, based on these two results, the

SFRC specimens have a higher impact resistance than PFRC.


19

Table 8. Test results of SFRC (Nataraja et al., 1999)

Avg.
Specimen thickness, Blows to Blows to
No. mm Mass, g first crack failure
1 64 2904 196 270
2 65 2914 98 140
3 63 2834 72 95
4 64 2798 46 80
5 62 2776 46 86
6 64 2880 153 181
7 62 2737 144 189
8 64 2800 160 210
9 61 2710 39 60
10 64 2932 35 70
11 63 2840 81 128
12 66 2990 130 153
13 62 2770 84 131
14 61 2760 160 222
15 67 3012 34 68
Mean 63.5 2844 98 139
S.D. 1.73 92 54 64
COV 2.72 3.2 55.1 46
Unit conversion: 1 mm = 0.0394 in, 1 kg = 2.205 lb

Similarly, Table 9 presents test results from the first batch of plain concrete

specimens, as recorded by Nataraja. The table shows that, although the average number

of blows for each level of damage decreased, the COV remained approximately the same

for plain concrete, 49.3 and 46.7 percent for FC and UR, respectively. The highest

number of blows to FC was 130, and the corresponding UR for that specimen was 136

blows. The lowest impact resistance recorded was with specimen 9, which had a FC

resistance of 21 blows and an UR of 30 blows. The mean was calculated to be 71 and 77

blows for FC and UR, respectively.


20

Table 9. Test results of plain concrete (Nataraja et al., 1999)

Avg.
Specimen thickness, Blows to Blows to
No. mm Mass, g first crack failure
1 64.0 2790 114 124
2 63.5 2826 86 92
3 64.0 2850 119 125
4 63.0 2852 51 55
5 63.5 2872 34 41
6 63.5 2780 38 42
7 63.0 2792 63 70
8 65.5 2950 130 136
9 63.0 2745 21 30
10 62.5 2800 60 62
11 65.0 2862 43 51
12 63.0 2690 79 83
13 63.5 2864 38 44
14 64.0 2800 90 96
15 62.0 2814 48 56
16 63.5 2818 120 130
Mean 63.53 2819 71 77
S.D. 0.87 59 35 36
COV 1.37 2.09 49.3 46.7
Unit conversion: 1 mm = 0.0394 in, 1 kg = 2.205 lb

3. STUDY OF OBJECTIVES

The objective of this research study was to verify the statistical benefits of using

the modified ACI drop-weight test (Badr and Ashour, 2005), rather than using the current

ACI method proposed by ACI Committee 544. Furthermore, the tests were used to

investigate the effectiveness of a high-volume FA-WF material at absorbing energy from

a repeated low velocity impact. Seven groups of specimens were tested using the

modified ACI drop-weight technique.


21

3.1 Test setup

The test setup and procedures follow those proposed by Badr and Ashour with a

few minor differences. These differences include:

1. All specimens were troweled, not cut.

2. The impact hammer was manual, so it could be carried to any location easily.

3. Specimens were not allowed to move laterally until fracture occurred.

Specimen molds were constructed from pvc pipe 6.4 mm (0.25 in.) thick with a

150 mm (6 in.) inner diameter. A 3.05 m (120 in.) piece of pvc pipe was cut into lengths

slightly over 51 mm (2 in.) to create 54 round molds. Each mold was reduced to

50.8±1.27 mm (2 ±.05 in.) using a lathe. Figure 3 displays the various stages of the

mold preparation, and Figure 3-a shows one mold positioned on the lathe. Once all the

molds were cut, a small hole was drilled through opposite sides of each mold using a drill

press (see Figure 3-b). Then, each mold was cut down its length so specimens could be

easily extracted once hardened (see Figure. 3-c). Enough triangular wood pieces were

cut for each mold using a miter saw. All the wood pieces were allowed to soak in

hydraulic oil for a period of 24 hours to prevent concrete from adhering to them. Two

wood pieces were screwed to the inside of each pvc mold to create notches in the drop-

weight specimens, as shown in Figure 3-d.

Instead of using an automated soil compactor, a manual device was fabricated to

conduct the tests. The test fixture consisted of three steel plates, four steel angle sections,

and a handheld 4.54 kg (10 lb) modified proctor hammer. The proctor hammer was

ordered from Humbolt Industries, and the steel plates and angle were purchased from

Rolla Rental. Both the top and bottom plates were 254 x 228.6 x 6.4 mm (10 x 9 x 0.25
22

in.). The middle plate was 254 x 149.2 x 6.4 mm (10 x 5.875 x 0.25 in.), but had three 51

mm (2 in.) diameter holes cut into it. Two holes were cut to allow for visual inspection

of the test specimen, and the impact piston was placed in the center hole. A ring with a

diameter of 54 mm (2.125 in.) was welded to the top of the center hole to hold the impact

piston in position. Figure 4 shows the test fixture. The weight of the piston was 848 g

(1.87 lb), and the weight of the entire test fixture was 204 g (45 lb).

(a) Mold thickness using lathe (b) Mold screw hole

(c) Mold cut for specimen release (d) Hydraulic oil applied to formwork

Figure 3. Drop-weight impact mold preparation


23

Proctor hammer

6.4 mm Plate 254 mm

Piston
ring 229 mm

Raised notches
476 mm

(a) Impact device (b) Impact schematic

Figure 4. Modified ACI drop-weight impact test fixture

A hole was cut into the top steel plate, so the hammer could slide into it. A

washer was spot welded to the outside casing of the hammer, and 19 mm (0.75 in.) bolts

were used to hold the washer and hammer to the top plate. A steel cylinder with a bar

welded across the bottom was used to transfer the impact onto the specimen, similar to

that used in the modified technique. This steel cylinder will be called the impact piston.

The cylinder is 51 mm (2 in.) in diameter and 51 mm (2 in.) long but has a flat groove cut

along its length to prevent rotation during the test. The piston slides into the ring welded

in the center of the middle plate. A small flat piece of steel was welded into the center

ring to prevent the piston from rotating during the test. The piston was not constrained

from moving in the vertical direction. The impact piston is shown in Figure 5.
24

Flat face

51 mm dia. cylinder
51 mm

13 mm steel bar

(a) Impact piston (b) Impact piston schematic

Figure 5. Impact piston

3.2 Materials and mix designs

3.2.1 Materials

Materials used in the preparation of the modified drop-weight specimens include:

Class C fly ash, type I Portland cement, wood fibers, limestone, sand, high-range water

reducers, and potable water.

ASTM Class C fly ash was provided by Encore Building Solutions (EBS) of St.

Louis, Missouri. Fly ash was required to fabricate four of the seven groups of drop-

weight specimens investigated in the study. EBS receives the fly ash from the Rush

Island Power Plant in Jefferson County, Missouri. Table 10 displays the chemical

composition and properties of the Class C fly ash.

Commercial grade type I Portland cement was used to fabricate five of the seven

groups of drop-weight specimens. Portland cement was patented by Joseph Aspdin in

1824 and is now the most widely used construction material in the world. Of the five

types of Portland cement, type I is the most widely available and is used in general
25

applications of reinforced concrete construction. The Portland cement used for this study

complied with ASTM C 150-05 specifications. The cement had a dry density of

approximately 1506 kg/m3 (94 lb/ft3). Figure 6 displays samples of the Class C fly ash

and Portland type I cement.

Table 10. Chemical composition of fly ash (Joshi et al., 2005)

Rush Island Type I Portland


Parameter
fly ash (%) cement (%)
Sulfur in ash 0.7 -
Sulfur in ash (SO3) 1.75 2.5
Fineness (325 sieve) 81.9 -
Moisture 0.03 -
Loss of ignition (LOI) 0.17 1.4
Density 2.73 -
Specific gravity 2.74 -
Titanium oxide as TiO2 1.23 -
Aluminum oxide as Al2O3 17.06 4.9
Calcium oxide as CaO 26.12 64.4
Iron oxide as Fe2O3 6.31 2.1
Potassium oxide as K2O 0.39 -
Magnesium oxide as MgO 5.77 3.5
Sodium oxide as Na2O 1.87 -
Silicon oxide as SiO2 35.43 20.08
Phosphorus oxide as P2O5 0.9 -
Slagging index 0.34 -

The milled wood fibers of oak trees were provided by EBS. The fibers are

recycled by milling old wooden loading pallets. The mechanical properties of oak wood

are listed in Table 11.

The gradation of the milled wood fibers ranged from a maximum size of 12.7 mm

(0.5 in.) to fine particles of dust. The majority of the fibers were about 6.35 mm (0.25
26

in.) in length. In every group that wood fibers were used, the fibers were added to the

other contents of the mixture in a fairly dry state with a moisture content of roughly 10

percent, determined in accordance with ASTM C 566-04. The dry density of the

compacted wood fibers was determined to be 275.5 kg/m3 (17.2 lb/ft3). A sample of the

milled wood fibers is shown is Figure 7, along with other constituents in the mix designs.

(a) Class C fly ash (b) Portland cement, type I

Figure 6. Class C fly ash and Portland cement

Table 11. Mechanical properties of oak (Joshi et al., 2005)

Mechanical Properties Green Air Dried


3
Weight (kg/m ) 1009 753
Modulus of Rupture (MPa) 55.85 95.84
Modulus of Elasticity (MPa) 8274 11170
Maximum crushing strength parallel to grain (MPa) 24.3 48.5
Compression perpendicular to grains (MPa) 5.86 9.72
Maximum shearing strength parallel to grain (MPa) 8.76 13.03
3 3
Unit conversion: 1 kg/m = 0.0624 lb/ft ; 1 MPa = 145.04 psi

Presented in Figure 7-b, Gasconade dolomitic limestone from Capital Quarry,

located north of Rolla, MO, was used in the mix designs for Groups 2, 3, 5, and 6. The

limestone had a nominal maximum size of 12.7 mm (0.5 in.) and a bulk specific gravity
27

of 2.70 in an oven-dried condition. The absorption of the aggregate was measured to be

1.2 percent. The moisture content of the limestone in each group remained below 0.1

percent during the mixing processes.

(a) Wood fibers (b) ½ in. limestone

(c) River sand (d) High-range water reducers

Figure 7. Consitutents of drop-weight test mix designs

The sand had a bulk specific gravity of 2.54 in an oven-dried condition, and the

absorption was calculated to be approximately 1.4 percent. Little Piney Creek near Rolla,

Missouri, was the source of the sand. The moisture content of the sand did not exceed

0.75 percent in any of the groups. A picture of the river sand is presented in Figure 7-c.
28

Glenium 3000 NS, a high-range water reducer (HRWR) was added in various

quantities to each mix as needed. The superplasticizer was added to increase the

workability and cohesiveness of the mix. Another benefit of using the admixture was a

low water-cement ratio, which increased the compressive strength of each mix. Glenium

300 NS is produced by BASF and meets ASTM C 494-05 requirements for type A and

type F admixtures. Containers of HRWR are presented in Figure 7-d.

Collated polypropylene fibrillated fibers were used in the Group 3 mix. The fiber

is made to mechanically bond with the concrete matrix, thus enhancing the impact

resistance and durability of the concrete. Polypropylene fibers are most commonly used

as a secondary reinforcement for temperature and shrinkage considerations but are used

in blast-resistant structures as well. The polypropylene fibers used in this study comply

with ASTM C 1116-06 specifications, as well as with other national building codes.

Mechanical properties of the fibers are listed in Table 12. Figure 8 shows a photograph

of the polypropylene fibers used in Group 3.

Table 12. Specification data for polypropylene fibers (Nycon, 2007)

Fiber Type Homopolymer polypropylene


Fiber Length (mm) 19
Color White / Clear
Ultimate elongation 20% at 21°C
Melting point (°C) 165
Ignition point (°C) 594
Specific gravity 0.91
Tensile strength (MPa) 379.2
Youngs modulus (GPa) 4.14
Unit conversion: 1 mm = 0.03937 in, 21°C = 70°F, 1 MPa = 0.145 ksi
29

Rediron 9000 capping compound, purchased from Gilson Company, Inc., was

used to cap the ends of the cylinders before conducting the compression and modulus of

elasticity tests. The compound was allowed to melt in a warming pot to a temperature of

approximately 135°C (275°F). The compressive strength of a 50.8 mm (2 in.) cube of the

sulfur compound exceeds 55.1 MPa (8,000 psi) after two hours of curing (Gilson

Company, Inc., 2007). Figure 8-b shows the hardened flakes of the Rediron 9000

capping compound.

(a) Polypropylene fibrillated fibers (b) Rediron 9000 capping compound

Figure 8. Polypropylene fibers and capping compound

3.2.2 Mix proportions and processes

Seven groups of specimens were evaluated for impact resistance using the

modified ACI drop-weight test. The mix proportions for each group are shown in Table

13.

The first group of drop-weight specimens was fabricated from Class C fly ash,

type I Portland cement, wood fibers, and potable water. This mix was designated as the

FA-C-WF mix. A high-range water reducer was also added to the mix. The mixture
30

portions are given in the second column of Table 13. In preparation for making the

specimens, the 54 pvc forms were attached to a 1.22 x 2.44 m (4 x 8 ft) sheet of plywood.

The forms were spaced approximately 200 mm (3 in.) apart to allow for a handheld form

vibrator to be placed between them. The base of each pvc form was attached to the

plywood using silicone caulking. The silicone was allowed to cure for at least 12 hours

before concrete was placed in the molds.

Table 13. Mix proportions by weight

Group 5 Group 7
Group 1 Group 2 Group 3 Group 4 FA-WF- Group 6 Concrete
Component FA-C-WF Concrete PFRC FA-WF A WF Con layer
Class C fly ash 462.9 - - 839.4 519.0 - -
Portland cement
(type I) 278.7 410.1 410.1 - - 451.7 410.1
White oak wood
fibers 112.1 - - 163.4 120.1 136.2 -
1/2" limestone - 999.6 999.6 - 611.9 808.9 999.6
Sand - 799.3 799.3 - 576.7 647.1 799.3
Water 281.9 144.2 144.2 299.5 248.3 136.2 144.2
High-range water
reducer (ml/kg) 2.6 5.2 5.2 2.6 2.6 5.2 5.2
Polypropylene
fibers - - 3.20 - - - -
Water / cement
ratio 0.38 0.35 0.35 0.36 0.48 0.30 0.35
% Wood fiber by
weight 10.0 0.0 0.0 12.5 6.0 6.2 0.0
Slump (mm) 76 178 127 51 178 51 153
3 3 3
All applicable units are in kg/m ; Unit conversion: l kg/m = 1.686 lb/yd

Note: The top layer of Group 7 is the FA-C-WF mix used in Group 1

The forms were brushed with hydraulic oil an hour after the silicone was applied

and again just before the mixing process began. Components of the mix were weighed in
31

buckets to the nearest half pound. A total of 0.085 m3 (3 ft3) of material was needed to

fill all 54 forms and produce enough cylinders for compression, split cylinder, and

modulus tests. Since the material was fairly difficult to mix, the total volume was broken

into two separate batches of 0.0425 m3 (1.5 ft3).

Shown in Figure 9, a conventional rotary drum mixer was used for mixing. First,

the mixer was washed to dampen the inside of the drum. Then, all the fly ash, cement,

and half the water were added to the drum and allowed to mix for one minute. The

HRWR was added to the other half of the water. After approximately one minute of

mixing, the inside of the drum was scraped to release any material stuck to the sides or

back of the drum. Then, half of the remaining water was added to the mixer, along with

the wood fibers. The fibers were added slowly to prevent balling of the material.

Finally, the remaining portion of water was added to the mixer. Mixing continued for

another 5 minutes after all the materials were added to the drum.

Once a uniform distribution of wood fibers was achieved, the material was poured

into a wheelbarrow and placed into the molds. After the molds were filled, a vibrator was

placed around each pvc mold to ensure there were no air voids or segregation in the

specimens. Figure 9-b displays several forms with the fresh material inside them. A

portion of the material was used for a slump test to check workability according to

ASTM C 143-05. The slump was determined to be 76 mm (3 in.). The specimens were

finished using trowels and then covered with a sheet of plastic. Compression, split

cylinder, and modulus specimens were made in compliance with ASTM C 192-06.

After a 24 hour period, the specimens were removed from the molds and placed in

a moist cure room until the time of testing. The moisture room was kept at about 22°C
32

(72°F) with 100 percent humidity. Specimens were tested at the following ages: 7 days,

14 days, and 28 days. Eighteen specimens were tested at each test age.

(a) Rotating drum mixer (b) Specimen preparation

Figure 9. Batching drop-weight impact specimens

Group 2 was composed of 54 specimens of plain concrete to be used as a control

group for comparison. The mix design is shown in the third column of Table 13. The

mix was batched in much the same way as Group 1; however, the entire 0.085 m3 (3 ft3)

required was mixed in one batch. First, the coarse aggregate, fine aggregate, and

Portland cement were mixed in the dry state for about 1 minute. Then, approximately

half the mixing water was added. After 2 minutes of mixing, the remaining portion of

water was added along with the HRWR. Mixing continued for approximately another 5

minutes to achieve a homogeneous mix. The slump value for the mix was about 178 mm

(7 in.). Figure 10-a displays 2 pvc forms filled with fresh concrete.

Group 3 was essentially the same mix design used in the previous study on

concrete reinforced with polypropylene fibers (Badr and Ashour, 2005), and it is listed in

the fourth column of Table 13. The PFRC mix was batched using the same process used
33

for Group 2 along with the addition of polypropylene fibers. The limestone, sand, and

Portland cement were mixed in a dry state for roughly 1 minute. Then, about half the

mixing water was added, and the HRWR was added to the remaining portion of water.

The remaining water and HRWR was added after approximately 2 minutes of mixing.

Mixing continued for another 4 minutes before the polypropylene fibers were added to

the mix. The fibers were added by hand to avoid balling of the concrete. Generally, the

smallest specimen dimension should be at least 3 times larger than the fiber length or

maximum aggregate size. Therefore, 19 mm (0.75 in.) fibers where chosen for the mix.

The slump of the fresh mix was measured at 127 mm (5 in.). Figure 10-b shows a fiber-

reinforced specimen.

(a) Plain concrete specimens (b) Fiber-reinforced concrete specimen

Figure 10. Concrete drop-weight impact specimens

Group 4 was composed of a FA-WF mixture developed in a previous study

conducted at the University of Missouri-Rolla (UMR) (Joshi et al., 2005). The mix

design is listed in the fifth column of Table 13. The mix design used in the previous

study was modified by slightly decreasing the relative quantity of wood fibers. This
34

action was done to increase the workability of the mix for larger test specimens. The

volume was split into two batches of 0.0425 m3 (1.5 ft3) to alleviate problems caused by

the material adhering to the sides of the mixer and to improve the quality of the mix.

First, a slurry consisting of all the fly ash and half the water was mixed for 1 minute.

After 1 minute of mixing, the material was removed from the sides of the drum using a

shovel or concrete scoop. Then, the material was allowed to mix while slowly adding

half the wood fibers. Finally, the remainder of the water and HRWR was added, along

with the other half of the wood fibers. The material was allowed to mix for 5 minutes

until the fibers were uniformly distributed. The FA-WF material was poured into a

wheelbarrow and then placed into the pvc molds. Once the molds were full, the fresh

material was consolidated using a tamping rod and vibrated with a handheld vibrator.

The slump of the FA-WF material was measured at 51 mm (2 in.).

Group 5 consisted of coarse and fine aggregates mixed with fly ash and wood

fibers. Therefore, this mixture was designated as FA-WF-A. The purpose of the

aggregates was to provide increased stiffness to the FA-WF mix. The materials were

mixed using relatively the same procedures listed for the previous groups. The

aggregates and fly ash were mixed in a dry state first. Then, half the mixing water was

added. After mixing for one minute, the wood fibers were added slowly, followed by the

remaining water and HRWR. Group 5 specimens were vibrated and finished using

trowels. The slump was measured at 178 mm (7 in.).

The specimens in Group 6 were batched using a normal weight concrete mix with

the addition of wood fibers. Table 13 contains the mix design used for the Group 6

specimens. The wood fibers were added in hopes of increasing the impact absorption
35

capabilities of the mix. The mixing procedures for Group 6 were the same as those used

for the previous groups. The slump was determined to be 51 mm (2 in.). Figure 11

shows a comparison between the wood fiber concrete and plain concrete. Notice the

significant amount of wood fibers in the specimen in Figure 11-a.

The seventh group was a layered construction of groups 1 and 2. A plain concrete

mix was batched first and allowed to cure for a 24 hour period. The molds were only

filled half way, about 25.4 mm (1 in.). The following day, the FA-C-WF mix used for

the first group was batched to fill the remaining portion of the molds. Therefore, the

specimens had a 25.4 mm (1 in.) plain concrete base and a 25.4 mm (1 in.) FA-C-WF

layer set on top. Each layer was mixed according to the procedures mentioned previously

for Group 1 and Group 2. The bottom layer of plain concrete was left in a roughened

state to provide some amount of shear interlock between the two layers.

(a) Wood fiber concrete (b) Plain concrete

Figure 11. Comparison of wood fiber concrete to plain concrete

Specimens were removed from the molds 24 hours after the top layer was placed

and then put in a moist cure room until testing age. Slump values for the FA-C-WF layer
36

and the concrete layer were 64 and 153 mm (2.5 and 6 in.), respectively. Figure 12

shows the fabrication of the two layers composing the Group 7 specimens.

3.3 Mechanical properties

Several mechanical properties were determined for each group of specimens.

These properties include the material’s compressive strength, indirect tensile strength,

and modulus of elasticity (MOE). Cylinders were capped with a sulfur compound before

the compressive strength and modulus were determined.

(a) Base concrete layer of Group 7 (b) Top WF-FA layer

Figure 12. Layered construction of Group 7

3.3.1 Compressive strength

The compressive strength of each group was determined using either a standard

specimen size of 150 x 300 mm (6 x 12 in.) or 100 x 200 mm (4 x 8 in.). Although the

150 mm (6 in.) cylinder provides a better representation of the material, 100 mm (4 in.)

diameter specimens were used in most cases because less material was needed to produce

them. The specimens were prepared in the lab according to ASTM C 192-06

specifications. The 150 mm (6 in.) diameter cylinders were made in 3 equal layers and
37

rodded 25 times per layer using a 16 mm (0.625 in.) diameter tamping rod. The 100 mm

(4 in.) diameter cylinders were made in only 2 layers. The specimens were removed

from the molds after 24 hours and placed in a moist cure room until testing age.

Before testing, specimens were capped at the two bases to ensure parallel surfaces

according to ASTM C 617-98 specifications. Rediron capping compound was melted to

a temperature of approximately 135°C (275°F). Then, the compound was poured, using a

ladle, in a machined metal plate about 13 mm (0.5 in.) deep. With the aid of an

alignment device, a dry end of the specimen was placed into the capping compound on

the plate and held in place until the compound cooled. Figure 13 displays a 100 x 200

mm (4 x 8 in.) concrete specimen. The capping process is shown in Figure 13-a.

In most cases, two cylinders were tested, and the average of the two was used to

define the compressive strength of the mix. The cylinders were tested according to

ASTM C 39-05. A load rate of 4.5 kN/sec (1,000 lb/sec) was used for the 150 mm (6 in.)

specimens, while the 100 mm (4 in.) specimens were loaded at a rate of approximately

2.25 kN/sec (500 lb/sec). In most cases, the Forney LC-4 compression testing machine

was used to carry out the compression tests. The Forney is calibrated to 1780 kN

(400,000 lb), well exceeding the capacity of any of the specimens. For the 150 mm (6

in.) specimens, the Tinius Olsen universal testing machine was employed. The Tinius

has a data acquisition system (DAS) that is controlled with integrated computer software,

which automatically generates load-deflection plots. The Tinius has a capacity of 890 kN

(200,000 lb). Figure 13-b shows a 150 mm (6 in.) specimen undergoing a compressive

test on the Tinius Olsen universal testing machine.


38

(a) Sulfur capping (b) Compression test

Figure 13. Determination of material strength

The compressive strengths for all seven groups are shown in Table 14. Group 3

had the highest compressive strength out of all 7 groups, with an average 28-day strength

of 61.4 MPa (8,900 psi). The polypropylene fibers added to Group 3 increased the

compressive strength of the plain concrete by approximately 8.2 percent. Fibers usually

only have a minor effect on the compressive strength of a FRC specimen. The real

benefit of the FRC is the post-peak strength retained with increasing deformation beyond

the maximum load (ACI 544.2R-89). Group 2 consisted of plain concrete with an

average compressive strength of 56.7 MPa (8,219 psi) at 28 days of age, 632 percent

greater than the compressive strength of Group 6.

Groups 1, 4, and 6 had promising results, considering each group contained a

large percentage of wood fibers. Results from the compressive tests show that the

addition of wood fibers in the mixture considerably reduces the strength of the hardened

material. Group 6 had the highest strength and stiffness of the three groups, which was a

result of the amount of coarse and fine aggregates in the mix. Groups 1 and 4 had

average 28-day strengths of 7.5 and 4.4 MPa (1089 and 643 psi), respectively. Although
39

the mix designs of the two groups were similar, Group 1 had a 3 to 5 ratio of Portland

cement and fly ash. Group 4 had no cement added to the mix. The addition of Portland

cement to Group 1 possibly increased the strength of the mix.

The compressive failure modes of the wood fiber specimens of Groups 1, 4, and 6

were much different than those of the plain concrete and FRC specimens. The specimens

of Group 2 and Group 3 fractured at strain levels slightly over the strain at peak load,

whereas specimens from Groups 1, 4, and 6 held together at strains well beyond the

maximum stress. Although the strength of the FA-WF material is much lower than that

of plain concrete, the ductile nature of the material is an added benefit in impact and blast

resistance.

Group 7 consisted of two parts — the mix designs of Group 1 and Group 2. The

top half of the specimens had the same mix design as Group 1. The material had an

average compressive strength of 6.5 MPa (940 psi), slightly less than that of Group 1.

The 28-day compressive strength of the plain concrete mix of Group 7 was 53.3 MPa

(7,733 psi).

Table 14. Compressive strengths of drop-weight impact groups

Group 7 Day 14 Day 28 Day


No. Spec 1 Spec 2 Average Spec 1 Spec 2 Average Spec 1 Spec 2 Average
1 3.89 4.68 4.28 6.47 5.69 6.08 7.98 7.05 7.52
2 39.79 43.07 41.43 53.09 52.18 52.64 55.82 57.52 56.67
3 48.10 49.50 48.80 52.20 55.42 53.81 60.72 61.89 61.31
4 3.67 2.54 3.10 3.74 4.26 4.00 4.46 4.40 4.43
5 1.28 1.01 1.15 1.81 1.70 1.76 1.61 1.50 1.55
6 5.56 5.45 5.50 7.79 5.75 6.77 8.20 7.29 7.74
7-a - - - 5.22 5.61 5.42 6.25 6.71 6.48
7-b - - - 52.50 49.04 50.77 53.01 53.63 53.32
Units are in MPa / Units conversion: 1 MPa = 145 psi
40

3.3.2 Splitting tensile strength

Split-tension tests were performed on 100 x 200 mm (4 x 8 in.) cylinders to

indirectly measure the tensile strength of the concrete according to ASTM C 496-04.

Supplementary steel bearing plates were used since the diameter of the upper head of the

Forney LC-4 compression testing machine was smaller than the length of the specimen.

The specimen was loaded along its vertical diameter at a constant rate of 556 N/sec (125

lb/sec) until failure. Failure occurred due to tension developed in the transverse

direction. The indirect tensile strength was computed using equation (4), where T equals

the tensile strength (kPa), P is the load at failure (kN), and L and d represent the length

and diameter of the specimen (m), respectively.

2P
T= Eq. (4)
πLd

Table 15 presents the tensile strengths determined from the split cylinder tests.

Generally, the tensile strength of concrete is roughly 10 percent of its compressive

strength. The tensile strength of Group 2 was 4.4 MPa (635 psi), which was 8 percent of

its compressive strength. Group 1 had a tensile strength of 1.1 MPa (155 psi), which was

14 percent of its compressive strength. The tensile strengths of Group 4 and Group 6

were 14 and 12 percent of their compressive strengths, respectively. Group 5 was

omitted from the table due to a lack of available data, which is explained in section 3.4.5.

Split cylinder tests were not conducted for Group 7. It was assumed that the tensile

strengths of the materials used in Group 7 were similar to those of Group 1 and Group 2.

The results show that the wood fibers added to groups 1, 4, and 6 lead to a percentage

increase in tensile strength relative to the compressive strength of the material when
41

compared to plain concrete. Figure 14 displays mechanical testing of the specimens.

Figure 14-a represents a split-cylinder test on a 100 x 200 mm (4 x 8 in.) specimen.

Table 15. Tensile strengths of fiber-reinforced materials

Mix 1 Mix 2 Mix 3 Mix 4 Mix 6


Spec 1 Spec 2 Spec 1 Spec 2 Spec 1 Spec 2 Spec 1 Spec 2 Spec 1 Spec 2
Applied load
(kN) 29.9 39.6 131.4 152.7 162.5 151.7 20.1 21.9 32.9 27.3
Splitting tensile
strength (kPa) 930 1206 4065 4685 4995 4685 620 689 1034 861
Average splitting
tensile strength
(kPa) 1068 4375 4840 655 948
Unit conversion: 1 kN = 224.8 lb; 1 kPa = 0.145 psi

3.3.3 Modulus of elasticity

The MOE of each group, with exception of Group 5, was determined using the

Tinius Olsen universal testing machine in accordance with ASTM C 469-02. Figure 14-b

displays a 150 x 300 mm (6 x 12 in.) cylinder in a compressometer device. The

compressometer consists of 3 yokes. The bottom yoke is rigidly attached to the

specimen, and the other 2 are attached at 2 diametrically opposite points, so the yokes are

allowed to rotate. A pivot rod was used to maintain a constant distance between the top

and bottom yokes. Opposite the rod, a linear variable differential transformer (LVDT)

was used to measure the change in distance between the two yokes, which is referred to

as the gage reading. The gage reading is the sum of the displacement due to specimen

deformation and displacement due to rotation of the yoke about the pivot rod. Assuming

the distances from the pivot point to the pivot rod and LVDT are equal, the deformation

of the specimen is half the gage reading.


42

(a) Split-cylinder test (b) Compressometer

Figure 14. Determination of tensile strength and material stiffness

To obtain the MOE, a 150 x 300 mm (6 x 12 in.) specimen was loaded to 60

percent of the specimen’s compressive strength at a load rate of 4.5 kN/sec (1,000 lb/sec)

and unloaded at the same rate. Then, the specimen was reloaded once more at the same

rate and magnitude. The chord modulus, or MOE, was determined between a point

corresponding to a very small strain value and a point corresponding to 40 percent of the

ultimate stress.

Figure 15 displays the MOE stress-strain curve developed for Group 1. The MOE

was determined to be 2,928 MPa (425 ksi). Notice the large amount of residual strain in

the specimen after unloading. This residual strain did not occur in the concrete

specimens of Group 2 and Group 3.

Figure 16 shows the relative modulus curves for 5 of the 7 impact groups. The

compressive strength of Group 5 was not high enough to conduct a MOE test without the

risk of damaging the compressometer, and it was assumed that the top and bottom layers

of Group 7 had the same MOE values as those of Group 1 and Group 2, respectively.
43

Group 3 had the highest stiffness, followed closely by Group 2. The stiffnesses of

Groups 1, 4, and 6 were much smaller than those of the plain and PFRC specimens,

which was primarily due to the addition of wood fibers and the removal of aggregates

from the mix. The reduction of aggregate in the mix had an adverse effect on the

material stiffness. For example, although the compressive strength of Group 6 was only

3 percent greater than that of Group 1, the stiffness of Group 6 was 250 percent greater

than the stiffness of Group 1.

4
Stress (MPa)

Ec = 2928 MPa
3

0
0 0.0002 0.0004 0.0006 0.0008 0.001 0.0012 0.0014 0.0016 0.0018
Strain (in/in)

Unit conversion: 1 Mpa = 145 psi

Figure 15. Modulus of elasticity curve for Group 1

Table 16 summarizes the mechanical properties of the six base materials

investigated in the drop-weight impact test. The MOE values for the plain concrete and

PFRC were 40.7 and 43.8 GPa (5,900 and 6,350 ksi), respectively. Group 6 had some
44

portion of coarse and fine aggregates, along with wood fibers, resulting in a MOE value

of 10.3 GPa (1,500 ksi). Groups 1 and 4, which contained no amount of limestone or

sand, had MOE values of 2.9 and 2.1 GPa (425 and 300 ksi), respectively.

35
FA-C-WF
30 Concrete
PFRC
25 FA-WF
Stress (MPa)

WF Concrete
20

15

10

0
0 0.0005 0.001 0.0015 0.002
Strain (in/in)

Unit conversion: 1 Mpa = 145 psi

Figure 16. Modulus of elasticity comparison

Table 16. Summary of properties of base mix designs

Group No. 1 2 3 4 5 6
3
Density (kg/m ) 1698 2467 2467 1426 - 1852
Modulus of Elasticity (GPa) 2.93 40.68 43.78 2.07 - 10.34
Split cylinder strength (kPa) 1068 4375 4840 655 - 948
Compressive strength (MPa) 7.52 56.67 61.31 4.43 1.55 7.74
Mean 28-day FC (blows) 13 5 18 8 2 15
Mean 28-day UR (blows) 27 6 32 15 3 19
Unit conversion: 1 kPa = 0.145 psi
45

3.4 Impact resistance

As previously discussed, the repeated drop-weight impact test characterizes the

impact resistance of FRC by measuring the number of blows required to achieve a

prescribed level of distress. The results of the test are useful for comparing the relative

merits of different fiber concrete mixtures. Large variations in the test are common,

which indicates that the dependability of the test is uncertain. Therefore, several

specimens must be tested to keep the error under 10 percent. Statistical studies on impact

resistance of concrete using the ACI repeated drop-weight test have determined that a

minimum of 35 to 40 specimens must be tested to keep the average percent error under

10 percent at a 90 percent level of confidence. One study conducted using the modified

technique determined that approximately 20 to 25 specimens are required to keep the

error below 10 percent at a 90 percent level of confidence (Badr and Ashour, 2005).

Seven unique groups of specimens were tested at 7, 14, and 28 days of age. The

repeated impact test was achieved using techniques developed in a previous study by

Badr and Ashour and the testing apparatus shown previously in Figure 4. After sliding

the impact piston into the steel ring welded to the middle plate, a specimen was centered

on the bottom base plate. With exception of the first group, specimens were placed

between the raised square steel tubes, as shown in Figure 17. The purpose of the tubes

was to prevent the specimen from rotating or moving laterally during the test.

Once the specimen was centered properly with the line of impact parallel to the

notched plane, the hammer was raised to its maximum height of 457 mm (18 in.) and

dropped. The hammer impacted the piston, which transferred the load directly to the

specimen. The process of dropping the hammer was continued until a crack developed in
46

the specimen, always within one of the two notches. The number of blows to reach that

level of damage was recorded, and the process was continued until ultimate failure

occurred.

Steel notches

Steel tongue

Steel notch

(a) Raised notches on base plate (b) Base plate

Figure 17. Base plate modifications

Once all the data was recorded for each group, the mean, standard deviation, and

COV were calculated for each set of data. Equation (5), equation (6), and equation (7)

were used to calculate the mean (η), standard deviation (σ), and coefficient of variation

(v), respectively, where N is the total number of specimens and y is the number of blows

applied to a single specimen.

η=
∑y Eq. (5)
N

∑ ( y - η)
2

σ=+ Eq. (6)


N -1

v = σ/η Eq. (7)


47

Histograms and normal probability plots were also used to represent the

distribution of impact data. Once the mean and the variance of the data were calculated,

the entire normal distribution was characterized. For example, Figure 18 represents the

distribution of the 28-day FC data for the FA-C-WF material of Group 1. Figures in

Appendix A illustrate the normal distribution curves for all the groups, which overlap the

histograms presenting the scatter in the test results.

Normal probability curves for 28-day test results of six test groups are presented

in Appendix A to analyze the normality of the distribution of the impact data. Group 5

was neglected due to the small amount of data available for analysis. Data was lacking

due to the low number of specimens, which resulted from a faulty mix design. Many of

the specimens broke apart when they were removed from the molds. Figure 19 is a

cumulative normal probability curve for Group 1. The normal probability curve indicates

that about 70 percent of the specimens tested from Group 1 will crack within 15 blows

and fail within 30 blows. Group 1 had the largest average percent increase in the number

of blows from FC to UR at 28 days of age, which was roughly 103 percent.

Standardized normal distribution curves were also developed for each group. The

standardized normal distribution illustrates the number of specimens lying above and

below the mean number of blows required to crack and fail the specimens. Generally,

most of the data points were within two standard deviations on either side of the mean.

Figure 20 presents the standardized distribution for Group 1. The standardized normal

distribution curves for the other test groups are shown in Appendix A.
48

4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22
7 0.3

6 0.25

5
0.2
Frequency

4
0.15
3
0.1
2

0.05
1

0 0
0 2 4 6 8 10 12 14 16 18 20 22
First crack resistance in blows

Figure 18. Distribution of 28-day FC test results for Group 1

100
2
R = 0.978 2
80 R = 0.9711
Cumulative percent

60

40
First crack
Ultimate
20
resistance

-20
0 5 10 15 20 25 30 35 40
Impact resistance in blows

Figure 19. Normal probability curve for Group 1


49

Standardized normal distribution


2

-1 First crack
Ultimate
resistance
-2

-3
0 5 10 15 20 25 30 35 40
Impact resistance in blows

Figure 20. Standardized normal distribution for Group 1

3.4.1 Group 1 (FA-C-WF)

Group 1 was represented with a total of 54 specimens tested in 3 groups of 18 at

7, 14, and 28 days of age. Figure 21 displays the stages of impact testing. Figure 21-a

displays a specimen from Group 1 before testing began. Notice that the 12.7 mm (0.5 in.)

steel bar is aligned directly on the notched plane. The ultimate failure of the first group,

consisting primarily of fly ash, cement, and wood fibers, was somewhat subjective.

Compared to unreinforced concrete or FRC specimens, the stiffness of the

material was relatively low, approximately 2,758 to 3,447 MPa (400 to 500 ksi).

Furthermore, the average density of the hardened material was roughly 1,698 kg/m3 (106

lb/ft3). Therefore, the impacts caused localized damage to the specimen. The bar of the

impact piston created a groove in the surface of each specimen from Group 1, shown in
50

Figure 21-b. Ultimate failure was declared when the specimen separated into two halves,

or the 12.7 mm (0.5 in.) diameter bar was completely submerged into the specimen, and

the bottom of the cylinder began penetrating it, as shown in Figures 21-c and 21-d.

Normally, failure was declared due to the latter of the two.

(a) Group 1 specimen before impact (b) Groove formation on FA-WF specimen

(c) Failure of FA-WF specimen (d) Piston penetration in FA-WF specimen

Figure 21. Group 1 impact specimens

Table 17 presents the impact resistance results for the 54 specimens in Group 1.

In the table, FC denotes the number of blows to first crack and UR signifies the number
51

of blows to failure. The sample mean of the data set varied from 7 blows for the 7-day

FC to 27 blows for the 28-day UR. The average coefficients of variation were 22.8 and

16.6 percent for FC and UR values, respectively. The COV remained approximately the

same, around 20 percent, for each testing age. The average standard error of the mean

was 0.68 blows.

Table 17. Group 1 impact test results

7 Day Strength 14 Day Strength 28 Day Strength


Specimen FC UR FC UR FC UR
1 5 11 10 23 10 18
2 7 15 12 29 13 27
3 10 18 10 24 12 25
4 6 14 8 16 9 23
5 4 11 9 20 18 33
6 13 21 11 23 12 26
7 6 15 7 18 15 33
8 9 20 9 24 15 30
9 9 19 9 22 17 32
10 7 14 8 17 13 27
11 8 15 13 28 10 24
12 7 16 8 21 14 31
13 8 17 6 21 16 29
14 5 12 10 23 13 27
15 7 17 6 18 13 26
16 7 16 12 27 11 21
17 8 15 10 22 15 25
18 5 13 13 29 14 24
Min 4 11 6 16 9 18
Max 13 21 13 29 18 33
Stand. Dev 2.1 2.8 2.1 3.8 2.4 4.0
Mean 7.3 15.5 9.5 22.5 13.3 26.7
C.O.V 28.5 17.9 22.0 17.0 17.9 14.9

For the 28-day test age, the 95 percent confidence interval about the UR mean

was 26 to 28 blows. Impact resistance increased as the material gained strength from
52

curing. Table 17 shows that the mean UR at 7 days of age was 15.5, and the mean UR at

28 days was 26.7 — a 72 percent increase in resistance. The frequency distribution for

the FC data in Figure 18 follows the superimposed normal distribution curve well, as

does the UR frequency distribution for Group 1 shown in Figure 1A of Appendix B.

Table 18 compares the statistical parameters of Group 1 with those recorded for

the PFRC specimens. The average number of blows to FC and UR were 70 percent and

51 percent less, respectively. Therefore, according to these two tests, PRRC has a higher

resistance to repeated impacts compared to the FA-C-WF specimens. The overall COV

reported for the PFRC specimens was 39.4 and 35.2 percent for FC and UR. Comparing

these values to the COVs of Group 1, 17.9 and 14.9 percent, the variations in Group 1 are

less than half those reported for the PFRC specimens.

Table 18. Statistical comparison of impact test results

Overall
Results
Test Parameter FC UR
Mean (drop) 44 55
Polypropylene fiber- Standard deviation
reinforced concrete1 (drop) 17.3 19.4
COV, % 39.4 35.2
Mean (drop) 103 142
Steel fiber-reinforced Standard deviation
concrete2 (drop) 59 66
COV, % 57.3 46.5
Mean (drop) 13.3 26.7
Group 1 wood fiber
Standard deviation
mix at 28 day
(drop) 2.4 4.0
strength
COV, % 17.9 14.9
1
Badr and Ashour, 2005
2
Nataraja et al., 1999
53

Furthermore, a statistical summary of the test involving SFRC specimens

conducted by Nataraja is also shown in Table 18 (Nataraja et al., 1999). The test was

conducted using the ACI 544 guidelines instead of the modified technique, which is

possibly the reason that the mean number of drops is much larger, 103 and 142 for the FC

and UR, respectively. Also, the COV for the SFRC specimens is large, 57.3 and 46.5

percent for the FC and UR.

3.4.2 Group 2 (Concrete)

Group 2 was composed of 54 specimens of unreinforced concrete with an average

density of 2,467 kg/m3 (154 lb/ft3), tested in three groups of 18. Table 19 displays the

data recorded for all the specimens in Group 2. The impact resistance of Group 2 was

very low compared to the other groups. The low resistance was attributed to the brittle

nature of the concrete. Unlike Group 1, no local deformation occurred around the impact

piston, and there was almost no post-cracking resistance. In several cases, the FC and

UR of the specimen occurred simultaneously.

The average resistance increased only slightly, from 3.67 blows at 7 days of age

to 5.61 blows at 28 days of age. The average coefficients of variation were 34.9 and 35.6

percent for FC and UR values, respectively. The average standard error of the mean was

0.4 blows. The 95 percent confidence interval about the mean for the FC and UR values

were 4 to 6 blows and 4.5 to 6.5 blows, respectively.

Histograms in Figure A2 of Appendix A present the distribution in impact

resistance of Group 2 for the FC and UR at 28 days of age. The normal distribution

curve is overlapping each histogram. This figure shows that the FC distribution is

skewed to the left side.


54

Table 19. Group 2 impact test results

7 Day Strength 14 Day Strength 28 Day Strength


Specimen FC UR FC UR FC UR
1 2 3 4 4 4 4
2 3 4 4 5 8 9
3 3 3 6 7 5 6
4 2 3 2 3 3 3
5 3 4 4 5 3 4
6 2 3 3 3 6 7
7 1 2 3 3 7 7
8 2 2 5 5 4 4
9 3 4 4 4 6 6
10 4 6 6 6 3 3
11 4 5 4 4 8 9
12 5 6 6 7 5 6
13 2 3 8 10 4 5
14 3 3 4 4 3 4
15 4 5 5 5 4 4
16 3 4 5 6 9 10
17 1 2 7 9 3 3
18 3 4 5 6 5 7
Min 1 2 2 3 3 3
Max 5 6 8 10 9 10
Stand. Dev 1.0 1.2 1.5 1.9 1.9 2.1
Mean 2.8 3.7 4.7 5.3 5.0 5.6
C.O.V 37.1 32.8 30.6 35.9 37.7 38.1

Two types of normal probability plots for Group 2 are shown in Figure A8 of

Appendix A. The plots represent the data recorded for the impact resistance at 28 days of

age. According to the standardized normal distribution, most the data points fall within

two standard deviations of the mean. The normal probability plot for the ultimate

resistance shows a 70 percent probability that a plain concrete specimen will fail within 8

blows. The data is not close to a straight line, which indicates the data set does not fit

closely with a normal distribution curve.


55

Although the standard deviations are small, the COV for Group 2 is comparable

to that recorded for the PFRC specimens (Badr and Ashour, 2005). The COV for Group

2 is 37.7 and 38.1 percent for the FC and ultimate resistance UR, respectively. The COV

for the PFRC specimens was 39.4 and 35.2 percent for the FC and UR. Note that

although the materials are slightly different, the COV remains approximately the same.

Statistical results from the drop-weight study conducted by Nataraja are shown in

Table 20, along with results from Group 2. Both groups consist of plain concrete, but an

enormous difference exists in the average impact resistance. Although the previous study

was conducted using the ACI 544 guidelines, at least a 173 percent difference occurs

between the average FC and UR values of the two groups. The difference may be

associated with the thickness of the specimens. Specimens tested under ACI guidelines

were approximately 63 mm (2.5 in.) thick, while specimens in Group 2 were only 50 mm

(2 in.) thick. Other possibilities might be the compressive strength, brittleness, and

surface roughness of the two groups. Specimens of Group 2 had rough surfaces because

they were finished with a trowel, but the other group had smooth cut surfaces.

Table 20. Comparison of plain concrete

Overall Results
Test Parameter FC UR
Mean (drop) 5 5.6
Group 2: 8000 psi Standard
plain concrete deviation (drop) 1.9 2.2
COV, % 37.7 38.1
4000 psi plain Mean (drop) 70 77
concrete using ACI Standard
544 guidelines1 deviation (drop) 36 39
(32 samples tested) COV, % 53.7 50.6
1
Nataraja et al., 1999
56

Figure 22 displays several failed specimens from Group 2. Notice that the crack

develops through the notches. Figure 22-b shows the specimen’s rough surface. Also, no

local deformation from the impact piston is visible in the figure.

(a) Group 2 specimens (b) Group 2 notched fracture

Figure 22. Group 2 impact specimens

3.4.3 Group 3 (PFRC)

Group 3 consisted of 54 specimens of the exact mix design as Group 2 except

with the addition of 19 mm (0.75 in.) polypropylene fibers. The average density of the

mix was 2467 kg/m3 (154 lb/ft3). The specimens were tested in 3 groups of 18, just like

groups 1 and 2. The impact resistance of Group 3 was the highest of all seven groups

investigated in the study. No local deformation occurred around the impact zone, which

proved the mix was much stiffer than the FA-C-WF material used in Group 1.

Furthermore, the addition of polypropylene fibers increased the cracking resistance and

provided the specimens with significant post-cracking strength. The average number of

blows to FC and UR increased from 12.1 and 24.6 at 7 days of age to 18.1 and 32.4 at 28
57

days of age. The addition of polypropylene fibers basically increased the FC strength and

UR of Group 2 by 260 and 471 percent, respectively.

Table 21 presents the data recorded for Group 3 for each testing age. The average

COVs of the impact test results were roughly 35.6 and 24.7 percent for FC and UR

values, respectively. The COV of the FC results were generally higher than those for

UR. The average standard error of the mean was approximately 1.5 blows. The 95

percent confidence interval about the mean FC resistance at 28 days of age was 15 blows

to 21 blows, and the corresponding interval for the UR was 29 to 36 blows.

Table 21.Group 3 impact test results

7 Day Strength 14 Day Strength 28 Day Strength


Specimen FC UR FC UR FC UR
1 13 30 10 23 17 35
2 8 19 9 21 15 26
3 11 24 8 21 22 35
4 8 21 12 23 17 32
5 10 22 24 37 14 29
6 12 29 15 23 22 34
7 20 33 9 23 31 48
8 18 28 13 25 21 33
9 13 25 21 31 15 27
10 7 12 7 17 18 33
11 11 27 17 26 12 23
12 11 25 33 49 28 44
13 8 18 10 22 13 28
14 12 25 11 22 23 42
15 15 33 18 27 20 38
16 9 17 20 32 18 29
17 21 37 17 25 11 25
18 10 18 20 31 9 22
Min 7 12 7 17 9 22
Max 21 37 33 49 31 48
Stand. Dev 4.0 6.3 6.6 7.2 5.6 7.0
Mean 12.1 24.6 15.2 26.6 18.1 32.4
C.O.V 33.0 25.6 43.0 27.1 31.0 21.6
58

Figure A3 in Appendix A presents the scatter of the impact test results for the 28-

day impact test. The histograms reveal a poor distribution of the data, which is skewed to

one side. The data sets do not follow the normal curve overlapping them. In both cases,

the resistance values for the majority of the specimens are above the mean resistance

values. The normal probability plots in Figure A9 of Appendix A reaffirm the skewed

distribution of the impact tests because the data is not close to a straight line. According

to the plots, 70 percent of the fiber-reinforced specimens from Group 3 will crack within

20 blows and will fail within approximately 37 blows.

Table 22 shows a comparison between the two PFRC groups. The overall results

of the test conducted by Badr and Ashour conclude that the PFRC specimens had an

average FC and UR of 44 and 55 blows, respectively. The recorded average is based on

testing 40 specimens in accordance with the modified technique they developed (Badr

and Ashour, 2005). At the 28-day test age, the average number of blows to FC and UR

were 18 and 33, respectively, for Group 3, based on the 18 specimens tested. A 59

percent difference exists between the URs of the two groups. Although the thicknesses

of the two groups are approximately the same, the difference in the average might be

caused by several other variables. These variables could include the surface finish,

aggregate size, concrete strength, and fiber length.

The surfaces of all specimens in Group 3 were finished using a trowel, which

created a rougher surface than if the specimen were cut with a diamond saw. The rough

surface prevented the impact piston from lying smoothly on the specimen, creating stress

concentrations along the length of the bar. Also, the limestone used in Groups 2 and 3

had a maximum size of 19 mm (0.75 in.), while the nominal maximum size of the other
59

group was less than 12.7 mm (0.5 in.). The concrete strength of Group 3 was

approximately 55.16 MPa (8000 psi), compared to 41.37 MPa (6000 psi) for the PFRC

specimens tested by Badr. Furthermore, the fibers in Group 3 were approximately 60

percent longer than fibers used in the previous study (Badr and Ashour, 2005).

The COV for Group 3 was 31.0 percent for the FC values and 22 percent for the

UR values. These values are comparable to the COV values reported in the previous

study — 39.4 and 35.2 percent for FC and UR, respectively.

Table 22. Comparison of PFRC

Overall Results
Test Parameter FC UR
Mean (drop) 18 33
Group 3: 8000 psi
Standard
polypropylene fiber-
deviation (drop) 5.6 7
reinforced concrete
COV, % 31.0 22.0
Mean (drop) 44 55
6000 psi polypropylene Standard
fiber-reinforced concrete1 deviation (drop) 17.3 19.4
COV, % 39.4 35.2
1
Badr and Ashour, 2005

3.4.4 Group 4 (FA-WF)

Group 4 consisted primarily of fly ash, water, and wood fibers. No cement was

added to the mix. Eighteen specimens were tested at each of the three testing ages for a

total of 54 specimens. With an average density of 1,426 kg/m3 (89 lb/ft3), Group 4

behaved in a similar manner to Group 1. Due to the low stiffness of the material, local

deformations formed around the impact zone. Therefore, the ultimate failure of the

specimen was subjective. Failure was declared when the 12.7 mm (0.5 in.) diameter steel
60

bar on the bottom of the impact piston was completely submerged or the specimen

fractured into two pieces, whichever occurred first.

Table 23 shows that the average number of blows to FC and UR were 8.0 and

15.2, respectively, at 28 days of age. These resistance values are relatively low compared

to Group 1. However, Group 4 has a lower MOE, and the compressive strength of Group

1 is approximately 70 percent greater than that of Group 4. The average coefficients of

variation for FC and UR were 28.5 and 18.9 percent, respectively. The average standard

error of the mean was 0.5 blows; therefore, the 95 percent confidence interval about the

28-day mean UR was approximately 14 to 16 blows.

The average FC and UR of Group 4 increased from 4.3 and 10.2 at 7 days of age

to 8.0 and 15.2 at 28 days of age. The average UR of Group 4 at 28 days of age was 15.2

compared to 5.6 for the unreinforced concrete specimens of Group 2. Therefore, the FA-

WF mix has a higher capability to absorb repeated impact, although the compressive

strength and stiffness of the mix is much lower than that of plain concrete.

Figure A4 in Appendix A presents the distribution of FC and UR results for

Group 4. The distributions are skewed to the right; however, both distributions follow

the standard curve moderately well. Approximately an equal number of results occur on

either side of the mean for the FC resistances. Both plots show the highest frequency

occurs at the mean, and the frequencies decrease as the results move away from the

mean. More tests are needed to better define the distribution of the results.

Figure A10 in Appendix A shows the probability plots for the results of Group 4.

The standard normal distribution reports that the majority of data points fall within two
61

standard distributions from the mean. According to the normal probability plots, 70

percent of the specimens of Group 4 will crack within 9 blows and fail within 17 blows.

Table 23. Group 4 impact test results

7 Day Strength 14 Day Strength 28 Day Strength


Specimen FC UR FC UR FC UR
1 5 13 6 11 9 17
2 3 9 8 16 8 15
3 5 11 5 9 12 21
4 3 8 4 10 7 15
5 4 10 7 13 6 13
6 7 16 6 12 11 16
7 5 11 8 14 13 20
8 2 6 4 10 6 12
9 7 12 6 13 7 15
10 5 11 5 11 9 16
11 2 7 4 9 8 13
12 4 9 5 13 7 16
13 6 8 4 12 5 13
14 4 13 5 13 8 14
15 5 11 8 15 7 13
16 3 12 4 11 6 14
17 4 10 5 14 9 16
18 3 6 6 15 6 15
Min 2 6 4 9 5 12
Max 7 16 8 16 13 21
Stand. Dev 1.5 2.5 1.4 2.0 2.1 2.3
Mean 4.3 10.2 5.6 12.3 8.0 15.2
C.O.V 33.8 25.0 24.9 16.5 26.7 15.1

3.4.5 Group 5 (FA-WF-A)

Only 21 specimens were tested from Group 5. Many of the specimens broke

apart and crumbled when they were removed from the forms, which left 21 acceptable

specimens for testing. Table 24 displays the data recorded for Group 5. Seven

specimens were tested at each of the three testing ages. Group 5 performed the worst of
62

all the seven groups investigated in the study, with an average UR of 2.8 blows at 28 days

of age. The average COVs were 32.7 and 16 percent for FC and UR, respectively. No

distribution of the results from Group 5 is presented due to low impact resistances and

lack of available data. The mix design for Group 5 should be revised, and cement should

be added to assist the fly ash in the paste matrix in bonding of the aggregates.

Table 24. Group 5 impact test results

7 Day Strength 14 Day Strength 28 Day Strength


Specimen FC UR FC UR FC UR
1 1 3 2 3 2 3
2 1 2 1 3 1 3
3 1 2 2 3 1 2
4 2 3 1 2 2 3
5 2 3 2 3 2 3
6 1 2 1 2 2 3
7 1 3 2 3 1 3
Min 1 2 1 2 1 2
Max 2 3 2 3 2 3
Stand. Dev 0.45 0.49 0.49 0.45 0.49 0.35
Mean 1.3 2.6 1.6 2.7 1.6 2.9
C.O.V 35.1 19.3 31.5 16.6 31.5 12.3

3.4.6 Group 6 (WF Concrete)

Group 6 consisted of 32 concrete specimens with the addition of wood fibers.

The average density of the material was 1,852 kg/m3 (115.6 lb/ft3). The wood fibers

accounted for 6.25 percent of the weight of the mix, and increased the 28-day ultimate

impact resistance of the plain concrete by 250 percent. Group 2 had an average FC and

UR of 5 and 5.6 blows, respectively. With the addition of wood fibers, Group 6 had an

average FC and UR of 15.3 and 19.2 blows, respectively. By comparing the average FC

and UR of the two groups, obviously the addition of wood fibers to concrete is beneficial
63

to energy absorption from repeated impact. However, the compressive strength of Group

2 was about eight times greater than that of Group 6.

As shown in Table 25, the impact resistance of Group 6 increased from an

average FC of 8.9 blows and a UR of 12.5 blows at 7 days of age to 15.3 and 19.2 blows,

respectively, at 28 days of age. The average COVs for Group 6 were 33.1 and 39.5

percent for FC and UR, respectively. COV values for each testing age remained low

compared to COV values obtained in the previous studies (Badr and Ashour, 2005;

Nataraja et al., 1999).

Table 25. Group 6 impact test results

7 Day Strength 14 Day Strength 28 Day Strength


Specimen FC UR FC UR FC UR
1 8 13 10 13 28 32
2 6 8 16 23 23 26
3 8 12 8 12 22 27
4 15 20 10 16 9 16
5 9 12 6 10 18 23
6 11 16 11 16 10 14
7 8 11 17 24 12 15
8 7 9 13 17 14 18
9 8 11 8 11 10 12
10 9 13 7 11 9 13
11 - - - - 13 15
12 - - - - 15 19
Min 6 8 6 10 9 12
Max 15 20 17 24 28 32
Stand. Dev 2.4 3.3 3.5 4.7 6.0 6.1
Mean 8.9 12.5 10.6 15.3 15.3 19.2
C.O.V 26.8 26.1 33.3 30.7 39.1 32.0

Histograms showing the distribution of impact test results at 28 days of age are

presented in Figure A5 in Appendix A. The distribution indicates a poor normality of the


64

impact test results. Several gaps exist in the distributions. For example, no test samples

cracked within 19 to 21 blows, but 3 of 12 tests had FC resistances greater than 22 blows.

The UR distribution has a mean of approximately 20 blows, but the distribution has the

highest frequency between 13 to 15 blows.

Figure A11 in Appendix A presents normal probability plots for the 28-day test

results of Group 6. The majority of the test results fall within two standard deviations of

the mean. The normal probability plot, which is not close to a straight line, indicates a

poor normality of the distribution. The plot also shows a 70 percent probability that a

Group 6 specimen will crack within 20 blows and fail within 24 blows.

3.4.7 Group 7 (Bi-layered)

Group 7 was unique in that it involved two separate materials. The specimens

were constructed of two layers of material, each approximately 25.4 mm (1 in.) thick.

The base material was plain concrete, the same mix design used for Group 2. The FA-C-

WF mixture used for Group 1 was placed on top of the concrete after the concrete was

allowed to cure for 24 hours. A representative sample of Group 7 is shown in Figure 23.

The specimen consisted of a soft top layer to absorb impact and a hard base to increase

the strength and stiffness of the specimen. Note that there is no reinforcement holding

the two layers together. The fresh concrete was roughened to enhance the bond

characteristics between the two layers.

Table 26 presents the impact results for Group 7. Results show that the average

number of blows to achieve the FC and UR of the specimens increased from 12.3 and

16.6 blows at 7 days of age to 23.2 and 24.7 blows at 28 days of age.
65

Layers
crack
FA-WF layer
together
cracks

(a) Non-composite action (b) Composite action

Figure 23. Group 7 impact specimens

Although the soft layer increased the impact resistance of the plain concrete,

results show significantly less post-cracking strength than solid FA-WF specimens. Once

the impact piston penetrated the FA-C-WF layer, the concrete base broke easily. The

COV values for Group 7 are slightly higher than the COV values of the other six groups.

This result could possibly be related to the two different failure modes of the group.

In several cases, the soft top fiber layer split apart before the base developed any

cracks. In these cases, the bond between the two layers was not strong enough to permit

composite action. Therefore, stress was not carried to the concrete layer, and the

concrete did not crack. This effect prolonged the life of the concrete base, which was

used to determine the impact resistance. The FC and UR of the top layer was ignored.

However, composite action occurred in other cases where both layers cracked in the same

location with the same number of blows applied. This action, in effect, reduced the

impact resistance of the specimen.


66

Table 26. Group 7 impact test results

7 Day Strength 14 Day Strength 28 Day Strength


Specimen FC UR FC UR FC UR
1 7 8 13 14 32 37
2 8 10 15 15 10 10
3 10 15 18 20 20 22
4 11 27 19 19 32 34
5 20 32 22 24 38 39
6 14 20 19 22 5 6
7 24 29 9 10 13 14
8 13 15 18 20 36 38
9 7 9 17 18 34 35
10 8 11 8 10 21 22
11 9 9 13 16 10 11
12 13 15 16 18 26 28
13 15 16 26 27 27 28
14 16 18 18 20 25 27
15 6 6 27 30 15 16
16 8 9 28 29 17 18
17 19 22 9 9 30 32
18 14 18 11 12 26 28
Min 6 6 8 9 5 6
Max 24 32 28 30 38 39
Stand. Dev 4.9 7.4 5.9 6.2 9.5 10.1
Mean 12.3 16.1 17.0 18.5 23.2 24.7
C.O.V 40.0 46.0 34.5 33.2 41.2 40.7

The average COVs for Group 7 were 38.6 and 40.0 percent for FC and UR, in that

order. The average standard error about the mean was roughly two blows. Using the 68-

95-99.7 rule, the 95 percent confidence interval about the mean was 20 to 26 blows for

FC and 22 to 27 blows for UR values.

The COV values for Group 7 at 28 days of age were 41.2 and 40.7 percent for the

FC and UR, respectively. COV values reported in a previous study, based on 40 PFRC

specimens, were 39.4 and 35.2 percent (Badr and Ashour, 2005). These results, along
67

with results from the other six groups, confirm that the modified drop-weight impact test

provides reasonable COV values for FRC as well as high volume FA-WF materials.

Figure A6 in Appendix A presents the distributions of the FC and UR resistances

for Group 7. The frequencies do not follow the normal curve well, indicating poor

normality of the distribution. The distribution of the FC results is evenly spread to the

left of the mean, while the right side of the curve follows the normal distribution more

closely. Likewise, the UR results are evenly spread below the mean value, while

frequencies above the mean more closely resemble a normal distribution. Higher

frequencies occur at the upper and lower bounds of the curve rather than at the mean. A

larger sample size is needed to derive more reliable conclusions about the normality of

the distribution.

Normal probability plots representing the 28-day impact test data for Group 7 are

shown in Figure A12 of Appendix A. The standard normal distribution shows that all the

results fall within two standard deviations from the mean, verifying the 68-95-99.7 rule.

The normal probability plot indicates fair normality of the distribution, and the R2 values,

0.98 and 0.99, for both data series are the highest of all the groups.

3.4.8 Summary of impact resistance

Figure 24 illustrates a bar graph reporting the mean FC and UR values for all

seven test groups at 28 days of age. The I-shaped line in each bar represents the standard

deviation of the results for the ultimate resistances. Group 3, the PFRC group, had the

highest mean impact resistance with a mean of roughly 33 blows. Group 1 (FA-C-WF)

came in second with a mean impact resistance of roughly 27 blows, followed closely by
68

Group 7 (Bi-layer) with a mean of 25 blows. The bi-layered specimens also had the

largest standard deviation of 10 blows, followed by Group 3 with 7 blows.

Groups 4 (FA-WF) and 6 (WF Conc) had average strengths of 15 blows and 20

blows, respectively. Group 2 (Concrete), consisting of plain concrete, had an average

impact resistance of 5 blows. The average impact resistance of Group 5 (FA-WF-A) was

3 blows, the least of the seven groups investigated in the study. The low impact

resistance is most likely due to a faulty mix design. The bi-layered system had the

highest FC resistance, followed by the PFRC specimens of Group 3.

45
I - indicates SD
± 7.2
40 FC
± 10.3
35 UR
Mean / Standard dev. (blows)

± 4.1
30
± 6.4
25

20 ± 2.4

15

10 ± 2.2

5 ± 0.4

0
FA-C-WF Concrete PFRC FA-WF
0 FA-WF-A WF Conc. Bi-layer
Mix designation

Figure 24. Mean ultimate resistance to impact at 28 days of age

Figure 25 presents ratios of the mean URs divided by the mean FC resistances

presented previously in Figure 24. The figure shows that the FA-C-WF material has the
69

highest level of impact ductility with a ratio of two. The plain concrete specimens and

the bi-layered specimens had the lowest levels of impact ductility with ratios of 1.12 and

1.07, respectively. The PFRC specimens had high impact ductility as well, with a ratio of

1.79.

2.25

2.00
Ultimate / first crack resistance

1.75

1.50

1.25

1.00

0.75

0.50

0.25

0.00
FA-C-WF Concrete PFRC FA-WF
1 FA-WF-A WF Conc. Bi-layer
Mix designation

Figure 25. Ratio of mean ultimate and first crack resistances

The mean percent increase in the number of blows from FC to UR of each group

is shown in Table 27. Group 1 had the highest post cracking resistance with a 142

percent increase at 14 days and 103 percent at 28 days. Group 4 had the highest 7 day

value with a 152 percent increase from FC to UR. Group 6, with the wood fibers added

to the concrete, had slightly higher post cracking resistances than Group 2 at all three test

ages.
70

The bi-layered construction of Group 7 increased the mean UR of the plain

concrete from 5 blows to 17 blows. However, the mean percent increase in the number

of blows from FC to UR stayed approximately the same as that of the plain concrete. The

25.4 mm (1 in.) fly ash layer provided additional benefit up to cracking, but did not

provide post cracking resistance.

Table 27. Mean percent increase in the number of blows from FC to UR

Testing Age
Group No. 7 day (%) 14 day (%) 28 day (%)
1 120 142 103
2 38 13 12
3 109 89 85
4 152 128 97
5 114 86 100
6 41 46 31
7 30 10 7

The minimum number of tests (n) required to guarantee that the percent error in

the measured average is below a specified limit (e) at a certain level of confidence was

calculated using equation (3) discussed previously. Table 28 shows that if the error is to

be kept under 10 percent, the minimum number of tests should be roughly 24 for the

plain concrete at a 90 percent confidence interval. Slightly more tests are needed for the

bi-layered construction of Group 7. However, the FA-WF material making up Group 1

and Group 4 had much less variation, and only 4 to 12 tests are needed to keep the error

under 10 percent at a 90 percent level of confidence.


71

3.5 Summary

Figure 26 presents a comparison of the average FC impact resistances of all seven

test groups at each testing age. Group 7 had the highest FC values at all three test ages,

followed by the PFRC of Group 3. Group 7 also had the highest average increase in FC

resistance from the 14 day test age to the 28 day test age. Groups 1 and 4 had higher FC

resistances than the plain concrete, Group 2, at the three test ages. Furthermore, the

increase in the FC resistance due to curing was greater for groups 1, 4, and 6 than for the

plain concrete, which did not increase much beyond the 14 day test. The bi-linear curves

in Figure 26 show that the increase in average impact resistance due to curing is not

linear.

Table 28. Minimum number of tests required for 10% error

95% confidence 90% confidence


Group No. FC UR FC UR
1 9 6 5 4
2 38 39 23 24
3 26 13 16 8
4 19 6 12 4
5 27 4 16 2
6 41 28 25 17
7 46 45 28 27

Figure 27 shows a comparison of the average URs for all three test ages. The

PFRC specimens of Group 3 had the highest average UR values for all three testing ages,

although Group 7 had the highest FC values. The FA-WF-C mixture of Group 1 had

relatively high impact resistances as well. The average impact resistance of groups 2 and

5 barely increased between the 7 and 28 day tests.


72

25

G1
20 G2
G3
Avg. Number of blows

G4
15 G5
G6
G7
10

0
0 5 10 15 20 25 30
Days

Figure 26. First crack impact resistance with increasing age

35
G1
30
G2
G3
25
Avg. Number of blows

G4
G5
20
G6
G7
15

10

0
0 5 10 15 20 25 30
Days

Figure 27. Ultimate impact resistance with increasing age


73

The results of the drop-weight impact study show that PFRC provides the highest

amount of impact resistance and toughness of all seven groups of specimens investigated

in the study. The impact resistance of Groups 1, 3, 4, 6, and 7 increased with varying

amounts between test ages. However, the impact resistance of the plain concrete and FA-

WF-A material remained roughly the same for every test age.

4. CONCLUSIONS

A modified version of the current ACI drop-weight impact test was used to

determine the relative impact resistances of seven unique groups of specimens.

Comparing the results presented herein to previous studies using the ACI repeated drop-

weight impact test, one might conclude that the modified drop-weight test used in this

impact study is a more reliable measure of impact resistance. The modified drop-weight

impact test was developed in a previous impact study (Badr and Ashour, 2005).

Several conclusions can be drawn from this study.

1. Due to the large variations in impact resistance test results, a larger sample size is

necessary to obtain more dependable conclusions regarding the normality of the

distributions. Although the COV values for the seven groups investigated in the

study are considerably lower than those reported in previous studies, not enough

specimens were tested in each group to develop a normal distribution of the

results.

2. Based on the variations of the impact test results, a proposal can be made as to the

number of tests needed to prevent the error in results from rising beyond a certain

percentage. Results from this study show that at least 16 tests are required to keep

the error below 10 percent for PFRC specimens based on a 90 percent level of
74

confidence. Likewise, 12 FA-WF specimens should be tested to keep the error

below 10 percent.

3. Based on the R2 value on the normal probability plots in Appendix A, Group 7 fit

the normal distribution curve better than the other groups. However, Group 7 also

had the highest COV values.

4. PFRC had the highest drop-weight UR, but the composite layer of FA-WF

material applied to Group 7 provided the best FC resistance values. The FA-WF

material proved to have excellent energy absorption characteristics, although the

material has much less strength and stiffness than plain concrete and FRCs. The

plain concrete had a low impact resistance and a brittle failure mode.

5. The impact test results of the FA-WF specimens of groups 1 and 4 had lower

COVs than the results for the other groups. The low stiffness and subjective

failure mode of the material lead to lower COV values.

6. The FA-C-WF material had the highest level of impact ductility with a value of 2,

compared to PFRC, which had an impact ductility of 1.79. The bi-layered

specimens had the lowest level of ductility with a value of 1.07, just below plain

concrete.

7. Regarding specimen preparation, specimens should be cut to the right thickness

using a diamond saw rather than finished with a trowel. This preparation would

create smooth finished surfaces and would provide more accurate results.

8. Although a portable impact test fixture may prove to be a great asset, the base

plate should be rigidly attached to an immovable foundation.


75

5. ACKNOWLEDGEMENTS

The research conducted herein on the drop-weight impact resistance of a high-

volume FA-WF material was funded by the Air Force Research Laboratory.

6. REFERENCES

ACI Committee 544, “Measurement of Properties of Fiber Reinforced Concrete (ACI


544.2R-89),” American Concrete Institute, Farmington Hills, Michigan, 1989, 11
pp.

ACI Committee 544, “Report on Fiber Reinforced Concrete (ACI 544.1R-96),”


American Concrete Institute, Farmington Hills, Michigan, 1996, 66 pp.

ACI Committee 232, “Use of Fly Ash in Concrete (ACI 232.2R-03),” American Concrete
Institute, Farmington Hills, Michigan, 2003, 41pp.

American Society for Testing and Materials (ASTM C 617-98). Standard Practice for
Capping Cylindrical Concrete Specimens, American Society for Testing and
Materials, West Conshohocken, PA, 1998.

American Society for Testing and Materials (ASTM C 192/C 192M-06). Standard
Practice for Making and Curing Concrete Test Specimens in the Laboratory,
American Society for Testing and Materials, West Conshohocken, PA, 2006.

American Society for Testing and Materials (ASTM C 494/C 494M-05a). Standard
Specification for Chemical Admixtures for Concrete, American Society for
Testing and Materials, West Conshohocken, PA, 2005.

American Society for Testing and Materials (ASTM C 1116-03). Standard Specification
for Fiber-Reinforced Concrete and Shotcrete, American Society for Testing and
Materials, West Conshohocken, PA, 2003.

American Society for Testing and Materials (ASTM C 470/C 470M-02). Standard
Specification for Molds for Forming Concrete Test Cylinders Vertically,
American Society for Testing and Materials, West Conshohocken, PA, 2002.

American Society for Testing and Materials (ASTM C 150-05). Standard Specification
for Portland Cement, American Society for Testing and Materials, West
Conshohocken, PA, 2005

American Society for Testing and Materials (ASTM C 39/C 39M-05). Standard Test
Method for Compressive Strength of Cylindrical Concrete Specimens, American
Society for Testing and Materials, West Conshohocken, PA, 2005.
76

American Society for Testing and Materials (ASTM C 143/C 143M-05). Standard Test
Method for Slump of Hydraulic-Cement Concrete, American Society for Testing
and Materials, West Conshohocken, PA, 2005.

American Society for Testing and Materials (ASTM C 496/C 496 M-04). Standard Test
Method for Splitting Tensile Strength of Cylindrical Concrete Specimens,
American Society for Testing and Materials, West Conshohocken, PA, 2004.

American Society for Testing and Materials (ASTM C 469-02). Standard Test Method
for Static Modulus of Elasticity and Poisson’s Ratio of Concrete in Compression,
American Society for Testing and Materials, West Conshohocken, PA, 2002.

American Society for Testing and Materials (ASTM C 566-97). Standard Test Method
for Total Evaporable Moisture Content of Aggregate by Drying, American
Society for Testing and Materials, West Conshohocken, PA, 1997.

American Society for Testing and Materials (ASTM D 1557-02). Standard Test Methods
for Laboratory Compaction Characteristics of Soil Using Modified Effort,
American Society for Testing and Materials, West Conshohocken, PA, 2002.

Badr, A., Ashour, A. F., “Modified ACI Drop-Weight Impact Test for Concrete,” ACI
Materials Journal, V. 102, No. 4, July-Aug. 2005, pp. 249-255.

Falk, R. H., “Housing Products from Recycled Wood,” CIB TG 16, Sustainable
Construction, Tampa, FL, 1994

Glenium® 3000 NS product brochure, BASF, http://www.basf-admixtures.com, accessed


January, 2007.

Joshi, N., Myers, J.J., “Investigation of an Alternative Wood Fiber-Fly Ash Material for
Infill Wall Systems (CIES 06-60),” Center for Infrastructure Engineering Studies,
University of Missouri, Rolla, MO, 2005.

Moore, D. S., McCabe, G. P., Introduction to the Practice of Statistics, W. H. Freeman


and Company, 1989, 790 pp.

Nataraja, M. C., Dhang, N., and Gupta, A. P., “Statistical Variations in Impact Resistance
of Steel Fiber Reinforced Concrete Subjected to Drop Weight Test,” Cement and
Concrete Research, V. 29, No. 6, 1999, pp. 989-995.

Nycon ConTrolPCF Collated Polypropylene Fibrillated Fibers product information,


Nycon®, http://www.nycon.com/pdf/cntrlpcfpi.pdf, accessed January, 2007.
77

PAPER II

INVESTIGATION OF A HIGH-VOLUME FLY ASH-WOOD FIBER MATERIAL


FOR MITIGATING BLAST PRESSURES

ABSTRACT

This research program was developed to assess the effectiveness of a high-volume

fly ash-wood fiber (FA-WF) material at mitigating dynamic pressure loads. Blast tests

were conducted on panel systems to determine if the material may be useful in a barrier

system to protect other structures and the people in those structures. Test panels were

subjected to various charge weights at decreasing standoff distances in an effort to

compare different material types and reinforcement ratios. Field tests conducted at the

University of Missouri-Rolla’s (UMR) experimental mine demonstrated that systems

incorporating the blast mitigation material had improved blast resistance compared to

plain reinforced concrete (RC) slabs when subjected to near field blast events. The two-

layered panel system also performed relatively well compared to slabs reinforced with

carbon fiber reinforced grids.

1. INTRODUCTION

This report covers a small portion of a multi-organizational project to create

architectural standards for blast-resistant barricade systems. The endeavor is lead by the

UMR Rock Mechanics and Explosives Research Center (RMERC). Other organizations

involved include Kontek Industries, UMR’s Department of Civil, Architectural, and

Environmental Engineering (CArEE), the Department of Architectural Studies from the


78

University of Missouri-Columbia (UMC), and UMC’s National Center for Explosion

Resistant Design (NCERD). The project was funded by the Air Force Research

Laboratory (AFRL) Airbase Technologies Division, which also provides management

assistance and a testing site for large explosive tests. This specific task was undertaken

by personnel from UMR’s CArEE department and from the RMERC.

With ever increasing energy costs, engineers are researching new ways to utilize

and recycle waste products. This research project investigates the effectiveness of using

two common waste products, fly ash and wood fiber, in a blast barrier application. The

high-volume FA-WF material has a lower density than normal weight concrete and can

undergo large strains without a brittle failure (Joshi and Myers, 2005).

Fly ash is a by-product of the combustion of pulverized coal. Its pozzolanic

characteristics make it a beneficial ingredient in concrete. Fly ash improves the

concrete’s resistance to deterioration from sulfates, improves the workability of fresh

concrete, and provides higher strengths at later ages of hardened concrete (ACI 232.2R-

03). However, only 20 percent of the 90 million tons of fly ash produced in the United

States per year is used in the production of concrete and concrete products (Joshi and

Myers, 2005).

Wood fiber is another common waste product that can be recycled from wooden

pallets and containers, lumber salvaged from building demolition, old utility poles and

railroad ties, upper limbs not processed in wood products, and other miscellaneous

products made from wood. In 1994, approximately 13.2 million metric tons of solid

wood waste was generated, and only 1.3 million tons were used for recycling or

compositing. The discarded wood was either burned or placed in landfills (Falk, 1994).
79

At UMR, a great effort has been made to combine these two materials and use

them in a practical manner. Previous studies show that the material has excellent freeze-

thaw resistance and has a relatively high impact resistance compared to plain concrete. It

is believed that the low stiffness and low density of the material will make it a likely

candidate for use as a sacrificial material in a blast application. This assumption came

about from reports of demolishing adobe bunkers in the Middle East. The military

bunkers, formed from a type of adobe brick, would not concede to the explosives. The

blast would demolish localized areas of the bunker, but the pressure wave would not

destroy the entire structure. Therefore, this research effort was devoted to determine the

blast resistance capabilities of the high-volume FA-WF material, which hopefully has

many of the same beneficial properties as the adobe material.

2. RELATED WORK

2.1. Nature of explosives

Explosions are classified in three main categories: physical, chemical, and

nuclear. The most common artificial explosives are chemical explosives, usually

involving a rapid and violent oxidation reaction that produces extreme gas pressures and

heat. The rapid expansion of the gas results in a blast wave that moves through air or

solid materials, destroying anything within close proximity to the detonation. Explosives

are also classified as primary or secondary explosives depending on how they are

initiated. Primary explosives are dangerous because they can be detonated by a spark,

open flame, or impact. Secondary explosives, such as TNT and RDX, are usually

detonated using blasting caps (El-Domiaty et al., 2002). RDX-based C-4 was the primary

explosive used in this study.


80

A detonation wave is an extremely rapid wave of chemical reaction that travels at

a supersonic speed. Detonation velocities for high explosives usually range between

6,700 to 8,500 m/s (22,000 to 28,000 ft/sec). The detonation wave converts the explosive

into a hot, high pressure gas, creating pressures in excess of 18,616 MPa (2,700,00 psi)

behind the detonation front. For bare explosives, the blast wave propagates out into the

surrounding air. The blast wave decays in strength, lengthens in duration, and decreases

in velocity as it moves away from the detonation source (Robinson, 1944).

Any point in space near a detonation will experience a certain pressure profile.

Blast pressure profiles are important pressure time histories for any point in space

subjected to a blast wave. The characteristic pressure profile decays exponentially from a

peak overpressure into a pressure region below ambient pressure called the negative

overpressure phase. Typically, the negative pressure phase is ignored in design and in

many analytical models. The pressure curve takes the form of the modified Friedlander’s

equation shown in equation (1).

t

+ t ⎞ -b +
p(t) = po + P ⎜1- + ⎟ e T
s Eq. (1)
⎝ T ⎠

In equation (1), t is measured from the time of arrival, Ps+ is the peak

overpressure, po is the ambient atmospheric pressure, and b is the decay coefficient

(Chock and Kapania, 2001). The area under the pressure profile above ambient pressure

is equivalent to the positive phase impulse, I+. Figure 1 displays a typical blast pressure

profile for any point in the vicinity of a blast event.


81

+
Ps

Impulse
Pressure

Pa
Ta T
+ -
T

Time

Figure 1. Typical blast pressure profile (Chock and Kapania, 2001)

For design purposes, the blast pressure profile is usually simplified as a triangle

impulse loading, as shown in Figure 2.

+ +
Ps T
Pressure

Pa

Time

Figure 2. Simplified triangular blast pressure profile (Lu et al., 2005)


82

Only the peak overpressure, Ps+, and the duration of the blast impulse, T+, are

required to define the blast loading using the simplified profile. These two parameters

can be related to the charge weight and standoff distance using a few simple equations

(Lu et al., 2005). The peak pressure may be expressed in terms of the scaled distance, Z,

as shown in equations (2) and (3).

6.7
Ps = +1 bar (Ps ≥ 10 bar) Eq. (2)
Z3

0.975 1.455 5.85


Ps = + 2 + 3 - 0.019 bar (0.1 ≤ Ps ≤ 10 bar) Eq. (3)
Z Z Z

Scaling the properties of blast waves from explosives is very common. Scaled

distances are used to predict parameters of large-scale explosions based on small-scale

tests. Several methods of scaling blast parameters are used in analysis to generalize the

results, so they may be used in blast simulations with various amounts of energy and

standoff distance. One of the most common methods of scaling blast parameters is the

Hopkinson-Cranz blast scaling. Hopkinson hypothesized that if two different charge

weights of the same explosive were detonated, both charges would produce similar

pressure profiles at an identical scaled distance. This scaled distance formula is presented

in equation (4), where R is the distance from the center of the explosive source (m), and

W is the TNT equivalent charge weight (kg) (Baker, 1983).

R
Z= 1
Eq. (4)
W 3
83

Normally, W represents the weight of a standard explosive such as TNT. When

other types of explosives are used, the mass of the explosive can be converted into a TNT

equivalent mass using a conversion factor. The conversion factor is simply a ratio of the

specific energy of a particular explosive and the specific energy of TNT. Several

common explosives are shown in Table 1.

Table 1. TNT equivalence values for common explosives (Baker, 1983)

Specific TNT Detonation Detonation


Energy Equivalent Density velocity pressure
Explosive QX (KJ/kg) QX/QTNT (Mg/m3) (km/s) (Gpa)
RDX (Cyclonite) 5360 1.185 1.65 8.70 34.0
Nitroglycerine (liquid) 6700 1.481 1.59 - -
PETN 5800 1.282 1.77 8.26 34.0
Pentolite 50/50
(50% PETN, 50% TNT) 5111 1.129 1.66 7.47 28.0
TNT 4520 1.000 1.60 6.73 21.0
Composition C-4 5876 1.3 1.58 - -
HMX 5680 1.256 1.90 9.11 38.7
Unit conversion: 1 KJ/kg = 0.43 Btu/lb

Another model based on scaled distance was developed by the Department of

Defense Explosives Safety Board (DDESB). For the past several years, the DDESB has

had an important role in producing an explosion effects computation program known as

the Blast Effects Computer (BEC). BEC version 5.0 was used in this study to calculate

the incident and reflected air blast pressures resulting from the detonation of various

weights of C-4 explosive. Figures B1 through B4 in Appendix B show the calculated

incident and reflected pressures at various locations on the surface of the panel for the

charge weights used in the blast testing. Version 5 of the program takes into account the

effect of selected potential explosion sites, various types of weapons, the TNT
84

equivalence of the explosive, and the altitude of the event. The BEC algortithms are

based on experimental results, and outputs are usually within a few percent of actual

measured values. The BEC computes the time of arrival, incident overpressure, reflected

pressure, and other blast wave properties. The incident overpressure and reflected

pressure were the only properties compared in this study. The equations used to calculate

the incident overpressure are shown in equation (5) (Swisdak, 2003). The scaled

distance, Z, is based on an equivalent weight of TNT, so a factor of 1.3 was multiplied to

the weight of the C-4. The equations presented here are based on U.S. customary units.

Scaled distances should be expressed in ft/(lb1/3), and pressures are expressed in psi.

-4 2 2
For Z < 7.25 Pi = 1006z-1.44 e1x10 ln(z) (685ln(z) -1416ln(z)-2815)

-4 2 2
For 7.5 < Z < 60 Pi = 6658z-3.7e-1x10 ln(z) (127ln(z) -733ln(z)-2709) Eq. (5)

Scaled distances larger than 18.3 m (60 ft) were not considered, but a separate

equation exists for those values up to a scaled distance of 1,524 m (5,000 ft). The

atmospheric parameter, Sp, was used convert the calculated overpressures at sea level to

pressures that would be developed in the atmospheric conditions existing during the blast

testing. The Sp parameter is simply the ratio of the atmospheric pressure at the blast

location and the atmospheric pressure at sea level. Considering Rolla, Missouri, is

approximately 343 m (1,125 ft) above sea level, Sp was taken to be 0.9605 for the

pressure calculations.

Reflected pressures were also calculated using equation (6). Due to very low

scaled distance values investigated in this study, the equations shown here are not

applicable and, therefore, are inaccurate. The BEC program displays an “out of range”
85

warning for scaled distances below 0.3 ft/(lb1/3). Furthermore, the BEC model assumes

100 percent of the blast wave is reflected, which is not true. Some amount of energy is

absorbed by the test panel. The amount of energy the test panels absorbed could not be

quantitatively measured during the blast test.

For Z < 4
-4 2 4 3 2
Pr = 8774z-1.751e-1x10 ln(z) (118ln(z) -696ln(z) +128ln(z) +2199ln(z)+2877)

For Z ≤ 100 Eq. (6)


-6 2 4 5 3 6 2 6 6
Pr = 173z9.16e-1x10 ln(z) (8181ln(z) -1.6x10 ln(z) +1.3x10 ln(z) -5.6x10 ln(z)+11.9x10 )

The two models previously discussed are represented in Figure 3. The model

developed by the DDESB is more conservative than the model referenced by Lu et al.

(2005), but the curves follow the same trends. The corresponding pressures for scaled

distances below 1 m/(kg1/3) begin to increase exponentially toward infinity. Infinite

pressure is not possible, so scaled distance values were limited to a minimum of 0.3

ft/lb1/3. As stated previously, the BEC program displays an “out of range” warning for

the scaled distances used in this study, which were smaller than 0.3 ft/lb1/3. The program

still calculates incident and reflected pressure values, but the model is no longer accurate.

2.1.1 Dynamic strength of materials

Rapid strain rates occuring from a blast lead to increases in the strength of the

concrete and reinforcement. These increased dynamic strengths are used to calculate the

dynamic resistance of the material to the applied blast load. Therefore, the ultimate

resistance of a material subjected to a blast load is larger than its static load resistance. A

dynamic increase factor (DIF) is applied to static strength values to approximate the
86

dynamic strength of the material. The DIF is a ratio of the dynamic material strength to

static strength. Therefore, the factor is a function of the type of material and the strain

rate applied to it. Table 2 displays DIF values for various construction materials and

stress types.

1000000
Incident
Incident Pressure
Pressure (DDESB)
Incident Pressure
(Mays and Smith)
Incident or Reflected Pressure (kPa)

Incident (Mays
Model)
Reflected
Reflected Pressure (DDESB)
Pressure
10000

100

1
0 10 20 1/3
30 40
Scaled distance, Z (m/kg )

Unit conversion: 1 kPa = 0.145 psi

Figure 3. Theoretical incident and reflected pressure curves

Table 2. Dynamic increase factors (TM 5-1300, 1990)

Reinforcing bars Concrete Masonry


Stess type Fdy/Fy Fdu/Fu f'dc/f'c f'dm/f'm
Flexure 1.17 1.05 1.19 1.19
Diagonal tension 1.00 1.00 1.00 1.00
Direct shear 1.10 1.00 1.10 1.00
Compression 1.10 1.00 1.12 1.12
Bond 1.17 1.05 1.00 1.00
87

The ultimate strength and ductility of the material is important when predicting

the behavior of a structural element subjected to a blast load. Ductile materials require

less strength than brittle materials to resist the same applied blast load. Brittle materials

tend to fail rapidly, unable to absorb much energy in the plastic range; however, ductile

materials maintain strength through large plastic strains (TM 5-1300, 1990).

2.1.2 Shock wave behavior in solids

A basic understanding of how shock waves propagate through solids is helpful to

better understand the modes of failure resulting from a blast event. The shock wave is

generated by the sudden contact of the hot gases with the surrounding air immediately

after the detonation of the explosive. The shock wave then propagates through any

nearby solids. The shock wave in the solid is basically treated as a discontinuity in

density, pressure, and temperature. The equations applying to this discontinuity were

first developed by Rankine and Hugoniot. The wave moves through the material at a

velocity corresponding to the maximum pressure in the pulse. When a shock wave

encounters an interface between two different materials, some of the wave is transmitted

into the new material, and some of the wave is reflected (Rinehart, 1975).

Two boundary conditions must be met at the interface of the two materials —

continuity of pressure and continuity of particle velocity. This condition is known as

impedance mismatch. The relative intensities of the both waves are dependent on the

density and stiffness of the adjoining materials. The reflected wave may be either in

compression or tension depending on the impedance mismatch between the two materials

(Rinehart, 1975). In the case of the panels tested in this study, the reflected stress waves

were in tension because the panel had a higher density than air. The collision of the
88

reflected tensile stresses from the adjoining sides of the panels caused a tension failure in

the stiff RC panels.

2.2. Retrofitting reinforced concrete slabs with composites

In a previous study, five RC slabs were tested under real blast loads at various

standoff distances and charge weights. The purpose of the test was to assess the

possibility of using the displacement based design (DBD) method to predict the blast

resistance of a RC slab. The RC slabs were strengthened with carbon fiber reinforced

polymers (CFRP) and steel reinforced polymers (SRP). Test results proved that the DBD

method can successfully estimate the blast loads needed to cause a specified level of

damage. Results also demonstrated that RC slabs retrofitted with fiber-reinforced

polymer (FRP) on both faces have a much higher blast resistance than slabs retrofitted on

one side only (Lu et al., 2005).

The test matrix developed in the previous study to assess the DBD method was

used in this study, so results from the two studies could be easily compared. The RC

slabs used in the previous study had nominal dimensions of 1200 x 1200 x 89 mm (47.25

x 47.25 x 3.5 in.). For Lu’s study, one slab was used as a control for comparison, and it

was not reinforced with FRP. Two slabs (2A and 2B) were retrofitted with CFRP, and

two slabs (3A and 3B) were retrofitted with SRP. Slabs 2A and 3A were retrofitted on

the tension face only, and slabs 2B and 3B were strengthened on both sides. The slabs

were tested in the experimental mine at UMR. The specimens were simply supported on

two box beams, and the charges were suspended above the specimens using a wire.

Charges were composed of desensitized RDX high explosive, the equivalent to military

C-4 demolition explosive.


89

2.2.1 Material properties

Each of the five specimens was batched with 28 MPa (4.06 ksi) concrete and had

a reinforcement ratio of 0.18 percent in each direction at mid depth. The steel

reinforcement had a tensile strength of 410 MPa (60 ksi) with an elastic modulus of 200

GPa (29,000 ksi). The CFRP and SRP laminates exhibited elastic behavior up to their

ultimate tensile strengths, which were 3,790 MPa (550 ksi) and 1,170 MPa (170 ksi),

respectively. The elastic moduli of the CFRP and the SRP were 230 GPa (33,359 ksi)

and 78 GPa (11,313 ksi), respectively.

2.2.2 Test results

Charge weights and standoff distances were chosen using the DBD method to

achieve two specified displacement ductility levels, 1 and 4. Ductility level 1

corresponds to minor cracks or no damage, and level 4 corresponds to visible cracks and

crushing of the cover concrete. The RC control slab was subjected to two blast events.

The first event, a charge of 0.45 kg (1.0 lb) at a 915 mm (36 in.) standoff, caused no

damage as expected. The second event was a 0.9 kg (2.0 lb) charge at a 300 mm (12 in.)

standoff, which caused major flexural cracks at the mid-span of the slab. The residual

displacement at the center of the slab was measured at 21 mm (0.875 in.), and the

residual displacement at the midpoint along the edge was measured at 11 mm (0.5 in.).

The RC slab strengthened with CFRP on the tension face, slab 2A, was loaded

with a 1.35 kg (3.0 lb.) charge at a standoff distance of 300 mm (12 in.). The event

severely damaged the slab to the extent that no residual deformations could be measured.

Slab 2B was strengthened with CFRP on both faces and subjected to the same charge

weight at the same standoff distance. With no major flexural cracks, slab 2B performed
90

much better with a residual deflection of 44 mm (1.75 in.) at center and 28 mm (1.10 in.)

along the edge. Slab 3A, which was retrofitted with SRP on the tension face, failed under

the same blast load and standoff as slab 2A. Furthermore, slab 3B had a similar amount

of damage as slab 2B, and also developed two major shear cracks at the supports. The

residual deflections on slab 3B were the same as those for 2B.

Two main conclusions were drawn from the study. First, the DBD method

accurately estimated the charge weight and standoff distance required to impose a

specified displacement ductility level. Additionally, results proved that slabs must be

strengthened on both faces to significantly improve their resistance to blast loads.

Results did not show any distinction between the two types of reinforcement used in the

study.

3. EXPERIMENTAL PROGRAM

The main purpose of the blast testing was to investigate the blast mitigation

properties of a high-volume FA-WF material being developed at UMR. The material has

low strength and density but has a higher level of ductility than plain concrete.

Compression and modulus of elasticity tests revealed the material can undergo large

strains without fracturing. Although the material is not adequate to support the static

loads of a superstructure, the material’s ductile failure mode and energy absorbing

characteristics are necessities in blast resistant applications.

In this study, ten panels were tested using various charge weights and standoff

distances, some of which were prescribed in a previous blast study conducted at UMR

(Lu et al., 2005). The panels consisted of RC as well as a high-volume FA-WF blast

mitigation material (BMM). The blast testing was broken into two phases, and five
91

panels were tested in each phase. Test panels in the second phase were coated with a

spray-on polyurea, which is already being used in many building retrofits for increased

protection from improvised explosive devices (IEDs).

Tables 3 and 4 display the test matrix for each phase of testing. For each test

panel, the charge weight was increased, and the standoff distance was decreased with

each subsequent event until the panel failed. Comparisons were then made between the

failure modes and extent of damage of each panel.

Table 3. Phase 1 test matrix

Charge Standoff
Panel No. Event No. weight, grams distance, mm Description
1 454 915 Bi-layered construction with
2 680 610 concrete base and top layer of
Panel 1A BMM. 0.2% reinforcement ratio
3 907 305 in concrete and 0.16% in BMM
4 1360 305 layer [140 mm (5.5 in.) thick]
1 225 915 High volume fly ash-wood fiber
2 450 915 blast mitigation material with
Panel 2A reinforcement ratio of 0.2% in
3 680 610 each direction [89 mm (3.5 in.)
4 907 305 thick]
1 454 915 Normal-weight concrete with
addition of 6% wood fibers by
Panel 3A 2 680 610
weight. 0.2% reinforcment ration
3 907 305 each direction [89 mm thick]
1 454 910 Normal-weight concrete with
Panel 4A 2 1134 305 0.5% reinforcement ratio each
3 1360 152 direction [89 mm (3.5 in.) thick]

1 454 915
Bi-layered construction with
2 1134 305 0.5% reinforced concrete base
Panel 5A
3 1360 305 and top layer of BMM [140 mm
(5.5 in.) thick]
4 1360 Contact
92

Table 4. Phase 2 test matrix

Charge Standoff
Panel No. Event No. weight, grams distance, mm Description
1 680 610 Bi-layered construction with
2 907 305 concrete base and top layer of
Panel 1B BMM. 0.2% reinforcement ratio
3 1360 305 in concrete and 0.16% in BMM
4 1360 152 layer coated with polyurea

High volume fly ash-wood fiber


1 680 610
blast mitigation material with
Panel 2B reinforcement ratio of 0.2% in
each direction. Coated with
2 907 305
polyurea

1 680 610 Normal-weight concrete with


wood fibers. 0.2% reinforcment
Panel 3B 2 907 305
ration each direction. Coated with
3 1360 152 polyurea
1 680 610
Normal-weight concrete with
Panel 4B 2 1134 305 0.5% reinforcement ratio each
direction. Coated with polyurea
3 1360 152
1 680 610
FA-C-WF panel and RC panel
2 907 305 separated by 19 mm air gap.
Panel 5B
3 1360 305 Reinforcement ratio of each panel
was 0.2%
4 1360 152

3.1 Test setup

Mix designs chosen for the blast study were based on data collected from impact

tests performed at UMR (Tinsley and Myers, 2007). A modified version of the ACI

drop-weight impact test for concrete was carried out on seven various mix designs to

compare their relative impact resistances. The test is conducted by repeatedly dropping a

4.54 kg (10 lb) proctor hammer onto an impact piston, which applies a linear impact load
93

to the top surface of the test specimen. The test specimens are approximately 150 mm (6

in.) in diameter and 50 mm (2 in.) thick.

The relative impact resistance of each specimen is measured by simply counting

the number of blows to first crack (FC) and ultimate failure (UR). The tests revealed that

polypropylene fiber-reinforced concrete (PFRC) had the highest 28-day impact resistance

with an average of 33 blows to failure. The PFRC was followed closely by a material

composed of fly ash, Portland cement, and milled wood fibers (FA-C-WF). This

environmentally green material had an average 28-day impact resistance of 27 blows.

The blast study incorporated another mix design developed from the impact analysis that

also performed relatively well. The mix design included a normal weight concrete mix

with the addition of 6 percent wood fibers by weight. The average 28-day impact

resistance of that material was 19 blows. In comparison, the plain concrete had an

average 28-day impact resistance of 6 blows.

One important conclusion developed from the impact testing was the failure mode

of the various materials. The concrete failed in a brittle manner, while the FA-C-WF

material held together to some extent even as the impact piston penetrated the surface of

the specimen. Therefore, this material was chosen to be used as a sacrificial layer in the

blast study. The sacrificial layer was designed to fail, and in doing so, absorb some

amount of energy from the blast wave.

3.1.1 Materials

Several mix designs were used to fabricate the two series of test panels. The

panels were composed of the following materials: Class C fly ash, Portland cement,
94

wood fibers, limestone, and river sand. The mechanical properties of the mix designs are

discussed later in section 3.2.

ASTM Class C fly ash was donated from Encore Building Solutions (EBS) of St.

Louis, Missouri. The fly ash was a key ingredient in the low density BMM used in

several of the test panels. EBS received the fly ash from the Rush Island Power Plant in

Jefferson County, Missouri. Table 5 displays the chemical composition and properties of

the Class C fly ash.

Table 5. Chemical composition of fly ash (Joshi and Myers, 2005)

Rush Island Type I Portland


Parameter
fly ash (%) cement (%)
Sulfur in ash 0.7 -
Sulfur in ash (SO3) 1.75 2.5
Fineness (325 sieve) 81.9 -
Moisture 0.03 -
Loss of ignition (LOI) 0.17 1.4
Density 2.73 -
Specific gravity 2.74 -
Titanium oxide as TiO2 1.23 -
Aluminum oxide as Al2O3 17.06 4.9
Calcium oxide as CaO 26.12 64.4
Iron oxide as Fe2O3 6.31 2.1
Potassium oxide as K2O 0.39 -
Magnesium oxide as MgO 5.77 3.5
Sodium oxide as Na2O 1.87 -
Silicon oxide as SiO2 35.43 20.08
Phosphorus oxide as P2O5 0.9 -
Slagging index 0.34 -
95

Commerical grade Quickrete type I Portland cement was an ingredient in all ten

test panels and complied with ASTM C 150-05 specifications. The dry density of the

cement is approximately 1506 kg/m3 (94 lb/ft3) (ASTM C 188-95).

Milled wood fibers were graciously donated from EBS. The fibers were recycled

from old loading pallets. The gradation of the milled wood fibers ranged from a

maximum size of 13 mm (0.5 in.) to very fine particles. The majority of the fibers were

between 6 to 13 mm (0.25 to 0.5 in.) in length. The mechanical properties of oak wood

are listed in Table 6.

Table 6. Mechanical properties of oak (Joshi and Myers, 2005)

Mechanical Properties Green Air Dried


3
Weight (lb/ft ) 63 47
Modulus of Rupture (psi) 8100 13900
Modulus of Elasticity (ksi) 1200 1620
Maximum crushing strength parallel to grain (psi) 3520 7040
Compression perpendicular to grains (psi) 850 1410
Maximum shearing strength parallel to grain (psi) 1270 1890
3 3
Unit conversion: lb/ft = 16.02 kg/m , 1 psi = 6.895 kPa

Gasconade dolomitic limestone from Capital Quarry was used in several of the

mix designs. The limestone had a nominal maximum size of 13 mm (0.5 in.) and a bulk

specific gravity of 2.70 in an oven-dried condition (ASTM C 127-04). The absorption of

the aggregate was roughly 1.2 percent, and the moisture content remained below 0.1

percent when batching each test panel.

The river sand had a bulk specific gravity of 2.54 in an oven-dried condition, and

the absorption was calculated to be approximately 1.4 percent (ASTM C 128-07). Little
96

Piney Creek near Rolla, Missouri, was the source of the sand. The moisture content of

the sand did not exceed 0.75 percent when batching the test panels.

An elastomeric polyurea was sprayed onto the top and bottom surfaces of the test

panels in Phase 2. The Air Force Research Laboratory at Tyndall Air Force Base in

Florida has already begun to investigate the use of polyurea in blast load applications

(Knox et al., 2000). The material is highly ductile and can easily be sprayed onto almost

any building surface. The polyurea offers an increased level of protection against an

explosive charge for occupants inside a building. The material bonds to the walls and

ceiling to form an elastic skin that prevents flying debris from entering the building. The

polyurea coating does not improve the structural integrity of the wall but will prevent

injuries by containing wall fragments. Recent studies show that polymer retrofits can

reduce required standoff distances by approximately 50 percent for a specific level of

damage (Knox et al., 2000).

Coupon tests were conducted on three samples of the polyurea applied to the test

panels in Phase 2 to characterize the material. The samples had nominal dimensions of

254 x 50 x 3 mm (10 x 2 x 0.125 in.). Thin sheets of aluminum were glued to each end

of the test specimens before they were tested to provide a grip bearing for the testing

machine. The coupon test was conducted using an Instron 4485 testing machine located

in the Interdisciplinary Engineering building at UMR.

Figure 4 shows the polyurea samples. Figure 4-a displays a sample undergoing

the tensile test, which was carried out at a rate of 51 mm/min (2 in./min). The average

modulus of elasticity of the material was calculated to be 82.68 MPa (12 ksi), with a yield

strength of 2,067 kPa (0.3 ksi) at a 0.2 percent offset. The elongation of the material was
97

measured at 279 percent. While the polyurea specimens could have elongated further the

test was aborted due to the range of the machine. Therefore, the ultimate stress of the

material could not be determined using the Innstron 4485 testing machine. Figure 4-b

also shows a comparison of three samples, two of which have residual strain from the

test. The sample on the right was not tested.

(a) Coupon test of polyurea (b) Samples of polyurea

Figure 4. Polyurea tensile test

Figure 5 displays the stress-strain relationship of the material. Notice the material

has a significant amount of ductility. The peak stress value is not actually the breaking

point. The material could not be ruptured, and the test was aborted due to limitations on

range of the machine.

Steel reinforcement was used in the panels as well. ASTM number 3 bars were

used as longitudinal reinforcement in all the panels, and a 6.3 mm (0.25 in.) cold rolled

round bar was used for stirrups in the bi-layered test panels. The 9.5 mm (0.375 in.)

rebar had a yield strength of 437.8 MPa (63.5 ksi) at a 0.50 percent offset and an ultimate
98

strength of 706.7 MPa (102.5 ksi). The elongation at failure was measured at

approximately 16 percent. The 6.3 mm (0.25 in.) cold rolled round bar had a yield

strength of approximately 582.6 MPa (84.5 ksi) and a peak stress of 604 MPa (87.6 ksi).

Figure 6 presents the tensile test setup, which was performed on the Tinius Olsen testing

machine.

5
Stress (MPa)

2 Specimen 1
Specimen 2
1 Specimen 3

0
0 50 100 150 200 250 300
Strain (%)

Unit conversion: 1 MPa = 145 psi

Figure 5. Stress-strain relationship for polyurea undergoing tensile load

3.1.2 Test specimen fabrication

Two sets of wooden forms were constructed to produce the blast panels. Forms

were made using two 13 mm (0.5 in.) sheets of plywood and several 25 x 102 mm (1 x 4

in.) and 25 x 152 mm (1 x 6 in.) sections of dimensional lumber. The forms produced

panels with nominal dimensions of 1180 x 1180 mm (46.5 x 46.5 in.). One form was
99

constructed to produce a panel thickness of 90 mm (3.5 in.), while the other was built to

produce panels with a thickness of 140 mm (5.5 in.). The thicker form was used when

constructing bi-layered systems composed of a 90 mm (3.5 in.) thick RC base with a 50

mm (2 in.) layer of a high-volume FA-WF composite applied to the surface. Once the

forms were constructed, an epoxy coating was applied to prevent concrete from adhering

to the bottom and sides of the forms. Plastic sheeting was also stapled to the forms to

allow the hardened specimens to be lifted out of them without having to remove the side

walls. Figure 7 shows the two sets of forms.

Figure 6. Tensile test on No. 3 rebar

As mentioned previously, standard size reinforcing bars with a number 3 ASTM

bar designation were used as the primary reinforcement in the panels. Wooden square

pegs served as chairs to provide 25.4 mm (1 in.) of cover below the rebar. The

reinforcement ratio was roughly 0.2 percent in both directions for the majority of the

panels. Number 3 bars were also bent into triangles to serve as lifting eyes. Three panels
100

fabricated during a previous blast study were also tested, and the reinforcement ratio for

those panels was approximately 0.5 percent (Lu et al., 2005). Figures B5 and B6 in

Appendix B display the two reinforcement layouts.

(a) 90 mm form (b) 140 mm form for 2-layer construction

Figure 7. Formwork for blast panel fabrication

Once the rebar mats were tied and properly placed in the forms, the material was

weighed and mixed using a rotary drum mixer. The mix designs used in the study are

shown in Table 7. Notice Panel 1A and 1B have the same mix design, as well as the

Panel 3 set. The mix design used to fabricate Panels 4A and 4B is not known since the

concrete was bought from a ready mix company.

A conventional rotary drum mixer was used for batching the 0.17 m3 (6.0 ft3)

needed to fill the formwork and cylinder molds for each panel. Mixing the BMM was

difficult due the high viscosity of the fresh material. First, the mixer was washed out to

dampen the inside of the drum. Then, all the fly ash, cement, and half the water were

added to the drum and allowed to mix for approximately one minute. A high-range water

reducer (HRWR) was added to the remaining portion of water. After mixing for one
101

minute, the inside of the drum was scraped clean of material build-up, as shown in Figure

8. Then, the mixing process proceeded, and half of the remaining water was added along

with the wood fibers. At this point in the mixing process, the mix had to be watched

carefully to ensure balling did not occur.

Table 7. Mixture proportions for blast panel fabrication

Panel 1 A&B Panel Panel 5B


Panel Panel Panel 3 5A
Component BMM Base 2A 2B A&B BMM BMM Base
Class C fly ash 462.9 - 462.9 462.9 - 462.9 462.9 -
Portland cement
(type I) 278.7 410.1 278.7 278.7 451.1 278.7 278.7 416.5
White oak wood
fibers 112.1 - 112.1 184.2 135.4 112.1 160.2 -
1/2" limestone - 999.6 - - 809.6 - - 1009.2
Sand - 799.3 - - 647.5 - - 674.4
Water 281.9 144.2 281.9 355.6 135.4 281.9 289.9 187.4
High-range water
reducer
(ml/ 100 kg) 2.6 5.2 2.6 3.9 5.2 2.6 1.3 2.6
Water / cement ratio 0.38 0.35 0.38 0.48 0.30 0.38 0.39 0.45
% Wood fiber by
weight 10.0 0.0 10.0 14.5 6.2 10.0 13.0 0.0
Units are in kg/m3: Unit conversion: 1 kg/m3 = 0.0624 lb/ft3
Note: Mix proportions for Panel 4 were not available

Finally, the remaining portion of water was added to the mixer. Mixing continued

for another five minutes after all the materials were added to the drum. After a uniform

distribution of wood fibers was achieved, the material was poured into a wheelbarrow

and placed into the form carefully to ensure the rebar chairs were not disturbed (see

Figure 8-b). The material was not vibrated due to its low workability. Instead, the sides

of the form were tapped with a rubber mallet to prevent voids. The panel was finished
102

smooth using trowels and covered with a sheet of plastic for 48 hours to avoid moisture

loss during curing.

A portion of the material was used for a slump test according to ASTM C 143-05

specifications. Slumps for the BMM ranged from 102 to 152 mm (4 to 6 in.), but the

slump test did not provide an accurate workability measurement when compared to a

concrete mix with the same slump. Compression and modulus specimens were made in

compliance with ASTM C 192/C 192M-06.

(a) Mixing BMM (b) Wooden rebar chair

Figure 8. Batching procedures

The normal-weight concrete mix was batched in much the same way as the BMM.

In this case, however, coarse and fine aggregates were used, which made the mixing

process much easier. First, the coarse and fine aggregates and Portland cement were

mixed in a dry state for about one minute. Then, approximately half the mixing water

was added to the mix. The remaining portion of water was added along with the HRWR

after another two minutes of mixing. Mixing continued for approximately another five

minutes to achieve a homogeneous mix. Then, the fresh concrete was shoveled into the
103

form, finished using concrete trowels, and covered with a sheet of plastic. A handheld

form vibrator was used to eliminate voids. The plastic was used to prevent moisture loss

for the first five days of curing. The test panels were allowed to cure in the forms for at

least five days before removing them. The slump values for the concrete ranged from

152 to 203 mm (6 to 8 in.). Compression and modulus specimens were made in

compliance with ASTM C 192/C 192M-06. These mixing procedures were used to

fabricate the concrete bases of Panels 1A, 1B, and 5B. These mixing procedures were

also followed when batching the concrete-wood fiber material used to fabricate Panels

3A and 3B, except the wood fibers were added before adding the remaining water and

HRWR.

Test Panels 1A and 1B were fabricated in two layers. The mix designs for both

layers are shown in the second and third columns of Table 7. The concrete layer had a

reinforcement ratio of 0.2 percent in both directions, while the BMM layer had a

reinforcement ratio of 0.16 percent in one direction only. The two layers were tied

together with 6.4 mm (0.25 in.) cold rolled steel bar. The concrete base was poured and

allowed to cure for 48 hours before adding the BMM on top of it. The surface of the

concrete was roughened to increase the bond between the two layers. Figure 9 shows the

fabrication of the system.

Panel 5A was a retrofit of a slab left over from a previous study. The concrete

slab had a reinforcement ratio of 0.5 percent in both directions. The reinforcement layout

for the slab is shown in Figure B5 of Appendix B. The panel was retrofitted with a 50

mm (2 in.) layer of BMM. The two layers were tied together using 6.4 mm (0.25 in.)

steel bars in the layout shown in Figure 10.


104

(a) Fresh concrete base (b) Addition of BMM

Figure 9. Fabrication of Panels 1A and 1B

Holes were drilled into the concrete, and the bars were attached using a two-part

epoxy. Three 6.4 mm (0.25 in.) bars were tied to the stirrups to provide longitudinal

reinforcement in the BMM layer. The concrete base was fabricated from a 27.6 MPa

(4,000 psi) mix design provided by Rolla Ready Mix of Rolla, Missouri, and the blast

mitigation layer was fabricated using procedures explained previously.

(a) Stirrup retrofit to concrete (b) Blast mitigation layer

Figure 10. Fabrication phases for Panel 5A


105

3.1.3 Spray-on polyurea application

The series of panels tested in the second phase of the blast study were coated with

a spray-on elastomeric polyurea. This process took place in the Engineering Research

Laboratory (ERL) at UMR. The polyurea consists of a resin blend and an aliphatic

isocyanate quasi-prepolymer. The two components were mixed at a 1 to 1 ratio in a

chamber on the spray gun. The materials were heated in two separate containers and

hoses to lower the viscosity of the two components while mixing. The combined mix

must leave the nozzle at or above a pressure of 13.8 MPa (2,000 psi), which then hardens

within seconds as it adheres to the test panel. Figure 11 shows the test panels being

coated with polyurea.

(a) Panel 1B (b) Panel 3B

Figure 11. Polyurea application

3.2 Mechanical properties of the material

Several mechanical properties were determined for each test panel from both

phases of blast tests. These include the compressive strength, indirect tensile strength,
106

and modulus of elasticity (MOE). Cylinders were capped with a sulfur compound before

the compressive strength and MOE were determined.

3.2.1 Compressive strength

The compressive strength of each material was determined using a standard

specimen size of either 150 x 300 mm (6 x 12 in.) or 100 x 200 mm (4 x 8 in.). The

specimens were prepared in the lab according to ASTM C 192-06 specifications. The

150 mm (6 in.) diameter cylinders were made in 3 equal layers and rodded 25 times per

layer using a 16 mm (0.625 in.) diameter tamping rod. The 100 mm (4 in.) cylinders

were made in 2 layers. The specimens were removed from the molds after 24 hours and

placed next to the test panels to member cure. The room temperature remained roughly

20°C (70°F).

Before testing, specimens were capped to ensure parallel surfaces according to

ASTM C 617-98 specifications. Rediron capping compound was melted to a temperature

of approximately 135°C (275°F). Then, the compound was poured in a machined metal

plate using a ladle. The end of the specimen was placed directly into the melted capping

compound with the aid of an alignment device and held in place until the compound

solidified.

In most cases, two cylinders were tested, and the average of the two was used to

define the compressive strength of the mix. Cylinders were tested according to ASTM C

39-05 specifications. A load rate of 4.5 kN/sec (1,000 lb/sec) was used for the 150 mm

(6 in.) concrete specimens. The load rate was reduced to 3.4 kN/sec (750 lb/sec) when

testing the blast mitigation material due to its low strength and high strain values. In

most cases, the Forney LC-4 compression testing machine, which is calibrated to 1,780
107

kN (400,000 lb), was used to carry out the compression tests. The average compressive

strength values for all the panels are shown in Table 8.

3.2.2 Modulus of elasticity

The MOE, or Young’s modulus, was determined using the Tinius Olsen universal

testing machine in accordance with ASTM C 469-02 specifications. A linear variable

differential transformer (LVDT) was attached to the compressometer and measured the

strain. The Tinius Olsen has a data acquisition system that is controlled with integrated

computer software which automatically generates stress-strain plots. To obtain the MOE,

each specimen was loaded to 60 percent of its compressive strength at a load rate of 4.5

kN/sec (1,000 lb/sec) to condition the specimen. Then, the specimen was loaded once

more at the same rate. The MOE was determined between a point corresponding to a

very small strain value and a point corresponding to 40 percent of the ultimate stress.

Table 8. Mechanical properties summary for blast panels

Density Compressive Young's Indirect tensile


Panel No. Material (kg/m3) Strength (MPa) Modulus (MPa) strength (kPa)
FA-C-WF 1605 9.37 3102 1103
Panel 1A
Concrete 2390 65.32 41370 4620
FA-C-WF 1530 8.77 - -
Panel 1B
Concrete 2365 68.98 - -
Panel 2A FA-C-WF 1485 7.34 1724 862
Panel 2B FA-C-WF 1315 1.69 - -
Panel 3A WF concrete 1730 12.83 7584 1034
Panel 3B WF concrete 1815 14.13 - -
Panel 4 A&B Concrete - > 27.58 - -
Panel 5A FA-C-WF 1515 7.74 3792 965
FA-C-WF 1370 10.53 5516 1138
Panel 5B
Concrete 2350 48.72 37921 4482
3 3
Unit conversions: 1 kg/m = 0.0624 lb/ft ; 1 MPa = 145 psi
108

Figure 12 displays the relative modulus curves for each blast panel. The normal

weight concrete, with MOE values in excess of 37,000 MPa (5,300 ksi), had a much

higher strength and stiffness than any mix with wood fibers. The strongest blast

mitigation mixture that contained wood fibers was used to fabricate panels 3A and 3B.

The mix design consisted of coarse and fine aggregates but also contained 6 percent dry

wood fibers by weight. As seen in Figure 12, the addition of wood fibers greatly

decreases the stiffness of the material. Modulus values for all the materials are listed in

Table 8. Panel 1B was assumed to have the same stiffness as that of Panel 1A because

they were fabricated simultaneously. The material strength of Panel 2B was so low that

the stiffness was not measured. Modulus data for Panel 4 was unavailable.

35
Panel 1-BMM
30 Panel 1- Concrete
Panel 1A-base
Panel 2A
Panel 3
25
Panel 5A-BMM
Panel 5B-BMM
Stress (MPa)

20
Panel 5B- Concrete
Panel 1B-base

15

10

0
0 0.0005 0.001 0.0015 0.002
Stain (mm/mm)

Unit conversion: 1 MPa = 145 psi

Figure 12. Modulus of elasticity curves for blast panels


109

3.2.3 Splitting tensile strength

The indirect tensile strength of the test materials were obtained according to

ASTM C 496-04 specifications. The split-tension test was performed on 100 x 200 mm

(4 x 8 in.) cylinders to indirectly measure the tensile strength of the concrete. Specimens

were loaded at 556 N/sec (125 lb/sec) along their lengths until failure, which occurred

due to tension developed in the transverse direction. The tensile strengths of the

materials are shown in Table 8.

4. EXPERIMENTAL TEST RESULTS

4.1 Phase 1 blast testing

Phase 1 of the blast mitigation barrier study was conducted on December 11,

2006, through December 13, 2006. Five panels were tested using a total of 16 events

with various charge weights and standoff distances. The panels were tested in the UMR

experimental mine. The preparation of each panel was simple. Four accelerometer clips

were glued to the bottom face of each panel before the panel was carried into the mine.

A Bobcat was used to carry the panel into the mine and place it on two steel w-sections.

Each panel was simply supported on the steel beams with a 127 mm (5 in.)

bearing on each end, as shown in Figure 13. Charges were hung from a support bar to a

specified standoff distance measured from the center of the explosive to the top face of

the test panel. The explosives used in Phase 1 consisted of a combination of Pentolite

cast boosters and Composition C4. Only C4 was used in Phase 2.

Accelerometers were clipped to the bottom face of the panel for use in events of

small charge weights up to a 0.91 kg (2 lb) charge at a 305 mm (12 in.) standoff distance.

The accelerometer cables were placed in pvc pipes to prevent debris from damaging
110

them. A Synergy portable data acquisition system from Hi-Techniques was used to

record the accelerations applied to the panels. Figure 14 shows the locations of the

accelerometers on the panel. Midspan deflections were measured using a 1.2 m (48 in.)

level and a tape measure. Crack widths were measured using a crack comparator card,

and photos were taken to document the damage incurred from each blast event.

(a) UMR Mine test site (b) Blast test setup

Figure 13. Test setup of Panel 1A

4.1.1 Panel 1A (Bi-layered system, ρ = 0.2 percent)

On Monday, December 11, 2006, Panel 1A was tested with four blast events.

Panel 1A was a layered construction consisting of a 90 mm (3.5 in.) thick reinforced RC

base with a 50 mm (2 in.) layer of BMM covering the compression face. The concrete

base was reinforced with three No. 3 bars in each direction, providing a reinforcement

ratio of 0.2 percent. The blast mitigation layer was reinforced with three 6.5 mm (0.25
111

in.) diameter smooth bars in one direction only. The two layers were tied together with

6.5 mm (0.25 in.) diameter stirrups. The nominal dimensions of the panel were 1180 x

1180 x 140 mm (46.5 x 46.5 x 5.5 in.). Table 9 displays the charge weights and standoff

distances for the four blast events applied to Panel 1A and describes the damage incurred

from each event. Acceleration data was recorded for the first two events. A

representative curve is shown in Figure 15, and the approximate peak accelerations are

shown in Table 9. Figure 16 shows a millisecond of time in which the impulse occurred.

Test panel

(a) Accelerometers on base of panel (b) Accelerometer locations

Figure 14. Accelerometer location

Figure 17 displays the flexural cracks caused by the blast pressure. The first

event, Event 1, produced no visible damage or residual deflection to Panel 1A (see Figure

17-a). Event 2 created a hairline crack in the concrete base that ran the length of the

panel, as shown in Figure 17-b. The flexural crack was located in the midspan of the
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panel, rising 13 mm (0.5 in.) from the bottom face. The crack width at the tension face

was 0.33 mm (0.013 in).

Table 9. Results for Panel 1A

Charge Peak
Event weight, W Standoff, R Residual midspan Max crack acceleration
No. (grams) (mm) deflection (mm) width (mm) (m/s2)
1 454 915 none no cracks 750
2 680 610 4 0.33 750
3 907 305 13 1.5 N.I.
4 1360 305 32 6.4 N.I.
Note: N.I. – Not instrumented
Unit conversion: 1 gram = 0.00221 lb; 1 mm = 0.0394 in.; 1 m/s2 = 3.28 ft/s2

800

600 Impulse

400

200
Acceleration (m/s2)

0
0 0.2 0.4 0.6 0.8 1
-200
Discharge in cables
-400

-600

-800

-1000
Time (sec)

Unit conversion: 1 m = 3.281 ft

Figure 15. Representative acceleration curve


113

Event 3 produced craters on the top face of the panel and burn spots due to the

fire ball from the explosion. The crack width increased to 1.5 mm (0.059 in.) at the

bottom face of the concrete, narrowing to 0.6 mm (0.024 in.) at a location 51 mm (2 in.)

from the bottom face. A residual deflection of 13 mm (0.5 in.) was measured at the

midspan of the panel. Since the panel failed in a flexural manner, the deflections

measured along the midspan were approximately the same at the center and ends of the

panel (see Figure 17-c).

800

600

400

200
Acceleration (m/s2)

0
72.5 72.7 72.9 73.1 73.3 73.5
-200

-400

-600

-800

-1000
Time (ms)

Unit conversion: 1 m = 3.281 ft

Figure 16. Acceleration impulse

Event 4 increased the amount of craters on the surface, but no cracks were visible

on the surface of the blast mitigation layer. The midspan crack in the concrete base
114

increased to 6.4 mm (0.25 in.) at the bottom face and spread through the thickness of the

base to the adjoining top layer of BMM. The residual mid-span deflection was measured

at 32 mm (1.25 in.). Also, the pressure from the blast moved the panel approximately 51

mm (2 in.) from its original location on the steel beams.

(a) Prior to Event 1 (b) Result of Event 2

(c) Expanded crack in Event 3 (d) Result of Event 4

Figure 17. Panel 1A (bi-layered system, ρ = 0.2 percent)

A reinforced concrete panel of similar dimensions was tested by Lu et al. (2005).

The panel had nominal dimensions of 1200 x 1200 x 90 mm (45 x 45 x 3.5 in) and a

reinforcement ratio of 0.2 percent. The panel was simply supported on steel w-sections
115

with a 125 mm (5 in.) bearing. Lu’s panel sustained no damage under the first event of

0.45 kg (1.0 lb) with a standoff of 915 mm (36 in.). The second event was generated by a

charge weight of 0.9 kg (2.0 lb) at a standoff distance of 305 mm (12 in.), which was

equivalent to the third event applied to Panel 1A. Under this blast load, Lu’s panel

sustained a major flexural crack at midspan. The maximum crack width was reported to

be 3 mm (0.12 in.), and the residual displacement at the center of the slab was measured

at 21 mm (0.83 in.). In comparison, the crack width of Panel 1A after the third event was

measured at 1.5 mm (0.06 in.), with a residual deflection of 13 mm (0.5 in.). In this

regard, the addition of the 50 mm (2 in.) layer of BMM to the top surface of the panel

decreased the crack widths and residual deflections by half.

In the same series of tests conducted by Lu, another similar RC panel retrofitted

with a CFRP grid on the tension face was tested using a charge weight of 1.36 kg (3 lb)

and a standoff of 305 mm (12 in.). The slab was severely damaged in the event, and no

residual deformation could be measured. Lu stated that slabs retrofitted with CFRP

laminates on only the tension face were not suitable in a blast resistant application. For

comparison purposes, Panel 1A was tested under the same load and standoff distance.

Although the concrete base cracked completely through its thickness, the system proved

to be much more ductile than the equivalent panel reinforced with CFRP. The blast load

applied to the panel reinforced with CFRP resulted in a brittle failure. Pieces of the panel

were scattered everywhere. Panel 1A failed, but it held together and created very little

debris.
116

4.1.2 Panel 2A (FA-C-WF)

Panel 2A was tested on Tuesday, December 12, 2006. The mix design used to

fabricate the panel is shown in Table 8. The dimensions of the panels are 1180 x 1180 x

140 mm (46.5 x 46.5 x 3.5 in.). Panel 2A was subjected to four events in a similar

fashion to Panel 1A. The charge weights and standoff distances are shown in Table 10.

Table 10. Results for Panel 2A

Charge Peak
Event weight, W Standoff, R Residual midspan Max crack acceleration
No. (grams) (mm) deflection (mm) width (mm) (m/s2)
1 225 915 none no cracks 490
2 454 915 none no cracks 492
3 680 610 13 1.5 N.I.
4 907 305 25.4 6.5 N.I.
Note: N.I. – Not instrumented
Unit conversion: 1 gram = 0.00221 lb; 1 mm = 0.0394 in.; 1 m/s2 = 3.28 ft/s2

For Panel 2A, no damage or residual deflection was created from the first two

events, although burn marks from the explosion were found on the top surface of the

panel, located directly below were the explosive was hanging. The third event created a

centerline crack in the same fashion as Panel 1A. The crack width was measured to be 1.5

mm (0.06 in.) at the bottom tension face and 0.2 mm at the top of the panel. The final

event, Event 4, resulted in a compressive failure, as well as an increase in the crack width

on the tension face. The entire panel failed in a flexural manner, and the BMM was not

able to resist the compressive stresses at the center of the panel. The crack width at the

bottom face was measured to be approximately 6.35 mm (0.25 in.). The residual

deflection at the center midspan was approximately 25.4 mm (1.0 in.), and the end
117

midspan deflection was 22 mm (0.875 in.). Figure 18 illustrates the damage resulting

from each event on Panel 2A. Figure 18-a is prior to the first event, and the panel had no

damage from the blast. Figure 18-b shows the flexural crack that developed along the

midspan after the third event. Figures 18-c and 18-d display the expanded crack created

by the last event.

(a) Event 1 – no damage (b) Event 3 – flexural crack at midspan

(c) Event 4 – crack along panel base (d) Event 4 - flexural failure

Figure 18. Panel 2A (FA-C-WF)


118

4.1.3 Panel 3A (wood fiber concrete)

Three blast events were applied to Panel 3A. The 225 gram (0.5 lb) charge at a

915 mm (36 in.) standoff was eliminated from the test matrix based on the fact that the

event did not create any damage to Panel 2A. The three events are shown in Table 11,

along with a summary of the residual midspan deflections and crack widths. The peak

acceleration at the center of the panel was obtained for the first event.

Table 11. Results for Panel 3A

Charge Peak
Event weight, W Standoff, R Residual midspan Max crack acceleration
No. (grams) (mm) deflection (mm) width (mm) (m/s2)
1 454 915 none no cracks 941
2 680 610 22.3 9.5 N.I.
3 907 305 102 51 N.I.
Note: N.I. – Not instrumented
Unit conversion: 1 gram = 0.00221 lb; 1 mm = 0.0394 in.; 1 m/s2 = 3.28 ft/s2

The first event applied to Panel 3A caused no visible damage or deflection. Event

2 created a 9.5 mm (0.375 in.) crack along the bottom face of the panel 254 mm (10 in.)

from the end, instead of the usual crack location at midspan. The unusual crack location

could possibly be caused by a flaw in the panel. Panel 3A was dropped from the truck

bed while transferring it at the mine. The residual deflection measured along this crack

was 22.3 mm (0.875 in.) at the center and 19 mm (0.75 in.) at the end.

Event 3 created a 51 mm (2 in.) crack at the tension face and a residual deflection

of 101.6 mm (4 in.). The rebar prevented the panel from breaking in half. No surface

craters were observed on Panel 3A. Figure 19 shows damages due to the various charges.
119

Figure 19-a shows the test setup prior to the first event. The other figures illustrate the

odd location of the flexural failure.

The maximum theoretical incident and reflected pressures calculated using the

BEC were 1,077 and 6,126 kPa (156 and 888 psi) at the center of the panel for the 915

mm (36 in.) standoff distance. The panel was not damaged under those pressures. The

scaled distances for Events 2 and 3 are out of range for the BEC, so the pressures are

inaccurate. However, the model estimated the incident and reflected pressures to be

3,120 and 23,183 kPa (452 and 3,362 psi), respectively, for Event 2.

(a) Prior to Event 1 (b) Event 3

(c) Results of Event 3 (d) Crack formation along rebar

Figure 19. Panel 3A (wood fiber concrete)


120

4.1.4 Panel 4A (reinforced concrete; ρ = 0.5 percent)

Panel 4A was subjected to the three events listed in Table 12. The first event

created no damage. The second event produced a 0.2 mm hairline crack through the

midspan of the panel on the tension face. Also, a small amount of cratering was found on

the top face of the panel. The residual deflection was approximately 3.2 mm (0.125 in.)

at midspan. The third event failed the panel, punching a 559 mm (22 in.) diameter hole

through the 90 mm (3.5 in.) thick panel. Radial cracks developed around the

circumference of the hole, and cracks developed in an x-pattern leading to the four

corners of the panel. These cracks were due to reflections from the shock wave.

Compressive stress waves created from the shock wave radiate outward from the

center of the panel. Once the waves reach the edge of the panel, some amount of the

stress wave is reflected back toward the center of the panel due to the impedance

mismatch between the density of the panel and air. The reflected stress waves travel back

toward the center in tension. The tensile stress waves from the adjoining edges meet

along the lines, which creates the x-pattern of cracking.

Table 12. Results for Panel 4A

Charge Peak
Event weight, W Standoff, R Residual midspan Max crack acceleration
No. (grams) (mm) deflection (mm) width (mm) (m/s2)
1 454 915 none no cracks 400
2 1134 305 3.2 0.2 N.I.
3 1360 152 - - N.I.
Note: N.I. – Not instrumented
Unit conversion: 1 gram = 0.00221 lb; 1 mm = 0.0394 in.; 1 m/s2 = 3.28 ft/s2
121

Figure 20 shows the damages from each event. Figure 20-a illustrates the

standoff distance for Event 2, which created minor residual deflection in the panel.

Figure 20-b shows the results of Event 3. The major damage resulted from a 226 gram

(0.5 lb) increase in the charge weight and a 152 mm (6 in.) decrease in the standoff

distance. Minor changes in the standoff distance and charge weight drastically increased

the level of damage.

(a) Prior to Event 2 (b) Event 3 – punching failure

Figure 20. Panel 4A (reinforced concrete, ρ = 0.5%)

4.1.5 Panel 5A (bi-layered system, ρ = 0.5 percent)

Panel 5A was a two-layered system similar to Panel 1A with a few minor

differences. The base was RC with a 0.5 percent reinforcement ratio, whereas the

concrete base of Panel 1A only had a 0.2 percent reinforcement ratio. Schematics of both

reinforcement layouts are shown in Figures B5 and B6 of Appendix B. The amount of

stirrups used to tie the two layers was also increased, but tests revealed that the increased

amount of ties was not a factor. Four events applied to Panel 5A are shown in Table 13.
122

Table 13. Results for Panel 5A

Charge Peak
Event weight, W Standoff, R Residual midspan Max crack acceleration
No. (grams) (mm) deflection (mm) width (mm) (m/s2)
1 454 915 none no cracks 490
2 1134 305 none no cracks N.I.
3 1360 305 6 0.33 N.I.
4 1360 Contact - - N.I.
Note: N.I. – Not instrumented
Unit conversion: 1 gram = 0.00221 lb; 1 mm = 0.0394 in.; 1 m/s2 = 3.28 ft/s2

The first blast load on Panel 5A created no damage or residual deflection.

Acceleration data was obtained for two out of four channels, and the peak acceleration

values are shown in Table 13. The second event caused some small craters on the surface

due to the fire ball from the explosion, but no cracks developed. Event 3 increased the

amount of craters on the surface and produced a 0.2 mm crack along the bottom face of

the panel. The crack width increased to approximately 0.33 mm at the panel’s center.

Since the first three events generated minimal damage, a 1.36 kg (3 lb) surface blast was

applied to Panel 5A for the fourth event. The surface blast punched a 610 mm (24 in.)

hole in the center and obliterated the back half of the panel, throwing debris away from

the test setup. The contact charge increased the damage to the structure exponentially.

Figure 21 shows the results from the four events on Panel 5A. Figure 21-a shows

the condition of Panel 5A after Event 1. Figure 21-b illustrates the 1,360 gram (3 lb)

charge centered above the test panel at a 305 mm (12 in.) standoff distance. Figures 21-c

and 21-d show the test panel before and after Event 4, respectively.
123

4.2 Phase 2 blast testing

Phase 2 of the blast mitigation study was conducted on February 19 and 21, 2007.

Five panel systems were tested by using a total of 16 blast events with various charge

weights and standoff distances. Test panels for both test phases were fabricated using

identical mix designs and mixing processes. However, the panels of the second phase

were coated with a 3.2 mm (0.125 in.) layer of polyurea.

(a) Event 1 (b) Prior to Event 3

(c) Event 4 - contact (d) Damage from contact

Figure 21. Panel 5A (bi-layered system, ρ = 0.5 percent)


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4.2.1 Panel 1B (bi-layered system with polyurea, ρ = 0.2 percent)

Panel 1B was subjected to the blast events shown in Table 14. Accelerations

were recorded at three locations on the base of the panel for the first two events. The first

event created a 0.1 mm (.005 in.) hairline crack at the edges of the midpan. No

measurable residual deflection occurred from the event. The blast produced small burn

spots on the polyurea covering the top surface of Panel 1B, but there were no apparent

areas of delamination. The peak acceleration recorded for the first event was 965 m/s2

(3,165 ft/ s2).

Table 14. Results for Panel 1B

Charge Peak
Event weight, W Standoff, R Residual midspan Max crack acceleration
No. (grams) (mm) deflection (mm) width (mm) (m/s2)
1 680 610 none 0.1 965
2 907 305 6.4 1.5 983
3 1360 305 22 13 N.I.
4 1360 152 - - N.I.
Note: N.I. – Not instrumented
Unit conversion: 1 gram = 0.00221 lb; 1 mm = 0.0394 in.; 1 m/s2 = 3.28 ft/s2

Event 2 created three cracks along the front side of Panel 1B and two cracks on

the opposite side of the panel. The front side with three cracks had a 1.5 mm (0.06 in.)

wide center crack running along the centerline of the panel. The other two cracks were

located approximately 102 mm (4 in.) to each side of the center crack, each measuring

0.2 mm (0.007 in.) in width. The two cracks on the opposite side were 0.8 mm (0.03 in.)

thick, separated by a distance of 127 mm (5 in.). The panel sustained minor amounts of

surface damage with areas of delamination approximately 50 mm (2 in.) in diameter. The


125

residual deflection was roughly 6.4 mm (0.25 in.) at the center of the panel. Figure 22

shows the damages from the first two events. Figure 22-a illustrates no damage after

Event 1, while Figure 22-b shows flexural cracks at the midspan of the test panel.

The third event expanded the cracks on the back side of the panel to 6.4 mm (0.25

in.) in width and increased the width of the center crack on the front side of the panel to

13 mm (0.5 in). The other two cracks on the front were approximately 0.8 mm (0.03 in.)

wide. The resulting residual deflection was measured to be 22 mm (0.875 in.) at the

panel’s center.

(a) Event 1 (b) Event 2 – midspan cracks

(a) Prior to Event 3 (b) Event 3 – midspan cracks

Figure 22. Panel 1B (bi-layered system with polyurea)


126

For the last event, Event 4, the charge weight remained at 1,360 grams (3 lb), but

the standoff distance was decreased to 152 mm (6 in.). The blast load punched a hole

through the polyurea covering the top surface of the panel and created a large crater in the

FA-WF BMM. The polyurea coating the tension face of the panel contained the concrete

fragments, preventing them from falling to the mine floor. The polyurea would serve the

same purpose when used in a barrier wall application, thereby preventing the fragments

from injuring occupants inside a building. Figure 23 documents the damage incurred

after the fourth event.

(a) Event 4 – front side (b) Event 4 – back side

(c) Event 4 – polyurea removed (d) Radial cracks and punching failure

Figure 23. Panel 1B after Event 4


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4.2.2 Panel 2B (FA-C-WF and polyurea, ρ = 0.2 percent)

Panel 2B was tested with two blast events. The charge weights and standoff

distances used are shown in Table 15. Accelerometers were used to capture the

accelerations for the first event, but none of the channels provided adequate results.

No cracks were visible after the first event due to the layer of polyurea covering

all surfaces of the panel. However, the residual deflection was approximately 19 mm

(0.75 in.) at midspan, and several small areas of delamination were discovered after the

event. Later it was determined that the delaminated pockets were caused by the failure of

the BMM bond rather than the bond between the polyurea and the BMM. The residual

deflection of 19 mm (0.75 in.) after Event 1 was greater than the residual deflection

created by an equivalent event applied to Panel 2A. The mix design used to fabricate

Panel 2B contained 14 percent wood fibers by weight, while Panel 2A only contained 10

percent wood fibers by weight. The increased amount of wood fibers in Panel 2B

reduced the strength and stiffness of the panel, resulting in larger crack widths and

deflections.

Table 15. Results for Panel 2B

Charge Peak
Event weight, W Standoff, R Residual midspan Max crack acceleration
No. (grams) (mm) deflection (mm) width (mm) (m/s2)
1 680 610 19 not visible -
2 907 305 89 - N.I.
Note: N.I. – Not instrumented
Unit conversion: 1 gram = 0.00221 lb; 1 mm = 0.0394 in.; 1 m/s2 = 3.28 ft/s2
128

The second event resulted in an 89 mm (3.5 in.) deflection at the center of the

panel and a 45 mm (1.75 in.) at the edge of the panel at midspan. Large areas of

delamination were found after the blast, which pulverized the FA-WF material. The

panel was basically obliterated after the second event. Therefore, panels constructed

from this material should be used as a sacrificial barrier and not as a structural element.

Figure 24 shows the damage resulting from the two events. Figure 24-b illustrates the

failure in the FA-C-WF bond, and Figure 24-c shows the residual sag in the panel after

Event 2.

(a) Event 1 (b) Event 2 – material bond failure

(c) Event 2 – delamination and residual deflection

Figure 24. Panel 2B (FA-C-WF coated with polyurea)


129

4.2.3 Panel 3B (WF concrete & polyurea, ρ = 0.2 percent)

Panel 3B was subjected to three blast events, which are shown in Table 16. The

panel was fabricated with the same mix design and reinforcement layout as Panel 3A;

however, Panel 3B was coated with a 3.2 mm (0.125 in.) layer of polyurea on the top and

bottom surfaces.

Event 1 produced no visible damage to the panel, and no residual deflections

could be measured. The peak acceleration was recorded at 945 m/s2 (3,100 ft/s2). Event

2 caused small patches of delamination on the surface of the panel, along with a burn spot

resulting from the fire ball. No cracks could be measured on the panel due to the

polyurea coat; however, the residual deflection at the center of the panel was measured at

38 mm (1.5 in.). The peak acceleration increased to 955 m/s2 (3,132 ft/s2). The

equivalent event applied to Panel 3A resulted in a 102 mm (4 in.) deflection. However,

Panel 3A was already damaged from two prior events and from unloading it from the

truck bed.

Table 16. Results for Panel 3B

Charge Peak
Event weight, W Standoff, R Residual midspan Max crack acceleration
No. (grams) (mm) deflection (mm) width (mm) (m/s2)
1 680 610 none no cracks 945
2 907 305 38 not visible 955
3 1360 152 - - N.I.
Note: N.I. – Not instrumented
Unit conversion: 1 gram = 0.00221 lb; 1 mm = 0.0394 in.; 1 m/s2 = 3.28 ft/s2

Event 3 significantly increased the amount of delamination and punched a hole

completely through the panel. The bottom layer of polyurea ruptured and was unable to
130

contain the fragments from the panel. The pressure from the blast was great enough to

pulverize the concrete. Figure 25 displays the stages of damage after each consecutive

event. Minimal damages resulted from Event 1, as shown in Figure 25-a. The figure also

displays the accelerometer cables, which lead to four locations on the base of the panel.

Figure 25-b shows Panel 3B prior to Event 3. A noticeable residual deflection can be

clearly seen in the panel. Figures 25-c and 25-d show the punching failure resulting from

Event 3.

(a) Event 1 (b) Event 2

(c) Event 3 – polyurea fails (d) Event 3 – punching failure

Figure 25. Panel 3B (WF Concrete and polyurea)


131

4.2.4 Panel 4B (reinforced concrete with polyurea, ρ = 0.5 percent)

Panel 4B was a plain RC panel with a 0.5 percent reinforcement ratio in each

direction. The panel was coated with polyurea on the top and bottom surfaces. Three

events were used to test the blast resistance of the panel. The charge weights and

standoff distances for the events are shown in Table 17. Accelerometers were used to

capture the response of the panel to the first two events. Figure 26 displays the damages

the panel incurred from the first two events. Figure 26-a shows minor deflections from

Event 1, and Figure 26-b illustrates multiple hairline cracks resulting from Event 2.

Table 17. Results for Panel 4B

Charge Peak
Event weight, W Standoff, R Residual midspan Max crack acceleration
No. (grams) (mm) deflection (mm) width (mm) (m/s2)
1 680 610 none 0.15 492
2 1134 305 13 0.4 -
3 1360 152 - 1.5 N.I.
Note: N.I. – Not instrumented
Unit conversion: 1 gram = 0.00221 lb; 1 mm = 0.0394 in.; 1 m/s2 = 3.28 ft/s2

A 0.15 mm (0.006 in.) crack was discovered at the midspan along one side of the

panel after the first event. Furthermore, the blast created a black burn spot on the top

surface of the polyurea directly below where the charge was hanging. The second event

spawned approximately six hairline cracks along the side of the panel around the midspan

ranging from 0.3 to 0.4 mm (0.012 to 0.016 in.) in width. Areas of delamination occurred

at the supports, and the residual deflection at midspan was roughly 13 mm (0.5 in.).
132

(a) Event 1- no damage (b) Event 2 – hairline cracks develop

Figure 26. Panel 4B (reinforced concrete with polyurea, ρ = 0.5 percent)

Event 3 increased the widths of the midspan cracks to approximately 1.5 mm

(0.06 in.) and punched a hole in the center of the panel measuring 483 mm (19 in.) in

diameter. The impulse from the blast bent the longitudinal reinforcement and ground the

concrete into small fragments within a 305 mm (12 in.) radius from the center of the

panel. Although the damage to the panel was extensive, the polyurea coating on the

bottom face of the panel contained all the fragments of concrete, creating a 102 mm (4

in.) deep basin underneath the panel. The top layer of polyurea detached almost

completely from the surface of the test panel and was easily remove by hand after the

blast event. After removing the polymer, radial cracks around the circumference of the

hole were visible. Cracks also ran to the four corners of the panel. Figure 27 displays the

punching failure on Panel 4B due to the fourth blast event. Figure 27-a shows the

damage with the polyurea still on the surface, and Figure 27-b shows the punching failure

with the polyurea removed from the panel.


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(a) Event 3 – failure in polyurea (b) Event 3 – punching failure

Figure 27. Panel 4B following Event 3

4.2.5 Panel 5B

Panel 5B actually consisted of a two panel system with a 19 mm (0.75 in.) air gap

separating the two panels. The top panel was fabricated using a FA-C-WF, and the

bottom panel was fabricated using a standard normal weight concrete mix design. Mix

designs for both panels are shown in Table 7. Both test panels in the system had nominal

dimensions of 1180 x 1180 x 90 mm (46.5 x 46.5 x 3.5 in.). The FA-C-WF panel was

coated with a 3.2 mm (0.125 in.) layer of polyurea on the tension face, and the concrete

panel was completely covered with the polyurea on all sides. The panels had

reinforcement ratios of 0.2 percent in each direction. During the blast test, the concrete

panel had a 127 mm (5 in.) bearing on the steel w-sections. Two 19 mm (0.75 in.) square

wood sections supported the FA-C-WF panel and provided an air gap between the two

panels as shown in Figure 28.

The charge weights and standoff distances for the four blast events applied to the

system are shown in Table 18. The first event created a hairline crack roughly 0.15 mm

(.006 in.) thick at the midspan of the blast mitigation panel. No residual deflections could
134

be measured, but a small amount of localized damage was noticed on the surface of the

top panel. The concrete panel sustained no damage.

Table 18. Results for Panel 5B

Charge Peak
Event weight, W Standoff, R Residual midspan Max crack acceleration
No. (grams) (mm) deflection (mm) width (mm) (m/s2)
1 680 610 none 0.15 -
2 907 305 10 0.8 896
3 1360 305 19 1.5 N.I.
4 1360 152 45 N.I.
Note: N.I. – Not instrumented
Unit conversion: 1 gram = 0.00221 lb; 1 mm = 0.0394 in.; 1 m/s2 = 3.28 ft/s2

The second event created four flexural cracks along the free span of the top panel

on the front surface and one crack on the rear surface. The cracks on the front surface

were spaced approximately 102 to 127 mm (4 to 5 in.) apart and ranged from 0.2 to 0.8

mm (0.008 to 0.03 in.) in thickness. The crack patterns are shown in Figure 28-b. The

residual deflection at the center of the panel was measured to be roughly 10 mm (0.375

in.).

Event 3 caused major amounts of surface damage and residual deflections.

Tension cracks also developed on the surface of the top panel due to the rebound effect

caused by the blast. The residual deflection of the top panel was measured at 19 mm

(0.375 in.). Although a small amount of residual deflection existed in the concrete panel,

any flexural cracks that may have existed at the panel’s midspan were concealed by the

polyurea coating.
135

20 mm air gap Wooden strip


hairline
cracks

(a) Test setup for Panel 5B (b) Panel 5B after Event 2

Figure 28. Panel 5B (panels separated by air gap)

Event 4 resulted in a 45 mm (1.75 in.) midspan deflection of the top panel, with

flexural cracks as large as 6.4 mm (0.25 in.) as well as shear cracks near the supports.

The concrete panel suffered major flexural damage as well. A flexural crack developed

at the midspan of the panel, which tore the polyurea coating along the panel’s length.

The crack width was approximately 13 mm (0.5 in.). The residual deflection measured at

the center of the panel was roughly 38 mm (1.5 in.). Radial cracks from punching shear

also developed on the concrete panel, which could be seen once the polyurea coating was

removed. Figure 29 shows the condition of the panel system after each consecutive

event.

4.3 Comparison of test results

A general comparison can be made between all the test panels from Phase 1 and

Phase 2 based on a given blast event. An event with a charge weight of 680 grams (1.5

lb) and a 610 mm (24 in.) standoff distance was common among almost all the panels,

and therefore, is used for comparison.


136

(a) Event 3 – flexural cracking (b) Event 4 – FA-C-WF panel

(c) Event 4 – flexural crack on RC panel (d) Event 4 – radial cracking on RC panel

Figure 29. Crack patterns for panel system 5B

Table 19 presents the residual deflections and crack widths for each test panel

following the event. BMM denotes the blast mitigation material. Results revealed that

the panels constructed of the FA-C-WF material failed in a flexural manner at the given

charge weight and standoff distance, producing residual deflections of 13 to 22 mm (0.5

to 0.875 in.) at midspan. The RC test panels, Panel 4A and 4B, had only hairline cracks

after the 680 gram (1.5 lb) event, and no residual deflections could realistically be

measured. The same result occurred for the two-layered systems. The maximum crack
137

width developed in the two-layered system from the 680 gram (1.5 lb) shot was 0.33 mm

(0.013 in.), and the maximum residual deflection was only 4 mm (0.125 in.).

Table 19. Summary of results for 680 gram charge at 610 mm (Z = 0.69 m/kg1/3)

Max Max crack Peak


Density
Panel No. f'c (Mpa) Ec (Mpa) deflection width acceleration
kg/m3
(mm) (mm) (m/s2)
1A (BMM) 1606.3 9.37 3103
4 0.33 750
1A (concrete) 2392.1 65.32 41369
1B (BMM) 1529.7 8.77 -
0 0.1 965
1B (concrete) 2366.5 68.98 -
2A 1487.2 7.34 1724 13 1.5 -
2B 1313.4 1.69 - 19 - -
3A 1729.8 12.83 7584 22 9.5 -
3B 1814.4 14.13 - 0 0 945
4B - >27.58 - 0 0.15 492
5A (BMM) 1513.7 7.74 3792
0 0 -
5A (concrete) - >27.58 -
5B (BMM) 1367.2 10.53 5516 0 0.15 -
5B (concrete) 2351.4 48.72 37921 0 0 -
Unit conversion: 1 kg = 2.21 lb; 1 MPa = 145 psi; 1 mm = 0.0394 in.; 1 m/s = 3.28 ft/s2
2

Based on the results of the test, the additional benefit provided by the FA-C-WF

layer is RC concrete panels performed as well as the bi-layered system at that scaled

distance. The higher reinforcement ratios of panels 4A, 4B, and 5A resulted in less

residual deflection than the bi-layered system at the same charge weight and standoff.

The bi-layered systems did perform relatively better than the RC when subjected

to the 1,360 gram (3 lb) charge weight at a 152 mm (6 in.) standoff distance. A punching

failure occurred in the concrete panels reinforced with a 0.5 percent reinforcement ratio.

The panel was unable to displace due to its rigidity and stiffness, so the shock wave was

able punch through it. In comparison, the lower reinforcement ratio of the bi-layered
138

system allowed the panel to bend, causing a flexural failure at the midspan. Therefore,

the x-pattern tensile cracks caused by the stress wave reflections did not occur due to the

fact that a flexural failure occurred first.

The FA-C-WF composite layer provided an added benefit by decreasing the

amount of fragmentation resulting from the shock wave. Figure 30 shows a comparison

between a RC panel, Panel 4A, and a FA-C-WF panel, Panel 5B, subjected to a 1,360

gram (3 lb) charge of C-4 at a 152 mm (6 in.) standoff distance. Notice the FA-C-WF

material failed in flexure along the midspan of the panel but not due to a punching

failure.

Although the polyurea coating did not increase the stiffness or capacity of the test

panels, it did prove useful in containing the debris from the spall. In most cases, the

polyurea applied to the tension face of the panel contained the fragments from the spall.

However, it was unclear if the polyurea coating on the compression face provided any

benefit, especially at close standoff distances. Figure 31 displays the benefits of the

polyurea applied to the tension face of the panels. Figure 31-a illustrates the tension face

of Panel 1B. Notice the panel failed through its midspan, and the polurea skin ruptured

toward the edge of the panel at midspan. However, the bulk of the fragments in the

center of the panel were contained. Figure 31-b shows the tension face of Panel 4B.

Notice the polyurea did not split in any location on the surface.
139

(a) Punching failure (b) Prevented punching

Figure 30. Failure modes of the test panels

(a) Panel 1B held fragments (b) Panel 4B held fragments

Figure 31. Benefits of polyurea

The polyurea delaminated along the unsupported edge of Panel 4B, as shown in

Figure 32-a. Therefore, in a barrier application, it may be necessary to anchor the

polyurea skin to the wall in various locations to prevent large areas of delamination. As

shown in Figure 32-b, the polyurea applied to the tension face of Panel 3B split open

during the third event. This case was the only one where the polyurea was unable to

contain the debris.


140

(a) Polyurea delamination on Panel 4B (b) Panel 3B – polyurea tore open

Figure 32. Polyurea delamination and fracture

5. CONCLUSIONS

Ten test panels with nominal dimensions of 1180 x 1180 x 90 mm (46.5 x 46.5 x

3.5 in) were tested under various blast loads. RDX-based C-4 was used as the primary

explosive. The panels were simply supported with a 127 mm (5 in.) bearing, proving a

free span of approximately 915 mm (36 in.). Each panel was tested with blast events

until the panel completely failed. The severity of each consecutive event was increased

by increasing the charge weight of the explosive and decreasing the distance between the

explosive and the test panel. Crack widths, residual deflections, and other damages were

documented after each event. Several conclusions can be drawn from this study.

1. The high-volume FA-C-WF material investigated in this study does not, in itself,

provide an improved resistance to blast loading when compared to reinforced

concrete. An improvement in blast resistance was noticed in the bi-layered

systems with the FA-C-WF lower density material layered on top of the

reinforced concrete panel at low scaled distances.


141

2. The FA-C-WF test panels failed in flexure with the increasing pressures created

from the consecutive blast events. Large flexural cracks developed at the mispan

after the second event. Therefore, the 1,360 gram (3 lb) charge at the shortest

standoff distance did not create a punching failure in the FA-C-WF panels. This

result is most likely because of the low strength and stiffness of the material.

3. The RC panels failed due to punching shear in the center of the panel as a result

of the 1,360 gram (3 lb) charge at the 152 mm (6 in.) standoff distance. The

shock wave from the blast created a 508 mm (20 in.) hole in the center of the

panel. An x-pattern cracking also formed as a result of reflections from the

compressive stress wave at the panel-air interface. The stress waves reflected

back toward the center of the panel as tensile waves. The tensile waves from the

adjoining sides of the panel meet long the diagonals of the panel. In most cases,

the tensile stress was large enough to cause a failure along those diagonals.

4. The FA-C-WF material on the two-layered panels did not fragment to the same

extent as the reinforced concrete base. Instead, the material permanently

deformed in a localized area where the shock wave impacted the panel. Although

this deformation process undoubtedly absorbed some amount of energy from the

shock, the tension face of the panel still experienced a large amount of spalling.

Spalling occured from compression stress wave reflection in tension off the

bottom of the panel.

5. In the second phase of blast testing, the polyurea coating did not provide

significant benefit to the flexural strength of the panels. However, the material

was useful in containing spalling and fragments from the panel. In a barrier
142

situation, containing the flying debris is critical for the protection of occupants

inside a structure or behind a barrier system.

6. The compressive strength and stiffness of the FA-C-WF material was much

higher at test age than originally planned, as a result of delayed testing. Future

work should investigate the behavior of a FA-C-WF material with a lower

strength and stiffness.

7. The 19 mm (0.75 in.) air gap used in the Panel 5B system was not large enough to

prevent a flexural failure of the concrete. The top FA-C-WF panel flexed enough

from the blast to make contact with the concrete panel below it, likely

transmitting load to the concrete.

8. Based on the results from both phases of blast tests, the optimum blast barrier

system is similar to Panel 5A. The RC panel with a reinforcement ratio of 0.5

percent increases the bending capacity of the panel, and the sacrificial layer of

FA-WF material prevents a shear punching failure from the shock wave.

Furthermore, the polyurea coating on the tension face of the panel contains all the

fragments of concrete and debris. However, increasing the thickness of the

sacrificial layer would dissipate a larger amount of shock energy, and reduce the

damage incurred to the RC panel. Preventing damage to structural load-bearing

wall systems is crucial to allow time for inhabitants of a building to evacuate.

9. Results from the drop-weight impact test do not correlate well with the results

from the blast study. The FA-C-WF material had a much higher drop-weight

impact resistance than concrete. However, the concrete panels had less damage

and deflection than the FA-C-WF panels when loaded with equivalent blast loads.
143

The failure modes of the materials remained the same for both tests. For example,

the FA-C-WF material exhibited a ductile failure in the drop-weight test and the

blast test, while the concrete failed in a brittle manner in both tests.

10. Incorporating the polyurea coating in a barrier system will increase the cost of the

barrier. Currently, the FA-WF material costs roughly 10 dollars per cubic yard.

The addition of a 3.2 mm (0.125 in.) layer of polyurea to both faces of the barrier

would cost approximately 30 dollars per square yard, increasing the fabrication

cost of the barrier by 600 percent. Adding cement to create the FA-C-WF mix

would also increase the cost. Cement would account for roughly 42 dollars per

cubic yard of FA-C-WF material if the current mix design is used. However, the

FA-C-WF mix still remains cheaper than the PFRC mix design, which may be

produced for 65 dollars per cubic yard. The addition of polypropylene fibers

would increase the cost by approximately 5 dollars per cubic yard of concrete.

6. FUTURE RECOMMENDATIONS

Future blast studies incorporating the FA-C-WF material should investigate the

following issues.

1. A greater variation in the strength and stiffness of the FA-C-WF material should

be considered by changing the proportions of the materials in the mix design.

2. The FA-C-WF material proved to be most useful when joined with a concrete

panel. Variable thicknesses and densities of the FA-C-WF layer may be

investigated for comparison.


144

3. The air gap used in Panel 5B was 19 mm (0.75 in.). The air gap should be

increased in future testing to prevent the FA-C-WF mitigation layer from

impacting the structural concrete when undergoing flexural displacements.

4. More testing should be conducted on a RC panel of an equivalent thickness to the

bi-layered systems without an air gap tested in this study to provide an equal

comparison based on the panel thickness.

5. Future research should include the development of a lower density mixture of fly

ash and clay-based materials to better replicate the adobe-type material found in

Southwest Asia. A material with a lower strength and stiffness could be achieved

by using Class C fly ash blended with clay particles.

6. The adobe-type walls used in Southwest Asia were thick load-bearing walls. The

blast resistance of the FA-C-WF material may increase significantly if the

thickness is increased. Therefore, future tests should consider thick, full-scale

barrier walls.

7. The field blast tests discussed herein were all near-field events. Future tests need

to incorporate larger scaled distances to observe the behavior of the sacrificial

layer without the intense effects of the shock front.

7. ACKNOWLEDGMENTS

This research effort was funded by the Air Force Research Laboratory (AFRL).

8. REFERENCES

ACI Committee 232, “Use of Fly Ash in Concrete (ACI 232.2R-03),” American
Concrete Institute, Farmington Hills, Michigan, 2003, 41pp.
145

American Society for Testing and Materials (ASTM C 617-98). Standard Practice for
Capping Cylindrical Concrete Specimens, American Society for Testing and
Materials, West Conshohocken, PA, 1998.

American Society for Testing and Materials (ASTM C 192/C 192M-06). Standard
Practice for Making and Curing Concrete Test Specimens in the Laboratory,
American Society for Testing and Materials, West Conshohocken, PA, 2006.

American Society for Testing and Materials (ASTM C 150-05). Standard


Specification for Portland Cement, American Society for Testing and Materials,
West Conshohocken, PA, 2005

American Society for Testing and Materials (ASTM C 39/C 39M-05). Standard Test
Method for Compressive Strength of Cylindrical Concrete Specimens, American
Society for Testing and Materials, West Conshohocken, PA, 2005.

American Society for Testing and Materials (ASTM C 188-03). Standard Test
Method for Density of Hydraulic Cement, American Society for Testing and
Materials, West Conshohocken, PA, 2003.

American Society for Testing and Materials (ASTM C 127-04). Standard Test
Method for Density, Relative Density (Specific Gravity), and Absorption of
Coarse Aggregate, American Society for Testing and Materials, West
Conshohocken, PA, 2004.

American Society for Testing and Materials (ASTM C 128-07). Standard Test
Method for Density, Relative Density (Specific Gravity), and Absorption of Fine
Aggregate, American Society for Testing and Materials, West Conshohocken,
PA, 2007.
American Society for Testing and Materials (ASTM C 143/C 143M-05). Standard
Test Method for Slump of Hydraulic-Cement Concrete, American Society for
Testing and Materials, West Conshohocken, PA, 2005.

American Society for Testing and Materials (ASTM C 496/C 496 M-04). Standard
Test Method for Splitting Tensile Strength of Cylindrical Concrete Specimens,
American Society for Testing and Materials, West Conshohocken, PA, 2004.

American Society for Testing and Materials (ASTM C 469-02). Standard Test
Method for Static Modulus of Elasticity and Poisson’s Ratio of Concrete in
Compression, American Society for Testing and Materials, West Conshohocken,
PA, 2002.

Baker, W.E., Explosion Hazards and Evaluation, Elsevier Scientific Publishing


Company, New York, NY, 1983.
146

Chock, J.M.K., Kapania, R.K., “Review of Two Methods for Calculating Explosive
Air Blast,” The Shock and Vibration Digest, V. 33, No. 2, March 2001, pp. 91-
102

El-Domiaty, K., Myers, J.J., Belarbi, A., “Blast Resistance of Un-reinforced Masonry
Walls Retrofitted with Fiber Reinforced Polymers (CIES 02-24),” Center for
Infrastructure Engineering Studies, University of Missouri, Rolla, MO, 2002.

Falk, R. H., “Housing Products from Recycled Wood,” CIB TG 16, Sustainable
Construction, Tampa, FL, 1994

Joshi, N., Myers, J.J., “Investigation of an Alternative Wood Fiber-Fly Ash Material
for Infill Wall Systems (CIES 06-60),” Center for Infrastructure Engineering
Studies, University of Missouri, Rolla, MO, 2005.

Knox, K.J., Hammons, M.I, Lewis, T., Porter, J.R., “Polymer Materials for Structural
Retrofit,” Air Force Research Laboratory Air Expeditionary Forces Technology
Division Force Protection Branch, Tyndall AFB, FL.

Lu, B., “Application of Displacement-Based Design Method to Blast-Resistant


Reinforced Concrete Structures,” Department of Civil Engineering, University of
Missouri-Roll, Rolla, Missouri, 2005.

Robinson, C.S. Explosions Their Anatomy and Destructiveness, New York and
London: McGraw-Hill Book Company, Inc., 1944.

Rinehart, J.S., Stress Transients in Solids, Hyper Dynamics, Santa Fe, New Mexico,
1975.

“Structures to Resist the Effects of Accidental Explosions,” Departments of the


Army, the Navy and the Air Force, Department of the Army Technical Manual
TM 5-1300, Department of the Navy Publication NAVFAC P-397, Department of
the Air Force Manual AFM 88-22, November 1990.

Swisdak, M.M. Jr., Ward, J.M., DDESB Blast Effects Computer Version 5.0 User’s
Manual and Documentation, Department of Defense Explosives Safety Board,
Alexandria, VA, May, 2003.

Tinsley, M.E., and Myers, J.J., “Impact Resistance of Blast Mitigation Material Using
A Modified ACI Drop-Weight Impact Test,” under review to be submitted to the
ASCE Journal of Materials, 2007.
147

APPENDIX A.

DISTRIBUTIONS OF IMPACT RESULTS


148

4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22
7 0.3

6 0.25

5
0.2
Frequency

4
0.15
3
0.1
2

0.05
1

0 0
0 2 4 6 8 10 12 14 16 18 20 22
First crack resistance in blows

a) Distribution of 28-day first crack impact test results


10
12
14
16
18
20
22
24
26
28
30
32
34
36
38
40
42
44
46
48
50
52
54
56
58
60
0
2
4
6
8

8 0.16

7 0.14

6 0.12

5 0.1
Frequency

4 0.08

3 0.06

2 0.04

1 0.02

0 0
0 5 10 15 20 25 30 35 40 45 50
Ultimate resistance in blows

b) Distribution of 28-day ultimate resistance impact test results

Figure A1. Distribution of Group 1 impact test results


149

-1 0 1 2 3 4 5 6 7 8 9 10 11 12
10 0.45

9 0.4

8 0.35
7
0.3
6
Frequency

0.25
5
0.2
4
0.15
3
0.1
2
1 0.05

0 0
0 2 4 6 8 10 12
First crack resistance in blows

a) Distribution of 28-day first crack impact test results


10
11
12
13
14
15
16
17
18
19
20
-8
-7
-6
-5
-4
-3
-2
-1
0
1
2
3
4
5
6
7
8
9

10 0.4

9 0.35
8
0.3
7
0.25
6
Frequency

5 0.2

4 0.15
3
0.1
2
0.05
1
0 0
0 3 6 9 12 15
Ultimate resistance in blows

b) Distribution of 28-day ultimate resistance impact test results

Figure A2. Distribution of Group 2 impact test results


150

0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40
7 0.12

6 0.1

5
0.08
Frequency

4
0.06
3
0.04
2

0.02
1

0 0
0 5 10 15 20 25 30 35 40
First crack resistance in blows

a) Distribution of 28-day first crack impact test results

1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31
7 0.09

0.08
6
0.07
5
0.06
Frequency

4 0.05

3 0.04

0.03
2
0.02
1
0.01

0 0
0 5 10 15 20 25 30 35 40 45 50 55
Ultimate resistance in blows

b) Distribution of 28-day ultimate resistance impact test results

Figure A3. Distribution of Group 3 impact test results


151

0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20
8 0.3

7
0.25
6
0.2
5
Frequency

4 0.15

3
0.1
2
0.05
1

0 0
0 2 4 6 8 10 12 14 16
First crack resistance in blows

a) Distribution of 28-day first crack impact test results


10
11
12
13
14
15
16

9 0.3

8
0.25
7
6 0.2
Frequency

5
0.15
4
3 0.1

2
0.05
1
0 0
0 2 4 6 8 10 12 14 16 18 20 22 24 26
Ultimate resistance in blows

b) Distribution of 28-day ultimate resistance impact test results

Figure A4. Distribution of Group 4 impact test results


152

0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30
4 0.12

0.1
3
0.08
Frequency

2 0.06

0.04
1
0.02

0 0
0 3 6 9 12 15 18 21 24 27 30 33
First crack resistance in blows

a) Distribution of 28-day first crack impact test results

0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40
5 0.12

0.1
4

0.08
3
Frequency

0.06

2
0.04

1
0.02

0 0
0 3 6 9 12 15 18 21 24 27 30 33 36
Ultimate reistance in blows

b) Distribution of 28-day ultimate resistance impact test results

Figure A5. Distribution of Group 6 impact test results


153

10
12
14
16
18
20
22
24
26
28
30
32
34
36
38
40
42
44
46
48
50
52
54
56
58
-8
-6
-4
-2
0
2
4
6
8
5 0.07

0.06
4
0.05

3
Frequency

0.04

0.03
2

0.02
1
0.01

0 0
0 5 10 15 20 25 30 35 40 45 50
First crack resistance in blows

a) Distribution of 28-day first crack impact test results


26 5
2
0

.
10
12
14
16
18
20
22
24

28
30
32
34
36
38
40
42
44
46
48
50
52
54
56
58
60
-1
-1
-8
-6
-4
-2
0
2
4
6
8

3
Frequency

0
0 5 10 15 20 25 30 35 40 45 50
Ultimate resistance in blows

c) Distribution of 28-day ultimate resistance impact test results

Figure A6. Distribution of Group 7 impact test results


154

Standardized normal distribution


2

-1 First crack
Ultimate
resistance
-2

-3
0 5 10 15 20 25 30 35 40
Impact resistance in blows

a) Standardized normal distribution

100
2
R = 0.978 2
80 R = 0.9711
Cumulative percent

60

40
First crack
Ultimate
20
resistance

-20
0 5 10 15 20 25 30 35 40
Impact resistance in blows

b) Normal probability

Figure A7. Normal probability plots for Group 1 impact test results
155

Standardized normal distribution 2

0 First crack
Ultimate
-1 resistance

-2

-3
0 2 4 6 8 10 12
Impact resistance in blows

a) Standardized normal distribution

100

2
80 R = 0.9793
Cumulative percent

60
2
R = 0.9785
First crack
40
Ultimate
resistance
20

0
0 2 4 6 8 10 12
Impact resistance in blows

b) Normal probability

Figure A8. Normal probability plots for Group 2 impact test results
156

Standardized normal distribution 2

0 First crack
Ultimate
resistance
-1

-2

-3
0 10 20 30 40 50 60
Impact resistance in blows

a) Standardized normal distribution

100

80
2
R = 0.9623
Cumulative percent

60 2
R = 0.9718

40
First crack
Ultimate
20 resistance

0
0 10 20 30 40 50 60
Impact resistance in blows

b) Normal probability

Figure A9. Normal probability plots for Group 3 impact test results
157

3
Standardized normal distribution

0
First crack
-1 Ultimate
resistance
-2

-3
0 5 10 15 20 25
Impact resistance in blows

a) Standardized normal distribution

100

80 2
R = 0.9659
Cumulative percent

2
60 R = 0.9496

40 First crack
Ultimate
resistance
20

0
0 5 10 15 20 25
Impact resistance in blows

b) Normal probability

Figure A10. Normal probability plots for Group 4 impact test results
158

Standardized normal distribution 2

First crack
-1 Ultimate
resistance
-2

-3
0 5 10 15 20 25 30 35
Impact resistance in blows

a) Standardized normal distribution

100

80
Cumulative percent

2
60 R = 0.9737
2
R = 0.9749

40 First crack
Ultimate
resistance
20

0
0 5 10 15 20 25 30 35
Impact resistance in blows

b) Normal probability

Figure A11. Normal probability plots for Group 6 impact test results
159

Standardized normal distribution 2

0
First crack
-1 Ultimate
resistance
-2

-3
0 5 10 15 20 25 30 35 40 45
Impact resistance in blows

a) Standardized normal distribution

100

80

2
R = 0.9846
Cumulative percent

60

2
40 R = 0.9872

20
First crack
Ultimate
0 resistance

-20
0 5 10 15 20 25 30 35 40 45
Impact resistance in blows

b) Normal probability

Figure A12. Normal probability plots for Group 7 impact test results
160

APPENDIX B

ANALYTICAL PRESSURES
AND REINFORCEMENT LAYOUTS
161

Radial distance from


center (mm)

IP = incident pressure (kPa)


RP = reflected pressure (kPa)

Unit conversions: 1 kPa = 0.145 psi, 1 mm = 0.0394 in.

Figure B1. Incident and reflected pressures (454 gram at 915 mm)
162

IP = incident pressure (kPa)


RP = reflected pressure (kPa)

Unit conversions: 1 kPa = 0.145 psi, 1 mm = 0.0394 in.

Figure B2. Incident and reflected pressures (680 grams at 610 mm)
163

IP = incident pressure (kPa)


RP = reflected pressure (kPa)

Unit conversions: 1 kPa = 0.145 psi, 1 mm = 0.0394 in.

Figure B3. Incident and reflected pressures (907 grams at 305 mm)
164

IP = incident pressure (kPa)


RP = reflected pressure (kPa)

Unit conversions: 1 kPa = 0.145 psi, 1 mm = 0.0394 in.

Figure B4. Incident and reflected pressures (1360 grams at 305 mm)
165

Figure B5. Reinforcement layout with 0.5 percent reinforcement ratio


166

Figure B6. Reinforcement layout for 0.2 percent reinforcement ratio

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