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Thermo Scientific 

DIONEX IC Pure 
Ultra pure water system
Service Instructions
50148298 Rev. B March 2016
© 2016 Thermo Fisher Scientific Inc. All rights reserved.

Trademarks

DIONEX IC Pure are registered trademarks of Thermo Scientific.

Thermo Scientific is a brand of Thermo Fisher Scientific Inc.

All other trademarks mentioned in the service instructions are the exclusive property of the respective
manufacturers.

Thermo Electron LED GmbH


Stockland 3
D - 56412 Niederelbert
Germany

Thermo Electron LED GmbH is a subsidiary company of:

Thermo Fisher Scientific Inc.


1214 Oakmead Parkway
Building 10
Sunnyvale, CA 94085, USA
Thermo Fisher Scientific Inc. provides this document to its customers with a product purchase to use in
the product operation. These operating instructions are protected by copyright. Any reproduction of the
whole or any part of this document is strictly prohibited, except with the written authorization of
Thermo Fisher Scientific Inc. The contents of this document are subject to change without notice. All
technical information in this document is for reference purposes only. System configurations and
specifications in this document supersede all previous information received by the purchaser.
Thermo Fisher Scientific Inc. makes no representations that this document is complete, accurate or error-
free and assumes no responsibility and will not be liable for any errors, omissions, damage or loss that
might result from any use of this document, even if the information in the document is followed
properly.

This document is not part of any sales contract between Thermo Fisher Scientific Inc. and a purchaser.
This document shall in no way govern or modify any Terms and Conditions of Sale, which Terms and
Conditions of Sale shall govern all conflicting information between the two documents.

Release history:

For Research Use Only. Not for use in diagnostics fields.


I

Contents

Preface . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . iii
Contact Information Thermo Fisher international sales organisations . . . . . . . . iii
Fundamental requirements for service work. . . . . . . . . . . . . . . . . . . . . . . . . . . . .iv
Skills of service personnel. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .iv
Process procedures for personnel . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .iv
Applicability of the instructions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . v
Original document for translation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . v
Legal Notice . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . v
Warranty . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . v
Explanatory notes on the operating instructions . . . . . . . . . . . . . . . . . . . . . . . . .vi
Standards and directives. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . vii

Chapter 1 Safety Precautions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Chapter 2 Spare parts and tools . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5


Positions Spare parts DIONEX IC Pure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
Overview spare parts DIONEX IC Pure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
Position spare parts external 20L Tank . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
Overview spare parts external 20L tank . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
Additionally required parts you need for replacing spare parts . . . . . . . . . . . . . . . 9
Requirement tools for changing Spare parts . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

Chapter 3 Technical Specifications. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13

Chapter 4 Controls . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
Description of control display . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
Flow chart system control . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18
Unlocking the system control . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19
Calibration menu. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
Calibration of the microcontroller . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
Setting the temperature sensor . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
Setting cell constant LF1 (Pure water measuring cell) . . . . . . . . . . . . . . . . . . . . 21
Setting cell constant LF2 (Feedwater measuring cell) . . . . . . . . . . . . . . . . . . . . . 21
Setting cell constant LF3 (TOC measuring cell) . . . . . . . . . . . . . . . . . . . . . . . . 22
Matching the TOC measurement . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 22
Error suppression. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23
Restore to Initial Calibration values . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23
Volume control . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24
Leaving calibration menu. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24

Thermo Scientific DIONEX IC Pure i


Inhaltsverzeichnis

UV-menu . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24
Setting the limiting value for the UV operating hours counter. . . . . . . . . . . . . . 25
Setting the limiting value for the UV intensity measurement . . . . . . . . . . . . . . . 25
Filter cartridge operating hours counter . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25
Reset the operating hours counter and measuring in a new UV- lamp . . . . . . . . 26

Chapter 5 Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27
Set up for calibrating ultra pure water measuring cell LF1 . . . . . . . . . . . . . . . . . 28
Calibration of the ultra pure water measuring cell LF1 . . . . . . . . . . . . . . . . . . . 34
Set up for calibrating feedwater measuring cell LF2 . . . . . . . . . . . . . . . . . . . . . . 35
Calibration of feedwater measuring cell LF2 . . . . . . . . . . . . . . . . . . . . . . . . . . . 36

Chapter 6 Replacing Hardware Components . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 43


Replacing Display Control part, . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 43
Replacing the Interface . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45
Replacing the UV ballast . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47

Chapter 7 Replacing Spare parts . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49


Overview screws rear side. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49
Explosion drawing system rear side . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 50
Replacing solenoid valve . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 51
Replacing feedwater measuring cell . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 52
Replacing Ultra pure water measuring cell . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53
Replacing TOC measuring cell . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 55
Replacing the pressure Booster pump . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 57
Replacing pressure hold valve. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 59
Adjust the pressure for “to pump“ and “to suppressor“ outlets . . . . . . . . . . . . . . 62
Content of “ Pressure adjustment kit“ . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62
Adjust the concentrate flow . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 65
Replacing tank indicator . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 66
Replacing the fuse from additional tank indicator . . . . . . . . . . . . . . . . . . . . . . . 67
Replacing tank indicator sensor on system . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 68
Replacing tank indicator sensor on external 20L tank . . . . . . . . . . . . . . . . . . . . 69

Chapter 8 Troubleshooting . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 71

Chapter 9 Terminal Assignment and Flow chart . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 75


Terminal Assignment DIONEX IC pure. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 75
Terminal assignment additional tank indicator . . . . . . . . . . . . . . . . . . . . . . . . . 76
Terminal assignment level control 20L tank . . . . . . . . . . . . . . . . . . . . . . . . . . . 77
Terminal assignment wire jumper . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 78
Terminal assignment control wire DIONEX IC pure to 20L tank. . . . . . . . . . . 79
Flow charts . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 80
Flow chart DIONEX IC Pure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 80
Flow chart DIONEX IC Pure with 20L tank. . . . . . . . . . . . . . . . . . . . . . . . . . . 81
Flow chart DIONEX IC pure with 20L tank and level control . . . . . . . . . . . . . 82
Schematic illustration with connected Suppressor . . . . . . . . . . . . . . . . . . . 83
ICS 2100 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 83
ICS 4000 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 85
ICS 5000+ . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 87

ii DIONEX IC Pure Thermo Scientific


Inhaltsverzeichnis

Chapter 10 Maintenance record . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 89

Thermo Scientific DIONEX IC Pure iii


Inhaltsverzeichnis

iv DIONEX IC Pure Thermo Scientific


P

Preface

Contact Information Thermo Fisher international sales


organisations

Europe, Middle East, Africa


Postal address Germany:
Thermo Electron LED GmbH
Robert-Bosch-Straße 1
D - 63505 Langenselbold

Enquiries from Germany:


Phone Sales 0800 1 536376
Phone Service 0800 1 112110
Fax Sales/Service 0800 1 112114
E-Mail: info.labequipment.de@thermofisher.com

Enquiries from Europe, Middle East and Africa:


Phone + 49 (0) 6184 / 90-6940
Fax + 49 (0) 6184 / 90-7474
E-Mail: info.labequipment.de@thermofisher.com

Americas
Postal address USA:
Thermo Fisher Scientific
275 Aiken Road
Asheville, NC 28804
USA

Thermo Scientific DIONEX IC Pure iii


Preface
Enquiries from North America:

Enquiries from North America:


Phone +1 800-879 7767
Fax +1 828-658 0363
E-Mail: info.labequipment@thermofisher.com

Enquiries from Latin America:


Phone +1 828-658 2711
Fax +1 828-645 9466
E-Mail: info.labequipment@thermofisher.com

Enquiries from Asia Pacific:


Phone +852-2711 3910
Fax +852-2711 3858
E-Mail: info.labequipment@thermofisher.com

Fundamental requirements for service work


These service instruction describe the Thermo Scientific™ DIONEX™ IC Pure™ Water Purification
System.

Please note that service maintenance of the device must be carried out only by certified factory service
engineers. Prior to repairs, please read these service instructions carefully.

Skills of service personnel


• The replacement of defined spare parts must be performed only by authorized service personnel
who have been trained and certified by Thermo Fisher Scientific.
• Electrical work must be carried out only by a qualified factory service engineer.

Process procedures for personnel


• Service must be carried out in accordance with all applicable local and national regulations.
• For any operations of this device, the service personnel must prepare clear and concise written
instruction in the language of the operating and cleaning personnel based on the operating
instructions, applicable safety data sheets, plant hygiene guidelines and technical regulations, in
particular:
– which protective measures apply when specific agents are used,
– which safety protocols in the event of an accident.
• Repairs to the device must be carried out only by factory certified and authorized personnel.

iv DIONEX IC Pure Thermo Scientific


Preface
Applicability of the instructions

Applicability of the instructions


Original document for translation
The contents of the service instructions are subject to change without further notice.
• Concerning translation into foreign languages, the German version of these service instructions is
binding.
• Keep this service instructions close to the device so that safety instructions and important
information are always accessible.
• Should you encounter problems that are not detailed adequately in these service instructions,
please contact Thermo Fisher Scientific immediately for your own safety.

Legal Notice

We reserve the right to any specification, conditions and price changes. Not all
products are available in all countries. Contact your local partner for more details.

Warranty
Thermo Electron LED GmbH guarantees the operational reliability and safety and proper functioning
of the Thermo Scientific DIONEX IC Pure Water Purification System under the following conditions:
• The unit is operated in line with the information on installation and use given in the operating
instructions.
• The unit has not been modified or altered.
• Only original spare parts and accessories approved by Thermo Electron LED GmbH are used in
the unit.
• Inspections and maintenance are performed at the specified intervals.
• An installation check is performed after starting the unit for the first time and repeated after every
inspection or servicing.
• The warranty period begins on the day the unit is delivered to the customer.
• The warranty conditions specified above are subject to the general business terms and conditions
in force at the time of sale.

Thermo Scientific DIONEX IC Pure v


Preface
Explanatory notes on the operating instructions

Explanatory notes on the operating instructions


EU Mark of Conformity

CSA - admission


Indicates a situation which, if not avoided, could result in damage to equipment or
property.


Indicates a hazardous situation which, if not avoided, could result in death or serious
injuries.


Indicates a hazardous situation which, if not avoided, will result in death or serious
injuries.


Is used for applicational hints and useful information.


Risk of electric shock. Electrical work on the system is only to be carried out by qualified personnel.

Protective conductor connection

Connect the power supply to an electrical socket with a protective connection.


Indicates a situation in which protective gloves or clothing must be worn.


Indicates a situation in which protective goggles must be worn.

vi DIONEX IC Pure Thermo Scientific


Preface
Standards and directives

For fast and proper service, always provide the following information for all inquiries or spare parts
orders for your unit:
• the serial number (located on the back of the unit on the nameplate)
• the catalog number

Standards and directives


The Thermo Scientific DIONEX IC Pure Water Purification System complies with the following
standards and directives:
• Low Voltage Directive 2006/95/EC
• EMC Directive 2014/35/EC
• Council Directive for Machinery 2006/42/EC
• ASTM D1193-6
• RoHs 2011/65/EU

This water purification system is also in line with a number of other international standards,
regulations and guidelines not listed here. If you have any questions regarding compliance with
national standards, ordinances and directives for your country, contact your Thermo Fisher Scientific
sales organization.

Thermo Scientific DIONEX IC Pure vii


Preface
Standards and directives

viii DIONEX IC Pure Thermo Scientific


1

Safety Precautions

Observe these safety precautions for your own safety!

DIONEX IC Pure is a modern water purification system intended only for the
treatment of potable water or water of ASTM Type II quality. The water it produces
is not intended for drinking.

Work may only be performed on the unit electronics when the unit has been
switched off and when ESD protection is in place. Only specially trained personnel
may work on the unit‘s electronics.

• Do not install or operate the unit until you have carefully read through these operating
instructions and the notes and notices contained therein.
• Lifting and carrying the Thermo Scientific Dionex IC Pure system, e.g. to the installation location,
should be carried out by two people. To do this, lift the unit in tandem at the two corner points
beneath the bottom plate.
• The CE mark is not longer valid if you make any structural changes to the unit or install products
from other manufacturers in/on the unit.
• Protect the system from frost. The temperature at the installation area must be between +2 °C and
+40 °C.
• Always observe the applicable, pertinent codes and regulations valid at the installation location of
the unit and follow all applicable accident prevention regulations.
• When an external tank filling station is used, the feedwater pressure must be at least 0.1 bar (1.45
PSI) and a maximum of 4 bar (58 PSI). An additional pressure reducer must be installed should it
be higher.
• A low pressure black check valve is recommended to prevent back flow of feedwater from water
system based on DIN EN 171:2011
• A grounded 100-240V, 50/60Hz electrical outlet must be available (see 'Technical Specifications'
on page 13).

Thermo Scientific DIONEX IC Pure 1


1 Safety Precautions

• Access to the power supply cord and plug must never be restricted or obstructed.
• Unplug the system from the power outlet for all maintenance performed on the system.
• An atmospherically vented floor drain with a nominal diameter of at least 63 mm (2.48 inch)
(DN50 tube) must be present at the installation location. If no drain is provided it is
recommended that a water detector is installed for safety reasons (for European specifications
only). Failure to provide this will release the manufacturer from liability for any water-induced
damage that may result.
• Proceed as follows if the unit is not to be operated for an extended period, e.g., over extended
weekend, or during a vacation period:
• Switch the system off (unplug the mains plug).
• Close the feedwater inlet (close the feedwater tap).
Damage to the pump may occur if the unit were to run without any supply of feedwater. The
manufacturer will not accept any liability should this occur.
• The surface or wall on which the unit is to be installed or mounted must have an adequate
load-carrying capacity (check the capacity and stability of the wall). The dry weight of the unit is
given under 'Technical Specifications' on page 13. When the internal tank is filled, the unit has a
weight during operation of approx. 32 kg / 70.55 lbs.
• The surface on which the unit is installed must be level and stable. A max. 2% deviation from
evenness is recommended not to be exceed.
• When installing the water purification unit, always ensure that there is adequate space all around
the unit (see 'Technical Specifications' on page 13) to ensure that ease of use or easy replacement of
materials (e.g., filter change, connection) is accessible at all times.
• Visually inspect the unit at regular intervals. Clean up any water or spills found around the unit
immediately.

Never look directly into a switched-on UV-lamp, as UV-light endangers eyesight!

To avoid the risk of pinching, crushing, cutting or electrical shock, never perform
maintenance on the unit without its protective housing, or while it is in operation.
Maintenance work on the unit may only be performed by factory trained and
authorized specialists.

2 DIONEX IC Pure Thermo Scientific


1 Safety Precautions

.
• Wear safety gloves when working with disinfectant solutions.
• If your skin should come into contact with a chlorine product, rinse it immediately with ample,
fresh water.
• The unit, or system components, may generate heat as a result of a defect. It is recommended to
always wear appropriate safety gloves to prevent skin damage or burns.

• Wear safety gloves when working with disinfectant solutions.


• If your eyes come into contact with a chlorine product, rinse them immediately with ample,
fresh water and contact a physician at once.

• To avoid tripping, ensure that the tubings do not lay over the floor.
• Apply the general rules of hygiene for laboratories when working with the system.
• Do not use any oxidative cleaning agents for cleaning the system as this may cause damage to the
unit.
• Proceed as follows when the unit has a defect:
• Switch the system off and unplug the unit from outlet.
• Shut off the supply of feedwater.
• Contact your local service organization.

Thermo Scientific DIONEX IC Pure 3


1 Safety Precautions

4 DIONEX IC Pure Thermo Scientific


2

Spare parts and tools

Positions Spare parts DIONEX IC Pure

Figure position spare parts

3 7

5
9

8 6
1 0

1 6

1 4
1 5

2 3

1 7

1 3

2 2
1 8
1 9

2 1

2 0

1 2
1 1

Thermo Scientific DIONEX IC Pure 5


1 Spare parts and tools

Overview spare parts DIONEX IC Pure


Figure overview spare parts

1
3

5
2

7
8 6 9

1 0
4
4

1 1

1 3
1 2 1 5
2 3

1 7
1 4

1 6
2 2

1 9
1 8
2 0
2 1

6 DIONEX IC Pure Thermo Scientific


1 Spare parts and tools

Part number Describtion


1. 50132730 Keyboard display sticker
2. 50132289 Display front part
3. 50134036 Display holder
4. 50142984, 50142982 Tank indicator, sticker for tank indicator
5. 17.0147 Display back part
6. 50134032 Rotary knob
7. 26.0025 Control Display part
8. 50133988 Dispensing valve
9. 50142245 CPC coupling bodies 1/4“
10. 16.0006 Quick connector 1/4“ with barrier
11. 15.0113 Concentrate adjust valve
12. 50133992 TOC measuring cell
13. 50133992 Ultra pure water measuring cell
14. 50133996 Quick connector for d8 mm tube
15. 50149264 Pressure booster pump
16. 50142981 Sensor for tank indicator
17. 50131190 Solenoid valve
18. 50142246 Pressure hold valve
19. 16.0126 Feedwater measuring cell
20. 50143154 Fuse holder
50150714 Fuse

21. 50150598 Check valve 1 bar

22. 50143195 UV booster unit

23. 50131346 Control interface part

Thermo Scientific DIONEX IC Pure 7


1 Spare parts and tools

Position spare parts external 20L Tank


Figure position spare parts

2 7 2 6

2 4

2 8
2 5

Overview spare parts external 20L tank

Figure overview spare parts

2 5
2 8

2 4
2 6
2 7

8 DIONEX IC Pure Thermo Scientific


1 Spare parts and tools

Part number Describtion


24. 50143200 Niveau electronic for automatically niveau filling
25. 50131190 Solenoid valve
26. 50132981 Sensor for tank indicator
27. 50148086 Float switch
28. 50148086 Float switch
29. 50145876 Wire jumper (not shown)
30. 50143964 Wire jumper (not shown)

Additionally required parts you need for replacing spare parts

• 18.0036 PE tube D8 mm (0.31 in)


• 18.0044 one ear clamp for D8 mm (0.31 in) tube

You need for press in the one ear clamp a special pliers with torque control.

• Teflon tape
• cable ties small to attach wires

Requirement tools for changing Spare parts


To facilitate the exchange of spare parts is described in this chapter which tolls are
needed.

Thermo Scientific DIONEX IC Pure 9


1 Spare parts and tools

Chapter Tools
'Replacing Display Control part,' on • Phillips screwdriver
page 43 • Screwdriver for slotted head screws, size 0.4 x 2.5 mm
• extension
• ratchet
• socket wrench for M3 threaded hexagon nut
• An ESD protection
'Replacing the Interface' on page 45 • Phillips screwdriver
• Screwdriver for slotted head screws, size 0.4 x 2.5 mm
• extension
• ratchet
• socket wrench for M3 threaded hexagon nut
• An ESD protection
'Replacing the UV ballast' on page 47 • Screwdriver for slotted head screws, size 0.4 x 2.5 mm
• Phillips screwdriver
• An ESD protection
'Replacing solenoid valve' on page 51 • Magnetic Phillips screwdriver
• Screwdriver for slotted head screws, size 0.4 x 2.5 mm
'Replacing feedwater measuring cell' on • Magnetic Phillips screwdriver
page 52 • Screwdriver for slotted head screws, size 0.4 x 2.5 mm
• Waterpump pliers
• Teflon tape
• Precision conductivity meter for feedwater
• An ESD protection
• D8 mm tubes
'Replacing Ultra pure water measuring • Magnetic Phillips screwdriver
cell' on page 53 • Screwdriver for slotted head screws, size 0.4 x 2.5 mm
• Precision conductivity meter for ultra pure water
• 1/4“ ratchet, 1/4“ extension
• 1/4“ socket wrench size 8
• double open ended spanner size 8
• double ended spanner size 17
• An ESD protection
• D8 mm tubes
'Replacing TOC measuring cell' on • Magnetic Phillips screwdriver
page 55 • Screwdriver for slotted head screws, size 0.4 x 2.5 mm
• 1/4“ ratchet, 1/4“ extension
• 1/4“ socket wrench size 8
• double open ended spanner size 8
• double ended spanner size 17
• An ESD protection

10 DIONEX IC Pure Thermo Scientific


1 Spare parts and tools

Chapter Tools
'Replacing the pressure Booster pump' • Long magnetic Phillips screwdriver
on page 57 • Screwdriver for slotted head screws, size 0.4 x 2.5 mm
• double open ended spanner size 8
• double open ended spanner size 22
• An ESD protection
'Replacing pressure hold valve' on • Magnetic Phillips screwdriver
page 59 • double open ended spanner size 8
'Adjust the pressure for “to pump“ and • Pressure adjustment kit Part No.: 50151154
“to suppressor“ outlets' on page 62 • One vessel for catch the water
• Double open ended spanner size 10/11
'Adjust the concentrate flow' on page 65 • Vessel for catch water (max. volume 200ml)
• Slot screw driver
'Replacing tank indicator' on page 66 • Magnetic Phillips screw driver
'Replacing the fuse from additional tank • Screwdriver for slotted head screws, size 0.4 x 2.5 mm
indicator' on page 67 • An ESD protection
'Replacing tank indicator sensor on
system' on page 68
'Replacing tank indicator sensor on
external 20L tank' on page 69

Thermo Scientific DIONEX IC Pure 11


1 Spare parts and tools

12 DIONEX IC Pure Thermo Scientific


3

Technical Specifications
Feedwater requirements
Model System with pretreatment cartridge System without pretreatment cartridge
Source Tap water according to DIN 2000:2000 Pretreated water (ASTM Type II)
Silt density index (SDI) <3 -- (not applicable)
Conductivity (reference 1200 μS/cm (0.0008 M·cm) < 1 μS/cm or > 1 M·cm
temperature +25 °C)
Free chlorine max. 0.1 ppb Max. 0.05 ppb
Manganese content max. 0.05 ppm -- (not applicable)
Iron content max. 0.2 ppm -- (not applicable)
pH range 4 - 11 4 - 11
TOC value < 2000 ppb max. 50 ppb
Bacteria count < 100 CFU/ml < 100 CFU/ml
Turbidity < 1.0 NTU < 1.0 NTU
Carbon dioxide (CO2) max. 30 ppm max. 30 ppm
Silicate max. 30 ppm max. 3 ppm
Temperature +2°C - +35°C +2°C - +35°C
Pressure for automatic 0.1 - 6 bar /1.45 - 87 PSI (at a pressure > 6 -- (not applicable)
filling bar / 87 PSI a pressure reducer must be
installed upstream of the unit. Pressure
reducer before recirculation pump has to be
adjusted to 25 psi.
Product water quality
Conductivity (reference temperature +25 °C) 0.055 μS/cm/ 18.2 M·cm
Resistance up to18.2 M·cm
TOC value max. 5 ppb
RNase < 0.003 ng/ml
DNase < 0.4 pg/ul
Bacteria < 1 CFU/ml
Bacterial endotoxines 0.1 EU/ml
Particles > 0.2 μm per ml <1
Flow rate without pretreatment cartridge at manually 0.6 l/min +/- 0.2 l min
operated POU
Flow rate with pretreatment cartridge at manually 0.2 l/min +/- 0.2 l min
operated POU
Dimensions and weight of DIONEX IC Pure with ultra pure cartridge
Height 550 mm 21.65 inch
Width 306 mm 12.05 inch
Depth 385mm 15.16 inch
Base area 277 x 372 mm 10.91 x 14.65 inch

Thermo Scientific DIONEX IC Pure 13


5 Technical Specifications

Dimensions and weight of DIONEX IC Pure with ultra pure cartridge


Weight including ultra pure cartridge 26 kg 57.2 lbs
Weight with full tank 32 kg 70.55 lbs
550

Fig.8
306 385
Dimensions and weight of external 20L tank with level control
Height 490 mm 19.29 inch
Width 190 mm 7.48 inch
Depth 485 mm 19.09 inch
Base area 340 x 483 mm 13.39 x 7.48 inch
Weight of dry tank 7 kg 18.07 lbs
Weight with full tank 27 kg 60 lbs
490

485 190 Fig.9

14 DIONEX IC Pure Thermo Scientific


5 Technical Specifications

Cell constants of the measuring cells


Feedwater conductivity 0.16 cm-1
Conductivity TOC 0.01 cm-1
Ultra pure conductivity 0.01 cm-1
Water connections DIONEX IC Pure
Feedwater tubing 8 mm / 0.31 inch o.d.
Rinse water tubing 8 mm / 0.31 inch o.d.
Connection to pump IC 30PSI 8 mm/ 0.31 o.d. on 1/8“ coupling
Connection to pump IC 3 PSI 8 mm/ 0.31 o.d. on 1/8“ coupling
Water connections for external 20L tank
Feedwater tubing 8 mm/ 0.31 inch o.d.
Return tubing 8 mm/ 0.31 inch o.d.
Water connections for external 20L tank with level control
Feedwater tubing 8 mm/ 0.31 inch o.d.
Tank overflow tubing 8 mm/ 0.31 inch o.d.
Electrical connections for DIONEX IC Pure and external 20L tank with level control
Input voltage AC 100 – 240 V, 50 – 60 Hz, 5 – 3.8 A
Output voltage DC 24 V, 3.8 A
System connection DC 24 V, 80 W
Protection class Class II (external SMPS certified as Class I)
Materials of parts which contact water
Adjustable pressure retaining valve NBR = Acrylnitril Butadien Rubber
Pump head Nylon with glass fibre
UV lamp High-purity synthetic quartz
UV Housing Stainless steel
Ultra pure cartridge PP = Polyethylene
UF Housing PC = Polycarbonate
Rinsing solenoid valve PA = Polyamide
Dispensing valve PET = Polyethyleneterephthalate
Conductivity measuring cell POM = Polyoxymethylen, Stainless steel
Distributor block POM = Polyoxymethylen
Connections POM = Polyoxymethylen
tubings PE = Polyethylene
O-Rings EPDM = Ethylene propylene diene rubber
Accessibility to DIONEX IC Pure and 20L tank
Space on left and right from the side of the unit at least 300 mm / 11.81 inch
Space to the back of the unit at least 200 mm / 7.87 inch
Top space at least 400 mm /15.75 inch
Space to front of unit Free accessibility

Thermo Scientific DIONEX IC Pure 15


5 Technical Specifications

Ambient conditions for DIONEX IC Pure and tank filling station


During operation Storage
Use Indoor rooms Indoor rooms
Height up to 2000 m up to 2000 m
Temperature range min. +2°C, max +35°C, 80% rel. rH, min. +2 °C, max. +60 °C, 90% rel. rH, non
non-condensing condensing
Line-voltage variation Not more than +/- 10 % of the line voltage -- (not applicable)
Transient overvoltages As usually occur in the supply network -- (not applicable)
(overvoltage category II acc. to IEC
60364-4-443) Note: The rated level of
transient overvoltage is the withstand
impulse voltage acc. to overvoltage category
II of IEC 60364-4-443.
Ventilation requirements no special requirements no special requirements
Degree of dust pollution 2 2

Airborne sound emission


Sound pressure level 49 db(A)

16 DIONEX IC Pure Thermo Scientific


4

Controls

Description of control display

Resistance value of the Indicates the TOC value.


Indicates the
current operating pure water
status of the unit

Temperature
measurement

Display for ON/OFF status,


temperature, resistance
For activating the
indicator and operating
NONSTOP mode for
status of the UV lamp.
sampling, for increasing
the numeric values in the

On/Off switch
Confirm the
program and
selection.

The Menu button provides access to the following


system parameters:
For activation of the UV button enables manual
• Feedwater limiting value INTERVAL mode, for operation of the UV lamp.
decreasing of numeric The desired value can be
• Ultra pure water limiting value
values in the menu changed in the Mode menu.
• UV-Lamp operating time and intensity
• Cartridge number and maintenance interval
• Rinsing
• Disinfection
• Display of fault storage
• Unlocking of the factory default settings using a
password

Thermo Scientific DIONEX IC Pure 17


4 Controls

Flow chart system control

Flow chart RWS-Control


Nonstop 96ppb
18.2 Mё·cm
18.5°C UV/TC

or
Interval
18.2 Mё·cm
18,5°C UV/TC

Menu key Menu+UV key

Interval+Nonstop key UV+Interval key

Feedwater OEM Menu Calibration Menu UV Menu


0.10 μS/cm Press enter Resistances ? Press enter
Limit value feed Press enter
2.0 μS/cm

Error display OEM Menu Calibration Menu UV Menu


Standby: Off Max. temp. Temperature Duration
Lim. val.pure w. 50 °C 10000 3000 h
0.2 μS/cm

UV Time OEM Menu Calibration Menu UV Menu


0000 h Rinse time Cell const. LF1 Intensity
enu or Enter key

UV Intensity 30 sek 0.0100 1/cm Off


80%

Ser. No. OEM Menu Calibration Menu Run Time


Cartridge Disinfect. time Cell const. LF2 Cartridge
Press Enter! 30 min 0.160 1/cm _450 Days
Step up by the menu levels with the menu

00000/12

Rinse ? OEM Menu Calibration Menu New UV lamp?


Press enter Pump interval Cell const. LF3 Press enter
05 min. ( 0.0100 1/cm )
auto calib.

Disinfection OEM Menu Calibration Menu


Press enter Rinse interval TOC value
0.5 sek 1000

Error history OEM Menu Calibration Menu


Press enter Day 30 Month 12 Error display
Year 2004 05 min
Hours 12 Min.30

Data printout OEM Menu Calibration Menu


Press enter Send interval Default values?
01:00 h:min Press enter

Code OEM Menu Calibration menu


Press enter Language Volume Control
____ English Yes

OEM Menu
μS/cm - Mȍ cm
μS/cm If the Dionex IC Pure system is connected
with the Dionex ICS systems about the con-
OEM Menu
Temp. comp. trol cable, it will appears in the Display Ana-
On
lyzer. In this mode there it is not possible to
OEM Menu
switch into the Interval mode.
Genpu. UV UF TOC
S.No.: 9999/12
SW Version 4.1

18 DIONEX IC Pure Thermo Scientific


4 Controls

Unlocking the system control

• Refer to the IC Pure Water Purification system Operator‘s manual for detailed
system control instructions under the ‘System Control‘ chapter.
• You need for unlock all levels of the system control a “All levels“ code.

To prevent unauthorized access to the settings and factory presetting, changes to settings can only be
made when a correct code number from the following Table is entered and confirmed with 'ENTER.
The unlocking is then active for a 5 minute period.
Press the 'Menu' key nine times. The display shows:

Code
Press enter
0000

To prevent unauthorized access to the settings and factory presettings, changes to settings can only be
made when a correct code number from the following Table is entered and confirmed with 'ENTER'.
Existing programs are given on three levels. The first level provides access only to the Menu level. A
second level provides access only to the Menu and OEM menu levels and a third level provides access
to all three levels.
Code no.:
No. Menu No. Menu + OEM menu No. All levels
1 0150 4 0450 7 0750
2 0250 5 0550 8 0850
3 0350 6 0650 9 0950


When you press the 'Menu' button the tenth time you exit the user menu and the
unit automatically resumes its last operating mode ('NONSTOP'/'INTERVAL' or
'Analyzer' mode).

Operating modes
• Interval mode after switching on the unit
• NONSTOP mode
• INTERVAL mode
• Analyzer mode
• OFF mode

Thermo Scientific DIONEX IC Pure 19


4 Controls

Calibration menu

When the code number for unlocking has been entered, the calibration menu can be called by
simultaneously
pressing the UV-key and the INT.-key. The Press enter! menu prompt appears. Confirm
this with Enter to come to the first sub-menu. Each further press on the menu-key brings you to the
next sub-menu.
• Changes must be confirmed with the Enter-key, otherwise none of them will be
saved.
• Refer to the chapter 'Description of control display' on page 17 to see what
buttons you can change the values.

Calibration of the microcontroller

The momentary resistances measured at the conductivity and temperature measuring cells by the
microcontroller are displayed here. This sub-menu is really only of interest to the manufacturer of the
controller to be able to reliably test the functioning of system control via fixed resistances.

Press the Menu key one time then the display shows:

Calibration Menu
Resistances?
Press enter

Setting the temperature sensor


The conductivity measurement for ultra pure water is equipped with a PT 1000 temperature sensor.
The unavoidable manufacturing tolerances of this are balanced out by means of a calibration factor.
Basic setting: 10000
Setting range:
Typical setting range: 09990 - 10010

Set values that are far outside of the typical setting range are not a problem as long as
the system works perfectly according to a reference instrument.
Such values occasionally indicate that the particular sensor could have a problem that
requires an exact test of the functioning of it, however.
Press the Menu key two times, then the display shows:

Calibration Menu
Temperature
10000

20 DIONEX IC Pure Thermo Scientific


4 Controls

Setting cell constant LF1 (Pure water measuring cell)


The cell constant of each conductivity measuring cell is determined prior to installing it and this cell
constant must be entered in the microcontroller, for this to be able to determine the conductivity from
the measured resistance.
Basic setting: 0.01
Setting range: 0.0050 - 0.0200
Typical setting range: 0.0085 – 0.0095

Set values that are far outside of the typical setting range are not a problem as long as
the system works perfectly according to a reference instrument.
Such values occasionally indicate that the particular sensor has a problem that
requires an exact test of the functioning of it, however.
Press the menu key three times, then the display shows:

Calibration Menu
Cell const. LF1
0,0100 1/cm

Setting cell constant LF2 (Feedwater measuring cell)


Basic setting: 0.16
Setting range: 0.05 - 0.3
Typical setting range: 0.12 - 0.20

The measuring cell is switched off when the cell constant is set to above 0.3. In this case „Off“ is then
shown in the display.

Set values that are far outside of the typical setting range are not a problem as long as
the system works perfectly according to a reference instrument.
Such values occasionally indicate that the particular sensor has a problem that
requires an exact test of the functioning of it, however.
Press the menu key fourth times, the display shows:

Calibration Menu
Cell const. LF2
0,160 1/cm

Thermo Scientific DIONEX IC Pure 21


4 Controls

Setting cell constant LF3 (TOC measuring cell)


The cell constant of measuring cell LF 3 has three different operating functions.
1. Cell constant off:
Use the arrow key to set it above the maximum of the setting range.
2. Cell constant on (this setting is not recommended):
The cell constant must be entered manually here. It must be previously correctly measured
and documented at a different location.
e.g.: By installing the measuring cell intended for installation as LF3 at the position LF1, as
well as correspondingly making connection of the wiring to the terminals for LF1. The cell
constant can now be measured using a reference instrument and via the calibration menu for
LF1. The measured values are to be subsequently simply transferred to LF3 and the
originally intended connection and wiring are re-made.
3. Cell constant auto (recommended setting):
Set this with two presses on the ? arrow key.
Measuring cell LF 1 is used as reference measuring cell. The cell constant of measuring
cell LF3 is automatically calculated and adjusted during circulation in Interval operation.

Basic setting: auto

Press the menu key five times, then the display shows:

Calibration Menu
Cell const. LF3
( 0,0100 1/cm )
auto calib.

Matching the TOC measurement


The TOC calibration factor enables the TOC-value displayed in the main display to be matched.
An exact calibration of the conductivity measuring cell enables a much more precise result to be
obtained in a much simpler way, however.
A separate calibration of the TOC-value is not recommended as it could have a negative effect on the
precision of the measurement.

Basic setting: Calibration factor: 1000


Setting range: 100 - 10000

Press the menu key six times, then the display shows:

Calibration Menu
TOC value
1000

22 DIONEX IC Pure Thermo Scientific


4 Controls

Error suppression
Water purification systems generally need time for the measured and displayed values to stabilize
subsequent to a change in the operating state.
The fault suppression time enables faults to be verified, so that only “genuine” faults are displayed that
still exist as such after the expiry of the suppression time.
When, after a change in the operating state, exceeded limiting values swing to below the set limit
within the set suppression time, the system recognizes this and does not consider such temporary
excesses to be a fault.

Basic setting: 1min


Setting range: 1- 10 min

Press the menu key seven times, then the display shows:

Calibration Menu
Error display
1 min

Restore to Initial Calibration values


In this menu, all settings can be returned to their default values.

This is not a “Factory setting” in the sense of a return to the “First set values” which
were factory calibrated!
This menu prompt returns system control back to the state it was in on delivery prior
to the first calibration. If you set back to the starting values, therefore, you must carry
out a complete new calibration of the measuring cells and enter new settings for all
basic settings and limiting values!

We so expressly warn against calling the starting values!


Press the menu key eight times, then the display shows:

Calibration Menu
Default values
Press enter

Thermo Scientific DIONEX IC Pure 23


4 Controls

Volume control

Not important for this system while Volume control not available for this system.
Ignore this point and press the menu key against to prompt to the next one.

Press the menu key nine times, then the display shows:

Calibration Menu
Volume Control
Yes

Leaving calibration menu


Press the menu key ten times, then the display shows the last chooses operating mode.( Intervall,
Nonstop, Analyzer)

UV-menu
• This menu is relevant if the operation hours counter or the filter cartridge
operating hours counter needs to be changed.
• In the operating instructions for the customer, the UV-lamp is declared as a
consumable and can be replaced by the customer.
• If the customer requests a service call to replace the UV-lamp, refer to the
Operator‘s manual under the Chapter ‘Change UV-lamp‘.

Simultaneous pressing of the menu-key and the UV-key calls the UV-menu.
The limiting values for the operating time of the UV-lamp and intensity monitoring can be set in this
menu. The “UV-time” fault message appears in line 4 of the display when the limiting value for the
UV-lamp operating time is exceeded.
As the UV-lamp is an option, a value higher than 10000 h must be entered in systems without this
option to switch the UV-lamp operating time off. The word “off” is then shown in the display.
When a UV-intensity value of 40% is set, evaluation of the UV-lamp is switched off and the word
“off” is shown in the display.
In this menu, the UV-lamp operating time counter can be set back to zero and the UV-lamp intensity
can be set to 100%.
To do this, and with the UV-lamp switched on, measure the UV-intensity for as long as it takes for the
measured value for the UV-intensity to remain stable. The word message “Please wait” is shown in the
display during the required time.

24 DIONEX IC Pure Thermo Scientific


4 Controls

Setting the limiting value for the UV operating hours counter


The limiting value is switched off when a setting higher than 10000 h is entered. The word “off” is
then shown in the display.
Basic setting: 3000 h, 80%
Setting range: 1000- 10000 h, 40-100%

Press the Menu key one times, then the display shows:

UV-Menu
Duration
3000h

Setting the limiting value for the UV intensity measurement

• These setting are not important for the system. There is not an accessory UV-
Sensor on the UV reactor.
• Make sure that the UV- intensity is switched off.

Basic setting: 50%


Setting range: 40-100%
Monitoring is switched off by entries above 40%.

Press the Menu key two times, then the display shows:

UV-Menu
Intensity
Off

Filter cartridge operating hours counter


Basic setting: 450 days
Setting range: 100- 1000 days
Monitoring is switched off when a setting longer than 1000 days is entered. The word “off” is then
shown in the display.

Press the Menu key three times, then the display shows:

Run Time
Cartridge
450 Days

Thermo Scientific DIONEX IC Pure 25


4 Controls

Reset the operating hours counter and measuring in a new UV- lamp
Confirmation of this menu prompt with Enter sets the UV-lamp operating time counter back to zero.
The UV-lamp is simultaneously switched on and measured in over a period of from 5 min. to 2 h. The
maximum intensity is determined during this time and is defined to be the 100% value. The system
always assumes here that the UV-lamp is a new one. Please do not use UV-lamps which have already
been put to use here, as the 100% value would then be wrongly defined. This would result in an
incorrect evaluation and so to an inadequate water quality.
When measuring in has been completed, the system returns to the Interval operating mode.

Press the Menu key four times, then the display shows:

New UV lamp?
Press enter

26 DIONEX IC Pure Thermo Scientific


5

Calibration

In the Calibration Menu, a cell constant is only set to provide the system with a
factor for the exact calculation of each individual measured value, so that the
complete measuring range is covered by a single factor per measuring cell.
Inaccuracies such as those which inevitably occur with individual fixed points are so
avoided.
The Calibration Menu must always be quit for the comparison and evaluation of the
actual measured values of the system with the reference instrument, provided that
calibration has been completely carried out or a further adjustment is required.

• Allow the system to warm up or to cool down to room temperature before


starting with calibration. It is recommend a cool down or warm up time up to
24h.
• You must be calibrate the different measuring cells only when a measuring cell
has experienced damage or any values of them are not correctly is shown on the
display.

To reach exact conductivity and temperature values in the calibration, carry


calibration of these out in this succession (pages listed reference this manual):
• Ultra pure water measuring cell LF1:

• Calibrate the temperature ((see chapter “Setting the temperature sensor”


on page 20)
• Calibrate the conductivity(see chapter (“Setting cell constant LF1 (Pure
water measuring cell)” on page 21)
• Feedwater measuring cell LF2:
• Calibrate the conductivity (see chapter “Setting cell constant LF2
(Feedwater measuring cell)” on page 21)
• TOC measuring cell LF3:
• Calibration is not necessary for the TOC measuring cell as it measures
unassisted. For this, though, ultra pure water measuring cell LF1, as
reference measuring cell, must be exactly calibrated.

Thermo Scientific DIONEX IC Pure 27


5 Calibration

Set up for calibrating ultra pure water measuring cell LF1


• Work may only be performed on the unit electronics when the unit has been
switched off.
• Unplug the power supply from the power outlet on the system.
• Take caution to ensure that the suitable power outlet and electronic components
do not get wet. Risk of an electric shock.
• Take caution that you have enough space by the system for the maintenance
work.

Step Action
The following steps are necessary to prepare to
1) calibrate the ultra pure water measuring cell.
1. Release the pressure by turning the rotary
knob on the dispensing valve.

Rotary
knob
• To prevent that water flows on the surface where
the system is stand on, place a container under the
3) water tap.
2. Remove the cartridge cover and the filter
cartridge. (see Operating instruction Chapter
Change filter cartridge)
3. Locate the ultra pure water measuring cell
and the ultrafilter.(see Fig. 51)
4. Remove the D8 mm tube from the 2 Fittings
by pressing retreat of the black ring on the
fitting and simultaneously pulling in and out
Pure water mea- Ultra filter
of the tube.(see Fig.52)
suring cell Fig.51

4)
Black ring

• Fig.53 on the next side shows you the flow


connections of the external conductivity meter
LR325/001.
• If you have another external conductivity meter,
the connections may be differ from the device
described in Fig.53 on the next side.

Fig.52

28 DIONEX IC Pure Thermo Scientific


5 Calibration

Step Action

5. Plug in one D8 mm tube into the inlet of the


external conductivity meter and the other end
into the top fitting of the ultra filter.(see Fig.
54)
6. Take a second D8 mm tube for connect the
External con-
ductivity meter- outlet of the external conductivity meter with
LR 325/001 the top fitting of the pure water measuring
cell.(see Fig.54)

• Before switching the system on, check the content


of the internal 5L tank or external 20L tank.
Outlet reference • If there not enough content in one of both tanks,
measuring cell Inlet feedwater refill them with Tap water, when a pretreatment
reference mea- cartridge is used in the system.
suring cell • If not a pretreatment cartridge in use and only a
filter cartridge, refill the tank with ASTM Type II
water.
Fig.53 • Check that the ICS system does not pump water
5) from the ICPure.
7. Plug in the power supply to the power inlet
from the system.

Out ultra-
pure water

Pure water mea-


suring cell

In ultrapu-
re water
Ultra filter Fig.54

Thermo Scientific DIONEX IC Pure 29


5 Calibration

Calibration of the ultra pure water measuring cell LF1 with temperature
• Calibration (comparative measurement) requires a measuring instrument which is highly
accurate and measures conductivities to three places after the decimal point. The cell constant of
the connected measuring cell should be 0.01
• The ultra pure water system must be in the Nonstop-mode for comparison measurements,
otherwise the reference conductivity meter will not show any relevant measured values.
• Description of the Calibration Menu see under chapter “Setting the temperature sensor” on
page 20.

Calibrate the temperature


Step Action

2)

Code
Code • Notice the value of the temperature on the
Press
Press enter
enter
0000 display from the system before you starting
0000 with the calibration.
1. Switch the system on.
3)
2. Press the menu button 9 times to arrive
the Code section.
3. Give in a „all level“ code to become
Code
Code access for all levels.
Press
Pressenter
enter
0000
0950
• To change the value use the „Nonstop and
Interval“ button. To get to the next digit use
4) the „UV button“.
4. After confirm with Enter you leave the
Code
Code Code
Nonstop 00ppb
Press Press enter „User menu“.
Pressenter
enter 18.2 MΩ∙cm
0000 0000
19.3 °C UV/TC
5. Press simultaneously the „Interval and
0950
UV“ key to arrive the Calibration Menu.
6. Press the „Menu“ key twice to jump to
5) the next calibration point in the
CodeMenu
Calibration Calibration Menu and adjust the
Press enter temperature value.
Resistance?
0000
Press enter

6) • To change the value use the „Nonstop and


Interval button. To get to the next digit use
CodeMenu
Calibration the „UV button“. Change the value in 5
Press enter
Temperature
0000 points to increase or reduce the value and
10000
confirm with „Enter“.
7. Leave after adjust the value the
Calibration
CodeMenu Calibration
CodeMenu
Press enter Press enter Calibration Menu by putting the
Temperature Temperature
0000
09995 0000
10005 „Menu“ key 8 times and control the
value of temperature on the Display with
or lower or higher the value of the reference instrument.(see
Fig.55 on next page)

30 DIONEX IC Pure Thermo Scientific


5 Calibration

Figure 55

Temperature value
agreement Display conductivity meter
Display System

18.2Mёͼcm
Nonstop000 ppb 11.7°C
…18.2Mёͼcm
18 2 Mё
….11.7°C..UV/TC
Menu02.02.2015
15:23

Fig.55

• If the values of both displays are not shown the same temperature, repeat the steps 2 - 6
as describe above.

Calibrate the ultra pure water measuring cell LF1

• Calibration (comparative measurement) requires a measuring instrument which is


highly accurate and measures conductivities to three places after the decimal point. The
cell constant of the connected measuring cell should be 0.01
• The ultra pure water system must be in the Nonstop-mode for comparison
measurements, otherwise the reference conductivity meter will not show any relevant
measured values.
• Description of the Calibration Menu see under “Setting cell constant LF1 (Pure water
measuring cell)” on page 21.

Thermo Scientific DIONEX IC Pure 31


5 Calibration

Step Action

2)

Code
Code • Notice the value of the MΩ·cm resistance on
Press
Press enter
enter
0000 the display from the system before you
0000 starting with the calibration.
1. Switch the system on.
3)
2. Press the menu button 9 times to arrive
the Code section.
3. Give in a „all level“ code to become
Code
Code access for all levels.
Press
Pressenter
enter
0000
0950
• To change the value use the „Nonstop and
Interval“ button. To get to the next digit use
4) the „UV button“.
4. After confirm with Enter you leave the
Code
Code Code
Nonstop 00ppb
Press Press enter „User menu“.
Pressenter
enter 18.2 MΩ∙cm
0000 0000
19.3 °C UV/TC
5. Press simultaneously the „Interval and
0950
UV“ key to arrive the Calibration Menu.
6. Press the „Menu“ key three times to
5) jump to the calibration point for the
CodeMenu ultra pure water measuring cell and
Calibration
Press enter
Resistance? adjust the value.
0000
Press enter
7. To change the value use the „Nonstop
and Interval button. To get to the next
digit use the „UV button“.
6)

CodeMenu
Calibration CodeMenu
Calibration
Press enter • Change the value in 2 points to increase or
Press enter
Resistance? Temperature
0000 0000
10000
reduce the value and confirm with „Enter“.
Press enter
8. Leave after adjust the value the
Calibration Menu by putting the
CodeMenu
Calibration
Press enter „Menu“ key 7 times and control the
Cell const. LF1
0000
0.0100 1/cm value of temperature on the Display with
the value of the reference instrument.(see
7) Fig.56 on next page)

CodeMenu
Calibration
CellPress
const.enter
LF1
0000
0.0100 1/cm

CodeMenu
Calibration Code Menu
Calibration
CellPress enter
const. LF1 CellPress enter
const. LF1
0000 0000
0.0098 1/cm 0.0102 1/cm

or lower or higher

32 DIONEX IC Pure Thermo Scientific


5 Calibration

Figure 56

Resistance value
agreement Display conductivity meter
Display System

18.2Mёͼcm
Nonstop000 ppb 11.7°C
…18.2Mёͼcm
18 2 Mё
….11.7°C..UV/TC
Menu02.02.2015
15:23

Fig.56

• If the values of both displays are not shown the same temperature, repeat the steps 2 - 8
as describe above.

Set up for feedwater measuring calibration

• Work may only be performed on the unit electronics when the unit has been
switched off.
• Unplug the power supply from the power outlet on the system.
• Take caution to ensure that the suitable power outlet and electronic components
do not get wet. Risk of an electric shock.
• Take caution that you have enough space by the system for the maintenance
work.

Thermo Scientific DIONEX IC Pure 33


5 Calibration

Step Action
The following steps are necessary to prepare to
1) calibrate the feedwater measuring cell.
1. Release the pressure by turning the rotary
knob in clockwise direction on the dispensing
valve.

Rotary
knob
• To prevent that water flows on the surface where
the system is stand on place a vessel under the
water tap.
2. Locate the connection panel and remove the
2)
tube jumper from the external 20L tank
outlet port on the panel from the system. .
Coupling
body
• There are coupling bodies on the tube jumper.
Press on the knob from the coupling body und
then you can remove the tube jumper.(see Fig. 57)
Tube
jumper
3. Remove the D8 mm tube of the tube jumper
from the internal tank outlet port of the panel
Coupling from the system by pressing retreat of the
body knob
black ring on the fitting and simultaneously
pulling in and out of the tube.(see Fig. 58)

Fig.57

3) • Fig.59 on the next side shows you the flow


connections of the external conductivity meter
Black ring LR325/001.

If you have another external conductivity meter, the


connections may be differ from the device described in
Fig.59 on the next side.

Tube
jumper

Fig.58

34 DIONEX IC Pure Thermo Scientific


5 Calibration

Step Action

4. Plug in one D8 mm tube into the inlet of the


external conductivity meter and the other end
into the outlet port internal tank outlet on
the panel.(see Fig. 60)
5. Take a second D8 mm tube and plug in a
External con-
ductivity meter- plug connector for D8 mm tube. After this
LR 325/001 put the plug in connector into the outlet port
external 20L tank inlet on the panel.(see
Fig.60)

• Before switching the system on, check the content


Outlet reference of the internal 5L tank.
measuring cell Inlet feedwater • If there not enough content in the tank, refill
reference mea- them with Tap water, when a pretreatment
suring cell cartridge is used in the system.
• If not a pretreatment cartridge in use and only a
filter cartridge, refill the tank with ASTM Type II
Fig.59 water.
4, 5) • Check that the ICS system does not pump water
from the ICPure.
6. Plug in the power supply to the power inlet
from the system.

Out feed-
water

D8 mm tubes

plug connec- In Fig.60


tor feedwater

Thermo Scientific DIONEX IC Pure 35


5 Calibration

Calibration of feedwater measuring cell LF2


• Calibration (comparative measurement) requires a measuring instrument which is
highly accurate and measures conductivities to three places after the decimal point. The
cell constant of the connected measuring cell should be 0.01
• The ultra pure water system must be in the Nonstop-mode for comparison
measurements, otherwise the reference conductivity meter will not show any relevant
measured values.
• When your system is working with a pretreatment cartridge and your feedwater quality
have a to high hardness (see “Technical Specifications” on page 13), adjust the feedwater
measuring cell off in the Calibration Menu.
• Description of Calibration Menu see under chapter “Setting cell constant LF2
(Feedwater measuring cell)” on page 25.

Step Action

2) 1. Switch the system on.


2. Press the menu button 9 times to arrive
Code
Code
Press the Code section.
Press enter
enter
0000 3. Give in a „all level“ code to become
0000
access for all levels.
3)
• To change the value use the „Nonstop and
Interval“ button. To get to the next digit use
Code
Code the „UV button“.
Press
Pressenter
enter 4. After confirm with „Enter“, you leave the
0000
0950 „User menu“.
5. Press the menu button once to see the
feedwater value in MΩ∙cm and notice it.
4)

Code
Code Code
Nonstop 00ppb
Press Press enter • When your system is working with a
Pressenter
enter 18.2 MΩ∙cm
0000 0000 pretreatment cartridge and your feedwater
0950 19.3 °C UV/TC
quality have a to high hardness (see
“Technical Specifications” on page 13), adjust
5) the feedwater measuring cell „off“ in the
„User menu“ with the „Nonstop and
Code
Feedwater Interval“ key and confirm with „Enter“.
Press
1.25 enter
MΩ∙cm
0000 feed
Limit value 6. Press simultaneously the „Interval and
2.0 µS/cm UV“ key to arrive the Calibration Menu.
6)
CodeMenu
Calibration
Press enter
Resistance?
0000
Press enter

36 DIONEX IC Pure Thermo Scientific


5 Calibration

Step Action

7) 7. Press the „Menu“ key 4 times to jump to


the calibration point for the feedwater
CodeMenu
Calibration CodeMenu
Calibration
Press enter Press enter measuring cell and adjust the value.
Resistance? Temperature
0000 0000
Press enter 10000 8. To change the value use the „Nonstop
and Interval“ button. To get to the next
CodeMenu
Calibration CodeMenu digit use the „UV button“.
Calibration
Press enter
Cell const. LF2 Press enter
0000 Cell const. LF1
0.0160 1/cm 0000
0.0100 1/cm
• Change the value in 2 points to increase or
8) reduce the value and confirm with „Enter“.
CodeMenu
Calibration 9. Leave after adjust the value the
CellPress
const.enter
LF2 Calibration Menu by putting the
0000 „Menu“ key 6 times.
0.0160 1/cm
10. Press the „Menu“ key once and control
the value of temperature on the Display
Code Menu
Calibration CodeMenu
Calibration
Press enter Press enter with the value of the reference
Cell const. LF2 Cell const. LF2
0000 0000 instrument.(see Fig.61)
0.0158 1/cm 0.0162 1/cm

or lower or higher
10)

NonstopCode
00ppb Code
Feedwater
Press
18.2 enter
MΩ∙cm Press
1.25 enter
MΩ∙cm
0000 UV/TC 0000 feed
Limit value
19.3 °C
2.0 µS/cm

Figure 61

Display System Resistance value Display conductivity meter


agreement

Feedwater 1.2518.2
MΩ∙cmMёͼcm
Nonstop000 ppb
1.25 MΩ∙cm
…18.2Mёͼcm
18 2 Mё 19.311.7°C
°C
….11.7°C..UV/TC
Limit value feed
Menu02.02.2015
2.0 µS/cm 15:23

• If the values of both displays are not shown the same resistance, repeat the steps 2 - 10 as
describe above.

Thermo Scientific DIONEX IC Pure 37


5 Calibration

Calibration of TOC measuring cell LF3


• Your system additional have an TOC measurement cell to measure the TOC proportion
in the pure water in ppb.
• This is only necessary for you to calibrate the TOC measurement cell if you have
replaced the TOC measuring cell. (see “Replacing TOC measuring cell” on page 55)

Step Action

2) 1. Switch the system on.


Code
Code
Press 2. Press the menu button 9 times to arrive
Press enter
enter
0000 the Code section.
0000
3. Give in a „all level“ code to become
3) access for all levels.
Code
Code
Press
Pressenter
enter
0000
0950 • To change the value use the „Nonstop and
Interval“ button. To get to the next digit use
4) the „UV button“.
Code
Code Code
Nonstop 00ppb
Press 4. After confirm with „Enter“, you leave the
Pressenter
enter Press
18.2 enter
MΩ∙cm
0000 0000 „User menu“.
0950 19.3 °C UV/TC
5. Press simultaneously the „Interval and
5) UV“ key to arrive the Calibration Menu.
CodeMenu
Calibration
Press enter
Resistance? 6. Press the „Menu“ key 5 times to jump to
0000
Press enter the calibration point for the TOC
measuring cell and adjust the value.
6) 7. To change the value use the „Nonstop
CodeMenu
Calibration CodeMenu
Calibration
Press enter
Resistance?
Press enter
Temperature and Interval“ button. To get to the next
0000 0000
Press enter 10000 digit use the „UV button“.

CodeMenu
Calibration CodeMenu
Calibration
Press enter Press
Cell enter
const. LF1
• Adjust the TOC measurement cell to the
Cell const. LF2 0000
0000
0.0160 1/cm 0.0100 1/cm value „auto calib.“
8. Leave after adjust the value the
CodeMenu
Calibration Calibration Menu by putting the
Press enter
Cell const.
0000
LF3 „Menu“ key 5 times.
(0.0100 1/cm)

CodeMenu
Calibration
Cell const.enter
Press LF3
0000
(0.0100 1/cm)

Code
Calibration Menu
CellPress
const.enter
LF3
(0.0100 1/cm)
0000
auto calib.

38 DIONEX IC Pure Thermo Scientific


5 Calibration

Matching the TOC-measurement


Step Action
1. Switch the system on.
2) 2. Press the menu button 9 times to arrive
Code
Code
Press the Code section.
Press enter
enter
0000 3. Give in a „all level“ code to become
0000
access for all levels.
3)
Code
Code
Press • To change the value use the „Nonstop and
Pressenter
enter
0000 Interval“ button. To get to the next digit use
0950
the „UV button“.
4) 4. After confirm with „Enter“, you leave the
„User menu“.
Code
Code NonstopCode
00ppb
Press enter
5. Press simultaneously the „Interval and
Press
Pressenter
enter 18.2 MΩ∙cm
0000 0000 UV“ key to arrive the Calibration Menu.
0950 19.3 °C UV/TC
6. Press the „Menu“ key 6 times to jump to
5) the calibration point for the TOC
CodeMenu
Calibration
Press enter
Resistance? measuring cell and adjust the value.
0000 7. To change the value use the „Nonstop
Press enter
and Interval“ button. To get to the next
6) CodeMenu digit use the „UV button“.
CodeMenu
Calibration Calibration
Press enter Press enter
Temperature
Resistance? 0000
0000 10000
Press enter
• Adjust the TOC measurement to the value
CodeMenu
Calibration CodeMenu
Calibration „1000“.
Press enter
Cell const. LF2 Press enter
Cell const. LF1 8. Leave after adjust the value the
0000 0000
0.0160 1/cm 0.0100 1/cm
Calibration Menu by putting the
„Menu“ key 4 times.
CodeMenu
Calibration CodeMenu
Calibration
Press
Cell enter
const. LF3 Press enter
TOC value
0000 0000
(0.0100 1/cm) 0900

7)
CodeMenu
Calibration
Press
TOC value enter
0000
0900

CodeMenu
Calibration
Press
TOC value enter
0000
1000

Thermo Scientific DIONEX IC Pure 39


5 Calibration

Adjust the error suppression


Step Action
1. Switch the system on.
2) 2. Press the menu button 9 times to arrive
Code
Code
Pressenter
Press enter the Code section.
0000
0950 3. Give in a „all level“ code to become
3)
access for all levels.
Code
Code
Pressenter
Press enter
0000
0950
• To change the value use the „Nonstop and
4) Interval“ button. To get to the next digit use
Code
Code Code
Nonstop 00ppb
Pressenter
enter Press
18.2 enter
MΩ∙cm
the „UV button“.
Press 0000
0000
0950 19.3 °C UV/TC 4. After confirm with „Enter“, you leave the
„User menu“.
5) 5. Press simultaneously the „Interval and
Code Menu
Calibration
Press enter
Resistance? UV“ key to arrive the Calibration Menu.
0000
Press enter
6. Press the „Menu“ key 5 times to jump to
6) the calibration point for the TOC
Code Menu
measuring cell and adjust the value.
Calibration Code Menu
Calibration
Press enter
Resistance? Press enter
Temperature 7. To change the value use the „Nonstop
0000 0000
Press enter 10000 and Interval“ button. To get to the next
digit use the „UV button“.
Code Menu
Calibrtaion Code Menu
Calibrtaion
Press
Cell enter
const.LF2 Press
Cell enter
const.LF1
0000
0.0160 1/cm 0000
0.0100 1/cm
• Adjust the error suppression to the value „1
Code Menu Code Menu
min“.
Calibrtaion Calibrtaion
Press
Cell enter
const.LF3 Press enter
TOC value
0000
(0.0100 1/cm) 0000
0900 8. Leave after adjust the value the
Calibration Menu by putting the
„Menu“ key 3 times.
Code Menu
Calibrtaion
Pressdisplay
Error enter
0000
1 min

Restore to Initial Calibration Values

• This is not a “Factory setting” in the sense of a return to the “First set values” which
were factory calibrated!
• This menu prompt returns system control back to the state it was in on delivery prior to
the first calibration. If you set back to the starting values, therefore, you must carry out a
complete new calibration of the measuring cells and enter new settings for all basic
settings and limiting values!
• We so expressly warn against calling the starting values!

40 DIONEX IC Pure Thermo Scientific


5 Calibration

Step Action
1. Switch the system on.
2) 2. Press the menu button 9 times to arrive
Code
Code
Pressenter
Press enter the Code section.
0000
0950 3. Give in a „all level“ code to become
3)
access for all levels.
Code
Code
Pressenter
Press enter
0000
0950
• To change the value use the „Nonstop and
4) Interval“ button. To get to the next digit use
Code
Code Code
Nonstop 00ppb
Pressenter
enter Press
18.2 enter
MΩ∙cm
the „UV button“.
Press 0000
0000
0950 19.3 °C UV/TC 4. After confirm with „Enter“, you leave the
„User menu“.
5) 5. Press simultaneously the „Interval and
Code Menu
Calibration
Press enter
Resistance? UV“ key to arrive the Calibration Menu.
0000
Press enter
6. Press the „Menu“ key 5 times to jump to
6) the calibration point for the TOC
Code Menu
measuring cell and adjust the value.
Calibration Code Menu
Calibration
Press enter
Resistance? Press enter
Temperature 7. To change the value use the „Nonstop
0000 0000
Press enter 10000 and Interval“ button. To get to the next
digit use the „UV button“.
Code Menu
Calibrtaion Code Menu
Calibrtaion
Press
Cell enter
const.LF2 Press
Cell enter
const.LF1
0000
0.0160 1/cm 0000
0.0100 1/cm
• Do not confirm with enter, because all
Code Menu Code Menu
calibrated values from the systems interface
Calibrtaion Calibrtaion
Press
Cell enter
const.LF3
0000
Press
TOC enter
value are going back to the delivery settings.
0000
(0.0100 1/cm) 0900

Code Menu Code Menu


• The Volume control is a programmed
Calibrtaion Calibrtaion
Press enter
Default values Pressdisplay
Error enter
0000
ingredients of the system control and
0000
Press enter 1 min available for the DIONEX IC Pure system.
Ignore this point in the Calibration menu.
Code Menu
Calibrtaion
Press enter
Code
Nonstop 00ppb 8. Leave the Calibration Menu by putting
Volume control Press
18.2 enter
MΩ∙cm
0000
Yes 0000
19.3 °C UV/TC the „Menu“ key 2 times.

Thermo Scientific DIONEX IC Pure 41


5 Calibration

42 DIONEX IC Pure Thermo Scientific


6

Replacing Hardware Components


Replacing Display Control part,
• Work may only be performed on the unit electronics when the unit has been
switched off and when ESD protection is in place.
• Unplug the power supply for all maintenance work from the power outlet on the
system.
• Take caution to ensure that the suitable power outlet and electronic components
do not get wet. Risk of an electric shock.
• Take caution that you have enough space by the system for the maintenance
work

Step Action
The following steps are necessary to replace the display.
1)

1. Swivel the Display forward.(see Fig.10)

Swivel
display

Fig.10

Thermo Scientific DIONEX IC Pure 43


5 Replacing Hardware Components

Step Action

2. Remove the screws designated (a), (b), (c).(see


2) Fig.11)
a)

Fig.11
• Do not mix these up when subsequently the new
Display display.
back part
3. Remove the display back side from the display
holder.
c) b) 4. Remove the 40-pin cable plug from the post
socket of the display.(see Fig.12)

• Use an ESD protection on place to prevent a damage


from the display.

Display holder a) 5. Screw out the 4 hexagon nuts designated (d) and
move out the Display.(see Fig.12)

4), 5)
• Due the display foil from the front side, it would be
Display possible that the display is somewhat difficult to
remove.
• Move so be careful the display back and forth while
pulling.
• Do not forget to remove the protective foil from the
new display, before mount it.
d) 6. Carry out the installation of the new display in
d) the reverse succession to that describe above.
7. Connect the system back to the power supply and
switch the system on.
8. Program all parameters of the system in the
system control and save it.(see Operating
instruction Chapter Operating Elements)

Fig.12
40-pin cable plug

44 DIONEX IC Pure Thermo Scientific


5 Replacing Hardware Components

Replacing the Interface

• Work may only be performed on the unit electronics when the unit has been
switched off and when ESD protection is in place.
• Unplug the power supply for all maintenance work from the power outlet on the
system.
• Take caution to ensure that the suitable power outlet and electronic components
do not get wet. Risk of an electric shock.

Step Action
The following steps are necessary to replace the Interface.
1)
1. Screw out the 2 screws designated (a).(see Fig.13)
2. Remove the cover from the top side. (see Fig.14)
3. Remove the 40-pin cable plug and all other
electrical connectors from the interface socket.(see
Fig.15 and Fig.16)

• Use an ESD protection on place to prevent a damage


from the display.
Fig.13
a) rear panel 4. Screw out the 4 hexagon nut designated (b) and
move out carefully the interface.(see Fig.15 and
2)
Fig.16)

• Do not touch with fingers on the top and under side


from the interface
Cover
5. Carry out the installation of the new display in
the reverse succession to that describe above.
Fig.14
6. Connect the system back to the power supply and
switch the system on
3,4)

Interface

b)
b)

40-pin
cable
Fig.15
plug

Thermo Scientific DIONEX IC Pure 45


5 Replacing Hardware Components

Step Action

Overview cable plugs connector Interface.


X2
X3

• Terminal assignment of the cable plugs connector for


Interface see “Terminal Assignment DIONEX IC
X4
pure” on page 75.

X1

X6

X5
Fig.16
40 pin cable plug connector

46 DIONEX IC Pure Thermo Scientific


5 Replacing Hardware Components

Replacing the UV ballast


• Work may only be performed on the unit electronics when the unit has been
switched off and when ESD protection is in place.
• Unplug the power supply for all maintenance work from the power outlet on the
system.
• Take caution to ensure that the suitable power outlet and electronic components
do not get wet. Risk of an electric shock.

Step Action
The following steps are necessary to replace the
2) UV-ballast.

• Use an ESD protection on place to prevent a damage


Cable plug
from the display.
connectors
UV ballast 1. Build up described in Chapter “Replacing the
Interface” on page 45, the interface.

Fig.17 2. Remove all electrical connectors from the UV-


ballast socket.(See Fig.17 and Fig.19)
3. Screw out the 2 screws designated (a) and move
Push here to pull out out carefully the UV-ballast.(see Fig 18)
the connecting wires
from the UV ballast. 4. Carry out the installation of the new UV-ballast
in the reverse succession to that describe above.
5. Connect the system back to the power supply and
switch the system on.
Push here to pull out
the connecting wires
from the UV ballast.

3)

a)

Fig.18

Thermo Scientific DIONEX IC Pure 47


5 Replacing Hardware Components

Step Action

Overview Terminal assignment UV-ballast.

• Terminal assignment of the UV- ballast see“Terminal


Assignment DIONEX IC pure” on page 75.
1
2
3
4
ElektronischesVorschaltgerät
ELEKTRONIKGERA
TypLTͲUVC1116ͲF/M24VDC
Typ LT UVC 1116 F/M 24V DC
24VDC

Fig.19
46
4 6

48 DIONEX IC Pure Thermo Scientific


7

Replacing Spare parts

• Work may only be performed on the unit electronics when the unit has been
switched off.
• Unplug the power supply for all maintenance work from the power outlet on the
system.
• Take caution to ensure that the suitable power outlet do not get wet. Risk of an
electric shock.
• Take caution that you have enough space by the system for the maintenance
work

Overview screws rear side


Step
rear panel

D D
Part no. and quantity of screws:
A 8x = 21.0128
B 3x = 21.0129
C 1x = 21.0133
A DifferentScrews D 4x = 21.0110

B

A C B D

D
C

Fig.20
D

Thermo Scientific DIONEX IC Pure 49


7 Replacing Spare parts

Explosion drawing system rear side

Step

1
3
B

Fig.21

B
1 = rear panel internal 5L tank
2 = Internal 5L tank with ring
3 = rear panel device
4 = Connection panel
5 = System IC Pure

A
Connecting
screws rear
panel device
Screws from connec-
tion panel to rear Part no. screws
panel device 2x 21.0110

Part no. screws:


2x 21.0076

Fig.23
Fig.22

50 DIONEX IC Pure Thermo Scientific


7 Replacing Spare parts

Replacing solenoid valve

• Unplug the power supply for all maintenance work from the power outlet on the
system.
• Take caution to ensure that the suitable power outlet do not get wet. Risk of an
electric shock.
• Take caution that you have enough space by the system for the maintenance
work

Step Action
The following steps are necessary to replace the solenoid
5) valve.
Solenoid valve

• Empty the rest content of the internal 5L tank. (see


Operating instructions IC Pure, chapter Drain
content of tank)
• Unplug the power supply from the power outlet on
Black the system.
rings • Do not mix up the screws from the rear panel. (see
chapter“Overview screws rear side” on page 49
1. Disassemble the rear panel from the internal 5L
tank. (see “Overview screws rear side” on page 49)
2. Place the internal 5L tank with ring backwards on
Fig.24
the surface.
3. Remove the cartridge cover and the Filter
7) cartridge from the system.(see operating
instructions, chapter change the filter cartridge)
4. Locate the solenoid valve.
5. Remove the d8 mm tubing by pressing retreat of
the black rings on the solenoid valve and
simultaneously pulling in and out of the tube.(see
a) Fig.24)
6. Disconnect the electrical wire from the solenoid
valve.
7. Locate the 2 screws from the solenoid valve
designated (a) on the right side of the system near
the Ultra pure water measuring cell and screw
them out.(see Fig.25)

Fig.25 8. Carry out the installation of the new solenoid


Ultra pure water measuring cell valve in the reverse succession to that describe
above.
9. Connect the system back to the power supply and
switch the system on.

Thermo Scientific DIONEX IC Pure 51


7 Replacing Spare parts

Replacing feedwater measuring cell


• Unplug the power supply for all maintenance work from the power outlet on the
system and when ESD protection is in place.
• Take caution to ensure that the suitable power outlet do not get wet. Risk of an
electric shock.
• Take caution that you have enough space by the system for the maintenance
work

Step Action
The following steps are necessary to replace the feedwater
4) measuring cell.
a)

• Use an ESD protection on place to prevent a damage


from the interface.
1. Proceed as described in chapter “Replacing
solenoid valve” on page 51 before but the tubings
can be attached to the valve.
Holder 2. Locate the holder with included feedwater
measuring cell and unscrew the 2 screws
designated (a).(see Fig.26)
Feedwater
measuring 3. Remove the cover from the systems interface.(see
cell “Replacing the Interface” on page 45)
4. Disconnect the electrical wire connectors from
Fig.26
the Interface position X5 3/4 and pull out the
7) wire from the feedwater measuring cell through
the housing.
5. Hold with one hand the holder and turn out in
Holder clockwise direction (see Fig.27) the feedwater
measuring cell with the other hand.
6. Carry out the installation of the new feedwater
measuring cell in the reverse succession to that
describe above.
7. Connect the system back to the power supply and
switch the system on.
8. Calibrate the feedwater measuring cell. (see
“Calibration” on page 27)

Fig.27
Feedwater
measuring
cell

52 DIONEX IC Pure Thermo Scientific


7 Replacing Spare parts

Replacing Ultra pure water measuring cell


• Unplug the power supply for all maintenance work from the power outlet on the
system and when ESD protection is in place.
• Take caution to ensure that the suitable power outlet do not get wet. Risk of an
electric shock.
• Take caution that you have enough space by the system for the maintenance
work

Step Action
The following steps are necessary to replace the Ultra pure
6) water measuring cell.

• Use an ESD protection on place to prevent a damage


from the interface.
1. Remove the cartridge cover and the filter
Ultra pure cartridge.(see Operating instruction Chapter
water mea- Change filter cartridge)
suring cell
2. Remove the cover from the systems interface.(see
“Replacing the Interface” on page 45)
3. Disconnect the electrical wire connectors from
TOC mea-
suring cell the Interface position X5 1/2.
Fig.28 4. Remove the rear panel and the internal 5L tank
a) with ring as described in Chapter “Replacing
solenoid valve” on page 51.
5. Pull out the wire from the Ultra pure water
measuring cell through the housing.
6. Locate the Ultra pure water measuring cell and
unscrew the 2 screws designated (a).(see Fig.28)

• The screws are screwed from the inside of the system


Feedwater with hexagon nuts designated (b) against and must be
measuring kept up. You will found them on the inside of the
cell system near the feedwater measuring cell.(see Fig.29)
Fig.29 Part no. and quantity of screws and hexagon nuts:

b) • a) 2x = 21.0043
• b) 2x = 21.0037

Thermo Scientific DIONEX IC Pure 53


7 Replacing Spare parts

Step Action

6) 7. Unpackaged the new Ultra pure water measuring


cell and mount the with supplied fittings into the
cell.(see Fig.30)
Male
connector
14.0405
Male thread
D8 mm • Disassemble one male connector Fitting D8 mm from
connector
14.0075 1/4“, the used Ultra pure water measuring cell for using
D8 mm onto the new measuring cell.
8. Carry out the installation of the new feedwater
measuring cell in the reverse succession to that
describe above.
9. Connect the system back to the power supply and
switch the system on.
10. Calibrate the Ultra pure water measuring cell. (see
“Calibration” on page 27)

• The part number 14.0297 should be tighten to a


torque of max. 1.5 Nm with a special tool.

Male
Male thread
connector
connector
14.0039
14.0297 1/8“,
Fig.30 D8 mm
D8 mm

54 DIONEX IC Pure Thermo Scientific


7 Replacing Spare parts

Replacing TOC measuring cell

• Unplug the power supply for all maintenance work from the power outlet on the
system and when ESD protection is in place.
• Take caution to ensure that the suitable power outlet do not get wet. Risk of an
electric shock.
• Take caution that you have enough space by the system for the maintenance
work

Step Action
The following steps are necessary to replace the TOC
6) measuring cell.

Use an ESD protection on place to prevent a damage from


the interface.
1. Remove the cartridge cover and the filter
Ultra pure
water mea- cartridge.(see Operating instruction Chapter
suring cell Change filter cartridge)
2. Remove the cover from the systems interface.(see
“Replacing the Interface” on page 45)
3. Disconnect the electrical wire connectors from
the Interface position X5 5/6.
TOC mea-
suring cell 4. Remove the rear panel and the internal 5L tank
with ring as described in Chapter “Replacing
Fig.31
solenoid valve” on page 51.
a)
5. Pull out the wire from the TOC measuring cell
through the housing.
6. Locate the TOC cell and unscrew the 2 screws
designated (a).(see Fig.31)

Feedwater • The screws are screwed from the inside of the system
measuring with hexagon nuts designated (b) against and must be
cell
kept up. You will found them on the inside of the
system near the feedwater measuring cell.(see Fig.32)

Part no. and quantity of screws and hexagon nuts:


• a) 2x = 21.0043
Fig.32 • b) 2x = 21.0037
b)

Thermo Scientific DIONEX IC Pure 55


7 Replacing Spare parts

Step Action

6) 7. Unpackaged the new Ultra pure water measuring


cell and mount the with supplied fittings into the
cell.(see Fig.33)
Male
8. Carry out the installation of the new feedwater
connector
14.0405 measuring cell in the reverse succession to that
Male thread describe above.
D8 mm
connector
14.0075 1/4“, 9. Connect the system back to the power supply and
D8 mm switch the system on.
10. Calibrate the TOC measuring cell. (see
“Calibration” on page 27)

• The part number 14.0297 should be tighten to a


torque of max. 1.5 Nm with a special tool.

Male
Male thread
connector
connector
14.0039
14.0297 1/8“,
Fig.33 D8 mm
D8 mm

56 DIONEX IC Pure Thermo Scientific


7 Replacing Spare parts

Replacing the pressure Booster pump


• Unplug the power supply for all maintenance work from the power outlet on the
system and when ESD protection is in place.
• Take caution to ensure that the suitable power outlet do not get wet. Risk of an
electric shock.
• Take caution that you have enough space by the system for the maintenance
work

Step Action
The following steps are necessary to replace the pressure
5) booster pump.

Use an ESD protection on place to prevent a damage from


the interface.
a) 1. Remove the cartridge cover and the filter
cartridge.(see Operating instruction Chapter
Change filter cartridge)
2. Remove the cover from the systems interface.(see
“Replacing the Interface” on page 45)
Rear panel
3. Disconnect the electrical wire connectors from
system
the Interface position X1 4/6.
4. Remove the rear panel and the internal 5L tank
Fig.34 with ring as described in Chapter “Replacing
solenoid valve” on page 51.
5. Disassemble the rear panel of the
system.Therefore unscrew the screws designated
(a) and (b).(see Fig.34 and Fig 35)
6. Disassemble the solenoid valve and the feedwater
measuring cell. (see “Replacing solenoid valve” on
b) page 51 Fig.25 and “Replacing feedwater
measuring cell” on page 52 Fig.26)

Fig.35
Connection
panel

Thermo Scientific DIONEX IC Pure 57


7 Replacing Spare parts

Step Action

7) 7. Locate the pressure booster pump and remove one


of the 2 D8 mm tubing by pressing retreat of the
black ring on the fitting and simultaneously
pulling in and out of the tube.(see Fig.24)
8. Pull out the wire from the pressure booster pump
through the housing.
9. Locate the 2 screws on the mounting panel near
D8 mm tube
the Ultra pure water measuring cell and screw
them out.(see Fig.37)

Booster • Fixed with one Hand the pressure booster pump from
pump the inside of the system. Thereby you prevent that the
pressure booster pump not suddenly fall down.
10. Pull out the second D8mm tube from the
pressure booster pump by pressing retreat of the
Fig.36
black ring on the fitting and simultaneously
9) pulling in and out of the tube and remove the
pump.

c)

Fig.37
Ultra pure water me-
asuring cell

58 DIONEX IC Pure Thermo Scientific


7 Replacing Spare parts

Step Action

11) 11. Disassemble the lock rings and Fittings from the
pressure booster pump and mount it onto the
new one. (see Fig.38).
Locking
Fitting rings Fitting
D8 mm D8 mm
• To facilitate to moving out the fittings use an size 8
double open ended spanner by pushing in the spanner
between the plugged into each other fittings.
12. Carry out the installation of the new pressure
booster pump in the reverse succession to that
describe above.
13. Connect the system back to the power supply and
switch the system on.

Fig.38

Replacing pressure hold valve

• Unplug the power supply for all maintenance work from the power outlet on the
system.
• Take caution to ensure that the suitable power outlet do not get wet. Risk of an
electric shock.
• Take caution that you have enough space by the system for the maintenance
work
• After installation a new pressure hold valve you must adjust the pressure with a
pressure gauge. If not any adjustment tool on place you have the possibility to
order the pressure adjustment kit from Thermo Fisher Scientific.

Thermo Scientific DIONEX IC Pure 59


7 Replacing Spare parts

Step Action

1)
Pressure hold valves The following steps are necessary to replace the pressure
hold valves.

1. Remove the rear panel and the internal 5L tank


with ring as described in Chapter “Replacing
solenoid valve” on page 51.
a)
2. Locate the pressure hold valve on the right outside
of the system and unscrew the screws designated
(a).(see Fig.39)
a)
3. Pull out the 2 D8mm tube from the pressure hold
valve by pressing retreat of the black rings on the
fitting and simultaneously pulling in and out of
the tube.(see Fig. 40)

Fig.39

3)

Fig.40
Pressure hold valve
D8 mm tubes

60 DIONEX IC Pure Thermo Scientific


7 Replacing Spare parts

Step Action

1)
Male connector D8 mm

4. move out the pressure hold valve and pull out the
2 fittings as described in Step 3 with the tubes.

• To facilitate to moving out the fittings use an size 8


double open ended spanner by pushing in the spanner
between the plugged into each other fittings.
5. Plug in the fittings as shown in Fig.41 for the
pressure hold valve “to suppressor“. If you are
changing the pressure hold valve for “to pump“
plug in the fittings as shown in Fig.42.
Fig.41
Pressure hold valve for
suppressor ICS
• The arrow on the pressure hold valve shows you the
flow direction. It must be shown upstairs.
6. Carry out the installation of the new pressure
Male connector D8 mm
hold valve in the reverse succession to that
describe above.
7. Connect the system back to the power supply and
switch the system on.

• After installation of a new pressure hold valve, you


must adjust the pressure new on the outlets of “to
pump“ and “to suppressor“ on the connection panel
of the system.

Male connector D8 mm

Fig.42

Pressure hold valve for


pump ICS D8 mm tubes

Thermo Scientific DIONEX IC Pure 61


7 Replacing Spare parts

Adjust the pressure for “to pump“ and “to suppressor“ outlets
• Take caution to ensure that the suitable power outlet do not get wet. Risk of an
electric shock.

• Take caution that you have enough space by the system for the maintenance
work
• After installation a new pressure hold valve you must adjust the pressure with a
pressure gauge. Use the “Pressure adjustment kit“ with part no. 50151154 to
adjust both pressure hold valves V4 and V3.
• The new setting of the pressure must be performed if subsequently a
pretreatment cartridge is installed or a pretreatment cartridge was retrofitted.
• Control the pressure onto the V3 and V4 outlets if a ultrapure cartridge or
pretreatment cartridge was changed.
• By change of pressure on a valve the pressure on the other one the second valve is
also changed. Both pressures on the valves are dependent from the respective
adjusted pressure on the valves.

Content of “ Pressure adjustment kit“


Pressure Kit 1, 0-1,6 bar

Pressure gauge 0-1,6 bar

Quick connector

Precision metering valve

Quick connector
Pressure kit 2, 0-6 bar

Pressure gauge 0-1,6 bar

62 DIONEX IC Pure Thermo Scientific


7 Replacing Spare parts

Step Action
1. Switch the system off and disconnect the control
2) cable on the connector “Ion Chromatograph“ of
Connection for control cable the connection panel.
2. Locate the 2 pressure outlets on the connection
Connection panel panel.(see Fig.43)
3. Plug in the Pressure Kit 1 into the pressure outlet
“to pump“ (see Fig. 44). Proceed the same way
with the pressure kit 2 for the pressure outlet “to
suppressor“ on the connection panel.

• For the next steps you need a vessel to catch the water
coming out from the „to pump“ outlet.
4. Switch the system on and bring the Dionex IC
Pure system into the Nonstop mode.
5. Turn the adjustment knob from the pressure hold
Fig.43
Pressure outlets to pump 3 psi V4
valve 4 until you see at the pressure gauge that the
pressure value increase.
Pressure outlets to suppressor 30 psi V3
6. Turn the adjustment screw on the precision
metering valve in clockwise direction until only a
3)
few drops flows at the end of the 1/8“ tube from
“to pump“ connection IC Pure system
the pressure kit 1 into the vessel.

Pressure Kit 1
• It doesn‘t matter how many drops in a certain time
comes out of the end of the 1/8“ tube. To adjust the
V4 valve, a slight flow from water must be ensured.
• If there are bubbles in the water line of V3, rinse the
IC Pure system as described in the operating
instructions.

“to suppressor“ connection IC Pure system 7. Adjust the pressure on V4 to the value of 30 psi
(see Fig.45).
8. Adjust the pressure on V3 to the value of 3 psi
Pressure Kit 2 (see Fig.45).
9. Control after adjust V3 the value of V4. If there is
not anymore showing the 30 psi, adjust it again to
the correct value.

Fig.44 • Action 7 - 9 should be repeated until the correct


values are reached as following on the next pages
notes.

Thermo Scientific DIONEX IC Pure 63


7 Replacing Spare parts

Step Action

7)
Increase pressure on V3

Reduce pressure on V4 • To increase the pressure on the pressure adjustment


valve V4 turn the adjustment knob in anti clockwise
direction. To reduce the pressure turn the adjustment
knob in clockwise direction.
• To increase the pressure on the pressure adjustment
valve V3 turn the adjustment knob in clockwise
direction. To reduce the pressure turn the adjustment
knob in anti clockwise direction.

• The pressure should be adjust on the “to pump“ outlet


to a value of min. 3 PSI/ 0.2 + 0.2 bar.
Increase pressure on V4 Reduce pressure on V3
• The pressure should be adjust on the „“to suppressor“
outlet to a value of 30 PSI/ 2 bar ± 0.4 bar.

10. If the adjustment of the pressure on the pressure


hold valves V4 and V3 finished, fix the
adjustment knob with the lock nut on the
pressure hold valves.

Fig.45

8)
Lock nuts

Double open ended spanner size 10/11

Fig.46

64 DIONEX IC Pure Thermo Scientific


7 Replacing Spare parts

Adjust the concentrate flow

• Unplug the power supply for all maintenance work from the power outlet on the
system and when ESD protection is in place.
• Take caution to ensure that the suitable power outlet do not get wet. Risk of an
electric shock.
• Take caution that you have enough space by the system for the maintenance
work
• The concentrate back flow must only adjust when the IC Pure system is
operating with a pretreatment cartridge or a external 20 L Tank without level
control is connect or a pretreatment cartridge was retrofitted.
• Make sure that the pressure on the V3 and V4 valves are adjust to the
requirement values.

Step Action

2) Connection panel IC Pure 1. Switch the system off.


2. Remove the tube with quick disconnect from the
left concentrate connection on the IC Pure
connection panel and route the o.d 8 mm (31 in)
concentrate tube (supplied with the unit) to the
drain.(Fig. 47)
Concentrate connections
3. If the external 20 L tank is connect pull out the
IC Pure system
concentrate tubing from the left connection of
Concentrate tube with quick the control housing of 20 L tank. (Fig. 48)
disconnect o.d 8 mm (31 in)
Fig.47 4. Switch the system on and choose the Nonstop
mode on the system control.
3) Control housing
external 20 L tank 5. Take the open end of the concentrate tubing into
the vessel and catch for 36 sec. the concentrate
water.

Concentrate
connection
external 20 L • Write down the value of content in the vessel.
tank
• The amount of concentrate back flow should be a
Fig.48
have value of 70 ml ± 10 ml/ 36 sec.
4)
Concentrate flow valve 6. Use a slot screw driver to turn the adjustment
Fig.49
screw from the concentrate flow valve (located on
the front side from IC Pure system) in clockwise
direction to reduce the concentrate flow and in
anti clockwise direction to increase the
Place for pretreatment
cartridge concentrate flow.
7. Remove action 1 - 5 until the amount of 70 ml ±
10 ml/ 36 sec of concentrate flow has reached.

Thermo Scientific DIONEX IC Pure 65


7 Replacing Spare parts

Replacing tank indicator


• Unplug the power supply for all maintenance work from the power outlet on the
system and when ESD protection is in place.
• Take caution to ensure that the suitable power outlet do not get wet. Risk of an
electric shock.
• Take caution that you have enough space by the system for the maintenance
work

Step Action
The following steps are necessary to replace the tank
1) indicator.
a)

Use an ESD protection on place to prevent a damage from


the tank indicator.
1. Locate the tank indicator on the front side of the
system and unscrew the 4 screws designated
(a).(see Fig.47)
Tank in- 2. Pull the tank indicator back and disconnect all
dicator electrical wires from the pins.(see Fig.48)

• The completely terminal assignment of the tank


indicator you will find under chapter “Terminal
Fig.50 assignment additional tank indicator” on page 76.
a)
3. Carry out the installation of the new tank
indicator in the reverse succession to that describe
above.
12/24 1 4. Connect the system back to the power supply and
VDC 2 switch the tank indicator on.
Tank Sign
TankSign. 4
Tank+ 5

• Verify the tank indicator with the content level of the


internal 5L tank or external 20L tank.
Fig.51 • If there any difference between tank indicator and
content level in the tank, adjust the tank indicator on
the tank indicator sensor. (see Operating instructions
Adapters Adjustment of the additional tank indicator)

66 DIONEX IC Pure Thermo Scientific


7 Replacing Spare parts

Replacing the fuse from additional tank indicator


• Unplug the power supply for all maintenance work from the power outlet on the
system and when ESD protection is in place.
• Take caution to ensure that the suitable power outlet do not get wet. Risk of an
electric shock.
• Take caution that you have enough space by the system for the maintenance
work.

The following steps are necessary to replace the fuse from the tank indicator.

Use an ESD protection on place to prevent a damage from the interface.


31. Disassemble the tank indicator as described in chapter “Replacing tank indicator” on page 66.
32. Pull the cable as far back until you see the fuse holder.
33. Turn off the fuse holder and replacing the fuse.
34. Carry out the installation of the new fuse in the reverse succession to that describe above.

Thermo Scientific DIONEX IC Pure 67


7 Replacing Spare parts

Replacing tank indicator sensor on system


• Unplug the power supply for all maintenance work from the power outlet on the
system and when ESD protection is in place.
• Take caution to ensure that the suitable power outlet do not get wet. Risk of an
electric shock.
• Take caution that you have enough space by the system for the maintenance
work.

Step Action
The following steps are necessary to replace the tank
1) indicator sensor on the system.

• Use an ESD protection on place to prevent a damage


from the tank indicator sensor.
1. Remove the cartridge cover and the filter
cartridge.(see Operating instruction Chapter
Change filter cartridge)
2. Locate the sensor for tank indicator near the cover
tank indica- plate and screw out the screw designated (a).(see
tor sensor Fig.49)
3. Move out the tank indicator sensor and unplug
the electrical wires from the pins.(see Fig.50)
Fig.52
a)

• The completely terminal assignment of the tank


3) indicator you will find under Chapter “Terminal
assignment additional tank indicator” on page 76.
4. Carry out the installation of the new tank
Voll indicator sensor in the reverse succession to that
describe above.
145

• After replacing the tank indicator sensor you must be


Sonde make a adjustment of the tank indicator. Therefore
look at the operating manual chapter Recalibrating
Ableiter
tank indicator sensor.

Fig.53

68 DIONEX IC Pure Thermo Scientific


7 Replacing Spare parts

Replacing tank indicator sensor on external 20L tank


• Unplug the power supply for all maintenance work from the power outlet on the
system and when ESD protection is in place.
• Take caution to ensure that the suitable power outlet do not get wet. Risk of an
electric shock.
• Take caution that you have enough space by the system for the maintenance
work.

Step StepAction
The following steps are necessary to replace the tank
1) indicator sensor on the external 20L tank.

• Use an ESD protection on place to prevent a damage


from the tank indicator sensor.

a)
1. Remove the cover from the control case by
unscrew the screws designated (a).(see Fig.51)
2. Locate the tank indicator sensor and screw out the
screw designated (b).(see Fig.52)
control case
3. Move out the tank indicator sensor and unplug
the electrical wires from the pins.(see Fig.48 on
page 68)

Fig.54 • The completely terminal assignment of the tank


indicator you will find under Chapter “Terminal
2) assignment additional tank indicator” on page 76.
4. Carry out the installation of the new tank
indicator sensor in the reverse succession to that
describe above.

• After replacing the tank indicator sensor you must be


make a adjustment of the tank indicator. Therefore
look at the operating manual chapter Recalibrating
tank indicator sensor.

Fig.55
b)

Thermo Scientific DIONEX IC Pure 69


7 Replacing Spare parts

70 DIONEX IC Pure Thermo Scientific


8

Troubleshooting

Fault Cause Remedy


The system does not start • No supply of power • Provide power
Dispensing not possible • Feedwater supply line for • Open the feedwater supply line
external tank filling station
closed
• Feedwater and rinse water • Replace connections
connections are mixed up
• Feedwater pressure < 0.1 bar • Increase feedwater pressure
• Sterile filter clogged • Replace the sterile filter
• Pretreatment cartridge • Install new pretreatment car-
blocked. tridge
Resistance < 18.2 M·cm • Poor feedwater • Correct the feedwater
• Temperature compensation • Activating temperature com-
deactivated, recalibration pensation ('TC' should appear
required in the display) Contact the ser-
vice organization for calibra-
tion
System control no longer reacts • Improper operation • Unplug the mains plug for 5
seconds.
Water flows out • Leaky hose connection • Check and seal the hose con-
nection
• Feedwater pressure > 6 bar • Install a pressure reducer
(external tank filling station
only)
Dispensed water flow rate is too • UF-Module blocked • Replace UF-module
low • Initial pressure too low • Set the pressure regulator
(external tank filling station
only)
• Internal pressure too low • Readjust pressure reducer
• Dispensed water flow rate • Control pretreatment cartridge
out of the tolerance range

Thermo Scientific DIONEX IC Pure 71


8 Troubleshooting

Fault Cause Remedy


Display of TOC content • UV lamp not broken in / • Replace the UV lamp and reset
permanently at 99 ppb counter reset the operating hours counter
• TOC measuring cell defec- • Replace the TOC measuring
tive cell
No analyzer is indicated at the • Settings in OEM menu are • Make settings in the OEM
ICpure unit for operation with incorrect menu
an analyzer. • Activate ICS
• ICS not activated
• Cable to IC not connected • Connect the cable to the ICS
• Cable break • Replace the cable
Wrong time or date • Time zone • Reset time and date
• Summer/winter time • Reset summer/winter time
Wrong language • Wrong language set • Correct language setting
Fault message: • Feedwater conductivity too • Check the feedwater measur-
'Limit value feed' high ing cell and deactivate in the
menu
• Limiting value set too low • Check and suit the limiting
value
Display indicates +IN • Measuring cell cable break • Replace measuring cell
Fault message: • Filter cartridge exhausted • Replace filter cartridge
'Pur.limit' • Check and suit the limiting
value
• Limiting value set too low
Fault message: • UV lamp operating time has • Replace the UV lamp)
'UV-time' been exceeded • Reset the operating time
counter
Fault message: • The temperature in the sys- • Switch the unit off and let it
'max.Temperature' tem is too high cool down
• Interval pump time too long • Reduce interval pump time
• Limiting value set too low • Check and suit the limiting
value
• Feedwater temperature too • Reduce feedwater temperature
high
Fault message: • Measuring cell cable break • Replace measuring cell
'Measuring cell LF1' • System control defect • Replace system control
• Conductivity of ultra Ultra • Adjust measuring cell or
pure outside measuring range replace it
Fault message: • Measuring cell cable break • Replace measuring cell
'Measuring cell LF2' • System control defect • Replace system control
• Feedwater conductivity out- • Adjust measuring cell or
side measuring range replace it

72 DIONEX IC Pure Thermo Scientific


8 Troubleshooting

Fault Cause Remedy


Fault message: • Measuring cell cable break • Replace measuring cell
'Measuring cell LF3' • System control defect • Replace system control
Fault message: • Measuring cell cable break • Replace measuring cell
'Measuring cell Temp.' • System control defect • Replace system control
Fault message: • Filter cartridge operating • Replace with new filter car-
'New Filter cartridge' time has expired tridge

Thermo Scientific DIONEX IC Pure 73


8 Troubleshooting

74 DIONEX IC Pure Thermo Scientific


9

Terminal Assignment and Flow chart

Terminal Assignment DIONEX IC pure

Thermo Scientific DIONEX IC Pure 75


9 Terminal Assignment and Flow chart

Terminal assignment additional tank indicator

76 DIONEX IC Pure Thermo Scientific


9 Terminal Assignment and Flow chart

Terminal assignment level control 20L tank

Thermo Scientific DIONEX IC Pure 77


9 Terminal Assignment and Flow chart

Terminal assignment wire jumper

78 DIONEX IC Pure Thermo Scientific


9 Terminal Assignment and Flow chart

Terminal assignment control wire DIONEX IC pure to 20L tank

Thermo Scientific DIONEX IC Pure 79


9 Terminal Assignment and Flow chart

Flow charts

Flow chart DIONEX IC Pure

80 DIONEX IC Pure Thermo Scientific


9 Terminal Assignment and Flow chart

Flow chart DIONEX IC Pure with 20L tank

Thermo Scientific DIONEX IC Pure 81


9 Terminal Assignment and Flow chart

Flow chart DIONEX IC pure with 20L tank and level control

82 DIONEX IC Pure Thermo Scientific


Eluent in

EGCVent

ICS 2100

Thermo Scientific
OverͲ
flow

4 Suppressor line
REGENIN

3 1 2
1
Schematic illustration with connected Suppressor

Connectionpanel Dionex ICPure Waste Precision


system: metering
Eluent in valve
1 To pump3psi
9

2 To suppressor 30psi

3 Drain

4 Tankoverflow

Note:

DIONEX IC Pure
1 TubingfromCDcelloutshouldberoutedtowaste
• PressurerestrictorcoilsarerequiredtobeinstallattheCDcelloutlet.

83
Terminal Assignment and Flow chart
9

84
Eluent line

Tee

DIONEX IC Pure
EGCVent EGCVent

nt line
Overflow

Eluen
Terminal Assignment and Flow chart

1 2 1 1
3

Waste

Connectionpanel Dionex ICPure Tee


system: Precision
1 To pump3psi metering
valve
2 To suppressor 30psi Suppressor line
REGENIN
3 Drain
Suppressor line Precision
4 Tankoverflow REGENIN metering valve

Note:
1 TubingfromCDcelloutshouldberoutedtowaste
• PressurerestrictorcoilsarerequiredtobeinstallattheCDcelloutlet.

Thermo Scientific
ICPureconnectedwithDionexICSͲ4000system

ICS 4000

Thermo Scientific
Eluent line

Overflow

2
1
3

Waste
Connectionpanel Dionex ICPure
system:
Suppressor line
1 To pump3psi REGENIN
9

2 To suppressor 30psi
Precision
3 Drain metering valve

4 Tankoverflow
1

Note:

DIONEX IC Pure
1 TubingfromCDcelloutshouldberoutedtowaste

85
Terminal Assignment and Flow chart
9

86
Overflow

DIONEX IC Pure
El
Eluent
t line
li
Terminal Assignment and Flow chart

Precision
4 metering valve
Tee
Suppressor line
l
REGENIN
2
3
1
Waste

Tee
1

Eluent line

Precision
metering valve

Suppressor line
REGENIN

Connectionpanel Dionex ICPure


system:

1 To pump3psi

2 To suppressor 30psi
1
3 Drain

4 Tankoverflow
Note:
1 TubingfromCDcelloutshouldberoutedtowaste

Thermo Scientific
ICS 5000+

Thermo Scientific
Connectionpanel Dionex ICPure
system:

1 To pump3psi

2 To suppressor 30psi
Eluent in
3 Drain
Overflow
4 Tankoverflow

4
3

2
Waste
1

Precisionmetering 1
valve
9

Suppressorline
REGENIN

Note:
1 TubingfromCDcelloutshouldberoutedtowaste
• PressurerestrictorcoilsarerequiredtobeinstallattheCDcelloutlet.

DIONEX IC Pure
87
Terminal Assignment and Flow chart
9

88
ICPureconnectedwith2DionexICSͲ5000+ systems
Eluent line

Precision
metering valve

DIONEX IC Pure
Overflow
Terminal Assignment and Flow chart

Suppressor line
REGENIN
2
1 Tee
3

Waste

Connectionpanel Dionex ICPure


Eluent line
system:
Tee
1 To pump3psi

2 To suppressor 30psi

3 Drain

4 Tankoverflow

Preciision
meteering valve
Suppressor line
REGENIN

Note:
1 TubingfromCDcelloutshouldberoutedtowaste
• PressurerestrictorcoilsarerequiredtobeinstallattheCDcelloutlet.

Thermo Scientific
10

·cmMaintenance record

Customer address: Location:


System type:
Serial no.:
Year made:

Date Feedwater UltraUltra Temperature TOC value UV-intensity UV-lamp


 resistance pure   operating
 resistance  time
[MΩ·cm] [MΩ·cm] [°C] [ppb] [%] [h]

Ultra Ultra
Last change  Last 
pure volume
of filter cleaning / Notes Signature
flow
cartridge disinfection
[l/h]

Thermo Scientific DIONEX IC Pure 89


10 ·cmMaintenance record

90 DIONEX IC Pure Thermo Scientific


I

Index

A Enquiries from Latin America iv


Accessibility to DIONEX IC Pure and 20L tank 15 Enquiries from North America iv
Additionally required parts you need for replacing spare erminal assignment control wire DIONEX IC pure to 20L
parts 9 tank 75
Adjust the error suppression 40 Error suppression 23
Adjust the pressure for "to pump" and "to suppressor" Explanatory notes on the operating instructions i, vi
outlets 62 Explantary notes on the operating instructions vi
Adjust the pressure for “to pump“ and “to suppressor“ Explosion drawing system rear side ii, 50
outlets ii, 62 F
Airborne sound emission 16 Filter cartridge operating hours counter 25
Ambient conditions for DIONEX IC Pure and tank filling Flow chart DIONEX IC Pure ii, 76
station 16 Flow chart DIONEX IC pure 76
Applicability of the instructions i, v Flow chart DIONEX IC Pure with 20L tank ii, 77
C Flow chart DIONEX IC Pure with 20L tank and level
Calibrate the temperature 30 control ii, 78
Calibrate the ultra pure water measuring cell LF1 31 Flow chart DIONEX IC pure with 20L tank and level
Calibration ii, 27 control 78
Calibration menu 20 Flow chart system control 18
Calibration of feedwater measuring cell LF2 36 Flow charts ii, 76
Calibration of the microcontroller 20 Fundamental requirements for service work i, iv
Calibration of the ultra pure water measuring cell LF1 30 I
Calibration of the ultra pure water measuring cell LF1 with ICS 2100 79
temperature 30 ICS 4000 81
Calibration of TOC measuring cell LF3 38 ICS 5000+ 83
Cell constants of the measuring cells 15 L
Contact Information Thermo Fisher international sales Leaving calibration menu 24
organisations i, iii Legal Notice i, v
Controls i, 17 M
Content of pressure adjustment kit, 62 Maintenance record 85
D Matching the TOC measurement 22
Demands made on the feedwater 13 Matching the TOC-measurement 39
Description of control display 17 Materials of parts which contact water 15
Dimensions and weight of DIONEX IC Pure with ultra O
pure cartridge 13 Original document for translation i, v
Dimensions and weight of external 20L tank with level Overview screws rear side ii, 49
control 14 Overview spare parts DIONEX IC Pure 6
E Overview spare parts external 20L tank 8
Electrical connections for DIONEX IC Pure and external P
20L tank with level control 15 Position spare parts external 20L Tank 8
Enquiries from Asia Pacific iv Positions Spare parts DIONEX IC Pure 5
Enquiries from Europe, Middle East and Africa iii Postal address Germany iii
Enquiries from Germany iii Postal address USA iii

Thermo Scientific DIONEX IC Pure 91


Index

Preface i, iii tank ii, 75


Process procedures for personnel i, iv Terminal Assignment DIONEX IC Pure ii
Product water quality 13 Terminal Assignment DIONEX IC pure 71
R Terminal assignment level control 20L tank ii, 73
Replacing additional tank indicator ii, 63 Terminal assignment wire jumper ii, 74
Replacing Display Control part 43 Troubleshooting 67
Replacing Display Control part, ii U
Replacing feedwater measuring cel 52 Unlocking the system control 19
Replacing feedwater measuring cell ii, 52 UV-menu 24
Replacing Hardware Components 43 W
Replacing pressure hold valve ii, 59 Warranty i, v
Replacing Pure water measuring cell ii, 53 Water connections DIONEX IC Pure 15
Replacing solenoid valve ii, 51 Water connections for external 20L tank 15
Replacing Spare parts 49 Water connections for external 20L tank with level control
Replacing tank indicator sensor on external 20L tank ii, 66 15
Replacing tank indicator sensor on system ii, 65
Replacing tank indicator sensor system 65
Replacing the Booster pump 57
Replacing the fuse from additional tank indicator ii, 64
Replacing the fuse from the additional tank indicator 64
Replacing the Interface ii, 45
Replacing the pressure Booster pump ii, 57
Replacing the UV ballast ii, 47
Replacing TOC measuring cell ii, 55
Replacing Ultra pure water measuring cell 53
Requirement tools for changing Spare parts 9
Reset the operating hours counter and measuring in a new
UV- lamp 26
S
Safety Precautions 1
Schematic illustration with connected Suppressor ii, 79
Set up for calibrating feedwater measuring cell 33
Set up for calibrating ultra pure water measuring cell LF1 28
Set up for feedwater measuring calibration 33
Setting back to starting values 23, 40
Setting cell constant LF1 (Pure water measuring cell) 21
Setting cell constant LF2 (Feedwater measuring cell) 21
Setting cell constant LF3 (TOC measuring cell) 22
Setting the limiting value for the UV intensity measurement
25
Setting the limiting value for the UV operating hours
counter 25
Setting the temperature sensor 20
Skills of personnel iv
Skills of service personnel i
Spare parts 5
Spare parts and tools 5
Spare parts Dionex IC Pure 5
Specifications 13
Standards and directives i, vii
T
Technical Specifications 13
Terminal Assignment 71
Terminal assignment additional tank indicator ii, 72
Terminal Assignment and Flow chart ii, 71
Terminal assignment control wire DIONEX IC Pure to 20L

92 DIONEX IC Pure Thermo Scientific


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