Method Validation No. 2

You might also like

Download as xlsx, pdf, or txt
Download as xlsx, pdf, or txt
You are on page 1of 6

RAW DATA

Date Sample Number Weight of Crucible Weight of Crucible + Flour


7/9/2023 1 19.26 21.26
2 18.15 20.15
3 18.79 20.79
4 18.98 20.98
5 18.22 20.22
8/9/2023 1 19.26 21.2
2 18.15 20.09
3 18.79 20.72
4 18.98 20.92
5 18.22 20.15
8/9/2023 1 19.26 21.18
2 18.15 20.08
3 18.79 20.71
4 18.98 20.89
5 18.22 20.14
11/9/2023 1 19.26 21.13
2 18.15 20.02
3 18.79 20.65
4 18.98 20.835
5 18.22 20.08
11/9/2023 1 19.26 21.103
2 18.15 19.99
3 18.79 20.63
4 18.98 20.82
5 18.22 20.06
12/9/2023 1 19.26 21.103
2 18.15 20
3 18.79 20.63
4 18.98 20.82
5 18.22 20.06
12/9/2023 1 19.26 21.103
2 18.15 20
3 18.79 20.628
4 18.98 20.821
5 18.22 20.058
Moisture Content
7.85
7.50
8.10
7.95
8.10
RAW DATA
Date Sample No. Weight of Crucible Weight of Crucible + Flour Moisture Content
12/9/2023 1 19.26 21.103 7.85
2 18.15 20 7.50
3 18.79 20.628 8.10
4 18.98 20.821 7.95
5 18.22 20.058 8.10
Mean 7.89999999999996
Standard Deviation 0.247487373415298

Grubbs' Test
Sample G Value
7.85 -0.20203050891
7.5 -1.61624407128
8.1 0.808122035642
7.95 0.202030508911
8.1 0.808122035642
DATA
Sample Moisture
Number Content MC CONTROL
1 7.85 +3 SD 9.014
2 7.5 +2 SD 8.688
3 8.1 +1 SD 8.361
4 7.95 Mean 8.035
5 8.1 -1 SD 7.708
6 8.2 -2 SD 7.382
7 7.75 -3 SD 7.055
8 7.85
9 8.55
10 8.5
Mean 8.035
SD 3 0.97992347
SD 2 0.65328231
SD 1 0.32664116

SGPT Level 3 LJ Chart

8.5

7.5

7
1 2 3 4 5 6 7 8 9 10

695497251.xlsx SMILE Document Page 3of 6 10/03/2023


LOD AND LOQ
SAMPLE NO. SET 1 SET 2

1 7.85 8.2
2 7.5 7.75
3 8.1 7.85
4 7.95 8.55
5 8.1 8.5
m 0.765306
STEYX 0.360326
LOD 1.412479
LOQ 4.708263
REPRODUCIBILITY
SAMPLE NO. SET 1 SET 2 DF MEAN

1 7.85 8.2 -0.35 8.025


2 7.5 7.75 -0.25 7.625
3 8.1 7.85 0.25 7.975
4 7.95 8.55 -0.6 8.25
5 8.1 8.5 -0.4 8.3
CONCLUSION REJECTED

REPEATABILITY
Mean 8.035
Mean x (0.01) 0.08035
ACV 1.3701808008284
SD 0.2684445939109
RSD 3.3409408078522
HORAT VALUE 2.438321136767
REPEATABILITY 9.2605266413105
SUPPORTING FACTOR 0.9134538672189
CONCLUSION REJECTED

REPEATABILITY
Mean 8.035
Mean x (0.01) 0.08035
ACV 1.370180801
SD 0.3266412
RSD 4.0652296204107
HORAT VALUE 2.9669293405978
REPEATABILITY 11.268133549202
SUPPORTING FACTOR 0.9134538673333
CONCLUSION REJECTED
SAMPLE NO. SET 1 (𝑋_𝑖−𝜇) 〖 (𝑋_𝑖−𝜇) 〗 ^2

1 7.85 -0.185 0.034225


2 7.5 -0.535 0.286225
3 8.1 0.065 0.004225
4 7.95 -0.085 0.007225
5 8.1 0.065 0.004225
6 8.2 0.165 0.027225
7 7.75 -0.285 0.081225
8 7.85 -0.185 0.034225
9 8.55 0.515 0.265225000000001
10 8.5 0.465 0.216225

No. of readings 10
Mean 8.035
Uncertainty 0.103293

Measurement at 95% confidence level = (8.035 ± 2 * 0.103293)


Measurement at 95% confidence level = (8.525 ± 0.206586)

You might also like