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Thermo Scientific Dionex Ic Pure Ultra Pure Water System: Service Instructions
Thermo Scientific Dionex Ic Pure Ultra Pure Water System: Service Instructions
DIONEX IC Pure
Ultra pure water system
Service Instructions
50148298 Rev. B March 2016
© 2016 Thermo Fisher Scientific Inc. All rights reserved.
Trademarks
All other trademarks mentioned in the service instructions are the exclusive property of the respective
manufacturers.
This document is not part of any sales contract between Thermo Fisher Scientific Inc. and a purchaser.
This document shall in no way govern or modify any Terms and Conditions of Sale, which Terms and
Conditions of Sale shall govern all conflicting information between the two documents.
Release history:
Contents
Preface . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . iii
Contact Information Thermo Fisher international sales organisations . . . . . . . . iii
Fundamental requirements for service work. . . . . . . . . . . . . . . . . . . . . . . . . . . . .iv
Skills of service personnel. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .iv
Process procedures for personnel . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .iv
Applicability of the instructions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . v
Original document for translation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . v
Legal Notice . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . v
Warranty . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . v
Explanatory notes on the operating instructions . . . . . . . . . . . . . . . . . . . . . . . . .vi
Standards and directives. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . vii
Chapter 4 Controls . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
Description of control display . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
Flow chart system control . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18
Unlocking the system control . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19
Calibration menu. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
Calibration of the microcontroller . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
Setting the temperature sensor . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
Setting cell constant LF1 (Pure water measuring cell) . . . . . . . . . . . . . . . . . . . . 21
Setting cell constant LF2 (Feedwater measuring cell) . . . . . . . . . . . . . . . . . . . . . 21
Setting cell constant LF3 (TOC measuring cell) . . . . . . . . . . . . . . . . . . . . . . . . 22
Matching the TOC measurement . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 22
Error suppression. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23
Restore to Initial Calibration values . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23
Volume control . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24
Leaving calibration menu. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24
UV-menu . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24
Setting the limiting value for the UV operating hours counter. . . . . . . . . . . . . . 25
Setting the limiting value for the UV intensity measurement . . . . . . . . . . . . . . . 25
Filter cartridge operating hours counter . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25
Reset the operating hours counter and measuring in a new UV- lamp . . . . . . . . 26
Chapter 5 Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27
Set up for calibrating ultra pure water measuring cell LF1 . . . . . . . . . . . . . . . . . 28
Calibration of the ultra pure water measuring cell LF1 . . . . . . . . . . . . . . . . . . . 34
Set up for calibrating feedwater measuring cell LF2 . . . . . . . . . . . . . . . . . . . . . . 35
Calibration of feedwater measuring cell LF2 . . . . . . . . . . . . . . . . . . . . . . . . . . . 36
Chapter 8 Troubleshooting . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 71
Preface
Americas
Postal address USA:
Thermo Fisher Scientific
275 Aiken Road
Asheville, NC 28804
USA
Please note that service maintenance of the device must be carried out only by certified factory service
engineers. Prior to repairs, please read these service instructions carefully.
Legal Notice
We reserve the right to any specification, conditions and price changes. Not all
products are available in all countries. Contact your local partner for more details.
Warranty
Thermo Electron LED GmbH guarantees the operational reliability and safety and proper functioning
of the Thermo Scientific DIONEX IC Pure Water Purification System under the following conditions:
• The unit is operated in line with the information on installation and use given in the operating
instructions.
• The unit has not been modified or altered.
• Only original spare parts and accessories approved by Thermo Electron LED GmbH are used in
the unit.
• Inspections and maintenance are performed at the specified intervals.
• An installation check is performed after starting the unit for the first time and repeated after every
inspection or servicing.
• The warranty period begins on the day the unit is delivered to the customer.
• The warranty conditions specified above are subject to the general business terms and conditions
in force at the time of sale.
CSA - admission
Indicates a situation which, if not avoided, could result in damage to equipment or
property.
Indicates a hazardous situation which, if not avoided, could result in death or serious
injuries.
Indicates a hazardous situation which, if not avoided, will result in death or serious
injuries.
Is used for applicational hints and useful information.
Risk of electric shock. Electrical work on the system is only to be carried out by qualified personnel.
Indicates a situation in which protective gloves or clothing must be worn.
Indicates a situation in which protective goggles must be worn.
For fast and proper service, always provide the following information for all inquiries or spare parts
orders for your unit:
• the serial number (located on the back of the unit on the nameplate)
• the catalog number
This water purification system is also in line with a number of other international standards,
regulations and guidelines not listed here. If you have any questions regarding compliance with
national standards, ordinances and directives for your country, contact your Thermo Fisher Scientific
sales organization.
Safety Precautions
Observe these safety precautions for your own safety!
DIONEX IC Pure is a modern water purification system intended only for the
treatment of potable water or water of ASTM Type II quality. The water it produces
is not intended for drinking.
Work may only be performed on the unit electronics when the unit has been
switched off and when ESD protection is in place. Only specially trained personnel
may work on the unit‘s electronics.
• Do not install or operate the unit until you have carefully read through these operating
instructions and the notes and notices contained therein.
• Lifting and carrying the Thermo Scientific Dionex IC Pure system, e.g. to the installation location,
should be carried out by two people. To do this, lift the unit in tandem at the two corner points
beneath the bottom plate.
• The CE mark is not longer valid if you make any structural changes to the unit or install products
from other manufacturers in/on the unit.
• Protect the system from frost. The temperature at the installation area must be between +2 °C and
+40 °C.
• Always observe the applicable, pertinent codes and regulations valid at the installation location of
the unit and follow all applicable accident prevention regulations.
• When an external tank filling station is used, the feedwater pressure must be at least 0.1 bar (1.45
PSI) and a maximum of 4 bar (58 PSI). An additional pressure reducer must be installed should it
be higher.
• A low pressure black check valve is recommended to prevent back flow of feedwater from water
system based on DIN EN 171:2011
• A grounded 100-240V, 50/60Hz electrical outlet must be available (see 'Technical Specifications'
on page 13).
• Access to the power supply cord and plug must never be restricted or obstructed.
• Unplug the system from the power outlet for all maintenance performed on the system.
• An atmospherically vented floor drain with a nominal diameter of at least 63 mm (2.48 inch)
(DN50 tube) must be present at the installation location. If no drain is provided it is
recommended that a water detector is installed for safety reasons (for European specifications
only). Failure to provide this will release the manufacturer from liability for any water-induced
damage that may result.
• Proceed as follows if the unit is not to be operated for an extended period, e.g., over extended
weekend, or during a vacation period:
• Switch the system off (unplug the mains plug).
• Close the feedwater inlet (close the feedwater tap).
Damage to the pump may occur if the unit were to run without any supply of feedwater. The
manufacturer will not accept any liability should this occur.
• The surface or wall on which the unit is to be installed or mounted must have an adequate
load-carrying capacity (check the capacity and stability of the wall). The dry weight of the unit is
given under 'Technical Specifications' on page 13. When the internal tank is filled, the unit has a
weight during operation of approx. 32 kg / 70.55 lbs.
• The surface on which the unit is installed must be level and stable. A max. 2% deviation from
evenness is recommended not to be exceed.
• When installing the water purification unit, always ensure that there is adequate space all around
the unit (see 'Technical Specifications' on page 13) to ensure that ease of use or easy replacement of
materials (e.g., filter change, connection) is accessible at all times.
• Visually inspect the unit at regular intervals. Clean up any water or spills found around the unit
immediately.
Never look directly into a switched-on UV-lamp, as UV-light endangers eyesight!
To avoid the risk of pinching, crushing, cutting or electrical shock, never perform
maintenance on the unit without its protective housing, or while it is in operation.
Maintenance work on the unit may only be performed by factory trained and
authorized specialists.
.
• Wear safety gloves when working with disinfectant solutions.
• If your skin should come into contact with a chlorine product, rinse it immediately with ample,
fresh water.
• The unit, or system components, may generate heat as a result of a defect. It is recommended to
always wear appropriate safety gloves to prevent skin damage or burns.
• To avoid tripping, ensure that the tubings do not lay over the floor.
• Apply the general rules of hygiene for laboratories when working with the system.
• Do not use any oxidative cleaning agents for cleaning the system as this may cause damage to the
unit.
• Proceed as follows when the unit has a defect:
• Switch the system off and unplug the unit from outlet.
• Shut off the supply of feedwater.
• Contact your local service organization.
3 7
5
9
8 6
1 0
1 6
1 4
1 5
2 3
1 7
1 3
2 2
1 8
1 9
2 1
2 0
1 2
1 1
1
3
5
2
7
8 6 9
1 0
4
4
1 1
1 3
1 2 1 5
2 3
1 7
1 4
1 6
2 2
1 9
1 8
2 0
2 1
2 7 2 6
2 4
2 8
2 5
2 5
2 8
2 4
2 6
2 7
• Teflon tape
• cable ties small to attach wires
To facilitate the exchange of spare parts is described in this chapter which tolls are
needed.
Chapter Tools
'Replacing Display Control part,' on • Phillips screwdriver
page 43 • Screwdriver for slotted head screws, size 0.4 x 2.5 mm
• extension
• ratchet
• socket wrench for M3 threaded hexagon nut
• An ESD protection
'Replacing the Interface' on page 45 • Phillips screwdriver
• Screwdriver for slotted head screws, size 0.4 x 2.5 mm
• extension
• ratchet
• socket wrench for M3 threaded hexagon nut
• An ESD protection
'Replacing the UV ballast' on page 47 • Screwdriver for slotted head screws, size 0.4 x 2.5 mm
• Phillips screwdriver
• An ESD protection
'Replacing solenoid valve' on page 51 • Magnetic Phillips screwdriver
• Screwdriver for slotted head screws, size 0.4 x 2.5 mm
'Replacing feedwater measuring cell' on • Magnetic Phillips screwdriver
page 52 • Screwdriver for slotted head screws, size 0.4 x 2.5 mm
• Waterpump pliers
• Teflon tape
• Precision conductivity meter for feedwater
• An ESD protection
• D8 mm tubes
'Replacing Ultra pure water measuring • Magnetic Phillips screwdriver
cell' on page 53 • Screwdriver for slotted head screws, size 0.4 x 2.5 mm
• Precision conductivity meter for ultra pure water
• 1/4“ ratchet, 1/4“ extension
• 1/4“ socket wrench size 8
• double open ended spanner size 8
• double ended spanner size 17
• An ESD protection
• D8 mm tubes
'Replacing TOC measuring cell' on • Magnetic Phillips screwdriver
page 55 • Screwdriver for slotted head screws, size 0.4 x 2.5 mm
• 1/4“ ratchet, 1/4“ extension
• 1/4“ socket wrench size 8
• double open ended spanner size 8
• double ended spanner size 17
• An ESD protection
Chapter Tools
'Replacing the pressure Booster pump' • Long magnetic Phillips screwdriver
on page 57 • Screwdriver for slotted head screws, size 0.4 x 2.5 mm
• double open ended spanner size 8
• double open ended spanner size 22
• An ESD protection
'Replacing pressure hold valve' on • Magnetic Phillips screwdriver
page 59 • double open ended spanner size 8
'Adjust the pressure for “to pump“ and • Pressure adjustment kit Part No.: 50151154
“to suppressor“ outlets' on page 62 • One vessel for catch the water
• Double open ended spanner size 10/11
'Adjust the concentrate flow' on page 65 • Vessel for catch water (max. volume 200ml)
• Slot screw driver
'Replacing tank indicator' on page 66 • Magnetic Phillips screw driver
'Replacing the fuse from additional tank • Screwdriver for slotted head screws, size 0.4 x 2.5 mm
indicator' on page 67 • An ESD protection
'Replacing tank indicator sensor on
system' on page 68
'Replacing tank indicator sensor on
external 20L tank' on page 69
Technical Specifications
Feedwater requirements
Model System with pretreatment cartridge System without pretreatment cartridge
Source Tap water according to DIN 2000:2000 Pretreated water (ASTM Type II)
Silt density index (SDI) <3 -- (not applicable)
Conductivity (reference 1200 μS/cm (0.0008 M·cm) < 1 μS/cm or > 1 M·cm
temperature +25 °C)
Free chlorine max. 0.1 ppb Max. 0.05 ppb
Manganese content max. 0.05 ppm -- (not applicable)
Iron content max. 0.2 ppm -- (not applicable)
pH range 4 - 11 4 - 11
TOC value < 2000 ppb max. 50 ppb
Bacteria count < 100 CFU/ml < 100 CFU/ml
Turbidity < 1.0 NTU < 1.0 NTU
Carbon dioxide (CO2) max. 30 ppm max. 30 ppm
Silicate max. 30 ppm max. 3 ppm
Temperature +2°C - +35°C +2°C - +35°C
Pressure for automatic 0.1 - 6 bar /1.45 - 87 PSI (at a pressure > 6 -- (not applicable)
filling bar / 87 PSI a pressure reducer must be
installed upstream of the unit. Pressure
reducer before recirculation pump has to be
adjusted to 25 psi.
Product water quality
Conductivity (reference temperature +25 °C) 0.055 μS/cm/ 18.2 M·cm
Resistance up to18.2 M·cm
TOC value max. 5 ppb
RNase < 0.003 ng/ml
DNase < 0.4 pg/ul
Bacteria < 1 CFU/ml
Bacterial endotoxines 0.1 EU/ml
Particles > 0.2 μm per ml <1
Flow rate without pretreatment cartridge at manually 0.6 l/min +/- 0.2 l min
operated POU
Flow rate with pretreatment cartridge at manually 0.2 l/min +/- 0.2 l min
operated POU
Dimensions and weight of DIONEX IC Pure with ultra pure cartridge
Height 550 mm 21.65 inch
Width 306 mm 12.05 inch
Depth 385mm 15.16 inch
Base area 277 x 372 mm 10.91 x 14.65 inch
Fig.8
306 385
Dimensions and weight of external 20L tank with level control
Height 490 mm 19.29 inch
Width 190 mm 7.48 inch
Depth 485 mm 19.09 inch
Base area 340 x 483 mm 13.39 x 7.48 inch
Weight of dry tank 7 kg 18.07 lbs
Weight with full tank 27 kg 60 lbs
490
Controls
Temperature
measurement
On/Off switch
Confirm the
program and
selection.
or
Interval
18.2 Mё·cm
18,5°C UV/TC
00000/12
OEM Menu
μS/cm - Mȍ cm
μS/cm If the Dionex IC Pure system is connected
with the Dionex ICS systems about the con-
OEM Menu
Temp. comp. trol cable, it will appears in the Display Ana-
On
lyzer. In this mode there it is not possible to
OEM Menu
switch into the Interval mode.
Genpu. UV UF TOC
S.No.: 9999/12
SW Version 4.1
• Refer to the IC Pure Water Purification system Operator‘s manual for detailed
system control instructions under the ‘System Control‘ chapter.
• You need for unlock all levels of the system control a “All levels“ code.
To prevent unauthorized access to the settings and factory presetting, changes to settings can only be
made when a correct code number from the following Table is entered and confirmed with 'ENTER.
The unlocking is then active for a 5 minute period.
Press the 'Menu' key nine times. The display shows:
Code
Press enter
0000
To prevent unauthorized access to the settings and factory presettings, changes to settings can only be
made when a correct code number from the following Table is entered and confirmed with 'ENTER'.
Existing programs are given on three levels. The first level provides access only to the Menu level. A
second level provides access only to the Menu and OEM menu levels and a third level provides access
to all three levels.
Code no.:
No. Menu No. Menu + OEM menu No. All levels
1 0150 4 0450 7 0750
2 0250 5 0550 8 0850
3 0350 6 0650 9 0950
When you press the 'Menu' button the tenth time you exit the user menu and the
unit automatically resumes its last operating mode ('NONSTOP'/'INTERVAL' or
'Analyzer' mode).
Operating modes
• Interval mode after switching on the unit
• NONSTOP mode
• INTERVAL mode
• Analyzer mode
• OFF mode
Calibration menu
When the code number for unlocking has been entered, the calibration menu can be called by
simultaneously
pressing the UV-key and the INT.-key. The Press enter! menu prompt appears. Confirm
this with Enter to come to the first sub-menu. Each further press on the menu-key brings you to the
next sub-menu.
• Changes must be confirmed with the Enter-key, otherwise none of them will be
saved.
• Refer to the chapter 'Description of control display' on page 17 to see what
buttons you can change the values.
The momentary resistances measured at the conductivity and temperature measuring cells by the
microcontroller are displayed here. This sub-menu is really only of interest to the manufacturer of the
controller to be able to reliably test the functioning of system control via fixed resistances.
Press the Menu key one time then the display shows:
Calibration Menu
Resistances?
Press enter
Set values that are far outside of the typical setting range are not a problem as long as
the system works perfectly according to a reference instrument.
Such values occasionally indicate that the particular sensor could have a problem that
requires an exact test of the functioning of it, however.
Press the Menu key two times, then the display shows:
Calibration Menu
Temperature
10000
Set values that are far outside of the typical setting range are not a problem as long as
the system works perfectly according to a reference instrument.
Such values occasionally indicate that the particular sensor has a problem that
requires an exact test of the functioning of it, however.
Press the menu key three times, then the display shows:
Calibration Menu
Cell const. LF1
0,0100 1/cm
The measuring cell is switched off when the cell constant is set to above 0.3. In this case „Off“ is then
shown in the display.
Set values that are far outside of the typical setting range are not a problem as long as
the system works perfectly according to a reference instrument.
Such values occasionally indicate that the particular sensor has a problem that
requires an exact test of the functioning of it, however.
Press the menu key fourth times, the display shows:
Calibration Menu
Cell const. LF2
0,160 1/cm
Press the menu key five times, then the display shows:
Calibration Menu
Cell const. LF3
( 0,0100 1/cm )
auto calib.
Press the menu key six times, then the display shows:
Calibration Menu
TOC value
1000
Error suppression
Water purification systems generally need time for the measured and displayed values to stabilize
subsequent to a change in the operating state.
The fault suppression time enables faults to be verified, so that only “genuine” faults are displayed that
still exist as such after the expiry of the suppression time.
When, after a change in the operating state, exceeded limiting values swing to below the set limit
within the set suppression time, the system recognizes this and does not consider such temporary
excesses to be a fault.
Press the menu key seven times, then the display shows:
Calibration Menu
Error display
1 min
This is not a “Factory setting” in the sense of a return to the “First set values” which
were factory calibrated!
This menu prompt returns system control back to the state it was in on delivery prior
to the first calibration. If you set back to the starting values, therefore, you must carry
out a complete new calibration of the measuring cells and enter new settings for all
basic settings and limiting values!
Calibration Menu
Default values
Press enter
Volume control
Not important for this system while Volume control not available for this system.
Ignore this point and press the menu key against to prompt to the next one.
Press the menu key nine times, then the display shows:
Calibration Menu
Volume Control
Yes
UV-menu
• This menu is relevant if the operation hours counter or the filter cartridge
operating hours counter needs to be changed.
• In the operating instructions for the customer, the UV-lamp is declared as a
consumable and can be replaced by the customer.
• If the customer requests a service call to replace the UV-lamp, refer to the
Operator‘s manual under the Chapter ‘Change UV-lamp‘.
Simultaneous pressing of the menu-key and the UV-key calls the UV-menu.
The limiting values for the operating time of the UV-lamp and intensity monitoring can be set in this
menu. The “UV-time” fault message appears in line 4 of the display when the limiting value for the
UV-lamp operating time is exceeded.
As the UV-lamp is an option, a value higher than 10000 h must be entered in systems without this
option to switch the UV-lamp operating time off. The word “off” is then shown in the display.
When a UV-intensity value of 40% is set, evaluation of the UV-lamp is switched off and the word
“off” is shown in the display.
In this menu, the UV-lamp operating time counter can be set back to zero and the UV-lamp intensity
can be set to 100%.
To do this, and with the UV-lamp switched on, measure the UV-intensity for as long as it takes for the
measured value for the UV-intensity to remain stable. The word message “Please wait” is shown in the
display during the required time.
Press the Menu key one times, then the display shows:
UV-Menu
Duration
3000h
• These setting are not important for the system. There is not an accessory UV-
Sensor on the UV reactor.
• Make sure that the UV- intensity is switched off.
Press the Menu key two times, then the display shows:
UV-Menu
Intensity
Off
Press the Menu key three times, then the display shows:
Run Time
Cartridge
450 Days
Reset the operating hours counter and measuring in a new UV- lamp
Confirmation of this menu prompt with Enter sets the UV-lamp operating time counter back to zero.
The UV-lamp is simultaneously switched on and measured in over a period of from 5 min. to 2 h. The
maximum intensity is determined during this time and is defined to be the 100% value. The system
always assumes here that the UV-lamp is a new one. Please do not use UV-lamps which have already
been put to use here, as the 100% value would then be wrongly defined. This would result in an
incorrect evaluation and so to an inadequate water quality.
When measuring in has been completed, the system returns to the Interval operating mode.
Press the Menu key four times, then the display shows:
New UV lamp?
Press enter
Calibration
In the Calibration Menu, a cell constant is only set to provide the system with a
factor for the exact calculation of each individual measured value, so that the
complete measuring range is covered by a single factor per measuring cell.
Inaccuracies such as those which inevitably occur with individual fixed points are so
avoided.
The Calibration Menu must always be quit for the comparison and evaluation of the
actual measured values of the system with the reference instrument, provided that
calibration has been completely carried out or a further adjustment is required.
Step Action
The following steps are necessary to prepare to
1) calibrate the ultra pure water measuring cell.
1. Release the pressure by turning the rotary
knob on the dispensing valve.
Rotary
knob
• To prevent that water flows on the surface where
the system is stand on, place a container under the
3) water tap.
2. Remove the cartridge cover and the filter
cartridge. (see Operating instruction Chapter
Change filter cartridge)
3. Locate the ultra pure water measuring cell
and the ultrafilter.(see Fig. 51)
4. Remove the D8 mm tube from the 2 Fittings
by pressing retreat of the black ring on the
fitting and simultaneously pulling in and out
Pure water mea- Ultra filter
of the tube.(see Fig.52)
suring cell Fig.51
4)
Black ring
Fig.52
Step Action
Out ultra-
pure water
In ultrapu-
re water
Ultra filter Fig.54
Calibration of the ultra pure water measuring cell LF1 with temperature
• Calibration (comparative measurement) requires a measuring instrument which is highly
accurate and measures conductivities to three places after the decimal point. The cell constant of
the connected measuring cell should be 0.01
• The ultra pure water system must be in the Nonstop-mode for comparison measurements,
otherwise the reference conductivity meter will not show any relevant measured values.
• Description of the Calibration Menu see under chapter “Setting the temperature sensor” on
page 20.
2)
Code
Code • Notice the value of the temperature on the
Press
Press enter
enter
0000 display from the system before you starting
0000 with the calibration.
1. Switch the system on.
3)
2. Press the menu button 9 times to arrive
the Code section.
3. Give in a „all level“ code to become
Code
Code access for all levels.
Press
Pressenter
enter
0000
0950
• To change the value use the „Nonstop and
Interval“ button. To get to the next digit use
4) the „UV button“.
4. After confirm with Enter you leave the
Code
Code Code
Nonstop 00ppb
Press Press enter „User menu“.
Pressenter
enter 18.2 MΩ∙cm
0000 0000
19.3 °C UV/TC
5. Press simultaneously the „Interval and
0950
UV“ key to arrive the Calibration Menu.
6. Press the „Menu“ key twice to jump to
5) the next calibration point in the
CodeMenu
Calibration Calibration Menu and adjust the
Press enter temperature value.
Resistance?
0000
Press enter
Figure 55
Temperature value
agreement Display conductivity meter
Display System
18.2Mёͼcm
Nonstop000 ppb 11.7°C
…18.2Mёͼcm
18 2 Mё
….11.7°C..UV/TC
Menu02.02.2015
15:23
Fig.55
• If the values of both displays are not shown the same temperature, repeat the steps 2 - 6
as describe above.
Step Action
2)
Code
Code • Notice the value of the MΩ·cm resistance on
Press
Press enter
enter
0000 the display from the system before you
0000 starting with the calibration.
1. Switch the system on.
3)
2. Press the menu button 9 times to arrive
the Code section.
3. Give in a „all level“ code to become
Code
Code access for all levels.
Press
Pressenter
enter
0000
0950
• To change the value use the „Nonstop and
Interval“ button. To get to the next digit use
4) the „UV button“.
4. After confirm with Enter you leave the
Code
Code Code
Nonstop 00ppb
Press Press enter „User menu“.
Pressenter
enter 18.2 MΩ∙cm
0000 0000
19.3 °C UV/TC
5. Press simultaneously the „Interval and
0950
UV“ key to arrive the Calibration Menu.
6. Press the „Menu“ key three times to
5) jump to the calibration point for the
CodeMenu ultra pure water measuring cell and
Calibration
Press enter
Resistance? adjust the value.
0000
Press enter
7. To change the value use the „Nonstop
and Interval button. To get to the next
digit use the „UV button“.
6)
CodeMenu
Calibration CodeMenu
Calibration
Press enter • Change the value in 2 points to increase or
Press enter
Resistance? Temperature
0000 0000
10000
reduce the value and confirm with „Enter“.
Press enter
8. Leave after adjust the value the
Calibration Menu by putting the
CodeMenu
Calibration
Press enter „Menu“ key 7 times and control the
Cell const. LF1
0000
0.0100 1/cm value of temperature on the Display with
the value of the reference instrument.(see
7) Fig.56 on next page)
CodeMenu
Calibration
CellPress
const.enter
LF1
0000
0.0100 1/cm
CodeMenu
Calibration Code Menu
Calibration
CellPress enter
const. LF1 CellPress enter
const. LF1
0000 0000
0.0098 1/cm 0.0102 1/cm
or lower or higher
Figure 56
Resistance value
agreement Display conductivity meter
Display System
18.2Mёͼcm
Nonstop000 ppb 11.7°C
…18.2Mёͼcm
18 2 Mё
….11.7°C..UV/TC
Menu02.02.2015
15:23
Fig.56
• If the values of both displays are not shown the same temperature, repeat the steps 2 - 8
as describe above.
• Work may only be performed on the unit electronics when the unit has been
switched off.
• Unplug the power supply from the power outlet on the system.
• Take caution to ensure that the suitable power outlet and electronic components
do not get wet. Risk of an electric shock.
• Take caution that you have enough space by the system for the maintenance
work.
Step Action
The following steps are necessary to prepare to
1) calibrate the feedwater measuring cell.
1. Release the pressure by turning the rotary
knob in clockwise direction on the dispensing
valve.
Rotary
knob
• To prevent that water flows on the surface where
the system is stand on place a vessel under the
water tap.
2. Locate the connection panel and remove the
2)
tube jumper from the external 20L tank
outlet port on the panel from the system. .
Coupling
body
• There are coupling bodies on the tube jumper.
Press on the knob from the coupling body und
then you can remove the tube jumper.(see Fig. 57)
Tube
jumper
3. Remove the D8 mm tube of the tube jumper
from the internal tank outlet port of the panel
Coupling from the system by pressing retreat of the
body knob
black ring on the fitting and simultaneously
pulling in and out of the tube.(see Fig. 58)
Fig.57
Tube
jumper
Fig.58
Step Action
Out feed-
water
D8 mm tubes
Step Action
Code
Code Code
Nonstop 00ppb
Press Press enter • When your system is working with a
Pressenter
enter 18.2 MΩ∙cm
0000 0000 pretreatment cartridge and your feedwater
0950 19.3 °C UV/TC
quality have a to high hardness (see
“Technical Specifications” on page 13), adjust
5) the feedwater measuring cell „off“ in the
„User menu“ with the „Nonstop and
Code
Feedwater Interval“ key and confirm with „Enter“.
Press
1.25 enter
MΩ∙cm
0000 feed
Limit value 6. Press simultaneously the „Interval and
2.0 µS/cm UV“ key to arrive the Calibration Menu.
6)
CodeMenu
Calibration
Press enter
Resistance?
0000
Press enter
Step Action
or lower or higher
10)
NonstopCode
00ppb Code
Feedwater
Press
18.2 enter
MΩ∙cm Press
1.25 enter
MΩ∙cm
0000 UV/TC 0000 feed
Limit value
19.3 °C
2.0 µS/cm
Figure 61
Feedwater 1.2518.2
MΩ∙cmMёͼcm
Nonstop000 ppb
1.25 MΩ∙cm
…18.2Mёͼcm
18 2 Mё 19.311.7°C
°C
….11.7°C..UV/TC
Limit value feed
Menu02.02.2015
2.0 µS/cm 15:23
• If the values of both displays are not shown the same resistance, repeat the steps 2 - 10 as
describe above.
Step Action
CodeMenu
Calibration CodeMenu
Calibration
Press enter Press
Cell enter
const. LF1
• Adjust the TOC measurement cell to the
Cell const. LF2 0000
0000
0.0160 1/cm 0.0100 1/cm value „auto calib.“
8. Leave after adjust the value the
CodeMenu
Calibration Calibration Menu by putting the
Press enter
Cell const.
0000
LF3 „Menu“ key 5 times.
(0.0100 1/cm)
CodeMenu
Calibration
Cell const.enter
Press LF3
0000
(0.0100 1/cm)
Code
Calibration Menu
CellPress
const.enter
LF3
(0.0100 1/cm)
0000
auto calib.
7)
CodeMenu
Calibration
Press
TOC value enter
0000
0900
CodeMenu
Calibration
Press
TOC value enter
0000
1000
• This is not a “Factory setting” in the sense of a return to the “First set values” which
were factory calibrated!
• This menu prompt returns system control back to the state it was in on delivery prior to
the first calibration. If you set back to the starting values, therefore, you must carry out a
complete new calibration of the measuring cells and enter new settings for all basic
settings and limiting values!
• We so expressly warn against calling the starting values!
Step Action
1. Switch the system on.
2) 2. Press the menu button 9 times to arrive
Code
Code
Pressenter
Press enter the Code section.
0000
0950 3. Give in a „all level“ code to become
3)
access for all levels.
Code
Code
Pressenter
Press enter
0000
0950
• To change the value use the „Nonstop and
4) Interval“ button. To get to the next digit use
Code
Code Code
Nonstop 00ppb
Pressenter
enter Press
18.2 enter
MΩ∙cm
the „UV button“.
Press 0000
0000
0950 19.3 °C UV/TC 4. After confirm with „Enter“, you leave the
„User menu“.
5) 5. Press simultaneously the „Interval and
Code Menu
Calibration
Press enter
Resistance? UV“ key to arrive the Calibration Menu.
0000
Press enter
6. Press the „Menu“ key 5 times to jump to
6) the calibration point for the TOC
Code Menu
measuring cell and adjust the value.
Calibration Code Menu
Calibration
Press enter
Resistance? Press enter
Temperature 7. To change the value use the „Nonstop
0000 0000
Press enter 10000 and Interval“ button. To get to the next
digit use the „UV button“.
Code Menu
Calibrtaion Code Menu
Calibrtaion
Press
Cell enter
const.LF2 Press
Cell enter
const.LF1
0000
0.0160 1/cm 0000
0.0100 1/cm
• Do not confirm with enter, because all
Code Menu Code Menu
calibrated values from the systems interface
Calibrtaion Calibrtaion
Press
Cell enter
const.LF3
0000
Press
TOC enter
value are going back to the delivery settings.
0000
(0.0100 1/cm) 0900
Step Action
The following steps are necessary to replace the display.
1)
Swivel
display
Fig.10
Step Action
Fig.11
• Do not mix these up when subsequently the new
Display display.
back part
3. Remove the display back side from the display
holder.
c) b) 4. Remove the 40-pin cable plug from the post
socket of the display.(see Fig.12)
Display holder a) 5. Screw out the 4 hexagon nuts designated (d) and
move out the Display.(see Fig.12)
4), 5)
• Due the display foil from the front side, it would be
Display possible that the display is somewhat difficult to
remove.
• Move so be careful the display back and forth while
pulling.
• Do not forget to remove the protective foil from the
new display, before mount it.
d) 6. Carry out the installation of the new display in
d) the reverse succession to that describe above.
7. Connect the system back to the power supply and
switch the system on.
8. Program all parameters of the system in the
system control and save it.(see Operating
instruction Chapter Operating Elements)
Fig.12
40-pin cable plug
• Work may only be performed on the unit electronics when the unit has been
switched off and when ESD protection is in place.
• Unplug the power supply for all maintenance work from the power outlet on the
system.
• Take caution to ensure that the suitable power outlet and electronic components
do not get wet. Risk of an electric shock.
Step Action
The following steps are necessary to replace the Interface.
1)
1. Screw out the 2 screws designated (a).(see Fig.13)
2. Remove the cover from the top side. (see Fig.14)
3. Remove the 40-pin cable plug and all other
electrical connectors from the interface socket.(see
Fig.15 and Fig.16)
Interface
b)
b)
40-pin
cable
Fig.15
plug
Step Action
X1
X6
X5
Fig.16
40 pin cable plug connector
Step Action
The following steps are necessary to replace the
2) UV-ballast.
3)
a)
Fig.18
Step Action
Fig.19
46
4 6
• Work may only be performed on the unit electronics when the unit has been
switched off.
• Unplug the power supply for all maintenance work from the power outlet on the
system.
• Take caution to ensure that the suitable power outlet do not get wet. Risk of an
electric shock.
• Take caution that you have enough space by the system for the maintenance
work
D D
Part no. and quantity of screws:
A 8x = 21.0128
B 3x = 21.0129
C 1x = 21.0133
A DifferentScrews D 4x = 21.0110
B
A C B D
D
C
Fig.20
D
Step
1
3
B
Fig.21
B
1 = rear panel internal 5L tank
2 = Internal 5L tank with ring
3 = rear panel device
4 = Connection panel
5 = System IC Pure
A
Connecting
screws rear
panel device
Screws from connec-
tion panel to rear Part no. screws
panel device 2x 21.0110
Fig.23
Fig.22
• Unplug the power supply for all maintenance work from the power outlet on the
system.
• Take caution to ensure that the suitable power outlet do not get wet. Risk of an
electric shock.
• Take caution that you have enough space by the system for the maintenance
work
Step Action
The following steps are necessary to replace the solenoid
5) valve.
Solenoid valve
Step Action
The following steps are necessary to replace the feedwater
4) measuring cell.
a)
Fig.27
Feedwater
measuring
cell
Step Action
The following steps are necessary to replace the Ultra pure
6) water measuring cell.
b) • a) 2x = 21.0043
• b) 2x = 21.0037
Step Action
Male
Male thread
connector
connector
14.0039
14.0297 1/8“,
Fig.30 D8 mm
D8 mm
• Unplug the power supply for all maintenance work from the power outlet on the
system and when ESD protection is in place.
• Take caution to ensure that the suitable power outlet do not get wet. Risk of an
electric shock.
• Take caution that you have enough space by the system for the maintenance
work
Step Action
The following steps are necessary to replace the TOC
6) measuring cell.
Feedwater • The screws are screwed from the inside of the system
measuring with hexagon nuts designated (b) against and must be
cell
kept up. You will found them on the inside of the
system near the feedwater measuring cell.(see Fig.32)
Step Action
Male
Male thread
connector
connector
14.0039
14.0297 1/8“,
Fig.33 D8 mm
D8 mm
Step Action
The following steps are necessary to replace the pressure
5) booster pump.
Fig.35
Connection
panel
Step Action
Booster • Fixed with one Hand the pressure booster pump from
pump the inside of the system. Thereby you prevent that the
pressure booster pump not suddenly fall down.
10. Pull out the second D8mm tube from the
pressure booster pump by pressing retreat of the
Fig.36
black ring on the fitting and simultaneously
9) pulling in and out of the tube and remove the
pump.
c)
Fig.37
Ultra pure water me-
asuring cell
Step Action
11) 11. Disassemble the lock rings and Fittings from the
pressure booster pump and mount it onto the
new one. (see Fig.38).
Locking
Fitting rings Fitting
D8 mm D8 mm
• To facilitate to moving out the fittings use an size 8
double open ended spanner by pushing in the spanner
between the plugged into each other fittings.
12. Carry out the installation of the new pressure
booster pump in the reverse succession to that
describe above.
13. Connect the system back to the power supply and
switch the system on.
Fig.38
• Unplug the power supply for all maintenance work from the power outlet on the
system.
• Take caution to ensure that the suitable power outlet do not get wet. Risk of an
electric shock.
• Take caution that you have enough space by the system for the maintenance
work
• After installation a new pressure hold valve you must adjust the pressure with a
pressure gauge. If not any adjustment tool on place you have the possibility to
order the pressure adjustment kit from Thermo Fisher Scientific.
Step Action
1)
Pressure hold valves The following steps are necessary to replace the pressure
hold valves.
Fig.39
3)
Fig.40
Pressure hold valve
D8 mm tubes
Step Action
1)
Male connector D8 mm
4. move out the pressure hold valve and pull out the
2 fittings as described in Step 3 with the tubes.
Male connector D8 mm
Fig.42
Adjust the pressure for “to pump“ and “to suppressor“ outlets
• Take caution to ensure that the suitable power outlet do not get wet. Risk of an
electric shock.
• Take caution that you have enough space by the system for the maintenance
work
• After installation a new pressure hold valve you must adjust the pressure with a
pressure gauge. Use the “Pressure adjustment kit“ with part no. 50151154 to
adjust both pressure hold valves V4 and V3.
• The new setting of the pressure must be performed if subsequently a
pretreatment cartridge is installed or a pretreatment cartridge was retrofitted.
• Control the pressure onto the V3 and V4 outlets if a ultrapure cartridge or
pretreatment cartridge was changed.
• By change of pressure on a valve the pressure on the other one the second valve is
also changed. Both pressures on the valves are dependent from the respective
adjusted pressure on the valves.
Quick connector
Quick connector
Pressure kit 2, 0-6 bar
Step Action
1. Switch the system off and disconnect the control
2) cable on the connector “Ion Chromatograph“ of
Connection for control cable the connection panel.
2. Locate the 2 pressure outlets on the connection
Connection panel panel.(see Fig.43)
3. Plug in the Pressure Kit 1 into the pressure outlet
“to pump“ (see Fig. 44). Proceed the same way
with the pressure kit 2 for the pressure outlet “to
suppressor“ on the connection panel.
• For the next steps you need a vessel to catch the water
coming out from the „to pump“ outlet.
4. Switch the system on and bring the Dionex IC
Pure system into the Nonstop mode.
5. Turn the adjustment knob from the pressure hold
Fig.43
Pressure outlets to pump 3 psi V4
valve 4 until you see at the pressure gauge that the
pressure value increase.
Pressure outlets to suppressor 30 psi V3
6. Turn the adjustment screw on the precision
metering valve in clockwise direction until only a
3)
few drops flows at the end of the 1/8“ tube from
“to pump“ connection IC Pure system
the pressure kit 1 into the vessel.
Pressure Kit 1
• It doesn‘t matter how many drops in a certain time
comes out of the end of the 1/8“ tube. To adjust the
V4 valve, a slight flow from water must be ensured.
• If there are bubbles in the water line of V3, rinse the
IC Pure system as described in the operating
instructions.
“to suppressor“ connection IC Pure system 7. Adjust the pressure on V4 to the value of 30 psi
(see Fig.45).
8. Adjust the pressure on V3 to the value of 3 psi
Pressure Kit 2 (see Fig.45).
9. Control after adjust V3 the value of V4. If there is
not anymore showing the 30 psi, adjust it again to
the correct value.
Step Action
7)
Increase pressure on V3
Fig.45
8)
Lock nuts
Fig.46
• Unplug the power supply for all maintenance work from the power outlet on the
system and when ESD protection is in place.
• Take caution to ensure that the suitable power outlet do not get wet. Risk of an
electric shock.
• Take caution that you have enough space by the system for the maintenance
work
• The concentrate back flow must only adjust when the IC Pure system is
operating with a pretreatment cartridge or a external 20 L Tank without level
control is connect or a pretreatment cartridge was retrofitted.
• Make sure that the pressure on the V3 and V4 valves are adjust to the
requirement values.
Step Action
Concentrate
connection
external 20 L • Write down the value of content in the vessel.
tank
• The amount of concentrate back flow should be a
Fig.48
have value of 70 ml ± 10 ml/ 36 sec.
4)
Concentrate flow valve 6. Use a slot screw driver to turn the adjustment
Fig.49
screw from the concentrate flow valve (located on
the front side from IC Pure system) in clockwise
direction to reduce the concentrate flow and in
anti clockwise direction to increase the
Place for pretreatment
cartridge concentrate flow.
7. Remove action 1 - 5 until the amount of 70 ml ±
10 ml/ 36 sec of concentrate flow has reached.
Step Action
The following steps are necessary to replace the tank
1) indicator.
a)
The following steps are necessary to replace the fuse from the tank indicator.
Step Action
The following steps are necessary to replace the tank
1) indicator sensor on the system.
Fig.53
Step StepAction
The following steps are necessary to replace the tank
1) indicator sensor on the external 20L tank.
a)
1. Remove the cover from the control case by
unscrew the screws designated (a).(see Fig.51)
2. Locate the tank indicator sensor and screw out the
screw designated (b).(see Fig.52)
control case
3. Move out the tank indicator sensor and unplug
the electrical wires from the pins.(see Fig.48 on
page 68)
Fig.55
b)
Troubleshooting
Flow charts
Flow chart DIONEX IC pure with 20L tank and level control
EGCVent
ICS 2100
Thermo Scientific
OverͲ
flow
4 Suppressor line
REGENIN
3 1 2
1
Schematic illustration with connected Suppressor
2 To suppressor 30psi
3 Drain
4 Tankoverflow
Note:
DIONEX IC Pure
1 TubingfromCDcelloutshouldberoutedtowaste
• PressurerestrictorcoilsarerequiredtobeinstallattheCDcelloutlet.
83
Terminal Assignment and Flow chart
9
84
Eluent line
Tee
DIONEX IC Pure
EGCVent EGCVent
nt line
Overflow
Eluen
Terminal Assignment and Flow chart
1 2 1 1
3
Waste
Note:
1 TubingfromCDcelloutshouldberoutedtowaste
• PressurerestrictorcoilsarerequiredtobeinstallattheCDcelloutlet.
Thermo Scientific
ICPureconnectedwithDionexICSͲ4000system
ICS 4000
Thermo Scientific
Eluent line
Overflow
2
1
3
Waste
Connectionpanel Dionex ICPure
system:
Suppressor line
1 To pump3psi REGENIN
9
2 To suppressor 30psi
Precision
3 Drain metering valve
4 Tankoverflow
1
Note:
DIONEX IC Pure
1 TubingfromCDcelloutshouldberoutedtowaste
85
Terminal Assignment and Flow chart
9
86
Overflow
DIONEX IC Pure
El
Eluent
t line
li
Terminal Assignment and Flow chart
Precision
4 metering valve
Tee
Suppressor line
l
REGENIN
2
3
1
Waste
Tee
1
Eluent line
Precision
metering valve
Suppressor line
REGENIN
1 To pump3psi
2 To suppressor 30psi
1
3 Drain
4 Tankoverflow
Note:
1 TubingfromCDcelloutshouldberoutedtowaste
Thermo Scientific
ICS 5000+
Thermo Scientific
Connectionpanel Dionex ICPure
system:
1 To pump3psi
2 To suppressor 30psi
Eluent in
3 Drain
Overflow
4 Tankoverflow
4
3
2
Waste
1
Precisionmetering 1
valve
9
Suppressorline
REGENIN
Note:
1 TubingfromCDcelloutshouldberoutedtowaste
• PressurerestrictorcoilsarerequiredtobeinstallattheCDcelloutlet.
DIONEX IC Pure
87
Terminal Assignment and Flow chart
9
88
ICPureconnectedwith2DionexICSͲ5000+ systems
Eluent line
Precision
metering valve
DIONEX IC Pure
Overflow
Terminal Assignment and Flow chart
Suppressor line
REGENIN
2
1 Tee
3
Waste
2 To suppressor 30psi
3 Drain
4 Tankoverflow
Preciision
meteering valve
Suppressor line
REGENIN
Note:
1 TubingfromCDcelloutshouldberoutedtowaste
• PressurerestrictorcoilsarerequiredtobeinstallattheCDcelloutlet.
Thermo Scientific
10
·cmMaintenance record
Ultra Ultra
Last change Last
pure volume
of filter cleaning / Notes Signature
flow
cartridge disinfection
[l/h]
Index