BRANCH INDUSTRIAL BIOTECHNOLOGY

22BES510 MASS TRANSFER OPERATIONS V

PREREQUISITES CATEGOR L T P C
Y
1. 22BES306 - Process Calculations and Heat transfer ES 3 1 0 4
2. 22BES407 - Fluid Mechanics

Course 1. To understand the basic laws of diffusion & to develop solutions for the
Objectives problem involving solid, liquids and gas systems.
2. To design the absorption column for the separation processes in single and
multistage modes.
3. To learn the process of distillation and to design the types of distillation
columns.
4. To know the principle and design features of extraction / leaching
equipment used in process industries.
5. To exploit the technological methods in design and troubleshooting of solid-
fluid operations in process industries.

UNIT – I DIFFUSION AND MASS TRANSFER 9+3 periods

Molecular diffusion in solids, liquids and gases; Inter-phase mass transfer; theories to
determine mass transfer coefficients; Analogies in Transport phenomenon
UNIT – II GAS - LIQUID OPERATIONS 9+3 periods
Principles of gas absorption; Single and Multistage absorption; Absorption with chemical
reaction; Design principles of absorbers; Industrial absorption equipment; HTU, NTU
concepts.
UNIT – III VAPOUR - LIQUID OPERATIONS 9+3 periods
Vapour-Liquid equilibria; Simple, Steam and Flash Distillation; Continuous distillation;
McCabe - Thiele & enthalpy concentration method; Industrial distillation equipment,
HETP, HTU and NTU concepts.
UNIT – IV EXTRACTION OPERATIONS 9+3 periods
Liquid-Liquid equilibria, Staged and continuous extraction, Solid-liquid equilibria,
Leaching principles, Equipment for extraction and leaching
UNIT-V SOLID - FLUID OPERATIONS 9+3 periods
Adsorption equilibria – Types - Batch and fixed bed adsorption; Drying – Mechanism -
Drying curves - Time of drying; Equipment for drying - Batch and continuous dryers
Contact Periods: 60
Lecture: 45 Periods Tutorial: 15 Periods Practical: 0 Periods Total: 60 Periods

TEXT BOOK
1 Yunus Cengel, “Heat and Mass Transfer – Fundamentals & Applications”, McGraw-
Hill, 5th edition 2015.
2 Geankoplis C.J, “Transport Processes and Unit Operations”, Prentice Hall of India, 4th
edition 2003.

REFERENCES
1 Incropera F.P., “Fundamentals of Heat and Mass Transfer”, John Wiley, 7th edition.
2011.
2 McCabe W.L., Smith J.C, “Unit Operations in Chemical Engineering”, McGraw-Hill,
7th edition. 2014.
3 Treybal R.E, “Mass Transfer Operations”, McGraw-Hill, 3rd edition. 1981.

COURSE OUTCOMES: Bloom’s

Taxonomy
On completion of the course, the students will be able to: Mapped
CO1 Understand the basic laws of diffusion & to develop solutions for the K1
problem involving solid, liquids and gas systems
CO2 Design the absorption column for any complex separation processes K1
CO3 Design and operate the various classes of distillation columns for V-L K2
operations
CO4 Design the extraction / leaching equipment for L-L & S-L K3
operations.
CO5 Design the drying and adsorption equipment for S-F operations. K3

a) Course Articulation Matrix

PO PO PO PO PO PO PO PSO
COs/POs PO1
2
PO3 PO4
5
PO6
7
PO8
9 10 11 12 1
PSO2
CO1 3 2 1 - - - - - 3 1 - 1 3 3
CO2 3 - 3 2 2 - - - 3 2 - 2 3 3
CO3 1 1 2 2 2 - - - 2 1 - 1 1 2
CO4 2 2 2 2 2 - 2 1 2 2 - 2 1 2
CO5 2 1 2 1 1 - - 2 2 2 2 2 2 3
22BES510 3 2 2 2 2 - 2 1 3 2 2 2 1 3
1 – Slight, 2 – Moderate, 3 – Substantial

ASSESSMENT PATTERN – THEORY

Test / Remembe Understandi Applyin Analyzin Evaluatin Creatin Tota
Bloom’s ring (K1) ng (K2) % g (K3) g (K4) % g (K5) % g (K6) l%
Category* % % %
CAT1 50 10 10 10 10 10 100
CAT2 50 10 10 10 10 10 100
Assignment 20 20 20 20 10 10 100
1
Assignment 20 20 20 20 10 10 100
2

Course Contents and Lecture Schedule:

Unit No. Topic No. of Periods

(Times New Roman, Size 11) (Times New Roman, Size 11, Sentence case)

Prepared by Checked by Head of the Department