Professional Documents
Culture Documents
Metallography: Standard Terminology Relating To
Metallography: Standard Terminology Relating To
for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: E7 − 22
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
banded structure (banding)—alternate bands parallel with body-centered—having an atom (or group of atoms) separated
the direction of working resulting from the elongation of by a translation of 1⁄2, 1⁄2, 1⁄2 from a similar atom (or group
segregated areas. of atoms). The number of atoms in a body-centered cell must
be a multiple of two.
barrel distortion— See distortion.
boiling pressure—at a specified temperature, the pressure at
basal plane—that plane of a hexagonal or tetragonal crystal
which a liquid and its vapor are in equilibrium.
which is perpendicular to the axis of highest symmetry. Its
Miller indices are (0001) or (001), respectively. boiling temperature—at a specified pressure, the temperature
at which a liquid and its vapor are in equilibrium.
bellows length—the distance from the eyepiece to the photo-
sensitive material or viewing screen in a photomicrographic bonded abrasive disk—a rigid support surface with an
apparatus. abrasive, typically diamond, bonded to the surface by a
ceramic, resin, or metal based material.
Bertrand lens—an auxiliary removable lens in the body of a
microscope, used to examine images in the back focal plane boundary grain—in the Jeffries’ method for grain size
of the objective, for example, interference figures with measurement, a grain that is intersected by the boundary of
polarized light. the standard area and is, therefore, counted only as one-half
grain. (See also Jeffries’ Method.)
beta structure—structurally analogous body-centered cubic
phases (similar to beta brass), or electron compounds, that Bragg angle—the angle between the incident beam and the
have ratios of 3 valence electrons to 2 atoms. lattice planes considered.
biased gun—an electron gun in which there is a bias voltage Bragg equation:—
on the cathode cap. (See also self-biased gun.) nλ 5 2dsinθ (2)
burning (burnt, burned)—a term applied to metal which has certified reference material—a reference material, the com-
been permanently damaged by having been heated to a position or properties of which are certified by a recognized
temperature close to or within the melting range. This results standardizing agency or group. Typically such a material is
in a structure exhibiting incipient melting or intergranular accompanied by documentation (certificate).
oxidation. characteristic curve—the curve showing the relationship
calibration—1) the act or process of determining the relation- between exposure and resulting density in a photographic
ship between a set of standard units of measure and the image. It is usually plotted as the density against the log
output of an instrument or test procedure, exposure. Called also the “H and D curve” and the “sensi-
2) the graphical or mathematical relationship relating the tometric curve.”
desired property (expressed in a standard unit of measure characteristic radiation—X-radiation of a particular set of
such as micrometers or Kg/mm2) to the instrument output wavelengths, produced by and characteristic of a particular
(instrument units such as filar divisions or pixels). element used as a target whenever its excitation potential is
caliper diameter (Feret’s diameter)—the length of a line exceeded.
normal to two parallel lines, tangent to opposite edges of a
charge neutralizer gun—an electron gun used to dissipate the
phase or object.
charges which tend to build up on specimen surfaces, within
calcite—a doubly refracting mineral used in the manufacture an electron-diffraction camera, which would introduce un-
of polarizing prisms. desired electrostatic fields.
DISCUSSION—It is uniaxial negative and in the trigonal diversion of
the hexagonal system of crystals. Its indexes are ε = 1.486, ω = 1.658; chemical potential—(µ i or Ḡ i) the partial molar free energy
its hardness is 3 on the Mohr scale and specific gravity 2.711. (E175) of component i, that is, the change in free energy of a
solution upon adding one mole of component i to an infinite
Canada balsam——see balsam, Canada. (E175) amount of solution of given composition,
carbide—a compound of carbon with one or more elements, ~ δG/δn i ! T,P,n 5 Ḡ i 5 µ i (4)
1···
which, in customary formulation, are considered as being
more positive than carbon. where:
G = Gibbs free energy, and
case—in a ferrous alloy, the outer portion that has been made ni = number of moles of the i thcomponent.
harder than the inner portion (see core) as a result of altered
composition, or structure, or both, from treatments such as Chinese script eutectic—a configuration of eutectic
carburizing, nitriding, and induction hardening. constituents, found particularly in some cast alloys of
aluminum containing iron and silicon and in magnesium
cassette—a light-tight film or plate holder. alloys containing silicon, which resembles in appearance the
cast replica—See replica. characters in Chinese script.
cast structure—the structure, on a macroscopic or micro- chlorine or volatile halide extraction—See extraction.
scopic scale, of a casting.
chromatic aberration—a defect in a lens or lens system as a
cathode lens—a lens field terminated on one side by a surface result of which the lens possesses different focal lengths for
at zero potential (cathode) normal to the optic axis. A radiation of different wavelengths.
cathode lens occurs in any system in which a cathode is
Class I quaternary equilibrium—in a four-component
imaged by its own electron emission, be it thermionic,
system, the stable univariant coexistence of five phases, one
photoelectric, secondary, or field emission.
of which must disappear upon lowering the temperature or
cementite—a very hard and brittle compound of iron and pressure; for example, the quaternary eutectic equilibrium,
carbon corresponding to the empirical formula Fe3C. It is L = α + β + γ + δ.
continuous spectrum (X-rays)—the polychromatic radiation critical point—in a phase diagram, that specific value of
given off by the target of an X-ray tube, containing all composition, temperature, pressure or combinations thereof
wavelengths above a certain minimum value called the short at which the phases of a heterogeneous equilibrium become
wave length limit. identical. (See also transformation temperature.)
contrast enhancement (electron optics)— an improvement in critical pressure—that pressure above which the liquid and
electron image contrast by the use of an objective aperture vapor states are no longer distinguishable.
diaphragm, shadow casting, or other means.
critical surface—in a ternary, or higher order, phase diagram,
contrast perception—the ability to differentiate various com- the area upon which the phases in equilibrium become
ponents of the object structure by different intensity levels in identical.
the image.
critical temperature—that temperature above which the va-
contrast, photographic—the word contrast has been used in por phase cannot be condensed to liquid by an increase in
many different senses in connection with various photo- pressure.
graphic characteristics; there are different types of photo-
graphic contrast and different methods of measuring it. It is cross direction—one of three mutually perpendicular direc-
frequently used to designate the magnitude of the density tions used to define a worked material, specifically that
difference resulting from a given exposure difference. (For direction in the plane of working which is at right angles to
another use, see gamma.) the direction of maximum elongation.
conversion, hardness—the exchange of a hardness number crystal—a solid composed of atoms, ions, or molecules
determined by one method for an equivalent hardness arranged in a pattern which is periodic in three dimensions.
number of a different scale. crystal, birefringent——a pertaining to the use of a micro-
cooling curve—graphical representation of the course of scope. (E175)
temperature fall of a chemical mixture as a function of time crystal analysis—a method for determining crystal structure,
commonly exhibiting more or less abrupt changes of rate at, for example, the size and shape of the unit cell and the
or near, those temperatures at which phase changes begin; location of all atoms within the unit cell.
used in finding the temperatures at which phase changes
occur. Occasionally, some property or function other than crystallite—a crystalline grain not bounded by habit planes.
time may be used; for example, thermal expansion. crystal system—one of seven groups into which all crystals
cooling rate—the average slope of the time-temperature curve may be divided; triclinic, monoclinic, orthorhombic,
taken over a specified time and temperature interval. hexagonal, rhombohedral, tetragonal, and cubic.
core—(1) case hardening—interior portion of unaltered cube texture—a texture found in wrought metals in the cubic
composition, or microstructure, or both, of a case-hardened system, in which nearly all the crystal grains have a plane of
steel article. the type (100) parallel or nearly parallel to the plane of
(2) clad products—the central portion of a multilayer com- working and a direction of the type [001] parallel or nearly
posite metallic material. parallel to the direction of elongation.
coring—a variable composition between the center and outside cubic—having three mutually perpendicular axes of equal
of a unit of structure, (such as a dendrite, grain, carbide length.
deep etching—macroetching; etching preliminary to macro- depth of field—the depth or thickness of the object space that
examination, intended to develop gross features such as is simultaneously in acceptable focus.
segregation, grain flow, cracks or porosity. depth of focus—the depth or thickness of the image space that
define (X-rays)—limit a beam of X-rays by passage through is simultaneously in acceptable focus.
apertures in order to obtain a parallel, divergent, or conver- derived differential curve—the curve derived from the data
gent beam. obtained by the use of the differential method of thermal
definition—the clarity or sharpness of a microscopical image. analysis. The changes in the temperature difference ∆(θ – θ'),
between a specimen and a neutral body, for a constant
deformation bands—bands produced within individual grains interval of temperature ∆θ are plotted against the tempera-
during cold working which differ variably in orientation ture. An arithmetic treatment of the differential data resulting
from the matrix. in a plot of ∆(θ – θ')/∆θ versus θ. (See differential curve.)
dezincification—a type of corrosion found with some copper- diffusion zone—the zone of viable composition at the junction
zinc alloys which occurs by solution of a small region and between two different materials, such as in welds or between
immediate redeposition of the copper in a spongy porous the surface layer and the core of clad materials or bearings,
form, thus giving the impression of selective removal of zinc in which interdiffusion between the various components has
from the alloy. taken place.
diagonal—in hardness testing, a line joining two opposite dilatometer—the instrument used in dilatometry for measur-
corners of a diamond pyramid indentation. ing lengths or volume changes.
diaphragm—a fixed or adjustable aperture in an optical dilatometry—the measurement of length or volume changes
system. Diaphragms are used to intercept scattered light, to of a substance undergoing a change in temperature, pressure,
limit field angles, or to limit image-forming bundles or rays. or state. See Practice E80.
(E175) direct print—a photographic print of an original negative.
differential curve: ( 1) in thermal analysis——a curve result- discontinuous stringer—three or more Type B or C inclusions
ing from the differential method of thermal analysis when aligned in a plane parallel to the hot working axis and offset
the difference in temperature (θ − θ') between a specimen by no more than 15 µm with a separation of less than 40 µm
and a neutral body is plotted against the temperature of the (0.0016 in.) between the two nearest neighbor inclusions
latter. (see Practices E45 and E1122).
(2) in dilatometry—a curve produced by plotting against
the temperature the difference in changes of length or disk, Airy—see airy disk. E175
volume between a body of known expansivity and a body disordered structure—the crystal structure of a solid solution
(specimen) of unknown expansivity. in which the atoms of different elements are randomly
distributed with respect to the available lattice sites.
differential interference contrast illumination—a micro-
scopical technique employing a beam-splitting double- dispersoid—in metallography, finely divided particles of rela-
quartz prism; that is a modified Wollaston prism placed tively insoluble constituents which can be seen in the
ahead of the objective with a polarizer and analyzer in the microstructure of certain alloys.
90° crossed positions. The two light beams are made to
coincide at the focal plane of the objective, thus rendering dissociation—as applied to heterogeneous equilibria, the
height differences visible as variations in color. The prism transformation of one phase into two, or more, new phases,
can be moved, shifting the interference image through the all of different composition.
range of Newtonian colors. dissociation pressure—at a designated temperature, the pres-
sure at which a phase will transform into two, or more new
differential thermocouple—two thermocouples placed in se-
phases, of different composition.
ries opposition (bucking).
distance, interpupillary—see interpupillary distance. (E175)
diffraction:—(1) a modification which radiation undergoes, as
in passing by the edge of opaque bodies or through narrow distortion—an aberration of lens systems where axial and
slits, in which the rays appear to be deflected. marginal magnifications are unequal.
(2) coherent scattering of X-radiation by the atoms of a (1)barrel distortion—the distortion in the image which
crystal which necessarily results in beams in characteristic occurs when the magnification of the image in the center of
directions. Sometimes called reflection. the field is greater than in the edge of the field. This is also
(3) the scattering of electrons, by any crystalline material, called negative distortion.
through discrete angles depending only on the lattice spac- (2) pincushion distortion—the distortion in the image
ings of the material and the velocity of the electrons. which results when the magnification in the center of the
eutectic carbides—in hypereutectic tool steels, the skeleton- exposure scale—in a photographic process, the range of
like structure of the eutectic carbide. exposure over which substantially correct reproduction is
obtained. This is measured by the ratio of the exposure
eutectic colony, grain—a two-phase region which solidified corresponding to the minimum useful gradient at the high
progressively from a simple center and, therefore, has some exposure end of the scale to that corresponding to the
uniformity of structural relationship. minimum useful gradient at the low exposure end.
eutectic equilibrium—a reversible univariant transformation extension lead wires—wires leading from a thermocouple to
in which a liquid, that is stable only at superior temperature, the voltage-measuring instrument. These wires should have
decomposes into two or more conjugate solid phases; for the same temperature-emf relationship as the thermocouple
example, L = α + β, L = α + β + γ, etc. wires.
fluorescent screen—a sheet of material which emits visible fracture test: (1) —generalthe production of a fracture in a
light when exposed to invisible radiation. metal sample to determine such things as discontinuities,
grain size, and composition.
fluorescent X-rays (fluorescent analysis)— characteristic (2) steel—a test which utilizes a hardened steel disk
X-rays excited by radiation of wavelength shorter than the section prepared from billet or bar stock which is fractured
corresponding absorption edge. parallel to the grain flow so that, among other things,
discontinuities due to inclusion segregates can be detected
focal length—the distance from the second principal point to visually.
the point on the axis where parallel rays entering the lens
will converge or focus. free-energy diagram—a graphical representation of the varia-
tion with concentration of the Gibbs Free Energy, at constant
focal spot—that area on the target of an X-ray tube which is pressure and temperature.
bombarded by electrons.
free-energy surface—in a ternary, or higher order, free energy
focus—a point at which rays originating from a point in the diagram, the locus of points representing the Gibbs Free
object converge or from which they diverge or appear to Energy as a function of concentration, with pressure and
diverge under the influence of a lens or diffracting system. temperature constant.
focus, principal—the point at which a lens focuses an axial freezing point—See melting point.
object pint.
frequency (X-ray)—the number of alternations per second of
DISCUSSION—Synonymous with focal point. (E175)
the electric vector of the X-ray beam. It is equal to the
focusing (X-rays)—the operation of producing a convergent velocity divided by the wavelength.
beam in which all rays meet in a point or line.
Fresnel fringes—a class of diffraction fringes formed when
focusing device (electrons)—a device which effectively in- the source of illumination and the viewing screen are at a
creases the angular aperture of the electron beam illuminat- finite distance from a diffracting edge. In the electron
ing the object, rendering the focusing more critical. microscope these fringes are best seen when the object is
slightly out of focus.
focusing magnifier: ( 1)—a low-power microscope, telescope
or simple lens used to observe the electron image formed on gamma (photography)—the tangent of the angle which the
a fluorescent screen. straight-line part of the characteristic curve makes with the
(2) a magnifying lens mounted so that its focal plane is log exposure axis and in a photographic film or plate is a
coincident with its base, used to obtain a sharp focus in the measure of the extent of development.
plane of the sensitive material in a camera.
gamma iron (γ Fe)—solid nonmagnetic phase of pure iron
foil—a thin sheet of a material, usually a metal, not exceeding which is stable at temperatures between 910 and 1400°C and
0.005 in. in thickness. possesses the face-centered cubic lattice.
folds—defects in metal, usually on or near the surface, caused gas holes—blow holes, channels, or porosity produced by gas
by continued fabrication of overlapping surfaces. evolution, usually during solidification.
isometric—a crystal form in which the unit dimension on all Köhler illumination—see illumination, Köhler. (E175)
three axes is the same. Konowalow’s law—the vapor of a binary mixture contains the
isomorphous—having the same crystal structure; usually re- larger proportion of that component, which, upon addition to
ferring to intermediate phases which form a continuous the liquid, will raise its vapor pressure.
series of solid solutions. lamination—imperfection in flat products resulting from the
isomorphous system—a complete series of mixtures in all presence of voids or inclusions aligned approximately par-
proportions of two, or more, components, wherein unlimited allel to the worked surface.
mutual solubility exists in both the liquid and solid states. lap—(1) a surface imperfection on worked metal caused by
isopleth—in a ternary, or higher order, temperature- folding over a fin overfill, or similar surface condition and
concentration, or pressure-concentration, phase diagram, a then impressing this into the surface by subsequent working
(vertical) two-dimensional section, having a linear compo- without welding it.
sition series along one axis and temperature, or pressure, (2) A flat surface which holds an abrasive for polishing
along the other axis. operations.
isotherm—section, at constant temperature, through a phase lapping—the abrasive removal of material using graded abra-
diagram. sive particles in a loose form as in a liquid slurry on a platen.
isotropic—having the same value for a property in all direc- latitude—when the photographic process is represented by an
tions. H and D curve, the latitude is the projection on the exposure
axis of that part of the curve which approximates a straight
isotropy—the condition of having the same values of proper-
line within the tolerance permitted for the purpose at hand.
ties in all directions.
Jeffries’ method—a method for determining grain size based lattice—(1) a space lattice is a set of equal and adjoining
on counting grains in a prescribed area. See Test Methods parallelopipeds formed by dividing up space by three sets of
E112. parallel planes, the planes in any one set being equally
spaced. There are seven ways of so dividing space, corre-
Jeffries’ multiplier—a factor used in the Jeffries’ method for sponding to the seven crystal systems. The unit paral-
grain size determinations. See Test Methods E112. lelopiped is usually chosen as the unit cell of the system.
(2) a point lattice is a set of points in space so located that
K radiation—characteristic X-rays produced by an atom when
each point has identical surroundings. There are fourteen
a vacancy in the K shell is filled by one of the outer
ways of so arranging points in space, corresponding to the 14
electrons.
Bravais lattices.
K series—the set of X-ray wavelengths making up K radiation.
lattice parameter—the term is used for the fractional coordi-
Kellner eyepiece—a positive eyepiece consisting of an achro- nates x, y, z of lattice points when these are variable. Also
matic eyelens and a single collective, in which the image used to indicate the lengths of the axes a, b, c, and their
plane and field diaphragm is external and near the collective. included angles α, β, γ.
leaded—characteristic of a metallic body containing metallic longitudinal direction—that direction which is parallel to the
lead in dispersed form. direction of maximum elongation in a worked material. (See
also cross direction).
Le Chatelier’s theorem—if a system in equilibrium is sub-
jected to a constraint by which the equilibrium is altered, a lot—a unit of material processed at one time and subjected to
reaction takes place which opposes the constraint, that is, similar processing variables.
one by which its effect is partially annulled. lower critical point—in a phase diagram, a specified value of
ledeburite—intimate mixture of austenite and cementite in composition, temperature and pressure or combinations
metastable equilibrium, formed on rapid cooling during the thereof occurring as a minimum in temperature, or pressure,
eutectic reaction in alloys of iron and carbon containing for the coexistence of two, or more, conjugate phases and at
greater than 2 percent but less than 6.67 percent carbon. which the conjugate phases become identical.
Further slow cooling causes decomposition of the austenite low reflecting coating—a dielectric coating applied to an
into ferrite and cementite (pearlite) as a result of the air-glass surface to reduce light reflection to a minimum.
eutectoid reaction.
L-radiation—characteristic X-rays produced by an atom when
lens—a transparent optical element, so constructed that it
a vacancy in the L-shell is filled by one of the outer
serves to change the degree of convergence or divergence of
electrons.
the transmitted rays. (E175)
lens, compound—a lens compound of two or more separate L-series—the set of X-ray wavelengths making up L-radiation.
pieces of glass or other optical material. Lüder’s lines—markings which appear on the surface of
DISCUSSION—These component pieces or elements may or may not be metals stretched past the yield point. The markings are
cemented together. A common form of compound lens is a two-element approximately parallel to the direction of maximum shear
objective, one element being a converging lens of crown glass and the
stress and essentially independent of crystal orientation; also
other a diverging lens of flint glass. The combination of suitable glasses
or other optical materials (plastics, minerals) properly ground and called stretcher strains, flow figures, Hartmann lines.
polished reduces aberrations normally present in a single lens. (E175) macroetch—controlled etching of the surface of a metallic
lens, negative—a lens that is thicker on the edges than in the specimen, intended to reveal a structure which is visible at
center, and which causes parallel light rays to diverge. low magnifications (not usually greater than 10 times).
DISCUSSION—Also called diverging lens. (E175) macrograph—a graphic reproduction of an object, slightly
lever principle—in a phase diagram, the relative proportions reduced in size, unmagnified, or magnified ten diameters or
of the conjugate phases, at a stated value of temperature and less (photomacrograph).
pressure, or both, is such that a state of mechanical balance magnetic alignment—See alignment.
would obtain, if the corresponding weight of each phase magnetic lens—a device for focussing an electron beam by
were placed upon its composition point upon the tie-element means of a magnetic field.
(tie-line, tie-triangle, etc.) and the fulcrum were located at
the gross composition point of the mixture. magnetic shielding—in electron microscopy, shielding for the
purpose of preventing extraneous magnetic fields from
lightfield illumination—See brightfield illumination.
affecting the electron beam in the microscope.
light filter—See color filter.
limited solid solution—a crystalline miscibility series whose magnetic transformation—an intensive property change
composition range does not extend all the way between the from a ferromagnetic to a paramagnetic state, or the reverse,
components of the system, that is, the system is not which occurs in certain solid materials under applied pres-
isomorphous. sure and temperature, or both. (See also Curie point.)
lineage structure—orientation deviations, of the order of magnification—a ratio of the size of an image to its corre-
minutes or a few degrees at most, from perfect alignment of sponding object. This is usually determined by linear mea-
the crystal axes of parallel arms of a dendrite. surement.
maximum sublimation point—in a PT phase diagram, the micromanipulator—a mechanical device for making small
highest pressure and temperature at which a solid species of movements in order to manipulate microscopic probes. E175
intermediate composition may exist in equilibrium with microindent—See indentation.
vapor of identical composition. micrometer eyepiece—an eyepiece that has a scale perma-
nently positioned in its focal plane, thus, in effect, superim-
McQuaid-Ehn grain size—the austenitic grain size developed
posing the scale on the image of the field being observed.
in steels by carburizing at 1700°F (927°C) followed by slow
cooling. See Test Methods E112. micro penetration hardness—the hardness number obtained
by use of a low load tester whose indentation is usually
measurement uncertainty—an estimate of potential inaccu-
measured with a high power microscope.
racies in a measured or derived quantity based on explicit
evaluation and combination of all sources of errors. Note - micro penetration tester—a testing machine capable of ap-
Quantitative uncertainty estimates are typically given in the plying low loads, usually in the range from 1 g to 5 kg to
form of variances (or standard deviations) and covariances form an indentation or a scratch or both, as a basis for
(or correlations) derived from statistical procedures combin- measuring hardness. Typical names associated with commer-
ing random, systematic, and calculational (modeling) uncer- cial testers are Bergsman, Eberbach, Knoop, Microcharacter,
tainties. Tukon, Vickers, etc.
measuring junction—the junction of a thermocouple placed at microphotograph—a microscopically small photograph.
a location where an unknown temperature is to be measured
microporosity—extremely fine porosity in castings.
or where an established temperature is to be maintained.
When the measuring junction is at a higher temperature than microradiography, contact—a method of making micro-
the reference junction it is commonly called the hot junction. graphs be means of X rays.
negative, photographic—a sensitized plate or film which has objective aperture—See aperture.
been exposed in a camera and which upon development has object evaporation—See shadowing.
the lights and shades inverse to those of the original subject. objective, fluorite—an objective using the mineral fluorite in
The plate or film does not become a negative until it is its construction. It is usually intermediate between achro-
exposed, after which it may be an undeveloped or a matic and apochromatic in correction, but may be more
developed negative. highly corrected. E175
negative print—a photograph having approximately the op- oblique illumination—nonspecular illumination under which
posite rendition of light and shade as the original subject. the light impinges at an oblique angle to the optical axis.
(See conical illumination; diffuse illumination; darkfield
negative replica—See replica.
illumination.)
network structure—a structure in which one constituent
occurs primarily at the grain boundaries, thus partially or oblique illumination—see illumination, oblique. E175
completely enveloping the grains of the other constituents; ocular—see eyepiece. E175
on a two-dimensional section cut through such a structure,
the grain boundary constituent will appear as a network. ocular micrometer—a glass disk, of a diameter which permits
introducing it into standard oculars, upon one surface of
Neumann bands—See twin bands. which a fine scale is engraved accurately.
neutral body—a comparison piece used in the differential
method of thermal analysis, which has nearly the same optical pyrometer—an instrument with the temperature of an
thermal properties as the test specimen, and which produces object is determined by comparing its brightness at some
no heat effects within the temperature range through which fixed wavelength with that of a standardized source.
the specimen is being tested. See Practice E80.
order (in X-ray reflection)—the factor n in the Bragg equa-
Nicol prism—a prism, used for polarizing or analyzing light, tion (see Bragg equation). In X-ray reflection from a
made by cementing together, with Canada balsam, two crystal, the order is an integral number which is the path
pieces of calcite in such a way that the extraordinary ray difference measured in wavelengths between reflections
from the first piece passes through the second piece while the from adjacent planes.
ordinary ray is reflected to the side into an absorbing layer of
black print. When two Nicol prisms are crossed, therefore, order-disorder transformation—a phase change among two
no light passes through. solid solutions having the same crystal structure but in which
the atoms of one phase, the disordered one, are randomly
nitride-carbide inclusion types—a compound with the gen- distributed and in the other, the different kinds of atoms
eral formula M x(C, N)y observed generally as colored occur in a regular sequence upon the crystal lattice, that is,
idiomorphic cubic crystals, where M includes Ti, Cb, Ta, Zr. in an ordered arrangement.
sinking indentation—a hardness indentation around which sorbite (an obsolete and ill-defined term)—an aggregate of
the metal has been depressed below the plane of the carbide and ferrite produced by tempering martensite at
specimen. temperatures in the vicinity of 600 °C and which may be
resolved readily at relatively low magnification (for
slip—translation of a portion of a crystal relative to the example, 500X).
adjacent portion.
DISCUSSION—The term has also been applied to very fine pearlite that
slip bands—See slip lines. cannot be resolved with the light microscope at 500X.
slip lines (slip bands)—traces of slip planes observed at low
magnifications on the polished surface of a crystal which has source (X-rays)—the area emitting primary X-rays in a
been deformed after polishing; since no differences in diffraction experiment. The actual source is always the focal
orientation exist, repolishing will remove the traces. With spot of the X-ray tube but the virtual source may be a slit or
increasing resolving power and magnification, an individual pinhole, depending on the conditions of the experiment.
line may be revealed as a series of parallel lines. The “line” space charge aberration—an aberration resulting from the
which is visible at low magnifications is then described as a mutual repulsion of the electrons in a beam. This aberration
slip band. is most noticeable in low-voltage, high-current beams. This
slip planes—in a given metal, slip occurs most easily along repulsion acts as a negative lens causing rays which were
certain crystallographic planes. Hence, these planes are originally parallel to diverge.
termed slip planes. space lattice—See lattice.
slit—a narrow aperture, usually rectangular in shape. spacing (between lattice planes)—See interplanar distance.
specimen grid—See specimen screen. sputtering—the production of specimens in the form of thin
specimen holder (electron optics)—a device which supports films by deposition from a cathode subjected to positive ion
the specimen and specimen screen in the correct position in bombardment.
the specimen chamber of the microscope. stage—a device for holding a sample in the desired position in
specimen screen (electron optics)—a disk of fine screen, the optical path.
usually 200-mesh stainless steel, copper, or nickel, which stage micrometer—a graduated scale used on the stage of a
supports the replica or specimen support film for observation microscope for calibration.
in the microscope.
standard—1) a physical reference used as a basis for com-
specimen stage—the part of the microscope which supports parison or calibration;
the specimen holder and specimen in the microscope, and 2) a concept that has been established by authority, custom,
can be moved in a plane perpendicular to the optic axis from or agreement to serve as a model or rule in the measurement
outside the column. of quality or establishment of a practice or procedure.
specimen stage controls—the external controls by means of standard (hardness) block—a carefully prepared metal block
which the stage can be moved. used to calibrate hardness test machines.
specimen strain—a distortion of the specimen resulting from
standard grain-size micrograph—a micrograph taken of a
stresses occurring during preparation or observation. In
known grain size at a known magnification, which is used to
electron metallography, strain may be caused by stretching
determine grain size by direct comparison with another
during removal of a replica or during subsequent washing or
micrograph or with the image of a specimen.
drying. Also, electrical and thermal stresses caused by the
electron beam may arise during observation. steadite—(1) ternary eutectic found in alloys of iron, carbon
and phosphorus. In cast irons it consists of austenite,
spectrograph (X-ray)—an instrument for recording photo-
cementite and iron phosphide or austenite and iron-
graphically at predetermined angles the results of diffraction
phosphide. If conditions are such that carbon is deposited as
experiments.
cementite, the three constituents of the eutectic are present.
spectrometer (X-ray)—(1) an instrument similar to a spectro- If, however, the carbon is deposited as graphite, that precipi-
graph but employing a movable X-ray measuring device, tated from the ternary eutectic crystallizes on existing flakes
such as a Geiger-Müller counter or ionization chamber, and the eutectic consists of two constituents only, namely,
instead of a photographic film. The measuring device moves austenite and iron-phosphide.
on a circle centered on the spectrometer axis. (2) Binary eutectic found in alloys of iron and phosphorus
(2) An instrument for recording, similar to the consisting of ferrite and iron-phosphide.
spectrograph, except that a Geiger-Müller counter, scintilla-
stepdown test—a test involving the preparation of a series of
tion counter, proportional counter, or ionization chamber
machined steps progressing inward from the surface of a bar
substitutes for the photographic recording.
for the purpose of detecting by visual inspection internal
speed (photographic or film) (see sensitivity)—a measure of laminations caused by inclusion segregates. See Practice
the response of sensitivity of the material to light, often E45.
thermocouple vacuum gage—a thermal conductivity or hot- transmission method—a method of X-ray or electron diffrac-
wire gage in which the temperature of an electrically heated tion in which the recorded diffracted beams emerge on the
fine wire varies as the thermal conductivity of the residual same side of the specimen as the transmitted primary beam.
gas. The thermocouple measures the temperature change. transmission microscope—a microscope in which the image
thermoelectric pyrometer—a device with which tempera- forming rays pass through (are transmitted by) the specimen
tures are measured by utilizing the thermoelectric effects. In being observed.
its simplest form, it consists of a thermocouple of two transverse direction— See cross direction.
dissimilar metals which develop an emf when the junctions triclinic—having three axes of any length, none of the in-
are at different temperatures and an instrument for measuring cluded angles being equal to one another or equal to 90°.
the emf developed by the thermocouple.
triple curve—in a P-T diagram, a line representing the
thermomechanical process, n—controlled thermal and defor- sequence of pressure and temperature values among which
mation treatment performed at an elevated temperature. two conjugate phases occur in univariant equilibrium.
threshold setting, in image analysis—the selected range of triple point—in a P-T diagram, the temperature and pressure
gray levels corresponding to a constituent in the field of the at which three phases occur in invariant equilibrium.
view.
troostite (an obsolete and ill-defined term)—an
tie line—in a binary or higher order phase diagram, an unresolvable, fine aggregate of carbide and ferrite produced
isothermal, isobaric straight line connecting the composi- by tempering martensite at temperatures in the vicinity of
tions of a pair of conjugate phases. 400 °C.
DISCUSSION—Term variously and erroneously applied to bainite and
tie tetrahedron—in a quaternary or higher order phase nodular fine pearlite. Confusion arose because of similarity in appear-
diagram, an isothermal, isobaric four-cornered space figure ance among the three structures before the advent of high-power
connecting the compositions of four conjugate phases. microscopy. With reference to tool steels, the term has been applied to
highly tempered high-carbon martensite or to upper bainite.
tie triangle—in a ternary or higher order phase diagram, an
isothermal, isobaric plane three-cornered, straight-sided fig- twin bands—bands across a crystal grain, observed on a
ure connecting the compositions of three conjugate phases. polished and etched section, the crystallographic orientations
of which have a mirror image relationship to the orientation
time-temperature curve—in thermal analysis, a curve pro- of the matrix grain across a composition plane which usually
duced by plotting time against the temperature. is parallel to the sides of the band.
(1) annealing twin—twin bands which are produced
traceability—the ability to demonstrate by means of an
during annealing following cold work.
unbroken chain of comparisons that a measurement is in
(2) mechanical twins—twin bands which are produced by
agreement within acceptable limits of uncertainty with
cold work.
comparable nationally or internationally recognized stan-
(3) Neumann bands—mechanical twins in ferrite.
dards.
T-X diagram—a two-dimensional, graphical representation of
transcrystalline cracking—cracking or fracturing which oc-
the isobaric phase relationships in a binary system; the
curs through or across a crystal; intracrystalline cracking.
coordinates of the graph are temperature and concentration.
transformation temperature—the temperature at which a ultramicroscopic—below the resolution of the microscope.
change in phase occurs. The term is sometimes used to
denote the limiting temperature of a transformation range. ultraviolet—invisible light radiation, adjacent to the violet end
Sometimes incorrectly and loosely referred to as Critical of the visible spectrum, with wavelengths from about 200 to
Point. 400 nm (nanometres).
(Nonmandatory Information)
X1.1 The following abbreviations are frequently used in the ODF orientation distribution function
field of metallography. PAGS prior austenite grain size
PFZ precipitate free zone
Å Angstrom unit. RA relative accuracy
K X-rays (See K radiation.) ROI region of interest
SAD selected area diffraction
X1.2 The following abbreviations and acronyms are fre- SAECP selected area electron channeling pattern
quently used in the area of metallography. SAED selected area electron diffraction
SAM scanning auger microscopy
AEM analytical electron microscope SANS small angle neutron scattering
AES auger electron spectroscopy SE secondary electrons
AFM atomic force microscope SEI secondary electron image
AGS average grain size SEM scanning electron microscope
AI anisotropy index SIM scanning ion microprobe
AIA automatic image analysis SIMS secondary ion mass spectroscopy
ALA as large as SLAM scanning laser acoustic microscope
APFEM atomic probe field emission microscopy SRMN Standard Reference Manual
ASM acoustic scanning microscope STEM scanning transmission electron microscopy
BEKP back scattered electron kikuchi pattern STIM scanning transmission ion microscopy
BSE back scattered electrons STM scanning tunneling microscope
BSI back scattered electron image TCP topologically close-packed
CBED convergent beam electron diffraction TEM transmission electron microscope
CCD charge coupled device TOF SIMS time-of-flight secondary ion mass spectrom-
CI confidence interval eter
CL confidence limit TSC thermal sprayed coating
CLM cathoodo luminescence UV ultraviolet
CM confocal microscopy WDS wavelength dispersive spectrometry
CV coefficeient of variation WORM write once read many
DIC differential interference contrast XRD X-ray diffraction
EBIC electron beam induced current XRF X-ray fluorescence
EBSP Electron Back Scattered Pattern XRM X-ray microscopy
ECP electron channeling pattern ZAF Z-Absorption fluorescence
EDS energy dispersive spectroscopy ZAP zone axis pattern
EDXA energy dispersive X-ray analysis ZOLZ zero order laue zone
EELS electron energy loss spectroscopy
EMMA electron microscopy micro analyzer
EMPA electron microprobe micro analysis
X1.3 The following are abbreviations of societies and insti-
EPMA electron probe micro analysis tutes applicable to the field of metallography.
ESCA electron spectroscopy for chemical analysis
AIME American Institute of Mining and Metallur-
FEM field electron microscopy
gical Engineers
FFT fast Fourier transform
AISI American Iron and Steel Institute
FIM field ion microscopy
ANSI American National Standards Institute
GCP geometrically close-packed
ASME American Society of Mechanical Engineers
HB Brinell hardness number
ASTM American Society for Testing and Materials
HEED high energy electron diffraction
DIN Deutsche Industrie Norm
HK Knoop hardness number
ICDD International Center for Diffraction Data (see
HOLZ high order laue zone
JCPDS)
HR Rockwell hardness number (requires a scale
IEC International Electrochemical Commission
designation; for example HRC)
IMS International Metallographic Society
HV Vickers hardness number
ISO International Organization for Standardiza-
HVDF high velocity oxy-fuel
tion
IA image analysis
JCPDS Joint Committee on Powder Diffraction
IR infrared
Standards (see ICDD)
JK Jernkontoret
JIS Japanese Industry Standard
LaB6 lanthanum-hexaboride cathode
MRS Materials Research Society
LEED low energy electron diffraction
MSA Microscopy Society of America
LM light microscopy
NIST National Institute for Standards &
LOM light optical microscopy
Technology
LP lorentz polarization
RMS Royal Microscopical Society
LSCM laser scanning confocal microscope
SAE Society of Automative Engineers
OCC ALA occasional as large as
TMS The Metals Society
OCF orientation correlation function
The following documents and publications may provide additional definitions of terminology in the field of metallography or
closely related fields.
ASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentioned
in this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the risk
of infringement of such rights, are entirely their own responsibility.
This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years and
if not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standards
and should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of the
responsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you should
make your views known to the ASTM Committee on Standards, at the address shown below.
This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,
United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the above
address or at 610-832-9585 (phone), 610-832-9555 (fax), or service@astm.org (e-mail); or through the ASTM website
(www.astm.org). Permission rights to photocopy the standard may also be secured from the Copyright Clearance Center, 222
Rosewood Drive, Danvers, MA 01923, Tel: (978) 646-2600; http://www.copyright.com/