TFC 003

P Copy No.
STANDARD OPERATING PROCEDURE FOR HIGH-SPEED MIX

BED RESIN REGENERATION WASTE WATER RECYCLING,
NEUTRALIZATION AND DISCHARGERGING OPERATION
(SOP-TFCWDP-0034)
PK237SOP24183K06145PC
Rev. 0
MarchDecemberJUNE 20198
PAEC PROPERTY
THIS DOCUMENT IS THE PROPERTY OF PAEC. NO EXPLOITATION OR TRANSFER

OF ANY INFORMATION CONTAINED HEREIN IS PERMITTED IN THE ABSENCE OF
AN AGREEMENT WITH PAEC AND NEITHER THE DOCUMENT NOR ANY SUCH
INFORMATION MAY BE RELEASED WITHOUT THE WRITTEN CONSENT OF PAEC.
KARACHI NUCLEAR POWER PLANT UNIT-2 (K-2)

PAKISTAN ATOMIC ENERGY COMMISSION
OPERATING PROCEDURE
STANDARD OPERATING PROCEDURE FOR HIGH-SPEED

MIX BED RESIN REGENERATION STANDARD OPERATING
PROCEDURE FOR WASTE WATER RECYCLING,
NEUTRALIZATION AND DISCHARGEING
LOADING AND UNLOADING OF BULK CHEMICALS AGENT
PK237SOP24183K06145PC
Rev. 0
Compiled by: Commissioning Division
Prepared by
Rashid PervaizWaqas
AhmedTypeyourname,
SJE
Checked by Reviewed by (CZEC) QA Reviewed by

Muhammad Usman, SE
M. Omer Iqbal,
M (QAD)
Approved by
Zakir Noor Khan,

GM (K-2/K-3)
Page 2 of 278
OPERATING PROCEDURE
STANDARD OPERATING PROCEDURE FOR HIGH-SPEED

MIX BED RESIN REGENERATION WASTE WATER
RECYCLING, NEUTRALIZATION AND DISCHARGEING
PK237SOP24183K06145PC
Rev. 0
REVISION CONTROL SHEET
DecemberJUNEMarc M. Omer Iqbal, Zakir Noor

0 3562 h First issue Khan,
M (QAD)
20198 GM (K-2/K-3)
Rev Page Reviewed QA Reviewed Reason for Approved
No. Date
. By By Modification By
(s)
Page 3 of 278
Karachi Nuclear Power Waste Water Neutralizationing, S2TFCWDP004
Plant Unit-2 Recycling and DischargeingLoading
and Unloading Of Bulk Chemicals
PK237SOP24183K06145PC Agent Rev. 0
CONTENT
1. DESCRIPTION..............................................................................................................6
1.1 REFERENCE DOCUMENTS....................................................................................6
1.2 SCOPE..........................................................................................................................7
1.3 AUTHORIZATION.....................................................................................................7
1.4 DEFINITIONS AND ABBREVIATIONS.................................................................8
2. SPECIFICATIONS AND PRECAUTIONS..............................................................9
3. PRELMINARY CONDITIONS...............................................................................10
3.1 Particular Requirement.............................................................................................10
3.2 Electrical Requirements............................................................................................10
3.3 Mechanical Requirements.........................................................................................10
4. STARTUP PREPARATION.....................................................................................12
4.1 Initial Condition.........................................................................................................12
4.2 Instrument Control Power........................................................................................13
4.3 System Alignment......................................................................................................13
4.4 Power Supply..............................................................................................................22
5. START UP..................................................................................................................23
5.1 Neutralization discharge operation of #1 waste water pond..................................23
5.2 Neutralization discharge operation of #2 waste water pond..................................24
6. SHUT DOWN.............................................................................................................27
6.1 Shutdown operation of #1 waste water pond neutralization.................................27
6.2 Shutdown operation of #2 waste water pond neutralization.................................27
7. IN-SERVICE INSPECTION....................................................................................29
7.1 Waste water neutralization discharge units............................................................29
8. PARTICULAR OPERATION INSTRUCTION....................................................30
9. INCIDENTS...............................................................................................................31
9.1 The outlet water conductivity is abnormal after the recycling water mix bed
operating.....................................................................................................................31
9.2 Wastewater pump outlet PH values are abnormal.................................................32
Page 4 of 278
10. LOCAL OPERATOR SHEET.................................................................................34

11. ANNEXURE...............................................................................................................35
1. DESCRIPTION............................................................................................................6
1.1 Reference Documents..................................................................................................6
1.2 Scope..............................................................................................................................7
1.3 Authorization................................................................................................................7
1.4 Definitions and Abbreviations....................................................................................7
2. SPECIFICATIONS AND PRECAUTIONS..............................................................9
3. PRELMINARY CONDITIONS...............................................................................14
3.1 Particular requirement..............................................................................................14
3.2 Electrical requirements.............................................................................................14
3.3 Mechanical requirements..........................................................................................14
4. STARTUP PREPARATION.....................................................................................16
4.1 Initial condition..........................................................................................................16
4.2 Instrument control power.........................................................................................17
4.3 System alignment.......................................................................................................17
4.4 Power supply..............................................................................................................21
5. START UP..................................................................................................................23
5.1 Unloading acid operation (31% hydrochloric acid)...............................................24
5.2 Unloading alkali operation (32% Alkali).................................................................26
5.3 Ammonia cylinder loading and unloading operations...........................................29
5.4 Coagulant, antiscalant agent, reducer agents, and other RO cleaning drugs
loading and unloading operations............................................................................33
6. SHUT DOWN.............................................................................................................34
7. IN-SERVICE INSPECTION....................................................................................35
7.1 1# Concentrated acid storage tank level meter m...........................................35
7.2 2# Concentrated acid storage tank level meter m...........................................35
7.3 1# Concentrated alkali storage tank level meter m........................................35
7.4 2# Concentrated alkali storage tank level meter m........................................35
8. PARTICULAR OPERATION INSTRUCTION....................................................36
Page 5 of 278
9. INCIDENTS...............................................................................................................37
9.1 Industrial hydrochloric acid spill emergency response..........................................38
9.2 Industrial liquid alkali spill emergency response...................................................41
9.3 Accident treatment of ammonia leakage.................................................................43
10. LOCAL OPERATOR SHEET.................................................................................49
11. ANNEXURE...............................................................................................................50
ANNEXURE I 50
ANNEXURE II 62
Page 6 of 278
1. DESCRIPTION
1.1 REFERENCE DOCUMENTS
SYSTEM MANUALS
 Demineralized water productionCondensate water polishing system

KK917TFC001E02045GN QF017SDA001B30845GN AB CFC Chapter 1.
KK917TFC002E02045GN QF017SDA002B30845GN A C CFC Chapter
2.,3,4,5
KK917TFC003E02045GN QF017SDA006B30845GN AB CFC Chapter
3.6.1
KK917TFC004E02045GN QF017SDA016B30845GN A CFC Chapter
4.6.2
5.6.3
6.1.3,6.5
6.2.6,6.7
6.37,8
6.4.9
KK917TFC046E02045GN QF017SDAR09B30845GN AC CFC Chapter
6.6.9.1
KK917TFC007E02045GN QF017SDAD09B30845GN AC CFC Chapter
7.9.2
Page 7 of 278

KK917TFC008E02045GN QF017SDAA09B30845GN A CFC Chapter
8.9.3
QF017SDA010B30845GN KK917TFCD09E02045GNC A CFC Chapter
9.2.10
 Condensate water polishing system KK917TFCS09E02045GN A CFC
Chapter 9.3
QF017SDA011B30845GNKK917TFC010E02045GN A CFC Chapter 10.1
KK917TFC011E02045GNQF017SDA012B30845GN A CFC Chapter 11.2

Demineralized water production system QF017SDA013B30845GN A CFC
Listing
Demineralized water production system QF032SDA001B30845GN B CFC
Manual setting
Demineralized water production system QF037SDAAA1B30845SS B CFC
Alarms Manual
Instrumentation and control system schematic diagram （ SDA ） 07060YA-
YKS01-003 B CFC
Demineralized water production plant and storage tanks electrical
construction drawings:0LKU001TB Main switchboard system diagram
07060YA-DQS01-004 B CFC
Demineralized water production plant and storage tanks electrical
construction drawings:0LKV001TB Main switchboard system 07060YA-
DQS01-005 B CFC
Running procedure
Demineralized water production (pre-treatment) running procedures A0 PRE
Other
Page 8 of 278
SDA、SED、SER System operating parameters and alarm settings (debugged

version) 2013.01.31
SDA、SED、SER Process control logic (debugged version) 2013.01.3
Fangjiashan demineralized water production control system manual (2013.02.05）
1.2 SCOPE
This procedure applies to:

 This procedure applies to the input operation, output operation and
regeneration operation of the high-speed mix bed resin Neutralizing
discharge of acid-alkaliCaustic waste water of condensate polishing
systemLoading and unloading operations of liquid ammonia cylinder.;
 Recycling operation of cleaning waste water after ion exchange resin
generationUnloading operations of hydrochloric acid;
 Unloading operations of alkali;
Loading and unloading operations of flocculants, anti-scalant agent, reducer agents,
and other RO rinsing drugs
1.3 AUTHORIZATION
 In MCR, all operations shall be performed by MCR operator.;

 In local, all operations shall be performed by local operator with the
responsibility of the MCR operator or Deputy Supervisor.
1.4 DEFINITIONS AND ABBREVIATIONS
ABBREVIATIONS:
CI: Conventional IslandThis is a sample table

LV AC Network 380V System (CI Condensate
EPX:BU
Polishing)Cofferdam sluice gate
380V System BOP Auxiliaries System (CI Condensate
EPY:EPG:
Polishing)LV AC Network 380V System (CI Auxiliaries)
Grounding and lighting protection system380V220V Operation
ETP:EPH
Auxiliary Bus System (EC)
Local level measurementLV AC 380V System (CI Unit
LN:EPQ
Auxiliaries)
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Local pressure measurementLV AC Network 380V System

LP:EPT:
(Main Building)
Flow rate measurement6.6kV AC Normal Power Distribution
MD:ESD:
System D
Level measurement6.6kV AC Normal Power Distribution
MN:ESE:
System E
MO:FI: Electric MotorFilter or strainer for liquids Electronic filter
Pressure measurementPlant Computer Information and Control
MP:IIC:
System
Temperature measurementPlant Process Control Cabinet
MT:IPC:
System
JA: Power Breaker or cut-off
VD:KG Dematerialized water valveGrouped control station on screen
VK:KS Liquid waste valveProcessed logic information on screen
VR:KT: Reagent valvePrimary temperature element
VT:LN: Potable water valveLocal level measurement
Instrument Compressed Air Distribution SystemLocal pressure
WAI:LP:
measurement
WAP:MD Compressed Air Production SystemFlow rate measurement
WAS:MN: Service Compressed Air Distribution SystemLevel measurement
Conventional Island Liquid Waste Collection SystemElectric
WLC:MO:
Motor
Nuclear Island Demineralized Water Distribution
WND:MP:
SystemPressure measurement
WPW:MT Portable Water SystemTemperature measurement
CI:MV: Conventional IslandMeasurement of thrust-expansions-vibration
EPX:PO LV AC Network 380V System (CI Condensate Polishing)Pump
380V System BOP Auxiliaries System (CI Condensate
EPY:RS
Polishing)Heater
Grounding and lighting protection systemLocal pressure
ETP:SD
measurement
LN:SN Local level measurementPower Sectioning Switch
Local pressure measurementMiscellaneous on-off physical
LP:SZ
signal
Page 10 of 278
MD:TF Flow rate measurementScreening drum or screen

MN:TFE: Level measurementCondensate Extraction System
MO:TTV: Electric MotorCondenser Vacuum System
MP:VA: Pressure measurementAir valve
MT:VC Temperature measurementCirculating water valve
PO:VD: PumpDematerialized water valve
Dematerialized water valveCondensed water and feed water
VD:VL:
valve
VK:VN: Liquid waste valveIntermediate cooling water valve
VR:VT: Reagent valvePotable water valve
VT:WLC: Potable water valveCI liquid waste collection system
CI: Conventional Island
WAI: Instrument Compressed Air Distribution System
WAS: Service Compressed Air Distribution System
WCD: Conventional Island Demineralized Water Distribution System
WCF Circulating Water Filtration
WCI: Conventional Island Closed Cooling Water System
WCL Circulating Water Pwnp Lubrication System
WCP Cathodic Protection System
WCT Circulating Water Treatment System
WCW Circulating Water System
WLC: Conventional Island Liquid Waste Collection System
WPW Potable Water System
WSS: Station Sewer System
WUC Auxiliary Cooling Water System
XU Voltage detection or setpoint relay-comparator
DEFINITIONS
NONE.
Page 11 of 278
2. SPECIFICATIONS AND PRECAUTIONS

TCondensate Polishing System (TFC) is provided with one complete set of neutralization
facilities for acids-alkaliCaustic regeneration wastewater. The wastewater is sent to
WLC CI waste collection system after it is neutralized to pH 6-9.
There is gel-type strong acid cation exchange resin and gel-type strong alkaline anion
exchange resin in the high-speed mix bed with the total height of 1100mm, and the
cation-anion resin ratio of 1: 2. Mix beds operations are controlled by differential
pressure, outlet water conductivity, sodium, silica, etc. When one high-speed mix
bed runs to any of the following indications: a) outlet water conductivity (25 ℃) ≥
0.30μs / cm; b) mix bed differential pressure > 0.3MPa; c) outlet resin trapper
differential pressure ≥ 0.lMPa; d) outlet water sodium ion> 0.06 μg / L; e) outlet
water silica> l0μg / L, the system will automatically put the spare bed into service
and split the faulted bed.
Condensate Polishing System (TFC) is provided with two complete sets of outside
regeneration devices. One is used for the scrubbing and regeneration of cation
resin for cation bed, the other is used for the scrubbing, stratification, separation
and regeneration of cation and anion resin of high-speed mix beds. The outside
regeneration devices for cation beds are two regeneration towers being spare for
each other which can be used as resin storage towers. The outside regeneration
device of high-speed mix beds contains one resin separation tower, one cation
resin regeneration tower, one anion resin regeneration tower, and one resin mixing
and pluralized storage tower.
Regeneration of ineffective high-speed mix bed resin 1 send the ineffective resin to the
separation tower, and perform the air scrubbing with the remained mixed resin in
the tower which can be performed for several times, in order to remove the
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impurities and the broken resin adsorbed on the resin surface. Then backwash the
resin step by step to make the mixed resin stratify under sufficient backwashing,
and there will form obvious cation, anion two parts of resin layers 2 send the
regenerated resin in the mix and pluralized storage tower to the emptied operating
mix bed 3 send respectively the cation and anion resin in separation towers to their
own regeneration towers for scrubbing in order to backwash the tiny, broken resin
out, and then perform the acid, alkali replacement regeneration to make the
ineffective cation, anion resin be transited into OH- type and H +-type respectively,
and then perform the washing standard reaching 4 Send the already regenerated
cation and anion resin to the resin mix and pluralized storage tower for thoroughly
mixing and washing until the effluent is qualified. The resin will be stored in the resin
mix and pluralized storage tower for spare.
The FTC system sets up dedicated acid-alkali system for regeneration of the fore cation
beds and high-speed Mix bed ion exchange resin, including transportation, storage
metering, etc. The acid and alkali used for resin regeneration and wastewater
neutralization are concentrated sulfuric acid (H2SO4 concentration is 98%) and
high purity alkali (NaOH concentration is 32%).
Acid and alkali are transported to the field by dedicated tanks, and then discharged into
the corresponding high-level acid, alkali storage tanks by acid, alkali unloading
pumps. The high-level acid, alkali storage tanks send acid, alkali to corresponding
metering tanks by gravity self-flow. The tops of high-level acid, alkali storage tanks
metering tanks are connected to moisture absorber by pipelines, and are stuffed
with granular silica gel to absorb the water in the intake gas. Similarly, the tops of
high-level acid, alkali storage tanks metering tanks are connected to CO2 absorber
by pipelines, and are stuffed with granular alkaline lime to absorb the CO2 in the
intake gas.
The acid for regeneration from the fore cation bed goes through the acid ejector and
diluted with demineralized water, then be transferred to # 1, # 2 fore cation bed
resin regeneration towers. Cation resin is regenerate by diluted H2SO4 solution
with concentration of 3.5% ~ 5.5%.
Condensate Polishing System (FTC) is provided with one complete set of neutralization
facilities for acids-alkali regeneration wastewater. The wastewater is sent to SEK CI
waste collection system after it is neutralized to pH 6-9.
Condensate Polishing System (FTC) is also provided with one complete set of
wastewater recycling facilities used for processing the micro-polluted washing
drainage of resin regeneration anaphase. After the washing water is treated and its
quality meets recycling standards, it will be transferred to the recycling tank.
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Otherwise, it will be discharged and treated by recycling water mix bed and sent
back, when it meets the standard, to resin regeneration cleaning process for reuse.
The input and output programs, and the resin regeneration program of FTC system for
cation beds are started and stopped by manual buttons, and must be executed with
manual intervention which is slightly different from fore cation bed fully automatic
start-stop program.
Shall start the wastewater neutralization operation before the regeneration of FTC system
high-speed mix bed, refer to S2 FTC 004 waste water recycling and neutralization
discharging operating procedure.
During the FTC operations, there is danger of the secondary circuit losing water, the
water being polluted to impact the unit safety operation, so must be particularly
rigorous to prevent mis operation during the operation process.
Before the acid-alkali related operations, the operators shall have worn fully protective
equipment (helmets, masks or glasses, anti-acid-alkali clothes and shoes).
he bulk chemicals agent used to Fangjiashan Demineralized water production are:

flocculants (PACondensate Polishing System (TFC) is also provided with one
complete set of wastewater recycling facilities used for processing the micro-
polluted washing drainage (conductivity ≤10μs / cm) of resin regeneration
anaphase. After the washing water is treated and its quality meets recycling
standards (conductivity ≤0.07μs / cm), it will be transferred to the recycling tank.
Otherwise, it will be discharged and treated by recycling water mix bed and sent
back, when it meet the standard, to resin regeneration cleaning process for
reuse.C), anti-scalant agent (GTCTM- P300), reducer agent (sodium bisulfite),
regenerating agent (31% hydrochloric acid, 32% of NaOH), PH adjusting agent
(liquid ammonia) and RO device chemical rinsing agent (EDTA) .etc.
The TFC wastewater neutralization and recycling programs are automatic, the
regeneration program of recycling water mix bed ineffective resin is started up by
manual buttons, of which the backwashing straitening operation is operated by local
manual manipulationFlocculants is composed of PAC. Solid PAC (including about
30% of AL2O3 ), powdery state , in bag (25Kg / bag), easy to hygroscopic moisture.
Liquid PAC (including about 10% of AL2O3 ), liquid PAC with a weak acid, a certain
corrosive characteristics, when operate shall wear acid-proof fatigue uniform,
protective masks, masks, acid-proof gloves, work shoes specifically, maintain good
ventilation in the workplace, the staff need to work in the windward to the best of his
abilities. If PAC entered into eyes accidentally. must flush with water immediately, if
Page 14 of 278
it is serious should take hospital treatment; if skin contacted, then must flush with
plenty of water immediately, if it is serious should take hospital treatment; if
swallowed incautiously, then wash mouth immediately , rushed to the hospital for
treatment.
In order to protect the safety of the environment and wastewater discharging facilities, the
acid and alkaliCaustic wastewater can be sent to WLC CI waste collection system
only after it is neutralized to pH of 6-9.Anti-scalant agent is composed of GTCTM-
P300, liquid in barrels, 5 gallons / barrel, slightly acidic state, there is a certain
corrosive characteristics, when operate shall wear acid-proof fatigue uniform,
protective masks, masks, acid-proof gloves, work shoes specifically, maintain good
ventilation in the workplace, the staff need to work in the windward to the best of his
abilities. If anti-scalant agent entered into eyes accidentally. must flush with water
immediately, if it is serious should take hospital treatment; if skin contacted, then
must flush with plenty of water immediately, if it is serious should take hospital
treatment; if swallowed incautiously, then wash mouth immediately , rushed to the
hospital for treatment.
The reducer agent is composed of sodium bisulfite, solid in barrels or bag, 25kg / barrel
(bag), easy to hygroscopic moisture, with a weak acid, a certain corrosive
characteristics; it produce SO2 gas in the air which has a special smell and can
stimulate and corrode respiratory tract; it has a strong reduction, it is strictly
prohibited mix with oxidizing materials, its storage sites require dark and ventilation.
when operate shall wear acid-proof fatigue uniform, protective masks, masks, acid-
proof gloves, work shoes specifically, maintain good ventilation in the workplace,
the staff need to work in the windward to the best of his abilities. If reducer agent
entered into eyes accidentally. must flush with water immediately, if it is serious
should take hospital treatment; if skin contacted, then must flush with plenty of
water immediately, if it is serious should take hospital treatment; if swallowed
incautiously, then wash mouth immediately , rushed to the hospital for treatment.
CBefore operations related to acid and alkaliCaustic, the operator must wear acid-
alkaliCaustic safety protection equipment’s (wear helmet, face shield or glasses,
anti acid-alkaliCaustic clothes and shoes).
ation resin regenerating agent is composed of hydrochloric acid. Concentration of of liquid

hydrochloric acid is 31%, should meet excellent grade requirements of the GB 320-
2006 " synthetic hydrochloric acid for industrial use " standard : concentration
≥31%, [Fe] ≤0.002%, amount of ignition residue≤0.05%, [SO42-] ≤0.005%.
Hydrochloric acid with strong-acid, volatile, and generate acid mist when it combine
with atmospheric water vapor, with a strong corrosive characteristics and irritating
characteristics. If the hydrochloric acid leak, it will lead to serious disasters of
Page 15 of 278
combustion, explosion, corrosion, poison, etc., Once contacted to the exposed

parts of the body will cause skin burns, severe even may disfigurement or life-
threatening, when operate shall wear acid-proof fatigue uniform, protective masks,
masks, acid-proof gloves, work shoes specifically, maintain good ventilation in the
workplace, the staff need to work in the windward to the best of his abilities. If
reducer agent entered into eyes accidentally. must flush with water immediately, if it
is serious should take hospital treatment; if skin contacted, then must flush with
plenty of water immediately, if it is serious should take hospital treatment; after
flushing with water it required local emergency medicine to clean(0.5% liquid
sodium bicarbonate); if swallowed incautiously, then wash mouth immediately ,
rushed to the hospital for treatment.
Cation resin regenerating agent is composed of sodium hydroxide. Concentration of liquid

NaOH is 32%, should meet the excellent grade requirements of "high purity of
sodium hydroxide" GB / T 11199-2006 : the concentration of NaOH ≥32%, sodium
carbonate ≤0.06%, sodium chloride ≤0.007%, ferric oxide ≤0.0005%, sodium
chlorate ≤0.002%, Al2O3 ≤0.0006%, SiO2 ≤0.002%, sulfate (Na2S04) ≤0.002%.
Sodium hydroxide with strong alkali, a strong corrosive characteristics and irritating
characteristics. If alkali lye leaked or spilled, Once contacted to the exposed parts
of the body will cause skin burns, severe even may disfigurement or life-
threatening, when operate shall wear acid-proof fatigue uniform, protective masks,
masks, acid-proof gloves, work shoes specifically, maintain good ventilation in the
workplace, the staff need to work in the windward to the best of his abilities. If
NaOH entered into eyes accidentally. must flush with water immediately, if it is
serious should take hospital treatment; if skin contacted, then must flush with plenty
of water immediately,, then it required local emergency medicine to clean (2% boric
acid solution), if it is serious should take hospital treatment; after flushing with water
it required local emergency medicine to clean (1% acetic acid); if swallowed
incautiously, then wash mouth immediately , rushed to the hospital for treatment..
PH regulating agent of SERWCD Demineralized water is composed of ammonia.

Ammonia is liquid ammonia which is in liquid ammonia tank, N.W. 400Kg / bottle
(bottles weighing about 500Kg), so the total weight of a bottle of ammonia
approximates 900Kg. Although alkaline of ammonia is not stronger than NaOH, but
once the ammonia leaked, a lot of smoke will emerge from the leak , and
surrounding environment will be a strong pungent odor, if there is fire, it is easy to
explosive. Inhale low concentrations will have a stimulating effect on the mucous
membranes, if concentrations is high, it may cause histolysis necrosis, and it cause
chemical pneumonia and burns. when operate shall wear acid-proof fatigue
uniform, protective masks, masks, acid-proof gloves, work shoes specifically,
maintain good ventilation in the workplace, the staff need to work in the windward to
Page 16 of 278
the best of his abilities. If accidentally skin or eyes contaminated with it, must flush
with plenty of water 15 minutes or more, and rushed to the hospital for treatment
immediately; if inhaled ammonia accidentally, be out of the contaminated area
quickly, if breathing is weak or stops, carry out artificial respiration immediately.
The regenerating agent which is used for cation resion regenerate of Fangjiashan
condensate Polishing is sulfuric acid, and the WDPSDA system used a hydrochloric
acid, so each time you unload, you must confirm the type of acid and acid delivery
locations to send personnel to avoid sending or mixing acid event mistaken. And
should identify eye-catching "hydrochloric acid" two words particularly in the mouth
of acid unloading, not only identified as "acid" or " alkali."
Acid unloading mouth, alkali unloading mouth, acid and alkali storage room, ammonia
bottle storage room must have a dedicated safety showers and eyewash near,
when accident , it facilitatefacilitates personnel emergency . In addition, it should
configure large flow flushing pipes and rinse nozzle, it is easy to clean、diluted and
fire extinguishing when acid, alkali leak..
According to regulations of the State Council, "The Regulations of Precursor Chemicals "
(State Council Decree No. 445) and the other laws, sulfuric acid, hydrochloric acid,
belongs to the third category of precursor chemicals, buy sulfuric acid, hydrochloric
acid should record the management by the public department , sales sulfuric acid、
hydrochloric acid should be recorded by safety supervision departments of the
district administration, the illegal trade of sulfuric acid, hydrochloric acid should be
investigated by the public, industry and commerce department ,safety supervision
departments ,in accordance with their respective responsibilities. So when
requisitioned hydrochloric acid, 10 to 15 days in advance, should call the
Commerce Department to prepare for the acid into, Commerce arrange for
personnel escorted the acid to the designated location. Operating personnel should
deal with the safekeeping of hydrochloric after it is put in storage, each outfall
should be strictly locked, set up special management.
In YADP building, it must have adequate amounts of the chemical cleaning agents within
period of validity after acid burns (0.5% sodium bicarbonate solution), must have a
sufficient amount of the chemical cleaning agents within period of validity after alkali
burns (1% acetic acid solution and 2% boric acid solution), facilitate emergency
personnel for acid- alkali leakage.
Ammonia cylinders stored in the warehouse of chemicals, required recipients to drive the
forklift when the shipment. In forklift transportation process, liquid ammonia cylinder
must be effective fixed not brakes in the way, ammonia cylinders easily slipped from
the forklift, if light, it damage to storage tanks, if severe ,it cause injury or ammonia
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leak. And speed of forklift travel is not more than 10 km / h.
Chemical storage room in YADP building should be equipped with forced ventilation
device, explosion-proof lights, and ensured to be available readily. Before personnel
enter to the storage room, forced ventilation should be operated, after forced
ventilation operated 1 to 2 minutes, then lit , after that staff can enter.
Chemicals in YADP building should be storage in strictly classified, the same class of
drugs should be stored in batches time of purchase, first come, first use; it must
have eye-catching logos and safe tips in medicines partition storage area to avoid
drug misuse, mix.
During chemical loading and unloading, the staff must wear protective equipment PH :
acid clothes, work shoes, gloves, masks and dip plastic gloves.。
Page 18 of 278
PRELMINARY CONDITIONS
Operation
Operation Steps Check Identification Remarks
Location
Particular Requirement
The operators have worn fully [ ][ ]

protective equipments
(helmets, masks and anti-acid
clothes)The operator has been
installed for safety equipment
(wear helmet, mask and anti-
acid clothes).
In the area that personnels may be [ ][ ]
acid burned, shall furnished
with the chemical cleaning
reagents (0.5% sodium
bicarbonate solution)In the
area of personnel may be acid
burns, must be equipped with
chemical cleaning agents after
acid burns (0.5% sodium
bicarbonate solution).
alkiline burned, shall furnished
with the chemical cleaning
reagents (1% acetic acid
solution and 2% boric acid
solution).In the area of
personnel may be
alkaliCaustic burns, must be
equipped with chemical
cleaning agents after
alkaliCausticne burns (1%
acetic acid solution and 2%
boric acid solution).
Page 19 of 278
Operation
Location
acid and alkiline burned, set
eyewashers and safety
showers which should be
available.Personnel may be
acid, alkaliCaustic burn area,
set eyewash, safety showers
and checked regularly to
ensure it becomes available.
2.2 Electrical requirementElectrical

requirementsRequirements
The following switchboard available

[ ]
The following electrical systems
should be available:1LV AC Network -
380V - (CI Condensate Polishing)
EP9EDLBX DPYA
K
10V DC Power System
(demineralization plant and auxiliary
boilers)
380V AC Power System [ ]

BLV AC Network - 380V - (CI
Condensate Polishing)
OPLow-voltage AC network 90EPYLKU DPYA
380V AC power supply system
(YADP building)
Available220V AC Power System [ ][ ]

(PLC control cabinet power supply)
BOP 380V AC power supply system 90ELKV DPYA
(DP building)Low-voltage AC
network 380V system (YA building)
Page 20 of 278
Operation
Location
110V DC Power
9ETP0LTR DPYA
SystemGrounding and
Lightning Protection system
Available48V DC Power []
System
Grounding and lighting 9ETP
protection system
AvailableTFC Control System [ ][ ] TFC
110V DC Power System
Mechanical
Rrequirementsequirements
AvailableThe following []
systems are available and in
service：
48V DC Power System [ ]
WPW0SEP
Potable Water Systems
AvailableDemineralized water [ ][ ] WND9WDP
from WND production system 0SDA
Conventional island liquid [
WLCSS0SE
waste systemStation Sewer ]
O
System
The following systems should also be [ ]
FMC0JPS
available:Mobile Fire Fighting System
The following systems should

also be available:Compressed
air Distribution systemEquipped [ ] WAI
with forklift truck which load
more than 1000 Kg.
Grounding and Lightning Protection

System
[ ][ ] 1LTRWAP 1MX702
AvailableCompressed Air Production
System
Page 21 of 278
Operation
Location
KIC System [ ][ ]
AvailableService compressed air KICWAS
distribution System
TFCATE Control System []
Available ATETFC 1MP
2.3 Mechanical requirement
Demineralized water from SED

Available [] SED 1MX
Compressed Air Production System

[] SAP ZC
Available
Service Compressed Air Distribution
[] SAT 1MX
Available
Condensate Polishing System
[] ATE 1MP
Available
Conventional Island Liquid Waste
Collection System [] SEK 1MX
Available
Condensate Extraction System
[] CEX 1MX
Available
Chemical Addition Building
HVAC System [] DVY 1MX、1MP
Available
Drinking Water System
[] SEP 1MX、1MP
Available
Page 22 of 278
3. STARTUP PREPARATION
Operator
location
INITIAL CCONDITION
When two
3.1 Initial conditionAt least one concentrated
waste water neutralization pond acid storage
is availableconcentrated acid tanks are
storage tank. available, after
the level
3.2 is available . dropped below
1.4 m then can
require to
High-speed mix bed is available #1 purchase
1# waste water pond Concentrated hydrochloric
acid storage tank acid (10
tons)；
1ATE201DE2
1MX101Y
availableAvailable [ ][ ] TFC471PS9W * Only one
BDT
DP501BA concentrated
available #2 2# waste water pond is acid storage
availableConcentrated acid storage [] 1ATE202DE 1MX101 tank is
tanks available, after
the level
dropped below
0.7m then can
1ATE203DE2
1MX101Y require to
availableAvailable [ ][ ] TFC472PS9W
BDT purchase
DP502BA
hydrochloric
acid (10
tons)；
available [] 1ATE204DE 1MX101
availableAcid and Caustic [ ][ ] 1ATE205DE 1MX101 When two
regeneration unit is concentrated
available.At least one alkali storage
concentrated alkali storage tank are
tank is available available, after
Page 23 of 278
Operator
location
Mix bed recirculation pump 2TFC411CW9

[ ] YBDT
available：Available WDP601BA
1ATE201PO2
AvailableAvailable [ ][ ] 1MX101
TFC412CW
Dehydrating Breather2#
the level
Concentrated alkali storage tank
dropped below
Condensate Polishing control system 2TFC411AD9 1.4 m then can
[ ] YBDT require to
available：Available WDP602BA
purchase liquid
1ATE001AR2 alkali (10
AvailableAvailable [ ][ ] 1MP302
TFC412AD tons)；
Available Only one
Available 1#CO2 Absorber concentrated
[] 1ATE002AR 1MP302
Anyone mix bed acid alkali storage
metering pump is available tank is
1ATE003AR2 available, after
1MP302Y the level
AvailableAvailable [ ][ ] TFC415PO9
BDT dropped below
WDP601DS
1ATE004AR2 0.7m then can
AvailableAvailable [ ][ ] 1MP302 require to
TFC416PO
purchase liquid
AvailableAnyone 2#CO2
alkali (10
Absorber of caustic storage [] 1ATE005AR 1MP302
tons)；
tank is available.
1ATE001HC2
1MP302Y
AvailableAvailable [ ][ ] TFC421CW9
BDT
WDP6021DS
1ATE002HC2
TFC422CW
At least one waste water

2TFC421AD9
neutralization pond is available, and [ ] YBDT
WDP601PO
is at low levelAvailable
1ATE471PS2
TFC422AD
Page 24 of 278
Operator
location
AvailableAnyone mix bed caustic
[] 1ATE472PS 1MX101
metering pump is available
Available [ ] 2TFC423PO
High-speed mix bed resin

regeneration units are [ ] 2TFC424PO
availableAvailable
AvailableWater Heater
[] 1ATE301CW 1MX101
Tank
1ATE302CW2
TFC431CW
AvailableSafety Shower [] 1ATE303CW 1MX101
1ATE304CW2
TFC600DO
AvailableTFC
Demineralized water tank,
flush pump and 1ATE306CW 1MX101
regeneration pump is
available.
TFC Demineralized water storage
tank
Acid, alkali regeneration units are [ ] 2TFC441BA

availableAvailable
Available # 1 Flushing Pump [] 1ATE411PO 1MP303

1ATE412PO2
TFC441PO
High acid storage tank

[] 1ATE411CW 1MP303
Available, level is higher than
0.5 m # 2 Flushing Pump
1ATE412CW2 1MP303
AvailableAvailable [ ][ ]
TFC442PO
Page 25 of 278
Operator
location
1MP303
[] 1ATE411EJ
Available #1 Regeneration pump
1ATE411AD2 1MP303
TFC443PO
Available #2 Regeneration 1ATE412AD2 1MP303
[]
pump TFC444PO
AvailableAvailable [ ][ ] 1ATE421PO 1MP303
AVAILABLEINSTRUMENT 1MP303
[] 1ATE422PO
CCONTROL PPOWER
1MP303
High alkali storage tank
[ ][ ] 1ATE421CW
Available level is higher than
0.5 mNone.
AVAILABLESYSTEM 1MP303
[] 1ATE423CW
AALIGNMENT
AvailableConcentrated acid 1MP303
[] 1ATE421EJ
system alignment
CO2 absorber Available 1MP303
[] 1ATE421AD
Close the following valve
1ATE423AD9 1MP303Y
CO2 absorber AvailableClose [ ][ ]
WDP510VK BDT
Safety shower Available Open
[] 1ATE441AD 11MP303
the following valve
Open [ ] 9WDP511VR YBDT
Condensate polishing demineralized
water tank, regeneration pumps, flush
[]
water pumps are available Close the
following valve
Polishing demineralized water
1ATE441BA9 1PBYBD
tank [ ][ ]
WDP512VTE T
AvailableClose
#1 flushing water pump
[] 1ATE441PO 1MX101
Available Open the following valve
Page 26 of 278
Operator
location
#2 flushing water pump 1ATE442PO9 1MX101Y
[ ][ ]
AvailableOpen WDP513VR BDT
#1 regeneration pump 1ATE443PO9 1MX101Y
[ ][ ]
#2 regeneration pump 1ATE444PO9 1MX101Y
[ ][ ]
Recycling water units are available
[]
Recycling tank 1ATE481BA9 1MX101Y
[ ][ ]
AvailableClose WDP520VK BDT
Recycling pump
[] 1ATE481PO 1MX101
Available Open the following valve
Recycling water mix bed 1ATE481DN9 1MX101Y
[ ][ ]
Compressed air units are 9WDP522VT
[ ][ ] YBDT
availableClose E
Instrument compressed air
storage tank [ ] 1ATE502CW 1MX301
AvailableOpen the following valve
Technology compressed air storage 1ATE501CW 1MX301Y
[ ][ ]
tank AvailableOpen 59WDP23VR BDT
At least two Roots fans are
[ ][ ] 9WDP525VR YBDT
vailableOpen
#1 roots blower available 1ATE461ZV9 1MX101Y
[ ][ ]
#2 roots blower available
[] 1ATE462ZV 1MX101
AvailableClose the following valve
#3 roots blower available 1ATE463ZV9 1MX101Y
[ ][ ]
AvailableClose WDP5010VR BDT
9WDP50417
Close [ ] YBDT
VR
Page 27 of 278
Operator
location
High-speed mix beds associated
solenoid valve boxes and sampling
detection units are [] 1MX101
availableUnloading acid pump outlet
check valve
High-speed mix bed #1 solenoid 9WDP50318
[ ] YBDT
valve boxAvailable VR
AvailableOpen the following valve [] 1ATE201AR 1MX101
High-speed mix bed #2 solenoid 9WDP687VT
[ ] YBDT
valve boxOpen 507VE
1ATE202AR9
1MX101Y
AvailableOpen [ ][ ] WDP50219V
BDT
R
High-speed mix bed #3 solenoid
valve box1# Concentrated acid
storage tank level meter
1ATE203AR9 1MX101Y
WDP501MN BDT
Net condensate pump and # 1 mix
bed instrument frame2#
Concentrated acid storage tank level
meter
1ATE202CR9 1MX101Y
WDP502MN BDT
Relevant Alignment of check
of compressed air
valvesConcentrated alkali
system alignment
Available [] 1ATE421AD 1MP303
Page 28 of 278
Operator
location
Condensate polishing demineralized

water tank, regeneration []
pumps, flush water pumps
are available
Available [] 1ATE441BA 1PB

Should have
at least one
Available [] 1ATE441PO 1MX101
station
available
Should have
at least one
station
available
Recycling water units are available []
Available [] 1ATE481BA 1MX101

[] 1ATE481DN 1MX101
Available
Compressed air units are available []
Available [] 1ATE502CW 1MX301

Available [] 1ATE501CW 1MX301
At least two Roots fans are available []
[] 1ATE461ZV 1MX101
Available
[] 1ATE462ZV 1MX101
Available
Page 29 of 278
Operator
location
[] 1ATE463ZV 1MX101
Available
High-speed mix beds associated

solenoid valve boxes and [] 1MX101
sampling detection units are
available
Available [] 1ATE201AR 1MX101

Available [] 1ATE203CR 1MX101
Alignment Check and

Operations of Waste water
Ponds.
Available Waste water collection
1ATE204CR2
Tank [ ][ ] 1MX101
TFC442BA
Available
#1 Waste water Transfer Pump
[ ] 2TFC473PO
Available
Available #2Waste water Transfer
1ATE301AR2
Pump [ ][ ] 1MX101
TFC474PO
Available
#3 Waste water Transfer Pump
[ ] 2TFC475PO
Available
Available #4 Waste water Transfer
1ATE302AR2
Pump [ ][ ] 1MX101
TFC476PO
Available
#1 Waste water pond
[ ] 2TFC471PS
Available
Available #1 Waste water pond inlet
1ATE303AR2
valve. [ ][ ] 1MX101
TFC631VK
Available
#1 Waste water discharge pump
[ ] 2TFC471PO
Available
Page 30 of 278
Operator
location
Available #1 Waste water discharge
1ATE304AR2
pump outlet check valve. [ ][ ] 1MX101
TFC636VK
Available
outlet valve [ ] 2TFC632VK
Open
Available#1 Waste water discharge
1ATE302CR2
pump recirculation valve. [ ][ ] 1MX101
TFC633VK
Closed
#1 Waste water pond Acid inlet valve
[ ] 2TFC629VR
Closed
Available#1 Waste water pond
1ATE403CR2
caustic inlet valve [ ][ ] 1MX101
TFC627VR
Closed
#1 Waste water pond pressure
gauge. [ ] 2TFC471LP
Available
Available#1 Waste water pond
1ATE305AR2
pressure gauge root valve. [ ][ ] 1MX101
TFC635VK
Open
#1 Waste water pond sampling
solenoid valve. [ ] 2TFC631EF
Closed
Available Waste water neutralizing
1ATE401AR2
discharge PH meter. [ ][ ] 1MX101
TFC470MG
Available
#2 Waste water pond
[ ] 472PS
Available
Available #2 Waste water pond inlet
1ATE401CR2
valve. [ ][ ] 1MX301
TFC641VK
Open
[ ] 2TFC472PO
Available
Available #2 Waste water discharge
1ATE402CR2
pump outlet check valve. [ ][ ] 1MP303
TFC646VK
Available
Page 31 of 278
Operator
location
3.3 Instrument Control Power

outlet valve [ ] 2TFC642VK
Open
recirculation valve. [ ] 2TFC644VK
Closed
#2 Waste water pond Acid inlet valve
[ ] 2TFC630VR
Closed
Closed#2 Waste water pond caustic
1LMC171JA2
inlet valve [ ][ ] 1MX702
TFC628VR
Closed
#2 Waste water pond pressure
gauge. [ ] 2TFC472LP
Available
Closed#2 Waste water pond pressure
1LMC2TFC64
gauge root valve. [ ][ ] 1MX702
5VK
Open
#2 Waste water pond sampling
solenoid valve. [ ] 2TFC641EF
Closed
ClosedAlignment check of [] 020JA 1ATE001
Checkacid storageoftank
ANYONE and
the acid AR
storage tank available.
020JA2TFC41
TrippingAvailable, the level > 0.5m [ ][ ] 1ATE001
1CW
Available, the level > 0.5m [ ] AR
2TFC412CW
Alignment of 2TFC411CW
Closed2TFC411CW blowdown primary 1ATE002
[] 020JA
AND secondary Valve. AR
Closed [ ] 2TFC536VR
Page 32 of 278
Operator
location
Closed2TFC411CW level 1ATE002
[] 020JA
meter AR
Available [ ] 2TFC411MN
Closed2TFC411CW level
1ATE003
meter root valve #1 and root [] 020JA
AR
valve #02
Open [ ] 2TFC538VR
Open [ ] 2TFC539VR
Closed2TFC411CW outlet 1ATE003
[] 020JA
primary AND secondary Valve AR
Primary valve, Open [ ] 2TFC534VR
Secondary valve, Open [ ] 2TFC535VR
Closed2TFC411CW 1ATE004
[] 020JA
dehydrating breather AR
Available [ ] 2TFC411AD
ClosedAlignment of 1ATE004
[] 020JA
2TFC412CW AR
2TFC412CW blowdown
primary AND secondary
Valve.
020JA2TFC54
ClosedClosed [ ][ ] 1ATE002
4VR
Closed [ ] AR
2TFC545VR
2TFC411CW level meter
020JA2TFC41 1ATE002
ClosedAvailable [ ][ ]
2MN AR
2TFC412CW level meter root
valve #1 and root valve #02
020JA2TFC54
ClosedOpen [ ][ ] 1ATE002
6VR
Open [ ] AR
2TFC547VR
Page 33 of 278
Operator
location
2TFC412CW outlet primary AND
secondary Valve
020JA2TFC54
ClosedOpen [ ][ ] 1ATE002
2VR
Open [ ] AR
2TFC543VR
2TFC412CW dehydrating breather
ANYONE mixed bed acid
metering pump
020JA2TFC41 1ATE002
ClosedAvailable [ ][ ]
5PO AR
Closed2TFC415PO inlet and 1ATE002
[] 020JA
Outlet valves AR
Inlet valve, Open [ ] 2TFC415PO
020JA2TFC41 1ATE003
ClosedOutlet valve, Open [ ][ ]
5PO AR
2TFC416PO inlet and Outlet
valves
020JA2TFC41 1ATE003
ClosedInlet valve, Open [ ][ ]
6PO AR
Outlet valve, Open [ ] 2TFC416PO
3.4 System alignmentMixed bed

acid metering outlet header 2TFC413LP
pressure gauge available
Confirm 1ATE programmable

cabinets, IPC have been put into
service. IPC operating screen is
available. Otherwise, notify by
telephone the instrument control
personnel to startup these devices.
Root valve, Open [ ] 2TFC566VR
Page 34 of 278
Operator
location
StartupMix bed acid metering pump
[] 1ATE002AR 1MP302
outlet acid concentration meters.
1ATE003AR2
StartupAvailable [ ][ ] 1MP302
TFC411MG
StartupStainless steel dilute acid
[] 1ATE004AR 1MP302
solution manual sampling valve
1ATE001HC2
Startup [ ][ ] 1MP302
TFC583VR
StartupCation Acid
[] 1ATE002HC 1MP302
metering pump inlet valve
Relevant alignment check of [ ] 2TFC553VR

compressed air pipelinesClosed
Alignment check of Caustic storage

tank and caustic metering pump.
ShutdownCheck ANYONE of the
[] 1029VA 1MX301
caustic storage tank available.
Available, the level > 0.5m [ ] 2TFC421CW
Available, the level > 0.5m [ ] 2TFC421CW
Available Alignment of 2TFC421CW [] 1030VA 1MX301
2TFC421CW blowdown primary
AND secondary Valve.
2029VA2TFC
ShutdownClosed [ ][ ]
736VR 1MX101
Closed [ ]
2TFC737VR
2TFC421CW level meter
2030VA2TFC
421MN
2TFC421CW level meter root valve
#1 and root valve #02
4830VA2TFC
ShutdownOpen [ ][ ]
738VR 1MX101
Open [ ]
2TFC739VR
Page 35 of 278
Operator
location
2TFC421CW outlet primary AND
secondary Valve
4833VA2TFC
AvailablePrimary valve, Open [ ][ ]
734VR 1MX301
Secondary valve, Open [ ]
2TFC735VR
2TFC421CW CO2 absorber
3712VA2TFC
ShutdownAvailable [ ][ ] 1MX101
421AD
Alignment of 2TFC422CW
Shutdown 2TFC422CW blowdown
[] 3812VA 1MX101
primary AND secondary Valve.
Shutdown 2TFC422CW level meter [ ] 3111VA 1MX101
Shutdown 2TFC422CW level meter
[ ] 3212VA 1MX101
root valve #1 and root valve #02
Open [ ] 2TFC746VR
Open [ ] 2TFC747VR
Shutdown 2TFC422CW outlet
[ ] 3312VA 1MX101
primary AND secondary Valve
Primary valve, Open [ ] 2TFC742VR
Secondary valve, Open [ ] 2TFC743VR
Shutdown 2TFC422CW CO2
[ ] 3412VA 1MX101
absorber
Available ANYONE mixed
[ ] 501CW 1MX301
bed caustic metering pump
4502VA2TFC
424PO
2TFC423PO inlet and Outlet
valves
4521VA2TFC
AvailableInlet valve, Open [ ][ ] 1MX301
750PO
Page 36 of 278
Operator
location
Outlet valve, Open [ ] 2TFC752PO
Available 2TFC424PO inlet
[ ] 4522VA 1MX301
and Outlet valves
Inlet valve, Open [ ] 2TFC753PO
4523VA2TFC
AvailableOutlet valve, Open [ ][ ] 1MX301
755PO
Mixed bed acid metering
2TFC4
outlet header pressure gauge
22LP
available
4504VA2TFC
AvailableRoot valve, Open [ ][ ] 1MX301
756VR
Mix bed acid metering pump
outlet acid concentration
meters.
4511VA2TFC
421MG
Stainless steel dilute acid
solution manual sampling
valve
4520VA2TFC
Available [ ][ ] 1MX301
773VR
Alignment check of
Regeneration pumps, Heating
tanks and Regeneration
pipelines.
Shut down Cation bed acid
[ ] 4505VA 1MX101
dilution line inlet valve
Available Mix bed acid dilution
[ ] 451MP 1MX301
inlet valve
[ ] 451LP 1MX301
inlet check valve
Page 37 of 278
Operator
location
Open Mix bed acid
[ ] 4571VL 1MX301
regeneration flowmeter
Available [ ] 2TFC411MD
Open Mix bed acid
regeneration flowmeter root [ ] 4573VL 1MX301
valve #1
Open [ ] 2TFC574VD
Open Mix bed acid
regeneration flowmeter root [ ] 4501VA 1MX101
valve #2
Open [ ] 2TFC575VD
Open Cation bed acid dilution inlet
[] 4503VA 1MX101
manual valve
Available [ ] 2TFC570VR
[ ][ ] 502CW 1MX301
inlet manual valve
Available [ ] 2TFC580VR
Available Mix bed caustic
[ ] 4524VA 1MX301
regeneration flow meter
Available [ ] 2TFC421MD
AvailableMix bed caustic
valve #1
Open [ ] 2TFC774VD
AvailableMix bed caustic
valve #2
Open [ ] 2TFC775VD
Shut downHot Water Tank [ ] 4510VA 1MX301
Available [ ] 2TFC431CW
AvailableHot Water Tank
[ ] 452MP 1MX301
upper drainage valve
Closed [ ] 2TFC783VK
AvailableHot water Tank
[ ] 452LP 1MX301
blowdown valve
Page 38 of 278
Operator
location
OpenHot water tank
thermostatic proportional [ ] 4572VL 1MX301
control valve
Available [ ] 2TFC780VD
OpenHot water tank safety
[ ] 4574VL 1MX301
valve
Available [ ] 2TFC784VJ
OpenHot water Tank Inlet
[ ] 4506VA 1MX301
valve
Open [ ] 2TFC781VD
OpenHot water tank pressure
[ ] 4508VA 1MX301
gauge
Available [ ] 2TFC431LP
OpenHot water tank pressure
[ ] 4541VA 1MX101
gauge root valve
Open [ ] 2TFC790VD
OpenHot water Tank pressure
[ ] 4542VA 1MX101
switch
Available [ ] 2TFC431SN
OpenHot water tank
[ ] 4543VA 1MX101
thermometer
Available [ ] 2TFC431LT
OpenRegeneration water
[ ] 4544VA 1MX101
Temperature switch
Available [ ] 2TFC421KT
OpenHot water Tank
[ ] 4545VA 1MX101
Temperature switch
Available [ ] 2TFC431KT
OpenRegeneration Pump
[ ] 4546VA 1MX101
pressure regulating valve
Open#1 Regeneration pump
[ ] 4547VA 1MX101
inlet and Outlet valve
Page 39 of 278
Operator
location
Inlet valve, Open [ ] 2TFC503VD
4548VA2TFC
OpenOutlet Valve, Open [ ][ ] 1MX101
513VD
#1 Regeneration pump outlet
check valve
4549VA2TFC
OpenAvailable [ ][ ] 1MX101
507VD
pressure gauge
4550VA2TFC
OpenAvailable [ ][ ] 1MX101
443LP
pressure gauge root valve
4551VA2TFC
OpenOpen [ ][ ] 1MX101
956VD
#2 Regeneration pump inlet
and Outlet valve
4552VA2TFC
OpenInlet valve, Open [ ][ ] 1MX101
504VD
Outlet Valve, Open [ ] 2TFC514VD
[ ] 4553VA 1MX101
outlet check valve
[ ] 4554VA 1MX101
outlet pressure gauge
Available [ ] 2TFC444LP
Set the following solenoid valve

boxes related valve control modes to
"Remote operation" state#2
Regeneration pump outlet pressure
gauge root valve
1ATE201AR2
Remote operationOpen [ ][ ] 1MX101
TFC957VD
Page 40 of 278
Operator
location
Remote
operationRegenerative pump [ ] 1ATE202AR 1MX101
outlet header flowmeter
1ATE203AR2
Remote operationAvailable [ ][ ] 1MX101
TFC442MD
Remote
operationRegenerative pump
[ ] 1ATE301AR 1MX101
outlet header flowmeter root
valve #1
1ATE302AR2
TFC958VD
Remote
operationRegenerative pump
[ ] 1ATE303AR 1MX101
outlet header flowmeter root
valve #2
1ATE304AR2
TFC959VD
Remote operationAlignment
Check and Operation of [ ] 1ATE401AR 1MX101
Demineralized water tank
Available [ ] 2TFC441BA
Demineralized water Tank
level meter
Remote operation [ ] 1ATE401CR 1MX301
Alignment confirmation and operation

of polishing sampling detection units
Demineralized water tank blowdown
valve
Available [] 001RC 1MX301

Page 41 of 278
Operator
location
inlet and outlet valve
Inlet valve, Available [ ] 2TFC516VD
Outlet valve, Open [ ] 2TFC500VD
Cooler of #1 mix bed water sample
211RF9WDP 1MX101Y
AvailableClose [ ][ ]
610VK BDT
Pressure relief valve of #1 mix bed
water sample Open the following
valve
2184VL9WD 1MX101Y
AvailableOpen [ ][ ]
P611VR BDT
Isolation valve 1 of #1 mix bed water
sample Close the following valve
2183VL9WD 1MX101Y
OpenClose [ ][ ]
P612VTE BDT
Isolation valve 2 of #1 mix bed water
sample Open the following valve
2190VL9WD 1MX101Y
OpenOpen [ ][ ]
P613VR BDT
Safety valve of #1 mix bed water
[ ] 9WDP614VR YBDT
sampleOpen
2185VL9WD 1MX101Y
P615VR BDT
Blowdown valve of #1 mix bed water
[ ] 9WDP616VR YBDT
sampleOpen
Closed 1#CO2 Absorber [] 2189VL 1MX101
Pressure gauge of #1 mix bed water
[ ] 9WDP601DS YBDT
sampleAvailable
Available Close the following valve [] 213LP 1MX101
Conductivity meters of #1 mix bed
[ ] 9WDP620VK YBDT
water sampleClose
AvailableOpen the following valve [] 211MG 1MX101
Page 42 of 278
Operator
location
211LG9WDP 1MX101Y
621VR BDT
Isolation valve of #1 mix bed water
sample conductivity metersClose the
following valve
2186VL9WD 1MX101Y
OpenClose [ ][ ]
P622VTE BDT
Flow meter of #1 mix bed water
sample conductivity metersOpen the
following valve
211LD9WDP 1MX101Y
623VR BDT
#1 mix bed water sample Na
[ ] 9WDP624VR YBDT
metersOpen
212MG9WDP 1MX101Y
625VR BDT
212LG9WDP 1MX101Y
626VR BDT
Isolation valve of #1 mix bed water
sample Na meter2#CO2 Absorber
2187VL9WD 1MX101Y
OpenAvailable [ ][ ]
P602DS BDT
Flow meter of #1 mix bed water
sample Na meterClose the following
valve
212LD9WDP 1MX101Y
AvailableClose [ ][ ]
6010VR BDT
#1 mix bed water sample Si 9WDP60417
[ ] YBDT
meterClose VR
AvailableUnloading alkali pump outlet
[] 204MG 1MX101
check valve
Isolation valve of #1 mix bed water 9WDP60318
[ ] YBDT
sample Si meterAvailable VR
OpenOpen the following valve [] 2188VL 1MX101
Page 43 of 278
Operator
location
Flow meter of #1 mix bed water 9WDP60219
[ ] YBDT
sample Si meterOpen VR
1# Concentrated alkali storage tank
level meter
Available [ ] 9WDP601MN YBDT
2# Concentrated alkali storage tank
level meter
Available [ ] 9WDP602MN YBDT
POWER SSUPPLY
#1 Waste water pump power
switchUnloading acid pump
power supply switch
Page 44 of 278
Operator
location
Closed [] 2101EO 1MX101
Available [] 211RF 1MX101
Available [] 2184VL 1MX101
Open [] 2183VL 1MX101
Open [] 2190VL 1MX101
Closed [] 2189VL 1MX101
Available [] 213LP 1MX101
Available [] 211MG 1MX101
Available [] 211LG 1MX101
Open [] 2186VL 1MX101
Available [] 211LD 1MX101
Open [] 2187VL 1MX101
Open [] 2188VL 1MX101
Open [] 2283VL 1MX101
Open [] 2290VL 1MX101
Open [] 2286VL 1MX101
Page 45 of 278
Operator
location
Open [] 2287VL 1MX101
Open [] 2288VL 1MX101
Open [] 2383VL 1MX101
Open [] 2390VL 1MX101
Open [] 2386VL 1MX101
Open [] 2387VL 1MX101
Open [] 2388VL 1MX101
Open [] 2483VL 1MX101
Open [] 2490VL 1MX101
Shut down [] 2489VL 1MX101
Page 46 of 278
Operator
location
Open [] 2486VL 1MX101
Open [] 2487VL 1MX101
Open [] 2488VL 1MX101
Open [] 2583VL 1MX101
Open [] 2590VL 1MX101
Open [] 2586VL 1MX101
Open [] 2587VL 1MX101
Open [] 2588VL 1MX101
Open [] 2091VL 1MX301
2TFC4
Closed (or Energized)
71PO
Page 47 of 278
Operator
location
Alignment check and operations of

#1 high-speed mix bed
Available [] 201DE 1MX101
1MX101
Closed [] 2101VL
Closed [] 2104VA 1MX101
Closed [] 2134VK 1MX101
Open [] 2131VL 1MX101
Open [] 2132VL 1MX101
Open [] 2182VL 1MX101
Available [] 211MD 1MX101
Open [] 2171VL 1MX101
Open [] 2172VL 1MX101
Available [] 211MP 1MX101
Open [] 2174VL 1MX101
Open [] 2175VL 1MX101
Open [] 2179VL 1MX101
Available [] 212MPd 1MX101
Open [] 2176VL 1MX101
Page 48 of 278
Operator
location
Open [] 2177VL 1MX101
Available [] 201CW 1MX101
Available [] 211SPd 1MX101
Open [] 2180VL 1MX101
Open [] 2181VL 1MX101
#2 Waste water pump power
switch
2TFC4
Closed (or Energized)
72PO
Page 49 of 278
Operator
location


Open [] 2231VL 1MX101
Open [] 2232VL 1MX101
Open [] 2282VL 1MX101
Open [] 2271VL 1MX101
Open [] 2272VL 1MX101
Open [] 2274VL 1MX101
Open [] 2275VL 1MX101
Open [] 2279VL 1MX101
Open [] 2276VL 1MX101
Page 50 of 278
Operator
location
Open [] 2277VL 1MX101
Open [] 2280VL 1MX101
Open [] 2281VL 1MX101
Alignment check and operations of #3

high-speed mix bed 1MX101
[]
Available 203DE
1
Alignment check and operations of M
#3 high-speed mix bed X1
AvailableAlignment check 01
and operations of #3 high- 1
speed mix bed [ M
Available ] 203DE X1
203DE 01
Page 51 of 278
Operator
location
Open [] 2331VL 1MX101
Open [] 2332VL 1MX101
Open [] 2382VL 1MX101
Open [] 2371VL 1MX101
Open [] 2372VL 1MX101
Open [] 2374VL 1MX101
Open [] 2375VL 1MX101
Open [] 2379VL 1MX101
Open [] 2376VL 1MX101
Open [] 2377VL 1MX101
Open [] 2380VL 1MX101
Page 52 of 278
Operator
location
Open [] 2381VL 1MX101
Alignment check and

operations of #4 high-speed
mix bed
#1 Flushing pump power

switch
1M
Available [ X1
] 204DE 01
Page 53 of 278
Operator
location
Available 204DE 1MX101
Open [] 2431VL 1MX101
Open [] 2432VL 1MX101
Open [] 2482VL 1MX101
Open [] 2471VL 1MX101
Open [] 2472VL 1MX101
Open [] 2474VL 1MX101
Open [] 2475VL 1MX101
Page 54 of 278
Operator
location
Open [] 2479VL 1MX101
Open [] 2476VL 1MX101
Open [] 2477VL 1MX101
Open [] 2480VL 1MX101
Open [] 2481VL 1MX101

1M
Available [ X1
] 205DE 01
Page 55 of 278
Operator
location
Alignment check and

operations of #5 high-speed
mix bed

Open [] 2531VL 1MX101
Open [] 2532VL 1MX101
Open [] 2582VL 1MX101
Open [] 2571VL 1MX101
Open [] 2572VL 1MX101
Open [] 2574VL 1MX101
Open [] 2575VL 1MX101
Open [] 2579VL 1MX101
Page 56 of 278
Operator
location
Open [] 2576VL 1MX101
Open [] 2577VL 1MX101
Open [] 2580VL 1MX101
Open [] 2581VL 1MX101

the mix bed inlet and outlet
pipelines, and the
recirculation pipelines

Open [ ] 2071VL 1MX101
Available [ ] 201PO 1MX101
Open [] 2081VL 1MX101
Open [] 2036VL 1MX101
Available [] 2030VA 1MX101
Available [] 201SE 1MX101
Page 57 of 278
Operator
location
Alignment check and operation of

mix bed resin separation
tower
Closed [ ] 3101VL 1MX101

Closed [ ] 3104VK 1MX101
Closed [ ] 3128VA 1MX101
Available [ ] 311SM 1MX101
Available [ ] 311LP 1MX101
Open [ ] 3171VL 1MX101

mix bed anion resin
regeneration tower

Page 58 of 278
Operator
location
Closed [ ] 3207VR 1MX101
Open [ ] 3271VL 1MX101
321LG、321
Available 1MX101
[ ] MG
Open [ ] 3271VK 1MX101
Closed [ ] 3201EF 1MX101

mix bed cation resin
regeneration tower

Page 59 of 278
Operator
location
Open [ ] 3371VL 1MX101
331LG、321
Available 1MX101
[ ] MG
Open [ ] 3371VK 1MX101

mix bed resin mixing and
storage tower

Open [ ] 3471VL 1MX101
341LG、301
Available 1MX101
[ ] MG
Open [ ] 3471VK 1MX101

high-speed mix bed resin
delivery pipelines

Available [ ] 2003VL 1MX101
Page 60 of 278
Operator
location
Related alignment check of flushing

pumps and their pipelines

Available [ ] 302MD 1MX101
Page 61 of 278
Operator
location
Open [ ] 3071VL 1MX101
Open [ ] 3072VL 1MX101
Available [ ] 4413VD 1MX101
Closed [ ] 4415VD 1MX101
Open [ ] 4477VL 1MX101
Open [ ] 4478VL 1MX101
Available [ ] 441SP 1MX101
Open [ ] 4475VL 1MX101
Open [ ] 4401VD 1MX101
Open [ ] 4403VD 1MX101
Open [ ] 4471VL 1MX101
Open [ ] 4404VD 1MX101
Open [ ] 4406VD 1MX101
Open [ ] 4472VL 1MX101
Alignment check of regenerative

pumps and their pipelines

Available [ ] 411MD 1MP303
Open [ ] 4171VL 1MP303
Open [ ] 4172VL 1MP303
Page 62 of 278
Operator
location
Available [ ] 421MD 1MP303
Open [ ] 4276VL 1MP303
Open [ ] 4275VL 1MP303
Available [ ] 4131VD 1MP303
Open [ ] 4130VD 1MP303
Closed [ ] 4204VD 1MP303
Closed [ ] 4205VD 1MP303
Available [ ] 431CW 1MX101
Open [ ] 4301VD 1MP303
Open [ ] 4230VD 1MP303
Open [ ] 4371VL 1MX101
Available [ ] 431SN 1MX101
Available [ ] 431LT 1MX101
Available [ ] 421KT 1MX101
Available [ ] 431KT 1MX101
Available [ ] 431RE 1MX101
Open [ ] 4407VD 1MX101
Open [ ] 4409VD 1MX101
Page 63 of 278
Operator
location
Open [ ] 4473VL 1MX101
Open [ ] 4410VD 1MX101
Open [ ] 4412VD 1MX101
Open [ ] 4474VL 1MX101
Open [ ] 4476VL 1MX101
Alignment check of Roots fans and

their related pipelines

Open [ ] 3014VA 1MX101
Open [ ] 3015VA 1MX101
Open [ ] 4671VL 1MX101
Available [ ] 2031VA 1MX101
Available [ ] 461ZV 1MX101
Open [ ] 4602VA 1MX101
Open [ ] 4602VA 1MX101
Open [ ] 4602VA 1MX101
Page 64 of 278
Operator
location
Open [ ] 4604VA 1MX101
Open [ ] 4602VA 1MX101
Open [ ] 4606VA 1MX101
Alignment check of wastewater resin

trapper and its blowdown
pipelines
Available [ ] 306CW 1MX101

Open [ ] 3030VK 1MX101
Open [ ] 3032VK 1MX101
Available [ ] 301MG 1MX101
Available [ ] 301LG 1MX101
Open [ ] 3071VK 1MX101
Available [ ] 301SE 1MX101
See S2 ATE
004
Set the neutralization discharging of wastewater
the wastewater neutralization pond to recycling and
automatic state neutralization
discharging
operating
procedure for
details
At least one inlet valve of #1, #2

wastewater neutralization ponds is
open
Page 65 of 278
Operator
location
2TFC4
Closed (or energized)
41PO
Open#2 Flushing pump power
4713VK 1MX101
switch
2TFC4
42PO
4714VK 1MX101
Power switch
2TFC4
43PO
#2 Regeneration pump Power switch
Alignment check of recycling water

tank
Available [ ] 481BA 1MX101

Available [ ] 481MN 1MX101
Open [ ] 481VL 1MX101
Open [ ] 481VL 1MX101
Open [ ] 4801VK 1MX101
2TFC4
44PO
Hot water tank #1 electric heater
power switch
Page 66 of 278
Operator
location

demineralized water tanks
Available，tank level is > 3.0m [ ] 441BA 1MP304

Available [ ] 441MN 1MP304
Open [ ] 441VL 1MP304
Open [ ] 441VL 1MP304
Closed [ ] 4432VK 1MP304
Open [ ] 4431VD 1MP304
Alignment check of high level acid

storage tank, acid metering
box
Available，tank level >0.5m [ ] 411CW 1MP303

Closed [ ] 4119VR 1MP303
Open [ ] 412VL 1MP303
Open [ ] 412VL 1MP303
Available [ ] 411AD 1MP303
Open [ ] 4117VR 1MP303
Open [ ] 4118VR 1MP303
Available [ ] 412CW 1MP303
Open [ ] 413VL 1MP303
Open [ ] 413VL 1MP303
Available [ ] 411MG 1MP303
Page 67 of 278
Operator
location
Available [ ] 411LG 1MP303
Available [ ] 411EJ 1MP303
Available [ ] 4127VR 1MX101
Open [ ] 4121VR 1MP303
Available [ ] 4123VR 1MP303
Open [ ] 4127VR 1MX101
2TFC4
31RE
Page 68 of 278
Operator
location
Alignment check of high level alkali

storage tank, alkali metering
box
Available，tank level >0.5m [ ] 421CW 1MP303

Open [ ] 423VL 1MP303
Open [ ] 423VL 1MP303
Open [ ] 4218VR 1MP303
Open [ ] 4219VR 1MP303
Available [ ] 423CW 1MP303
Open [ ] 425VL 1MP303
Open [ ] 425VL 1MP303
Available [ ] 421MG 1MP303
Available [ ] 421LG 1MP303
Available [ ] 421EJ 1MP303
Open [ ] 4222VR 1MP303
Open [ ] 4207VR 1MP303
Available [ ] 4223VR 1MP303
Open [ ] 4228VR 1MX101
Page 69 of 278
Operator
location
3.5 Power supply
Closed (Or energized) [] 1ATE201PO 1MX702

* At least one
flushing pump
is available
and
energized.
Closed(Or energized) [ ] 441PO 1MX702
* At least one
regeneration
pump is
available and
energized.
* At least one
Roots fan is
available and
energized.
Closed(Or energized) [ ] 461ZV 1MX702
* At least two
electric
heaters are
available and
energized.
Closed(Or energized) [ ] 1ATE431RE 1MX101
power switch
Page 70 of 278
Operator
location
2TFC4
32RE
power switch
2TFC4
33RE
power switch
2TFC4
34RE
Available, opening state [ ] 0SDA501PO YB
Unloading alkali pump power supply
switch
Available, opening state [ ] 0SDA601PO YB
913VD close [ ] 913VD YA005
901AD available [ ] 901AD YA005
Page 71 of 278
4. START UP
Operation
Location
* During the resin transfer operation
of condensate polishing devices,
there is risk of the secondary
circuit losing water!
* During the resin regeneration,
there is risk of acid burning!
* Be particularly rigorous during the
operation to prevent mis operating
valves (or point operating the
wrong valves)
UNEUTRALIZATION DISCHARGE
OPERATION OF #1 WASTE
WATER POND.NLOADING ACID
OPERATION (31%
HYDROCHLORIC ACID)
4.1 Output operation of high-speed
mix bed ineffective
resin
Output operation of # 1 high-speed
mix bed ineffective resin
On the "# 1 unit condensate
mix bed unit" control screen,
click the "#1 high-speed mix
bed" icon, and click the “Start”
button of “Resin output” on the
popped-up "#1 high-speed mix
bed operation" screen. The [ ]
dialog box “Transfer #1 high-
speed mix bed resin to SPT
separation tower?” appears,
click "Yes" button. The PLC will
transfer the resin according to
the set step sequence:
Open [ ] 2104VA 1MX101
Page 72 of 278
Operation
Location
After #1 High-speed mix bed
relieving the pressure
Startup one flushing water pump
(441PO or 442PO)
441PO
Startup [ ] Or 1MX101
442PO
Startup [ ] 442PO 1MX101
Gas transporting (about 120
seconds)
Open [ ] 3030VK 1MX101
Open [ ] 3119VK 1MX101
Page 73 of 278
Operation
Location
Open [ ] 3101VL 1MX101
Open [ ] 2023VL 1MX101
Open [ ] 2030VL 1MX101
VOn the "# 2 unit wastewater,
demineralized water unit"
control screen, click the icon
"# 1 wastewater pond " and
click the startup button of "
wastewater neutralization " on
the popped-up "# 1
wastewater pond operation "
screen, PLC will start
neutralization and discharging
[ 501BA
the wastewater of #1 YB
] 、502B
wastewater pond according to
A
the following steps:erify the
capacity margin of 1 #, 2 #
concentrated acid storage
tank is sufficient, tanks can
contain 10 tons of
hydrochloric acid (a car),
namely 1 #, 2 # concentrated
acid storage tank level should
≤1.4 meters.
V# 1 Wastewater pond stops
receiving waste
water: when #1 wastewater pond
level ≥4.0m, PLC control program
will automatically open #2
[ ]
wastewater pond inlet valve, and
close # 1 wastewater pond inlet
valve.erify unloading acid pump inlet
fitting in good condition, are
available.
Open [ ] 2127VL 1MX101
Open [ ] 2118VL 1MX101
Open [ ] 2029VA 1MX101
Page 74 of 278
Operation
Location
Gas-water mix transporting
(about 60 seconds)
120 seconds after the resin gas
transporting
Open [ ] 2129VL 1MX301
Water transporting (about 300
seconds)
60 seconds after the gas-water
mix transporting
Open [ ] 2126VL 1MX101
Open [ ] 2025VL 1MX101
300 seconds after the water
transporting
Pipe flushing (about 180
seconds)
Open [ ] 2019VL 1MX101

180 seconds after the pipe flushing


Shutdown flushing water pump
Shutdown [ ] 441PO 1MX101

Page 75 of 278
Operation
Location
#1 high-speed mix bed pressure
relieving and gas exhausting
Open [ ] 2104VA 1MX101

60 seconds after the exhausting

Separation tower pressure
Open [ ] 3114VA 1MX101


Output operation of #2 high-speed
mix bed unit" control screen,
bed" icon, and click the “Start”
button of “Resin output” on the
popped-up "#2 high-speed mix
bed operation" screen. The [ ]
dialog box “Transfer #2 high-
speed mix bed resin to SPT
separation tower” appears,
click "Yes" button. The PLC will
transfer the resin according to
Open [ ] 2204VA 1MX101
[ ] 2204VA 1MX101
relieving the pressure Closed
seconds)
Page 76 of 278
Operation
Location
Open [ ] 3030VK 1MX101
Open [ ] 3119VK 1MX101
Open [ ] 3101VL 1MX101
Open [ ] 2023VL 1MX101
Open [ ] 2030VL 1MX101
Open [ ] 2227VL 1MX101
Open [ ] 2218VL 1MX101
Open [ ] 2029VA 1MX101
(about 60 seconds)
transporting
Open [ ] 2229VL 1MX301

Water transporting (about
300 seconds)
mix transporting

ClosedVerify the safety shower,
eyewash near the mouth of unloading
[ ] 2TFC631VK
acid is available ground rinse water is
available.
Open [ ] 2029VA 1MX101
(about 60 seconds)
Page 77 of 278
Operation
Location
 120 seconds after the
resin gas transporting
Open [ ] 2129VL 1MX301
300 seconds)
60 seconds after the gas-
water mix transporting
Open [ ] 2126VL 1MX101
Open [ ] 2025VL 1MX101

300 seconds after the
water transporting

seconds)
Open [ ] 2019VL 1MX101
180 seconds after the pipe
flushing

Page 78 of 278
Operation
Location
Open [ ] 2104VA 1MX101

exhausting
Open [ ] 3114VA 1MX101

exhausting

Page 79 of 278
Operation
Location
mix bed ineffective resinOn
the "# 1 unit condensate mix
bed unit" control screen, click
the "#2 high-speed mix bed"
icon, and click the “Start”
button of “Resin output” on
the popped-up "#2 high-
[ ]
speed mix bed operation"
screen. The dialog box
“Transfer #2 high-speed mix
bed resin to SPT separation
tower?” appears, click "Yes"
button. The PLC will transfer
the resin according to the set
step sequence:
mix bed unit" control
screen, click the "#3 high-
speed mix bed" icon, and
click the “Start” button of
“Resin output” on the
popped-up "#3 high-speed
mix bed operation" screen.
[ ][ ] 2204VA 1MX101
The dialog box “Transfer #3
high-speed mix bed resin to
SPT separation tower?”
appears, click "Yes" button.
The PLC will transfer the
resin according to the set
step sequence:
Open
Pressure relieving of #3 high-
[ ] 2TFC641VK
speed mix bedOpen
[2.]
[3.] 2204V [4.] 1M
1. Closed [ 2.[5.]
A X101
]
Page 80 of 278
Operation
Location
Open 2304VA441P 1MX1011
[ ][ ]
Startup O MX101
relieving the pressure [ ] 442PO 1MX101
Startup
ClosedGas
transporting (about 120 [ ] 2304VA 1MX101
seconds)
Startup one flushing water
[ ]
pump (441PO or 442PO)
Startup 441PO3030V 1MX1011
[ ][ ]
Open K MX101
Startup 442PO3119V 1MX1011
[ ][ ]
Open K MX101
[ ] 3101VL 1MX101
seconds) Open
Open [ ] 2023VL 1MX101
Open [ ] 2030VL 1MX101

Open 3030VK2227V 1MX1011
[ ][ ]
Open L MX101
Open 3119VK2218V 1MX1011
[ ][ ]
Open L MX101
Open 3101VL2029V 1MX1011
[ ][ ]
Open A MX101
(about 60 seconds)
Open120
seconds after the resin [ ] 2023VL 1MX101
gas transporting
Open 2030VL2229V 1MX1011
[ ][ ]
Open L MX301
300 seconds)
Page 81 of 278
Operation
Location
Open60
seconds after the gas- [ ] 2327VL 1MX101
water mix transporting
Open 2318VL2029V 1MX1011
[ ][ ]
Closed A MX101
Open 2029VA2218V 1MX1011
[ ][ ]
Closed L MX101
(about 60 seconds) [ ] 2226VL 1MX101
Open
120 seconds after the resin
gas transporting [ ] 2025VL 1MX101
Open
Open300 seconds
after the water [ ] 2329VL 1MX301
transporting
[ ] 2226VL 1MX101
seconds) Closed
mix transporting [ ] 2025VL 1MX101
Closed
Closed 2029VA2227V 1MX1011
[ ][ ]
Closed L MX101
Closed 2318VL2229V 1MX1011
[ ][ ]
Closed L MX101
Open Pipe
flushing (about 180 [ ] 2326VL 1MX101
seconds)
Open 2025VL2019V 1MX1011
[ ][ ]
Open L MX101
transporting180 seconds
after the pipe flushing
Page 82 of 278
Operation
Location
2326VL2019V 1MX1011
ClosedClosed [ ][ ]
L MX101
2025VL2030V 1MX1011
ClosedClosed [ ][ ]
L MX101
2327VL2023V 1MX1011
ClosedClosed [ ][ ]
L MX101
Closed 2329VL441P 1MX1011
[ ][ ]
Shutdown O MX101
seconds) [ ] 442PO 1MX101
Shutdown
Open [ ] 2204VA 1MX101
Open60
seconds after the [ ] 2019VL 1MX101
exhausting
flushing [ ] 2204VA 1MX101
Closed
2019VL3114V 1MX1011
Closed Open [ ][ ]
A MX101
Closed60 seconds after the
[ ] 2030VL 1MX101
exhausting
2023VL3114V 1MX1011
Closed Closed [ ][ ]
A MX101
303
0 1
Closed
V
K
Closed Output
operation of #3 high-speed [ ] 3119VK 1MX101
Page 83 of 278
Operation
Location
Shutdown flushing water
pumpOn the "# 1 unit
condensate mix bed unit"
control screen, click the
"#3 high-speed mix bed"
button of “Resin output”
on the popped-up "#3
high-speed mix bed
[ ]
operation" screen. The
dialog box “Transfer #3
to SPT separation
tower?” appears, click
"Yes" button. The PLC
will transfer the resin
according to the set step
sequence:
ShutdownPr
essure relieving of #3 [ ] 441PO 1MX101
high-speed mix bed
Shutdown 442PO2304V 1MX1011
[ ][ ]
Open A MX101
pressure relieving and
gas exhaustingAfter #3
High-speed mix bed
relieving the pressure
Open 2304VA441P 1MX1011
[ ][ ]
Startup O MX101
exhausting [ ] 442PO 1MX101
Startup
ClosedGas
transporting (about 120 [ ] 2304VA 1MX101
seconds)
Page 84 of 278
Operation
Location
Separation tower pressure
relieving and gas
exhausting 3030VK
1MX101Y
OpenFurther verify 1 #, 2 [ ][ ] 501MN、502M
B
# concentrated acid N
storage tank level gauge
available.
OpenVerif
y motor insulation of 3119VK501P 1MX101Y
[ ][ ]
unloading acid pump O B
qualified（≥0.5MΩ）
Open
OpenVerify acid sent by [ ][ ][ 3114VA3101V 1MX1011
transport tankers is ] L MX101
(31% hydrochloric acid)
exhaustingFurther verify
[ ] 500VR YB
concentrated acid inlet
valve is closed
Closed
OpenSend personnel
[ ][ ][ 3114VA2023V 1MX1011
connected temporary pipe
] L MX101
between tankers and
unloading acid pump
OpenConfirm that
temporary unloading acid piping
[ ][ ] 2030VL 1MX101
didn’t connect to the wrong position,
and firm!
Open [ ] 2327VL 1MX101
Open [ ] 2318VL 1MX101
Open [ ] 2029VA 1MX101
Page 85 of 278
Operation
Location
mix bed ineffective
resinGas-water mix
transporting (about 60
seconds)
On the "# 1 unit
condensate mix bed unit"
"#4 high-speed mix bed"
button of “Resin output”
on the popped-up "#4
high-speed mix bed
operation" screen. The
dialog box “Transfer #4 [ ]
to SPT separation tower?”
appears, click "Yes"
button. The PLC will
transfer the resin
according to the set step
sequence:120 seconds
after the resin gas
transporting
1M
[ 2329V
Open X3
] L
01
Water transporting
(about 300 seconds)
60 seconds after the gas-water mix
transporting
1
M
202 X
Closed
9VA 1
0
1
Page 86 of 278
Operation
Location
1
M
23
X
Closed 18
1
VL
0
1
Open 2404VA2326V 1MX1011
[ ][ ]
Open L MX101
1
20 M
25 X
Open
VL 1
Open unloading acid [ ]
50 0
pump inlet valve
0V 1
R Y
Closed300
seconds after the water
transporting Open 2404VA517V 1MX101Y

[ ][ ]
R B
unloading acid pump
outlet valve
Page 87 of 278
Operation
Location
The risk of
spraying
acid
present in
the exhaust
process
steps, the
process
Startup one flushing water needs to
pump (441PO or 442PO) regulate
[ ][ ][
Closed Send personnel 2326VL 1MX101 traffic flow
]
slightly open the unloading to matches
acid valve of acid tanker with
unloading
acid pump
the acid
sent
personnel
take a
notice of
safety!
1
M
X
Startup 44 1
Closed After confirm 1P 0
unloading acid pump inlet [ ] O2 1
pipe filled with acid, 02 1
temporary unloading acid 5V M
joint no leakage L X
1
0
1
Startup
Closed Send personnel to [ ][ ][ 442PO2327V 1MX1011
open unloading acid valve of ] L MX101
the tanker
Page 88 of 278
Operation
Location
Gas transporting (about
120 seconds)
Closed Close the 2025VL0SDA 1MX101Y
[ ][ ]
unloading acid pump 501PO B
power supply switch, set
to "Local" position
Closed Start 2327VL501P 1MX101Y
[ ][ ]
unloading acid pump O B
1
M
X
30 1
30 0
Open VK 1
[ ]
Closed 20 1
25 M
VL X
1
0
1
If abnormal,
Open should be
Closed Verify unloading acid pump [ ][ ][ 3030VK2327V 1MX1011 shutdown
outlet pressure is normal (about ] L501LP MX101YB unloading
0.20MPa) acid pump
promptly
3101VL2TFC
OpenClosed [ ][ ] 1MX101
634VK
3101V 1M
OpenClosed L2TFC X1
631EF 01
OpenVerify unloading
acid pump outlet pipe no [ ][ ] 2023VL 1MX101

leakage
Page 89 of 278
Operation
Location
OpenNeutralization
discharge operation of #2 waste
water pond.When unloading the acid
pump outlet pressure indicator
dropped to "0", the acid tank unload

[ ][ ][ 2030VL501P 1MX101Y
completed, or 1 #, 2 # concentrated ] O B
acid storage tank level is higher than
the 1.8m, shutdown unloading acid
pump Verify unloading acid pump
outlet pipe no leakage
Page 90 of 278
Operation
Location
# 2 Wastewater pond
stops receiving waste
water: when #2
wastewater pond level
≥4.0m, PLC control
program will automatically
open #1 wastewater pond
inlet valve, and close # 2
wastewater pond inlet
valve.Close unloading
acid pump outlet valveOn
the "# 2 unit wastewater,
demineralized water unit"
icon "# 2 wastewater pond
51
" and click the startup
7V Y
button of " wastewater
R B
neutralization " on the
[ ] 50 Y
popped-up "# 2wastewater
[ ] 0V B
pond operation " screen,
R5 Y
PLC will start
01 B
neutralization and
PO
discharging the
wastewater of #2
wastewater pond
according to the following
steps:.Close unloading
acid pump inlet
valveWhen unloading the
acid pump outlet pressure
indicator dropped to "0",
the acid tank unload
completed, or 1 #, 2 #
concentrated acid storage
tank level is higher than
the 1.8m, shutdown
unloading acid pump
Page 91 of 278
Operation
Location
Ope
nClosedSend personnel
removal the temporary
unloading acid pipeline
between tanker and unloading
acid the pump, and rinse
venue# 2 Wastewater pond
stops receiving waste [
2427VL2TFC
water: when #2 wastewater ] 1MX101Y
641VK
pond level ≥4.0m, PLC control ] BYB
517VR500VR
program will automatically [ ][ ]
open #1 wastewater pond
inlet valve, and close # 2
wastewater pond inlet
valve.Close unloading acid
pump outlet valveClose
unloading acid pump inlet
valve
Before
removing the
temporary
unloading
acid pipeline,
OpenOpen should be
Disconnect the unloading acid reminded to
pump power supply switch send acid
Closed 2418VL2TFC Staff: there is
[ ][ ][
Send personnel removal the 631VK0SDA5 1MX101Y residual acid
][ ][ ]
temporary unloading acid 01PO2TFC64 BYB in pipe
[ ]
pipeline between tanker and 1VK517VR between
unloading acid the pump, and acid car and
rinse venueClose unloading unload acid
acid pump outlet valve pump
inlet ,.and
take a
notice of
safety burns
by acid!
Page 92 of 278
Operation
Location
Before
remov
ing
the
tempo
rary
unloa
ding
acid
pipelin
e,
should
be
remin
ded to
Wastewater re-circulation stirr
send
ing Make a good acid
acid
unloading operation records.
Staff:
Open Disconnect the [
2TFC there
unloading acid pump power ][
631VK is
supply switchSend personnel ][ YB
0SDA residu
removal the temporary ]
501PO al acid
unloading acid pipeline ]
in pipe
between tanker and unloading
betwe
acid the pump, and rinse
en
venue
acid
car
and
unloa
d acid
pump
inlet ,.
and
take a
notice
of
safety
burns
by
Page 93 of 278
Operation
Location
Open #2 waste water pond
recirculation valve Unloading
alkali operation (32% Alkali)W
[
astewater re-circulation stirrin 0SDA
] YB
g Make a good acid unloading 501PO
]
operation records. Disconnect
the unloading acid pump
power supply switch
OpenOpenVerify the
capacity margin of 1 #, 2 #
concentrated alkali storage
contain 10 tons of hydrochloric
2029VA2TFC
alkali (a car), namely 1 #, 2 #
[ ][ ] 644VK 1MX101Y
[ ][ ] 601BA、602B B
tank level should ≤1.4 meters.
A
Open #2 waste water pond
recirculation valve
Unloading alkali operation (32%
Alkali) Make a good acid
unloading operation records.
(about 60 seconds) Startup
#2 waste water pump Verify
unloading alkali pump inlet
available. Open Verify the
capacity margin of 1 #, 2 # 2TFC644VK
[ ]
concentrated alkali storage 601BA、602B YB
[ ]
tank is sufficient, tanks can A
contain 10 tons of
hydrochloric alkali (a car),
alkali storage tank level
should ≤1.4 meters.Unloading
alkali operation (32% Alkali)
Page 94 of 278
Operation
Location
gas transportingstartup Verify
the safety shower, eyewash
near the mouth of unloading
alkali is available ground rinse
water is available. Startup #2
waste water pump Verify
2TFC472PO
[ ][ ] 601BA、602B YB
available.Verify the capacity
A
margin of 1 #, 2 #
contain 10 tons of
hydrochloric alkali (a car),
should ≤1.4 meters.
OpenMeasuring
waste water PH valuesFurther
verify 1 #, 2 # concentrated
alkali storage tank level gauge
available. Startup Verify the [ ][ ] 2429VL
1MX301Y
safety shower, eyewash near [ ] 601MN、602M
B
the mouth of unloading alkali is [ ][ ] N2TFC472PO
available ground rinse water is
available.Verify unloading
alkali pump inlet fitting in good
condition, are available.
Page 95 of 278
Operation
Location
seconds)OpenVerify motor
insulation of unloading alkali
pump
qualified（≥0.5MΩ）Measuri
ng waste water PH
2TFC641EF6
valuesFurther verify 1 #, 2 # [ ]
01PO
[ ] YBYB
concentrated alkali storage 601MN、602M
[ ][ ]
N
tank level gauge
available.Verify the safety
shower, eyewash near the
mouth of unloading alkali is
available ground rinse water
is available.
Page 96 of 278
Operation
Location
water mix
transportingClosedVerify
alkali sent by transport
tankers is (31% hydrochloric

2TFC631EF2
alkali)OpenVerify motor [ ] TFC641EF60
[ ] 1PO YBYB
insulation of unloading alkali
[ ][ ] 601MN、602M
pump N
qualified （ ≥ 0.5MΩ ） Further
verify 1 #, 2 # concentrated
gauge available.
ClosedAdd
caustic for neutralization
Further verify concentrated
2029VA600V
alkali inlet valve is closed [ ][ ]
R 1MX101Y
Verify alkali sent by transport [ ]
2TFC BYB
tankers is (31% hydrochloric [ ][ ]
631EF601PO
alkali)Verify motor insulation
of unloading alkali pump
qualified（≥0.5MΩ）
Page 97 of 278
Operation
Location
Closed 20
minutes after waste water
recirculation, if waste water
neutralization discharge PH
≤6.0, then: Send personnel
connected temporary pipe
between tankers and [ ][ ][ 2418VL600V 1MX101Y
unloading alkali pump Add ] R B
caustic for Neutralization
Further verify concentrated
alkali inlet valve is
closedVerify alkali sent by
transport tankers is (31%
hydrochloric alkali)
OpenOpenCo
nfirm that temporary
unloading alkali piping didn’t
connect to the wrong position,
and firm! 20 minutes after
waste water recirculation, if
waste water neutralization [ ][ ][ 2426VL2TFC 1MX101Y
discharge PH ≤6.0, then: ] 628VR600VR B
Send personnel connected
temporary pipe between
tankers and unloading alkali
pump Further verify
concentrated alkali inlet valve
is closed
Page 98 of 278
Operation
Location
Open 30
seconds after adding caustic
Open unloading alkali pump
inlet valve Open Confirm that
2025VL600V
temporary unloading alkali [ ][ ]
R 1MX101Y
piping didn’t connect to the [ ]
2TFC B
wrong position, and firm!Send [ ][ ]
628VR
personnel connected
temporary pipe between
tankers and unloading alkali
pump
transportingClosedOpen
unloading alkali pump outlet
valve 30 seconds after adding
[ ] 2TFC628VR6
caustic Open unloading alkali YBYB
[ ][ ] 17VR600VR
pump inlet valveConfirm that
temporary unloading alkali
piping didn’t connect to the
wrong position, and firm!
Closed
Recirculate waste water for
15 minutes Send personnel
slightly open the unloading 2426VL2TFC
[ ][ ] 1MX101Y
alkali valve of alkali tanker 628VR
[ ][ ] BYB
ClosedOpen unloading alkali 617VR600VR
pump outlet valveOpen
valve
Page 99 of 278
Operation
Location
The risk of
spraying
alkali
Closed If the present in
PH value of water ≤ 6.0, the exhaust
repeat 5.2.4.1 ~ 5.2.4.3 steps process
until PH value is between 6.0 steps, the
and 9.0. After confirm process
unloading alkali pump inlet needs to
pipe filled with alkali, regulate
[ ][ ][ 2025VL617V 1MX101Y
temporary unloading alkali traffic flow
] R B
joint no leakage Recirculate to matches
waste water for 15 with
minutesSend personnel unloading
slightly open the unloading alkali pump
alkali valve of alkali tanker the alkali
Open unloading alkali pump sent
outlet valve personnel
take a
notice of
safety!
Page 100 of 278

Operation
Location
The risk of
spraying
alkali
present in
the exhaust
ClosedAdd acid for
process
neutralizationSend personnel to
steps, the
open unloading alkali valve of the
process
tanker If the PH value of water ≤
needs to
6.0, repeat 5.2.4.1 ~ 5.2.4.3 steps
regulate
until PH value is between 6.0 and [ ][ ][
2427VL 1MX101 traffic flow
9.0. After confirm unloading alkali ][ ]
to matches
pump inlet pipe filled with alkali,
with
temporary unloading alkali joint no
unloading
leakageSend personnel slightly open
alkali pump
the unloading alkali valve of alkali
the alkali
tanker
sent
personnel
take a
notice of
safety!
Closed 20
minutes after waste
water recirculation, if
waste water
neutralization discharge
PH ≥ 9.0 then:Add acid
for neutralizationSend
[ ][ ][
personnel to open 2429VL 1MX101
]
unloading alkali valve of
the tanker After confirm
unloading alkali pump
inlet pipe filled with
alkali, temporary
unloading alkali joint no
leakage
Page 101 of 278

Operation
Location
Pipe flushing (about 180 seconds)
Open #2 waste water pond acid inlet
valve Close the unloading alkali pump
power supply switch, set to "Local"
position 20 minutes after waste water [ ][ ] 0SDA601PO YB
recirculation, if waste water
neutralization discharge PH ≥ 9.0
then:Send personnel to open
unloading alkali valve of the tanker
OpenStart unloading alkali
pump Open #2 waste water
2TFC630VR6
pond acid inlet valve Close the [ ][ ][
01PO0SDA60 YBYB
unloading alkali pump power ]
1PO
supply switch, set to "Local"
position
Open 30
seconds after acid
additionVerify unloading
alkali pump outlet
pressure is normal 2019VL601LP
(about [ ][ ][ 2TFC630VR6 1MX101Y
0.20MPa)OpenStart ][ ][ ] 01PO0SDA60 BYBYB
unloading alkali 1PO
pumpClose the
power supply switch, set
to "Local" position
flushingClosedVerify
If abnormal,
should be
pipe no leakage 30 seconds
[ ][ ][ 2TFC630VR6 shutdown
after acid additionVerify YBYB
][ ] 01LP601PO unloading
alkali pump
pressure is normal (about
promptly
0.20MPa)Start unloading
alkali pump
Closed If the PH value [ ] 2 1 I
Page 102 of 278

Operation
Location
of water ≥ 9.0, repeat [ ][ ] 0 M f
5.1.5.1 ~ 5.1.5.3 steps 1 X a
until PH is between 6.0 9 1 b
and 9.0.When unloading V 0 n
the alkali pump outlet L 1 o
pressure indicator 6 Y r
dropped to "0", the alkali 0 B m
tank unload completed, 1 Y a
or 1 #, 2 # concentrated P B l
alkali storage tank level O ,
is higher than the 1.8m, 2 s
shutdown unloading T h
alkali pumpClosedVerify F o
unloading alkali pump C u
outlet pipe no 6 l
leakageVerify unloading 3 d
alkali pump outlet 0
pressure is normal V b
(about 0.20MPa) R e
6
0 s
1 h
L u
P t
d
o
w
n
u
n
l
o
a
d
i
n
g
Page 103 of 278

Operation
Location
a
l
k
a
l
i
p
u
m
p
p
r
o
m
p
t
l
y
Page 104 of 278

Operation
Location
ClosedWaste water
DischargingClose
inlet valve If the PH
value of water ≥ 9.0,
repeat 5.1.5.1 ~ 5.1.5.3
steps until PH is
between 6.0 and
9.0.When unloading the
alkali pump outlet [ ][ ][ 2030VL600V 1MX101Y
pressure indicator ][ ][ ] R601PO BYB
dropped to "0", the alkali
tank unload completed,
or 1 #, 2 # concentrated
is higher than the 1.8m,
shutdown unloading
alkali pumpVerify
outlet pipe no leakage
Closed After waste water
neutralization, if PH value is
between 6.0 and 9.0 then:Close
valveWaste water
DischargingClose unloading
alkali pump inlet valveWhen 2023VL617V
[ ][ ][ 1MX101Y
unloading the alkali pump outlet R600VR601P
][ ] BYBYB
pressure indicator dropped to O
"0", the alkali tank unload
completed, or 1 #, 2 #
concentrated alkali storage tank
level is higher than the 1.8m,
shutdown unloading alkali
pump
Page 105 of 278

Operation
Location
OpenSend personnel removal the
temporary unloading alkali pipeline
between tanker and unloading alkali
the pump, and rinse venue After
[ ][ ][ 2TFC643VK6
waste water neutralization, if PH YBYB
][ ] 17VR600VR
value is between 6.0 and 9.0
then:Close unloading alkali pump
outlet valveClose unloading alkali
pump inlet valve
Before
removing the
temporary
unloading
alkali
pipeline,
ClosedClosedDisc
should be
onnect the unloading alkali
reminded to
pump power supply
send alkali
switchOpenSend personnel 3101VL2TFC
[ ][ ][ Staff: there is
removal the temporary 644VK0SDA6 1MX101Y
][ ][ ] residual
unloading alkali pipeline 01PO2TFC64 BYB
[ ] alkali in pipe
between tanker and unloading 3VK617VR
between
alkali the pump, and rinse
alkali car
venueClose unloading alkali
and unload
pump outlet valve
alkali pump
inlet ,.and
take a
notice of
safety burns
by alkali!
Page 106 of 278

Operation
Location
Before
removing the
temporary
unloading
Closed When alkali
waste water pond level is pipeline,
lower than 0.5 m.Make a should be
good alkali unloading reminded to
operation send alkali
records.ClosedDisconnect the 3119VK2TFC Staff: there is
[ ][ ][ 1MX101Y
unloading alkali pump power 644VK0SDA6 residual
][ ][ ] B
supply switchSend personnel 01PO alkali in pipe
removal the temporary between
unloading alkali pipeline alkali car
between tanker and unloading and unload
alkali the pump, and rinse alkali pump
venue inlet ,.and
take a
notice of
safety burns
by alkali!
ShutdownAmmonia cylinder
loading and unloading
operations When waste water
2TFC4
pond level is lower than 0.5
72PO0
m.Make a good alkali YB
SDA6
unloading operation
01PO
records.Disconnect the
unloading alkali pump power
supply switch
Page 107 of 278

Operation
Location
2
T
F
C
6
4
3
V
K
ClosedFurther verify 9
one of liquid ammonia 0
tank 901BA, 902BA has 1
been B
empty.ShutdownAmmo [ ][ ][ ] A
nia cylinder loading and 、
unloading 9
operationsMake a good 0
alkali unloading 2
operation records. B
A
2
T
F
C
4
7
2
P
O
Page 108 of 278

Operation
Location
pumpClosedFurther verify
liquid outlet angle valve of
ammonia tank is closed 2TFC641EF
strict.ClosedFurther verify one [ ][ ][ 2TFC643VK
YA005
of liquid ammonia tank ] 901BA、902B
901BA, 902BA has been A
empty.Ammonia cylinder
loading and unloading
operations
ShutdownVerif
y 1 # ammonia cylinder outlet 441PO 1M
angle valve is closed strict 901BA X1
ClosedFurther verify liquid 2TFC6 01
outlet angle valve of ammonia 41EF YA
tank is closed strict.Further 901BA 005
verify one of liquid ammonia 、902B YA
tank 901BA, 902BA has been A 005
empty.
ShutdownVerify 2 #
ammonia cylinder outlet angle
valve is closed strict Verify 1 #
ammonia cylinder outlet angle [ ][ ][ 442PO901BA 1MX101YA
valve is closed strict Further ] 901BA 005YA005
verify liquid outlet angle valve
of ammonia tank is closed
strict.
relieving and gas exhaustingCheck
and confirm that there is no leak case
and aging for the connecting pipes [ ][ ][ YA005YA0
901BA901BA
Verify 2 # ammonia cylinder outlet ] 05YA005
angle valve is closed strict Verify 1 #
ammonia cylinder outlet angle valve
is closed strict
Page 109 of 278

Operation
Location
Remove empty ammonia
cylindersCheck and confirm that there
is no leak case and aging for the [ ][ ][ YA005YA0
901BA
connecting pipes Verify 2 # ammonia ] 05
cylinder outlet angle valve is closed
strict
OpenIf 1 # ammonia
cylinder (901BA) is empty: Use
wrench to remove slipknot behind 1#
ammonia cylinder outlet angle valve,
remove hose and fittings associated [ ][ ][ 1MX101YA
2404VA901BA
with 1 # ammonia cylinder ][ ] 005YA005
(901BA) .Remove empty ammonia
cylindersCheck and confirm that there
is no leak case and aging for the
connecting pipes
60 seconds after the exhaustingIf 2 #
ammonia cylinder (902BA) is empty:
Use wrench to remove slipknot
behind 2# ammonia cylinder outlet
angle valve, remove hose and fittings
associated with 2 # ammonia cylinder
[ ][ ][ YA005YA0
.If 1 # ammonia cylinder (901BA) is 902BA901BA
] 05
empty: Use wrench to remove
slipknot behind 1# ammonia cylinder
outlet angle valve, remove hose and
fittings associated with 1 # ammonia
cylinder (901BA) .Remove empty
ammonia cylinders
Page 110 of 278

Operation
Location
ClosedUse a forklift to
transport empty liquid ammonia tank
to chemical warehouse If 2 #
ammonia cylinder (902BA) is empty:
Use wrench to remove slipknot
behind 2# ammonia cylinder outlet
angle valve, remove hose and fittings [ ][ ][ 2404VA902B 1MX101YA
associated with 2 # ammonia cylinder ][ ] A901BA 005YA005
.If 1 # ammonia cylinder (901BA) is
empty: Use wrench to remove
slipknot behind 1# ammonia cylinder
outlet angle valve, remove hose and
fittings associated with 1 # ammonia
cylinder (901BA) .
Special note:
Due to degree
of the road go
into
Separation tower pressure relieving Fangjiashan
and gas exhaustingTake requisition, plant is large,
use a forklift to receive 3 to 5 bottles to avoid the
full of liquid ammonia cylinder (small falling during
cylinders, about 70Kg / bottle) from a tra liquid
chemical warehouse.Use a forklift to ammonia tank
transport empty liquid ammonia tank [ ][ ][ nsport, should
902BA YA005
to chemical warehouse If 2 # ] pad a suitable
ammonia cylinder (902BA) is empty: square
Use wrench to remove slipknot wooden
behind 2# ammonia cylinder outlet between front
angle valve, remove hose and fittings fork of the
associated with 2 # ammonia cylinder forklift and c
. liquid
ammonia tank
fixed cylinder
with a rope .
Page 111 of 278

Operation
Location
Special note:
recipients
should
confirm the
collar of liquid
ammonia tank
is full,
confirmed the
appearance
of liquid
ammonia
tank, apron
pad, the liquid
Use a forklift to transported full of
angle valve
liquid ammonia tank to the
without
desalination hall , then reuse bottles
injurySpecial
transported by private car to
note: Due to
ammonia bottle room, and fixed on
degree of the
the bracketTake requisition, use a [ ][ ][
YA005 road go into
forklift to receive 3 to 5 bottles full of ]
Fangjiashan
liquid ammonia cylinder (small
plant is large,
cylinders, about 70Kg / bottle) from a
to avoid the
chemical warehouse.Use a forklift to
falling during
transport empty liquid ammonia tank
tra liquid
to chemical warehouse
ammonia tank
nsport, should
pad a suitable
square
wooden
between front
fork of the
forklift and c
liquid
ammonia tank
fixed cylinder
with a rope .
Page 112 of 278

Operation
Location
Special note:
recipients
OpenConnected hose
should
and fittings of liquid ammonia tank
confirm the
outlet Use a forklift to transported full
collar of liquid
of liquid ammonia tank to the
ammonia tank
is full,
transported by private car to [ ][ ][ 1MX101YA
3114VA confirmed the
ammonia bottle room, and fixed on ] 005
appearance
the bracketTake requisition, use a
of liquid
forklift to receive 3 to 5 bottles full of
ammonia
liquid ammonia cylinder (small
tank, apron
cylinders, about 70Kg / bottle) from a
pad, the liquid
chemical warehouse.
angle valve
without injury
60 seconds after the exhaustingIf you
install 1 # ammonia cylinder (901BA):
connected hose and fittings which
connected to 1 # ammonia cylinder
(901BA) with cylinder 1# ammonia.an
outlet angle valve Connected hose
YA005YA0
and fittings of liquid ammonia tank [ ][ ] 901BA
05
outlet Use a forklift to transported full
of liquid ammonia tank to the
transported by private car to
ammonia bottle room, and fixed on
the bracket
Page 113 of 278

Operation
Location
ClosedIf you install 2
# ammonia cylinder (902BA):
outlet angle valveIf you install 1 #
[ ][ ][ 3114VA902BA 1MX101YA
ammonia cylinder (901BA):
] 901BA 005YA005
outlet angle valve Connected hose
and fittings of liquid ammonia tank
outlet
Take a good record of ammonia
cylinder loading and unloading
operations.If you install 2 # ammonia
cylinder (902BA): connected hose
and fittings which connected to 2 #
ammonia cylinder (902BA) with
YA005YA0
cylinder 2# ammonia.an outlet angle [ ][ ] 902BA901BA
05
valveIf you install 1 # ammonia
cylinder (901BA): connected hose
and fittings which connected to 1 #
ammonia cylinder (901BA) with
cylinder 1# ammonia.an outlet angle
valve
ClosedCoagulant,
antiscalant agent, reducer agents,
and other RO cleaning drugs loading
and unloading operations.Take a
good record of ammonia cylinder
3030VK902B 1MX101Y
loading and unloading operations.If [ ][ ]
A A005
you install 2 # ammonia cylinder
(902BA): connected hose and fittings
which connected to 2 # ammonia
cylinder (902BA) with cylinder 2#
ammonia.an outlet angle valve
Page 114 of 278

Operation
Location
When the amount of coagulant,
antiscalant agent, reducer agents and
other RO cleaning drugs are less
than normal amount of two
months ,then submit material
procurement application.Coagulant, [ ]
antiscalant agent, reducer agents,
and other RO cleaning drugs loading
and unloading operations.Take a
good record of ammonia cylinder
loading and unloading operations.
OUTPUT OPERATION OF #5
HIGH-SPEED MIX BED
INEFFECTIVE RESINWHEN THE
AMOUNT OF COAGULANT,
ANTISCALANT AGENT REDUCER
AGENTS, AND OTHER RO
CLEANING DRUGS IS LESS THAN
NORMAL AMOUNT OF 10 DAYS,
DRIVE THE TRUCK TO COLLECT
THE REQUIRED CHEMICAL IN
MATERIALS STORAGE.WHEN
THE AMOUNT OF COAGULANT, [ ][ ]
ANTISCALANT AGENT, REDUCER
AGENTS AND OTHER RO
CLEANING DRUGS ARE LESS
THAN NORMAL AMOUNT OF
TWO MONTHS ,THEN SUBMIT
MATERIAL PROCUREMENT
APPLICATION.COAGULANT,
ANTISCALANT AGENT, REDUCER
AGENTS, AND OTHER RO
CLEANING DRUGS LOADING AND
UNLOADING OPERATIONS.
Page 115 of 278

Operation
Location
On the "# 1 unit condensate mix bed
unit" control screen, click the "#5
high-speed mix bed" icon, and click
the “Start” button of “Resin output” on
the popped-up "#5 high-speed mix
bed operation" screen. The dialog
box “Transfer #5 high-speed mix bed
resin to SPT separation tower?”
appears, click "Yes" button. The PLC
will transfer the resin according to the
set step sequence:Materials shipped
to the YA building, according to
variety of materials, batch [ ][ ]
classification stored in the chemicals [ ][ ]
warehouse of YA building.When the
amount of coagulant, antiscalant
agent reducer agents, and other RO
cleaning drugs is less than normal
amount of 10 days, drive the truck to
collect the required chemical in
materials storage.When the amount
of coagulant, antiscalant agent,
reducer agents and other RO
cleaning drugs are less than normal
amount of two months ,then submit
material procurement application.
Page 116 of 278

Operation
Location
Pressure relieving of #5 high-speed
mix bedPrepare materials for the
storage of eye-catching logo, logo
items should contain the name,
material effective period and storage
time.Materials shipped to the YA
building, according to variety of
materials, batch classification stored [ ][ ][
in the chemicals warehouse of YA ]
building.When the amount of
coagulant, antiscalant agent reducer
agents, and other RO cleaning drugs
is less than normal amount of 10
days, drive the truck to collect the
required chemical in materials
storage.
Make a good operating record
storage of chemicals.Prepare
materials for the storage of eye-
catching logo, logo items should
contain the name, material effective [ ][ ][
period and storage time.Materials ]
shipped to the YA building, according
to variety of materials, batch
classification stored in the chemicals
warehouse of YA building.
OpenMake a good
operating record storage of
chemicals.Prepare materials for the
[ ][ ][
storage of eye-catching logo, logo 2504VA 1MX101
]
items should contain the name,
material effective period and storage
time.
After #5 High-speed mix bed relieving
the pressureMake a good operating [ ]
record storage of chemicals.
Page 117 of 278

Operation
Location
[ ]
(441PO or 442PO)
Open [ ] 2404VA 1MX101

Separation tower pressure relieving
and gas exhausting
Open [ ] 3114VA 1MX101


Close [ ] 3030VK 1MX101
the “Start” button of “Resin output” on
bed operation" screen. The dialog [ ]
box “Transfer #5 high-speed mix bed
resin to SPT separation tower?”
set step sequence:
Pressure relieving of #5 high-speed
mix bed
Open [ ] 2504VA 1MX101
Page 118 of 278

Operation
Location
pressure relieving and gas
exhausting
Open [ ] 2504VA 1MX101
[ ]
(441PO or 442PO)
Gas transporting (about 120 seconds)
Open [ ] 3030VK 1MX101
Open [ ] 3119VK 1MX101
Open [ ] 3101VL 1MX101
Open [ ] 2023VL 1MX101
Open [ ] 2030VL 1MX101
Open [ ] 2527VL 1MX101
Open [ ] 2518VL 1MX101
Open [ ] 2029VA 1MX101
Gas-water mix transporting (about 60
seconds)
transporting e
Open [ ] 2529VL 1MX301
seconds)
60 seconds after the gas-water mix
transporting
Open [ ] 2526VL 1MX101
Open [ ] 2025VL 1MX101
transporting
Page 119 of 278
Operation
Location
Open [ ] 2019VL 1MX101
Open [ ] 2504VA 1MX101
Separation tower pressure relieving
and gas exhausting
Open [ ] 3114VA 1MX101

4.2 Input operation of high-speed
Input operation of #1 high-speed mix
bed ineffective resin
Page 120 of 278

Operation
Location
the “Start” button of “Resin input” on
box “Transfer RST storage tower
resin to #1 high-speed mix bed”
set step sequence:
[ ]
(441PO or 442PO)
seconds)
Open [ ] 2027VK 1MX101
Open [ ] 2118VL 1MX101
Open [ ] 2126VL 1MX101
Open [ ] 2026VL 1MX101
Open [ ] 2024VL 1MX101
Open [ ] 3402VL 1MX101
Open [ ] 3415VL 1MX101
Gas-water mix transporting (about
120 seconds)
120 seconds after the resin water
transporting
Open [ ] 3412VA 1MX101
Open [ ] 3416VL 1MX101
seconds)
Page 121 of 278

Operation
Location
transporting

Open [ ] 3415VL 1MX101
transporting
Open [ ] 3019VL 1MX101
Open [ ] 2025VL 1MX301
120 seconds after the continued pipe
flushing
Water discharging (about 120 second
s)
Open [ ] 2104VA 1MX101
120 seconds after discharging
water
Startup two Roots fans
(461ZV、462ZV or 463ZV)
Startup [ ] 461ZV 1MX101
Resin mixing (about 120 seconds)
Page 122 of 278
Operation
Location
Open [ ] 2106VA 1MX101
Open [ ] 2105VA 1MX101
120 seconds after the resin mixing
flushing

Open [ ] 3014VA 1MX301
Open [ ] 3015VA 1MX301
Shut down Roots fan (461ZV、462ZV
or 463ZV)
Shutdown [ ] 461ZV 1MX101
#1 mix bed is full of water
Open [ ] 2126VL 1MX101
Open [ ] 2025VL 1MX101
Tuning fork switch 201SE acts after
the # 1 mix bed is full of water
# 1 mix bed washing (about 120
seconds)
Open [ ] 2027VK 1MX101
Open [ ] 2118VL 1MX101
120 seconds after the resin washing

#1 mix bed increasing pressure
(about 120 seconds)
Open [ ] 2018VL 1MX101
Page 123 of 278

Operation
Location
Open [ ] 2128VL 1MX101
120 seconds after #1 mix bed
increasing pressure (about 120
seconds)
Mix bed resin mixing and storage
tower is full of water
Open [ ] 3414VA 1MX101
Open [ ] 3415VL 1MX101
the mix bed resin mixing and storage
#1 mix bed cycling cleaning
Open [ ] 2101VL 1MX101
Startup recirculation pump
600 seconds after #1 mix bed self-
cycling cleaning
Open [ ] 2101EO 1MX101
600 seconds after #1 mix bed again
self-cycling cleaning
[ ] 3014VA 1MX301
Closed [ ] 2101EO 1MX101
Page 124 of 278

Operation
Location
Input operation of #2 high-speed
resin to #2 high-speed mix bed?”
set step sequence:
[ ]
(441PO or 442PO)
seconds)
Open [ ] 2027VK 1MX101

Open [ ] 2218VL 1MX101
Open [ ] 2226VL 1MX101
Open [ ] 2026VL 1MX101
Open [ ] 2024VL 1MX101
Open [ ] 3402VL 1MX101
Open [ ] 3415VL 1MX101
120 seconds)
transporting
Open [ ] 3412VA 1MX101
Open [ ] 3416VL 1MX101
Page 125 of 278

Operation
Location
seconds)
transporting
Open [ ] 3415VL 1MX101
transporting
Pipe flushing (about 240 seconds))
Open [ ] 3019VL 1MX101
Open [ ] 2025VL 1MX301
flushing
s)
Open [ ] 2204VA 1MX101
120 seconds after discharging water
(461ZV、462ZV or 463ZV)
Page 126 of 278

Operation
Location
Open [ ] 2206VA 1MX101
Open [ ] 2205VA 1MX101
flushing
Open [ ] 3014VA 1MX301
Open [ ] 3015VA 1MX301
Shutdown Roots fan (461ZV、462ZV
or 463ZV)
Open [ ] 2226VL 1MX101
Open [ ] 2025VL 1MX101
#2 mix bed washing (about 120
seconds)
Open [ ] 2027VK 1MX101
Open [ ] 2218VL 1MX101
(about 120 seconds)
Open [ ] 2018VL 1MX101
Page 127 of 278

Operation
Location
Open [ ] 2228VL 1MX101
seconds)
Open [ ] 3414VA 1MX101
Open [ ] 3415VL 1MX101
Open [ ] 2201VL 1MX101
cycling cleaning
Open [ ] 2201EO 1MX101
Page 128 of 278

Operation
Location
set step sequence:
(441PO or 442PO)
seconds)
Open [ ] 2027VK 1MX101
Open [ ] 2318VL 1MX101
Open [ ] 2326VL 1MX101
Open [ ] 2026VL 1MX101
Open [ ] 2024VL 1MX101
Open [ ] 3402VL 1MX101
Open [ ] 3415VL 1MX101
120 seconds)
transporting
Open [ ] 3412VA 1MX101
Open [ ] 3416VL 1MX101
seconds)
transporting
Page 129 of 278

Operation
Location
Open [ ] 3415VL 1MX101
transporting
Open [ ] 3019VL 1MX101
Open [ ] 2025VL 1MX301
flushing
s)
Open [ ] 2304VA 1MX101
(461ZV、462ZV or 463ZV)
Open [ ] 2306VA 1MX101
Open [ ] 2305VA 1MX101
Page 130 of 278

Operation
Location
flushing
Open [ ] 3014VA 1MX301
Open [ ] 3015VA 1MX301
Shut down Roots fan (461ZV、462ZV
or 463ZV)
Open [ ] 2326VL 1MX101
Open [ ] 2025VL 1MX101
seconds)
Open [ ] 2027VK 1MX101
Open [ ] 2318VL 1MX101
(about 120 seconds)
Open [ ] 2018VL 1MX101
Open [ ] 2328VL 1MX101
seconds)
Page 131 of 278

Operation
Location
Open [ ] 3414VA 1MX101
Open [ ] 3415VL 1MX101
Open [ ] 2301VL 1MX101
cycling cleaning
Open [ ] 2301EO 1MX101

Page 132 of 278

Operation
Location
set step sequence:
(441PO or 442PO)
seconds)
Open [ ] 2027VK 1MX101
Open [ ] 2418VL 1MX101
Open [ ] 2426VL 1MX101
Open [ ] 2026VL 1MX101
Open [ ] 2024VL 1MX101
Open [ ] 3402VL 1MX101
Open [ ] 3415VL 1MX101
120 seconds)
transporting
Open [ ] 3412VA 1MX101
Open [ ] 3416VL 1MX101
seconds)
transporting
Page 133 of 278

Operation
Location
Open [ ] 3415VL 1MX101
transporting
Open [ ] 3019VL 1MX101
Open [ ] 2025VL 1MX301
flushing
s)
Open [ ] 2404VA 1MX101
(461ZV、462ZV or 463ZV)
Open [ ] 2406VA 1MX101
Open [ ] 2405VA 1MX101
Page 134 of 278

Operation
Location
flushing
Open [ ] 3014VA 1MX301
Open [ ] 3015VA 1MX301
Shutdown Roots fan (461ZV、462ZV
or 463ZV)
Open [ ] 2426VL 1MX101
Open [ ] 2025VL 1MX101
seconds)
Open [ ] 2027VK 1MX101
Open [ ] 2418VL 1MX101
(about 120 seconds)
Open [ ] 2018VL 1MX101
Open [ ] 2428VL 1MX101
seconds)
Page 135 of 278

Operation
Location
Open [ ] 3414VA 1MX101
Open [ ] 3415VL 1MX101
Open [ ] 2401VL 1MX101
cycling cleaning
Open [ ] 2401EO 1MX101
Input operation of #5 high-speed
Page 136 of 278

Operation
Location
will transfer the resin according to
(441PO or 442PO)
seconds)
Open [ ] 2027VK 1MX101

Open [ ] 2518VL 1MX101
Open [ ] 2526VL 1MX101
Open [ ] 2026VL 1MX101
Open [ ] 2024VL 1MX101
Open [ ] 3402VL 1MX101

Open [ ] 3415VL 1MX101
120 seconds)
transporting
Open [ ] 3412VA 1MX101
Open [ ] 3416VL 1MX101
seconds)
Page 137 of 278

Operation
Location
transporting
Open [ ] 3415VL 1MX101
transporting
Open [ ] 3019VL 1MX101

Open [ ] 2025VL 1MX301
flushing
s)
Open [ ] 2504VA 1MX101

(461ZV、462ZV or 463ZV)
Page 138 of 278

Operation
Location
Resin mixing (about 120 secon
ds)
Open [ ] 2506VA 1MX101
Open [ ] 2505VA 1MX101
mixing flushing
Open [ ] 3014VA 1MX301
Open [ ] 3015VA 1MX301
Shut down Roots fan
( 461ZV、462ZV or 463ZV)
Open [ ] 2526VL 1MX101
Open [ ] 2025VL 1MX101
Tuning fork switch 201SE acts
after the # 1 mix bed is full of
water
#5 mix bed washing (about
120 seconds)
Open [ ] 2027VK 1MX101
Open [ ] 2518VL 1MX101
resin washing
Page 139 of 278

Operation
Location
(about 120 seconds)
Open [ ] 2018VL 1MX101
Open [ ] 2528VL 1MX101
increasing pressure (about
120 seconds)
Mix bed resin mixing and
storage tower is full of water
Open [ ] 3414VA 1MX101
Open [ ] 3415VL 1MX101
Tuning fork switch 301SE acts
after the mix bed resin mixing
and storage tower is full of
water
Open [ ] 2501VL 1MX101
Open [ ] 2501EO 1MX101
again self-cycling cleaning
Page 140 of 278

Operation
Location
4.3 Regeneration operation of
high-speed mix bed
ineffective resin
The scrubbing, stratification
and transportation of the
separation tower resin
Verification and setting of
separation tower
backwash layer
parameters
On the "# 1 unit mix bed
regeneration unit" control
screen, click the "SPT
separation tower" icon, and
click the “Time seeting”
button on the popped-up
"SPT separation tower [ ]
operation" screen. On the
pop-up "SPT separation
tower time setting" screen,
respectively, set the following
parameters of regeneration
step sequence:
Repeated scrubbing times
[ ]
Set to 4 times.
Water filling 1" time
[ ]
Set to 300 seconds.
Draining 1" time
[ ]
Set to 180 Seconds.
Air scrubbing 1" time
[ ]
Set to 600 Seconds.
Draining 2" time
[ ]
Set to 180 Seconds.
Primary separation 1" time
[ ]
Set to 60 Seconds.
Page 141 of 278

Operation
Location
[ ]
Set to 1200 Seconds.
[ ]
Set to 600 Seconds.
[ ]
Set to 300 Seconds
[ ]
Set to 300 Seconds
Waiting time of resin output"
[ ]
Set to 300 Seconds.
Anion resin output Time
[ ]
Set to 600 Seconds.
Secondary separation Time
[ ]
Set to 600 Seconds.
Cation resin output Time
[ ]
Set to 900 Seconds.
Pipe flushing" Time
[ ]
Set to 300 Seconds.
Anion tower water-filling time
[ ]
Set to 300 Seconds.
Cation tower water-filling time
[ ]
Set to 300 Seconds
resin repeated scrubbing

On the "#1-unit mix bed
regeneration unit" screen,
click the "Start" button of
"repeated scrubbing". The
PLC will perform the [ ]
repeated scrubbing of the
resin in the separation tower
steps:
Page 142 of 278
Operation
Location
Startup 1 Roots
fan （ 461ZV 、 462ZV or
463ZV）
Open [ ] 3030VK 1MX101
Open [ ] 3114VA 1MX101

* Water
filling 1
Open [ ] 3115VL 1MX101
filling
Open [ ] 3119VK 1MX101 * Draining 1
draining
Open [ ] 3128VA 1MX101
Closed [ ] 3015VA 1MX101 Scrubbing

scrubbing
Open [ ] 3014VA 1MX101
Open [ ] 3015VA 1MX101
180 seconds after the draining
Page 143 of 278

Operation
Location
Repeat the above scrubbing
process (" water filling"
"draining" " water filling ") 4 [ ]
times, and the scrubbing
ends.
Shut down Roots fan
Shutdown the flushing water
The resin backwashed to stratify

On the "#1 unit mix bed
"primary separation ". The
PLC will perform the
backwashing stratification of
the resin in the separation
tower according to the
following steps:
[ ]
Open [ ] 3104VL 1MX101
Open [ ] 3103VL 1MX101
Open [ ] 3001VL 1MX101
Page 144 of 278

Operation
Location
60 seconds later, adjust the
opening of the separating
tower backwash regulating
441MD 1MX101
valve in order to adjust the
backwash water flow to 70
m3/h.
Adjust the opening [ ] 3001VL 1MX101
Then 1200 seconds later,
adjust the opening of the
separating tower backwash
441MD 1MX101
regulating valve in order to
adjust the backwash water
flow to 45 m3/h.
Then 300 seconds later, adjust
the opening of the separating
tower backwash regulating
441MD 1MX101
valve in order to adjust the
backwash water flow to 25
m3/h.
Then 300 seconds later 441MD 1MX101
Then 300 seconds later
(441PO or 442PO)
Output anion resin
Page 145 of 278

Operation
Location
PLC will perform the anion
resin output of separation
following steps:
[ ]
Open [ ] 3214VA 1MX101
* Anion
Open [ ] 3215VL 1MX101 tower is full
of water
After the tuning fork switch
(301SE) acts
* Transport
Open [ ] 3210VK 1MX101
anion resin
Open [ ] 3126VL 1MX101
Open [ ] 3110VL 1MX101
600 seconds after the anion
resin output
Open [ ] 3103VL 1MX101
600 seconds after delaying
* Transport
anion resin
Page 146 of 278

Operation
Location
* Re-
Open [ ] 3104VK 1MX101
stratification
Open [ ] 3103VL 1MX101
300 seconds after the resin re-

stratification
Open [ ] 3114VA 1MX101

*Separation
tower is full
(301SE) acts
of water
Output cation resin
On the "1-unit mix bed
PLC will perform the cation
resin output of separation
following steps:
Open [ ] 3314VA 1MX101
Open [ ] 3315VL 1MX101
*Cation
tower is full
(301SE) acts
of water
* Output
Open [ ] 3310VK 1MX101
cation resin
Open [ ] 3301VL 1MX101
* Output
Open [ ] 3102VL 1MX101
cation resin
Open [ ] 3103VL 1MX101
Page 147 of 278

Operation
Location
900 seconds after the cation
resin output, and after the
resin interface photoelectric
switch 311SM acts
Open [ ] 3019VL 1MX101

flushing
Page 148 of 278

Operation
Location
Open [ ] 3119VK 1MX101
Open [ ] 3101VL 1MX101
Open [ ] 3130VL 1MX101
pipe flushing
Shutdown the flushing pump
Regeneration operation of
mix bed anion resin
Parameters setting of ART anion
regeneration tower
Page 149 of 278

Operation
Location
screen, click the "ART anion
regeneration tower" icon,
and click the "Time setting"
"ART anion tower operation"
screen. On the popped-up
"ART anion tower time
setting screen respectively
set the following parameters
of the regeneration
step sequence:
Repeated scrubbing times"

[ ]
Set to 10 times.
Water filling 1 time
[ ]
Set to 600 seconds.
Draining 1 time
[ ]
Set to 180 seconds.
air scrubbing 1 time
[ ]
Set to 600 seconds.
pressure increasing 1 time
[ ]
Set to 60 seconds.
side draining 1 time
[ ]
Set to 60 seconds.
bottom draining 1 time
[ ]
Set to 60 seconds.
alkali entering time
[ ]
Set to 3600 seconds.
Page 150 of 278

Operation
Location
replacement time
[ ]
fast flushing 1 time
[ ]
draining 2 time
[ ]
Set to 180 seconds.
[ ]
Set to 600 seconds.
[ ]
Set to 60 seconds.
[ ]
Set to 60 seconds
[ ]
Set to 60 seconds.
water filling 2 time
[ ]
Set to 600 seconds.
fast flushing " time
[ ]
Anion resin repeated scrubbing
On "ART anion tower
operation" screen, click the
"Start" button of "Repeated
scrubbing". The PLC
perform the repeated
scrubbing of the resin in
ART anion tower:
[ ]
Startup one Roots fan
(461ZV, 462ZV or 463ZV)
Page 151 of 278

Operation
Location
Open [ ] 3030VK 1MX101
Open [ ] 3214VA 1MX101
draining
Open [ ] 3211VA 1MX101
* Scrubbing
1
Open [ ] 3216VL 1MX101
scrubbing
Open [ ] 3014VA 1MX101
* Scrubbing
1
Open [ ] 3015VA 1MX101
Open [ ] 3212VA 1MX101

60 seconds after the pressure * Pressure
increasing and keeping increasing 1
Open [ ] 3227VK 1MX101
Open [ ] 3210VK 1MX101

* Fast
draining
Page 152 of 278
Operation
Location
Open [ ] 3214VA 1MX101
* Water-
Open [ ] 3216VL 1MX101
filling
filling
process ("draining 1"
"scrubbing 1" "pressure
increasing 1" "fast draining""
water filling") 10 times, and
the scrubbing ends.
Shut down Roots fan
* Full of
Open [ ] 3214VA 1MX101
water
Open [ ] 3215VL 1MX101

The anion tower is full of
water until the level switch
(301SE) acts
Open [ ] 3210VK 1MX101

5 minutes after the washing
* Washing
of the anion tower
Page 153 of 278

Operation
Location

Shutdown flushing water pum
p
Anion tower resin alkali entering

regeneration
On "ART anion tower
"Start" button of "Alkali
entering regeneration". The
PLC perform the alkali
entering regeneration of the
resin in ART anion
regeneration tower:
Open mix bed alkali metering
box （423CW）inlet valve
Open [ ] 4203VR 1MP303
*Metering
When the concentrated
box
alkali in metering box 425MN
alkali
(423CW) rises to 1.0m
entering
Startup one regeneration
[ ]
Open [ ] 3030VK 1MX101
Page 154 of 278

Operation
Location
Open [ ] 3210VK 1MX101
Open [ ] 3207VR 1MX101
* Pre-
Open [ ] 4204VD 1MX101
injection
The regeneration flow should
[ ] 421MD 1MX101
be between 25 ~ 28m3 / h
The regeneration water
temperature should be [ ] 421KT 1MX101
between 35 ~ 40 ℃
The vacuum pressure of
alikali inlet of alkali ejector
[ ] 421EJ
should be less than -
0.05MPa.
minutes after the pre-
injection
Open [ ] 4201VR 1MX101
* Alkali
Alkali concentration of
recycling solution should be entering
3.5% ~ 5.5% regeneration
3.5%~5.5% [ ] 421MG 1MX101
When the concentrated alkali

in the metering box 425MN
(423CW) drops to 0.15m
* Metering
Open [ ] 4203VR 1MP303 box alkali
entering
When the concentrated alkali
in the metering box 425MN
(423CW) rises to 1.0m
60 minutes after the alkali
enters into the anion tower
Page 155 of 278

Operation
Location
45 minutes after the
*
replacement of the anion
Replacement
regeneration tower
Shutdown one regeneration
(461ZV, 462ZV or 463ZV)
Open [ ] 3215VL 1MX101

20 minutes after the washing *Fast Red
of anion regeneration tower wash one
Open [ ] 3214VA 1MX101 * Draining 2
Open [ ] 3227VK 1MX101
* Draining 2
draining
Open [ ] 3211VA 1MX101
*Air
Open [ ] 3216VL 1MX101
scrubbing 2
Page 156 of 278
Operation
Location
600 seconds after the scrubbing
Open [ ] 3014VA 1MX101
Open [ ] 3015VA 1MX101
* Pressure
increasing 2
Open [ ] 3212VA 1MX101
60 seconds after the pressure
increasing and keeping
Open [ ] 3227VK 1MX101
* Fast
Open [ ] 3210VK 1MX101
draining 2
Open [ ] 3214VA 1MX101

* Water-
Open [ ] 3216VL 1MX101
filling 2
600 seconds after the water filling of
the anion tower
Page 157 of 278

Operation
Location
process ("draining 2" -
"scrubbing 2" - "pressure
[ ]
increasing 2" - "fast draining
2"-" water filling 2") 4 times, and
the scrubbing ends.
Shutdown Roots fan
[ ] 3327VK 1MX101
Open [ ] 3214VA 1MX101

* Full of
water
Open [ ] 3215VL 1MX101
Anion tower is full of water until the
level switch (301SE) acts
Open [ ] 3210VK 1MX101

5 minutes after the washing of anion * Fast
tower flushing 2
Open [ ] 3201EF 1MX101
When the conductivity of recycling
water is less than 10 us/cm
Open [ ] 3031VK 1MX101
* Fast
flushing 2
15 minutes after the washing of
anion tower
Page 158 of 278

Operation
Location
Closed [ ] 3031VK
Regeneration operation of mix bed
cation resin
Parameters setting of CRT cation

regeneration tower
On the "# 1-unit mix bed
screen, click the "CRT cation
regeneration tower" icon, and
click the "Time setting" button
on the popped-up "CRT cation
[ ]
tower operation" screen. On the
popped-up "CRT cation tower
time setting" screen,
parameters of the regeneration
step sequence:
Repeated scrubbing times

[]
Set to 10 Times.
[]
Set to 600 seconds.
Draining 1 time
[]
Set to 180 seconds.
[]
Set to 600 seconds.
[ ]
Set to 60 seconds.
[ ]
Set to 60 seconds.
Page 159 of 278

Operation
Location
[ ]
Set to 60 seconds.
alkali entering time
[ ]
replacement time
[ ]
fast flushing 1" time
[ ]
draining 2 time
[ ]
Set to 180 seconds.
[ ]
Set to 600 seconds.
[ ]
Set to 60 seconds.
[ ]
Set to 60 seconds.
[ ]
Set to 60 seconds.
water filling 2 time
[ ]
Set to 600 seconds.
fast flushing 2 time
[ ]
Cation resin repeated scrubbing
On "CRT cation tower operation"
screen, click the "Start" button
of "Repeated scrubbing". The
[ ]
PLC perform the repeated
scrubbing of the resin in CRT
cation tower
[ ]
(441PO or 442PO)
Startup one Roots fan (461ZV,
462ZV or 463ZV)
Page 160 of 278

Operation
Location
Open [ ] 3030VK 1MX101
Open [ ] 3314VA 1MX101 * Draining 1
Open [ ] 3311VA 1MX101
Open [ ] 3316VL 1MX101
* Scrubbing
1
Open [ ] 3014VA 1MX101
Open [ ] 3015VA 1MX101
Open [ ] 3312VA 1MX101
Open [ ] 3327VK 1MX101
Open [ ] 3310VK 1MX101
* Fast
draining
Open [ ] 3314VA 1MX101
* Water-
Open [ ] 3316VL 1MX101
filling
600 seconds after the water filling
Page 161 of 278

Operation
Location

[ ]
increasing 1" - "fast draining"-"
water filling") 10 times, and the
scrubbing ends.
Shutdown Roots fan
[ ] 443PO 1MX101
* Full of
Open [ ] 3314VA 1MX101
water
Open [ ] 3315VL 1MX101
The cation tower is full of water until

the level switch (301SE) acts
Open [ ] 3310VK 1MX101
Closed [ ] 3314VA 1MX101 * Washing

5 minutes after the washing of the
cation tower
Page 162 of 278

Operation
Location

Cation tower resin acid entering
regeneration
On "CRT cation tower operation"

screen, click the "Start" button
of "Acid entering regeneration".
The PLC perform the acid
entering regeneration of the
resin in CRT cation
regeneration tower:
Open mix bed acid metering box
(412CW) inlet valve
Open [ ] 4103VR 1MP303
[ ] 3311VA 1MX101
When the concentrated acid in *Metering
metering box (412CW) rises to 413MN box acid
1.0m entering
Startup one regeneration pump
[ ]
(443PO or 444PO)
Open [ ] 3030VK 1MX101
Open [ ] 4107VR 1MP303
Open [ ] 3310VK 1MX101

* Pre-
Open [ ] 3307VR 1MX101
injection
Open [ ] 4105VD 1MX101
Page 163 of 278

Operation
Location
The regeneration flow (411MD)
should be between 25 ~ 28m3 / [ ] 411MD 1MX101
h
* Pre-
injection
The vacuum pressure of acid inlet of
acid ejector should be less than [ ] 411EJ 1MP303
-0.05MPa.
5 minutes after the pre-injection

*Acid
Open [ ] 4101VR 1MX101 entering
regeneration
Acid concentration of recycling
solution should be 3.5% ~ 5.5%
3.5%~5.5% [ ] 411MG 1MX101
When the concentrated acid in the

metering box (412CW) drops to 413MN
0.15m
Open [ ] 4103VR 1MP303
When the concentrated acid in the *Metering
metering box (412CW) rises to 413MN box acid
1.0m entering
[ ]
60 minutes after the acid enters into
the cation tower
45 minutes after their placement of *
the cation regeneration tower Replacement
Page 164 of 278

Operation
Location
Shutdown one regeneration pump
[ ]
(443PO or 444PO)
[ ]
(441PO or 442PO)
Startup one Roots fan (461ZV,
462ZV or 463ZV)
Open [ ] 3315VL 1MX101
20 minutes after the washing of * Fast
cation regeneration tower flushing 1
Open [ ] 3314VA 1MX101
Open [ ] 3311VA 1MX101

*Air
Open [ ] 3316VL 1MX101
scrubbing 2
Open [ ] 3014VA 1MX101
Open [ ] 3015VA 1MX101
Page 165 of 278

Operation
Location
Open [ ] 3312VA 1MX101
Open [ ] 3327VK 1MX101
Open [ ] 3310VK 1MX101
* Fast
draining 2
Open [ ] 3314VA 1MX101

Open [ ] 3316VL 1MX101
600 seconds after the water * Water-
filling of the cation tower filling 2
[ ]
increasing 2" - "fast draining
2"-" water filling 2") 4 times,
and the scrubbing ends.
Shutdown Roots fan
Open [ ] 3314VA 1MX101
Open [ ] 3315VL 1MX101
Cation tower is full of water
until the level switch
(301SE) acts
Open [ ] 3310VK 1MX101
Page 166 of 278

Operation
Location
5 minutes after the washing
of cation tower
Open [ ] 3301EF 1MX101
When the conductivity of *Fast
recycling water is less than flushing 2
10 us/cm
Open [ ] 3031VK 1MX101
15minutes after the washing
of cation tower
Closed [ ] 3031VK
p
Strengthened cleaning
regenerated resin
click the "resin cleaning"
button. The PLC will clean
the resin of the ART anion
regeneration tower and the
CRT cation regeneration
following set step sequence:
Open [ ] 3031VK 1MX101
Page 167 of 278
Operation
Location
Open [ ] 3227VK 1MX101
Open [ ] 3327VK 1MX101
Open [ ] 3216VL 1MX101
Open [ ] 3316VL 1MX101
Open [ ] 3071EF 1MX101
120 minutes after the anion
tower resin cleaning
[ ] 3316VL 1MX101
120 minutes after the cation
tower resin cleaning
Open [ ] 3314VA 1MX101
Open [ ] 3315VA 1MX101
The cation tower is full of
(301SE) acts
Open [ ] 3310VK 1MX101
Open [ ] 3301EF 1MX101
10 minutes after the cation
tower washing
Open [ ] 3214VA 1MX101
Open [ ] 3215VA 1MX101
Page 168 of 278

Operation
Location
The anion tower is full of
(301SE) acts
Open [ ] 3210VK 1MX101
Open [ ] 3201EF 1MX101
10 minutes after the anion
tower washing
p
Output the cation and anion
towers regenerated resin to
the storage tower
Setting of cation tower resin
output parameters

screen, click the "CRT
cation regeneration tower"
icon, and click the "Time
setting" button on the
popped-up "CRT cation
tower operation" screen. On
the popped-up "CRT cation
respectively, set the
following parameters of the
regeneration
step sequence:
Page 169 of 278
Operation
Location
Hydraulic delivery time

[ ]
Set to 180 seconds..
Moisture delivery time
[ ]
Set to 600 seconds.
Pipe flushing time
[ ]
Set to 60 seconds.
Cation tower full water time
[ ]
Set to 60 seconds.
Cation tower resin outputted to
the storage tower
On "CRT cation tower

operation" screen,
click "Output cation
resin" button. The PLC will
deliver the resin in CRT
cation tower to RST storage
following steps:
Open [ ] 3031VK 1MX101

Open [ ] 3414VA 1MX101
Open [ ] 3415VL 1MX101
The RST storage tower is full
of water until the level
switch (301SE) acts
Open [ ] 3410VK 1MX101
Open [ ] 3401VL 1MX101
Page 170 of 278

Operation
Location
Open [ ] 3302VL 1MX101
Open [ ] 3316VL 1MX101
Open [ ] 3315VL 1MX101
delivery
Open [ ] 3312VA 1MX101
120 seconds after the gas
delivery
water mixed delivery
Open [ ] 3315VL 1MX101
flushing
Open [ ] 3314VA 1MX101

The CRT cation tower is full
switch (301SE) acts
p
Stop [ ] 441PO 1MX101
Stop [ ] 442PO 1MX101
Setting of anion tower resin
output parameters
Page 171 of 278

Operation
Location
screen, click the "ART anion
regeneration tower" icon,
and click the "Time setting"
"ART anion tower
popped-up "ART anion
regeneration
step sequence:
Hydraulic delivery time
[ ]
Set to 180 seconds
Moisture delivery time
[ ]
Set to 600 seconds
Pipe flushing time
[ ]
Set to 60 seconds
Anion tower full water time
[ ]
Set to 60 seconds
Anion tower resin outputted to the
storage tower
On "ART anion tower

operation" screen,
click "Output anion
resin" button. The PLC will
deliver the resin in ART
anion tower to RST storage
following steps:
Open [ ] 3031VK 1MX101

Page 172 of 278
Operation
Location
Open [ ] 3414VA 1MX101
Open [ ] 3415VL 1MX101
switch (301SE) acts
Open [ ] 3410VK 1MX101
Open [ ] 3401VL 1MX101
Open [ ] 3202VL 1MX101
Open [ ] 3216VL 1MX101
Open [ ] 3215VL 1MX101
delivery
Open [ ] 3212VA 1MX101
120 seconds after the gas
delivery
water mixed delivery
Open [ ] 3215VL 1MX101
flushing
Open [ ] 3214VA 1MX101
The ART anion tower is full of
(301SE) acts
Page 173 of 278
Operation
Location
p
Stop [ ] 441PO 1MX101
Stop [ ] 442PO 1MX101
Mix operation of the resin in the
RST storage tower
Settings of the RST storage tower
resin mixing parameters
On the "# 1-unit mix bed

screen, click the "RST
storage tower" icon, and
click the "Time setting"
"RST storage tower
popped-up "RST storage
regeneration
step sequence:
[ ]
Set to 180 seconds.
Draining Time
[ ]
Set to 300 seconds.
Air mixing time
[ ]
Set to 180 seconds.
[ ]
Set to 180 seconds.
Fast washing time
[ ]
Set to 600 seconds.
Page 174 of 278

Operation
Location
RSTstorage tower resin mixing
On RST storage tower

operation screen,
click "Resin mixing" button.
The PLC will mix the resin
in the RST storage tower d
steps:
Open [ ] 3031VK 1MX101
Open [ ] 3414VA 1MX101
Open [ ] 3415VL 1MX101
switch (301SE) acts
Open [ ] 3410VK 1MX101
120 seconds after the storage
tower draining
(461ZV, 462ZV or 463ZV)
Open [ ] 3411VA 1MX101
180 seconds after the RST
storage tower resin mixing
Page 175 of 278

Operation
Location
Open [ ] 3014VA 1MX101
Open [ ] 3015VA 1MX101
Shutdown Roots fan (461ZV,
462ZV or 463ZV)
120 seconds after the stewing

of the RST storage tower
resin
Open [ ] 3415VL 1MX101
switch (301SE) acts
Open [ ] 3410VK 1MX101
storage tower washing
Open [ ] 3401EF 1MX101
storage tower continued
washing
Shutdown the flushing water
pump
Page 176 of 278

5. SHUT DOWN
Operation
Location
Under normal condition, do not
perform the shutdown
operation during
programmable control process
of the resin transferring and
regeneration. If the pipelines,
equipment, or programs fault
during the operation, and the
given task (the resin input,
output, and regeneration)
cannot be continued to
perform, shall manually click
the “Stop” buttons on
corresponding control screens
to abort the program
execution, so that the device
status can be
reset.SHUTDOWN
WATER POND
NEUTRALIZATION NO
5.1 Shutdown operation of
outputOn the "#1 unit
wastewater, demineralized
water, unit" control screen,
click the icon "#1 wastewater
pond " and click the
“shutdown” button of "
wastewater neutralization " on
the popped-up "#1 wastewater
pond operation " screen, PLC
will shutdown neutralization
and discharging the
wastewater of #1 wastewater
pond according to the
following steps:
Page 177 of 278

Operation
Location
Shutdown operation of # 1 high-
speed mix bed resin [ ] 2TFC471PO
outputShutdown
On the "# 1 unit condensate Mix
bed unit" control screen, click
the "#1 High-speed mix bed "
icon, and click the “Stop” button
of the “Resin output” on the
popped-up "#1 High-speed mix
bed operation" screen. The
dialog box "Stop transferring the
#1 High-speed mix bed resin to []
the SPT separetion tower?"
appears, click "Yes" button. The
PLC will shut down the flushing
water pumps and close the
related valves according to the
pre-set step sequence. The
program will return to "0" to
reset.Close the following valves
[ ] 2TFC629VR
pumpsClosed
441PO2TFC
ShutdownClosed [ ][ ] 1MX101
633VK
442PO2TFC
ShutdownClosed [ ][ ] 1MX101
634VK
Close the following valvesClosed [ ] 2TFC631EF
ClosedSHUTDOWN
[] 2029VA 1MX101
WATER POND
NEUTRALIZATION
ClosedOn the "#1 [] 2019VL 1MX101
unit wastewater,
demineralized
water, recycling
water unit" control
Page 178 of 278
Operation
Location
screen, click the
icon "#2
wastewater pond "
and click the
“shutdown” button
of " wastewater
neutralization " on
the popped-up "#2
wastewater pond
operation " screen,
PLC will shutdown
neutralization and
discharging the
wastewater of #2
wastewater pond
according to the
following steps:
2025VL2TF
ClosedShutdown [ ][ ] 1MX101
C472PO
ClosedClose the
[] 2030VL 1MX101
following valves
2TFC628
Closed [ ]
VR
2104VA2TF
ClosedClosed [ ][ ] 1MX101
C630VR
2118VL2TF
ClosedClosed [ ][ ] 1MX101
C643VK
Closed [ ] 2TFC641EF
Page 179 of 278
Operation
Location
The PLC control program "Resin
output" will return to "0" to reset: the [] 1MP302
"Startup" control button is available.
Shutdown operation of #2 high-

speed mix bed resin output
Mix bed unit" control screen,
click the "#2 High-speed mix
bed " icon, and click the “Stop”
button of the “Resin output” on
the popped-up "#2 High-speed
The dialog box "Stop
transferring the #2 High-speed
[]
mix bed resin to the SPT
separetion tower?" appears,
click "Yes" button. The PLC
will shut down the flushing
reset.
Shutdown flushing water pumps
Shutdown [] 441PO 1MX101
Close the following valves
Page 180 of 278
Operation
Location
The PLC control program
"Resin output" will return to "0"
[] 1MP302
to reset: the "Startup" control
button is available.

speed mix bed resin output
mix bed operation" screen. The
dialog box "Stop transferring
the #3 High-speed mix bed []
resin to the SPT separetion
tower?" appears, click "Yes"
button. The PLC will shut down
the flushing water pumps and
close the related valves
according to the pre-set step
sequence. The program will
return to "0" to reset.
Page 181 of 278
Operation
Location
[] 1MP302
Shutdown operation of #4 high-speed

mix bed resin output
On the "# 1 unit condensate []
The dialog box "Stop
transferring the #4 High-speed
mix bed resin to the SPT
separetion tower?" appears,
click "Yes" button. The PLC
will shut down the flushing
Page 182 of 278

Operation
Location
reset.
[] 1MP302
mix bed resin output
On the "# 1 unit condensate Mix []
bed unit" control screen, click the
"#5 High-speed mix bed " icon, and
click the “Stop” button of the “Resin
output” on the popped-up "#5 High-
speed mix bed operation" screen.
Page 183 of 278

Operation
Location
The dialog box "Stop transferring
the #5 High-speed mix bed resin to
the SPT separetion tower?"
appears, click "Yes" button. The
PLC will shut down the flushing
water pumps and close the related
valves according to the pre-set step
sequence. The program will return
to "0" to reset.
6. Shutdown
Identifi
Operation / check Position Remarks
cation
Page 184 of 278

Operation
Location

output" will return to "0" to reset:
the "Startup" control button is [] 1MP302
available.
5.2[5.9] Shutdown operation of high-

speed mix bed ineffective resin
regeneration
regeneration
cation bed unit" control screen,
bed" icon and click the "Stop"
button of "resin input" on the
Page 185 of 278

Operation
Location
popped-up "#1 mix bed
operation" screen. The dialog
box: "Stop transferring the RST
storage tower resin to #1 high-
speed mix bed?" appears, click
"Yes" button. The PLC will,
according to the following pre-
set steps, shutdown flushing
water pumps, shutdown Roots
pumps, and close related
valves. The program will return
"0" to reset.
3 6. Shutdown 4
6
I
d
e
n
t
i
7Positi 8Rema
5 Operation / check f 9
on rks
i
c
a
t
i
o
n
10Shutdown flushing water pumps 11
Page 186 of 278

Operation
Location
Shutdown mix bed recirculation pump
Open [] 3014VA 1MX101
Open [] 3015VA 1MX101
Shutdown Roots fans
Page 187 of 278

Operation
Location
6. Shutdown
Identifi
cation

input" will return to "0" to reset:
available.
12
Page 188 of 278

Operation
Location
regeneration
click the "#2 high-speed mix bed"
icon and click the "Stop" button
of "resin input" on the popped-up
"#2 mix bed operation" screen.
The dialog box: "Stop
transferring the RST storage
tower resin to #2 high-speed mix []
bed?" appears, click "Yes"
button. The PLC will, according
to the following pre-set steps,
shutdown flushing water pumps,
shutdownshut down Roots
pumps, and close related valves.
The program will return "0" to
reset.
13
14Shutdown flushing water pumps 15
Open [] 3014VA 1MX101
Open [] 3015VA 1MX101
Page 189 of 278

Operation
Location
Shutdown Roots fans
6. Shutdown
Identifi
cation

Page 190 of 278
Operation
Location

16

input" will return to "0" to reset:
available.
17

regeneration
click the "#3 high-speed mix bed"
icon and click the "Stop" button
of "resin input" on the popped-up
"#3 mix bed operation" screen.
Page 191 of 278

Operation
Location
tower resin to #3 high-speed mix
bed?" appears, click "Yes"
button. The PLC will, according
to the following pre-set steps,
shutdown flushing water pumps,
shut down Roots pumps, and
close related valves. The
program will return "0" to reset.
18
19 6. Shutdown 20
22
I
d
e
n
t
i 23 24
21 Operation / check f Positio Remar 25
i n ks
c
a
t
i
o
n
26 Shutdown flushing water pumps 27
Page 192 of 278

Operation
Location
Open [] 3014VA 1MX101
Open [] 3015VA 1MX101
Shutdown Roots fans
Close the following valves:
Page 193 of 278

Operation
Location
6. Shutdown
Identifi
cation

28

"Resin input" will return to "0" to
reset: the "Startup" control [] 1MP302
29
Page 194 of 278

Operation
Location
regeneration

cation bed unit" control
screen, click the "#4 high-
speed mix bed" icon and click
the "Stop" button of "resin
input" on the popped-up "#4
tower resin to #4 high-speed []
mix bed?" appears, click "Yes"
button. The PLC will,
pre-set steps, shutdown
flushing water pumps,
shutdown Roots pumps, and
program will return "0" to
reset.
Page 195 of 278

Operation
Location
Open [] 3014VA 1MX101
Open [] 3015VA 1MX101
Shutdown Roots fans
6. Shutdown
IDE
NTIF REMARK
Operation / check POSITION
ICAT S
ION
Page 196 of 278

Operation
Location
Page 197 of 278

Operation
Location

"Resin input" will return to "0" [] 1MP302

regeneration
Page 198 of 278

Operation
Location

bed" icon and click the "Stop"
button of "resin input" on the
popped-up "#5 mix bed
operation" screen. The dialog
box: "Stop transferring the
RST storage tower resin to #5 []
high-speed mix bed?"
appears, click "Yes" button.
The PLC will, according to the
following pre-set steps,
shutdown flushing water
pumps, shutdown Roots
valves. The program will return
"0" to reset.
6. Shutdown
IDE
NTIF REMARK
ICAT S
ION
Page 199 of 278

Operation
Location
Open [] 3014VA 1MX101
Open [] 3015VA 1MX101
Shutdown Roots fans
Page 200 of 278

Operation
Location
Page 201 of 278

Operation
Location
6. Shutdown
IDE
NTIF REMARK
ICAT S
ION

"Resin input" will return to "0" to [] 1MP302
reset: the "Startup" control
Page 202 of 278

Operation
Location
5.3[5.10] Shutdown operation
of high-speed mix bed
ineffective resin regeneration
Shutdown operation of the SPT
separation tower
If the regeneration program is
performing the resin
scrubbing operation: on the
"SPT separation tower
"Stop" button of "Repeated
scrubbing". The PLC will,
set steps, stop the scrubbing
operation of the resin in SPT
separation tower, shutdown
flushing water pumps,
shutdown Roots pumps, and
reset.
Page 203 of 278

Operation
Location
Open [] 3014VA 1MX101
Open [] 3015VA 1MX101
Shutdown Roots fans
Shutdown [] 461ZV 1MX101
Page 204 of 278

Operation
Location
6. Shutdown
IDE
NTIF REMARK
ICAT S
ION
The PLC control program of

"repeated scrubbing" of SPT
separation tower will return to [] 1MP302
"0" to reset: the "Startup"
control button is available.

backwashing stratification
Page 205 of 278

Operation
Location
operation: on the "SPT
separation tower operation"
screen, click the "Stop" button
of "Primary separation". The
PLC will, according to the
following pre-set steps, stop
the backwashing stratification
operation of the SPT
separation tower, shutdown
flushing water pumps, and
reset.
Page 206 of 278

Operation
Location

"Primary separation" of SPT
6. Shutdown
IDE
NTIF REMARK
ICAT S
ION
If the regeneration program
is performing the anion resin
output operation: on the
"Stop" button of "Anion resin
output". The PLC will,
pre-set steps, stop the anion
Page 207 of 278
Operation
Location
resin output operation of the
SPT separation tower,
valves. The program will
Page 208 of 278

Operation
Location

"Anion resin output" of SPT
separation tower will return [] 1MP302
to "0" to reset: the "Startup"

is performing the cation resin
output operation: on the
"Stop" button of "Cation resin
pre-set steps, stop the cation
SPT separation tower,
Page 209 of 278

Operation
Location
6. Shutdown
IDE
NTIF REMARK
ICAT S
ION
Close the following valves [] 3114VA 1MX101
Page 210 of 278

Operation
Location

"Cation resin output" of SPT
Page 211 of 278

Operation
Location
Shutdown operation of the ART anion

tower

performing the ART anion
tower resin scrubbing
operation: on the "ART anion
tower operation" screen, click
the "Stop" button of
"Repeated scrubbing". The
PLC will, according to the
following pre-set steps, stop
the scrubbing operation of the
resin in ART anion tower,
6. Shutdown
IDE
NTIF REMARK
ICAT S
ION
Page 212 of 278

Operation
Location
Open [] 3014VA 1MX101
Open [] 3015VA 1MX101
Shutdown Roots pumps
Close the following valves：
Page 213 of 278

Operation
Location

"repeated scrubbing" of ART
anion tower will return to "0" to [] 1MP302

performing the alkali entering
regeneration operation of the
ART anion tower: on the "ART
anion tower operation"
screen, click the "Stop" button
of "Alkali entering
regeneration". The PLC will,
set steps, stop alkali entering
ART anion tower, shutdown
regeneration pumps, flushing
water pumps and Roots
Page 214 of 278
Operation
Location
6. Shutdown
IDE
NTIF REMARK
ICAT S
ION
Open [] 3014VA 1MX101
Open [] 3015VA 1MX101
[] 463ZV 1MX101
Shutdown
Page 215 of 278
Operation
Location
Close the following valves：
Closed [] 4203VR 1MP303
Closed [] 4204VD 1MP303
Closed [] 3207VR 1MX101
Page 216 of 278

Operation
Location
Shutdown regeneration pumps

"Alkali entering regeneration"
of ART anion tower will return [] 1MP302
to "0" to reset: the "Startup"
6. Shutdown
IDE
NTIF REMARK
ICAT S
ION
Page 217 of 278

Operation
Location
performing the anion resin
output to RST operation: on
the "ART anion tower
"Stop" button of "Anion resin
set steps, stop the anion resin
output operation of the ART
anion tower, shutdown
reset.
Page 218 of 278

Operation
Location
[] 1MP302
"Anion resin output" of ART
anion tower will return to "0"
Page 219 of 278

Operation
Location

Shutdown operation of the

CRT cation tower
Shutdown operation of the CRT

cation tower
6. Shutdown
IDE
NTIF REMARK
ICAT S
ION
is performing the CRT cation
tower resin scrubbing
operation: on the "CRT
cation tower operation"
screen, click the "Stop"
button of "Repeated
scrubbing". The PLC will,
pre-set steps, stop the
scrubbing operation of the
resin in CRT cation tower,
Page 220 of 278

Operation
Location
Open [] 3014VA 1MX101
Open [] 3015VA 1MX101
Page 221 of 278

Operation
Location

"repeated scrubbing" of CRT
cation tower will return to "0" [] 1MP302

is performing the acid
entering regeneration
operation of the CRT cation
tower: on the "CRT cation
tower operation" screen,
Page 222 of 278

Operation
Location
click the "Stop" button of
"Acid entering regeneration".
The PLC will, according to
the following pre-set steps,
stop acid entering
CRT cation tower, shutdown
regeneration pumps, flushing
water pumps and Roots
Open [] 3014VA 1MX101
Open [] 3015VA 1MX101
Page 223 of 278

Operation
Location
Closed [] 4105VD 1MP303
Page 224 of 278

Operation
Location
Shutdown regeneration pumps

"Acid entering regeneration" of
CRT cation tower will return to [] 1MP302

performing the cation resin
output to the RST operation:
on the "CRT cation tower
"Stop" button of "Cation resin
Page 225 of 278

Operation
Location
set steps, stop the cation
CRT cation tower, shutdown
reset.
Page 226 of 278

Operation
Location

"Cation resin output" of CRT
cation tower will return to "0" to [] 1MP302

Page 227 of 278
Operation
Location
strengthened cleaning
operation of the ART anion
tower and the CRT cation
tower: on the "1 # unit mix
bed regeneration unit"
screen, click the "Stop"
button of the "Resin
cleaning". The PLC will,
pre-set steps, stop the
resin cleaning operation of
the CRT cation tower,
Page 228 of 278

Operation
Location
1MP302
The PLC control program of [
"Resin cleaning" of CRT ]
cation tower will return to "0"
Page 229 of 278

Operation
Location

Shutdown operation of the RST

storage tower
Shutdown operation of the RST

storage tower
performing the resin mixing
operation of the RST storage
tower: on the "RST storage
tower operation" screen, click
the "Stop" button of the
"Resin mixing". The PLC will,
set steps, stop the resin
mixing operation of RST
storage tower, shutdown
flushing water pumps and
Roots fans, and close related
Page 230 of 278

Operation
Location
Open [] 3014VA 1MX101
Open [] 3015VA 1MX101
Page 231 of 278

Operation
Location

"Resin mixing" of RST storage
tower will return to "0" to reset: [] 1MP302
the "Startup" control button is
available.
Page 232 of 278

6. IN-SERVICE INSPECTION
Operation
Location
6.1 High-speed mix bedWaste water
Ranged
neutralization discharge units 1#
[ ] 501MN/LN YB from 0.3 to
Concentrated acid storage tank
1.8 m
level meter m
#1 High-speed mix bed#1 waste ≤4.5mRang
2TFC471MN5
water pond level 2# Concentrated [ ][ ] YB ed from 0.3
02MN/LN
acid storage tank level meter m to 1.8 m
At the terminal phase of resin * There
output, the residual resin at should be
the bottom of #1 High-speed 201DE2TFC47 almost no
[ ][ ] [ 1MX101Y
mix bed#2 waste water pond 2MN601MN/ residual
] B
level 1# Concentrated alkali LN resin≤4.5mR
storage tank level meter anged from
m 0.3 to 1.8 m
After the resin input, the resin
layer height of #1 High-speed * 1.10 m
201DE
mix bed.Waste water pump [ ][ ] [ 1MX101Y Ranged
2TFC470MG6
outlet PH value 2# ] B from 0.3 to
02MN/LN
Concentrated alkali storage 1.8 m
tank level meter m
After the resin input, the
outlet water anion
conductivity after the #1 High- 211MG2TFC4 <0.30μs /
[ ][ ] 1MX101
speed mix bed self-cycling 71LP cm ≤0.3MPa
cleaning# 1 waste water
pump outlet pressure
# 1 waste water pump outlet [ 2TFC4
≤0.3MPa
pressure ] 72LP
#2 High-speed mix bed#1, #2
waste water pond inlet valve switch
status
Page 233 of 278

Operation
Location
At the terminal phase of resin * There
output, the residual resin at 202DE2TFC63 should be
[ ][ ] 1MX101
the bottom of #2 High-speed 1VK almost no
mix bed residual
resinOne is
After the resin input, the resin open and the
202DE other is
layer height of #2 High-speed [ ][ ] 1MX101
2TFC641VK closed
mix bed.
* 1.10 m
outlet water anion
<0.30μs /
conductivity after the #2 High- [] 221MG 1MX101
cm
speed mix bed ter theater of
#3 High-speed mix bed

* There
At the terminal phase of resin
should be
output, the residual resin at
[] 203DE 1MX101 almost no
the bottom of #3 High-speed
residual
mix bed
resin
layer height of #3 High-speed [] 203DE 1MX101 * 1.10 m
mix bed.
outlet water anion
<0.30μs /
cm

* There
should be
residual
mix bed
resin
Page 234 of 278
Operation
Location
mix bed.
outlet water anion
<0.30μs /
cm

* There
should be
residual
mix bed
resin
mix bed.
after the resin input, the outlet
water anion conductivity after
<0.30μs /
the #5 high-speed mix bed [] 251MG 1MX101
cm
ter theater of self-cycling
cleaning
6.2 High-speed mix bed resin

regeneration unit
SPT resin separation tower
After the output of the spt

separation resin, the height of
the residual resin at the [] 301CW 1MX101
bottom of the separation
tower
Page 235 of 278

Operation
Location
After the input of the spt
separation resin, the total
[] 301CW 1MX101 * 3.60 m
height of the separation tower
resin layer
ART anion regeneration tower
* There
After the output of the ART
should be
anion regeneration tower
[] 302CW 1MX101 almost no
resin, the residual resin at the
residual
bottom of the tower
resin
After the input of the ART
anion regeneration tower
[] 302CW 1MX101 * 1.80 m
resin, the height of the resin
layer in the towe.
After the resin regeneration of

the ART anion regeneration
tower is over, the outlet water [] 321LG 1MX101
conductivity after the washing
of regeneration tower resin
CRT cation regeneration tower
* There
After the output of the CRT
should be
cation regeneration tower
resin, the residual resin at the
residual
bottom of the tower
resin
After the input of the CRT
cation regeneration tower
[] 303CW 1MX101 * 1.50 m
resin, the height of the resin
layer in the towe.
Page 236 of 278

Operation
Location
the CRT cation regeneration
tower is over, the outlet water [] 331LG 1MX101
RST resin storage tower
* There
After the output of the RST
should be
storage tower resin, the
residual resin at the bottom of
residual
the tower
resin
After the input of the RST
storage tower resin, the
[] 303CW 1MX101 * 1.50 m
height of the resin layer in the
towe.
the RST storage tower is
over, the outlet water [] 331LG 1MX101
6.3 Acids, alkalis and reproducing

apparatus
High level acid storage tank [] 412MN 1MP303 ≥ 0.50 m

High level alkali storage tank [] 423MN 1MP303 ≥ 0.50 m
Mix bed acid metering box
[] 413MN 1MP303 <1.50 m
level
Page 237 of 278

Operation
Location
* Acid
concentratio
Acid concentration of mix bed n during the
[] 411MG 1MP303
ejector outlet regeneration
: 3.5% ~
5.5%
Mix bed alkali metering box
[] 425MN 1MP303 <1.50 m
level
* Alkali
concentratio
Alakli concentration of mix n during the
[] 421MG 1MP303
bed ejector outlet regeneration
: 3.5% ~
5.5%
6.4 Wastewater and pool
#1 wastewater neutralizaiton
[] 471MN 1MX101
pond level
#2 wastewater neutralizaiton
[] 472MN 1MX101
pond level
Page 238 of 278

7. PARTICULAR OPERATION INSTRUCTION

Operation
Location
7.1 Unqaulified resin sent back to

the separation tower NONE
Parameters setting

screen, click the "RST storage
tower" icon, and click the
"Time setting" button on the
popped-up "RST storage tower
popped-up "Time setting of
RST outputs to SPT" screen,
parameters of the regeneration
step sequence:
"Hydraulic delivery" time

[ ]
SET TO 120 SECONDS.
"Gas delivery" time

[ ]
Set to 120 seconds.
"Moisture delivery" time

[ ]
Set to 120 seconds.
Page 239 of 278

Operation
Location
"RST cleaning" time

[ ]
Set to 300 seconds.
"Pipe flushing" time

[ ]
Set to 180 seconds.
Unqaulified resin sent back the

separation tower
On the "RST storage tower

operation" screen, click
"Unqualified resin sent to the
separation tower" button, and
then click the "Start" button. The
PLC will transfer the resin
according to the following steps:
Open [ ] 3031VK 1MX101

(441PO or 442PO) [ ]
Open [ ] 3130VL 1MX101
Open [ ] 3101VL 1MX101
Open [ ] 3119VK 1MX101
Page 240 of 278

Operation
Location
Open [ ] 3402VL 1MX101
Open [ ] 3416VL 1MX101
Open [ ] 3415VL 1MX101

delivery
Open [ ] 3412VA 1MX101
120 seconds after the gas delivery

mixed delivery
Open [ ] 3415VL 1MX101

cleaning
Open [ ] 3019VL 1MX101
180 seconds after the resin pipe

flushing
Page 241 of 278

Operation
Location
Ope
[ ] 3414VA 1MX101
n
Ope
[ ] 3415VL 1MX101
n
The
RST
stora
ge
towe
r is
full
of
wate
r
until
the
tunin
g
fork
switc
h
301S
E
acts
Clos
[ ] 3414VA 1MX101
ed
Clos
[ ] 3415VL 1MX101
ed
Page 242 of 278
Operation
Location
Shut
dow
n flu
shin
g wa
ter p
ump
s
Shut
[ ] 441PO 1MX101
dow
n
Shut
[ ] 442PO 1MX101
dow
n
Clos [ ] 3031VK 1MX101

ed
Page 243 of 278

8. INCIDENTS
Operation
Location
8.1 If it is found that the resin output

program of high-speed mix bed
aborts abnormally or there is
large amount of residual resin in
the resin bed, shall report
immediately and analyze the
reasons. Then, re-start the resin
output program and remove the
resin in resin bed.The outlet water
conductivity is abnormal after the
recycling water mix bed
operatingIndustrial hydrochloric
acid spill emergency response
Possible causes: Evacuation and

isolation. during the industry
hydrochloric acid transport, use,
storage, once it leaked, the first step is
to evacuate non-essential personnel,
isolation leakage polluted area.
Meanwhile, in case of protect
themselves security, local personnel [ ]
should be checked the accident site,
reported to the personnel relevant
industrial safety, medical aid, direct
leadership, etc., if necessary, call to
"119" alarm, requesting rescue to
professionals fire , while to protect,
control the scene.
Page 244 of 278

Operation
Location
8.2 If it is found that the resin input

program of high-speed mix bed
aborts abnormally or there is
large amount of residual resin in
the resin bed, shall report
immediately and analyze the
reasons. Then, re-start the resin
output program and transfer the
resin in regeneration tower to SPT
separation bed. Conductivity
meter sample water is
abnormal;Isolation system. [ ]
Isolation system is particularly
important for the treatment of
industrial hydrochloric acid
leakage, especially inlet and outlet
valves of the leak system, if do not
rapidly isolate systems, it will
result a larger amount of
hydrochloric acid leak. Before
leave isolation system, staff should
wear protective clothing, wear
protective equipment.
Page 245 of 278

Operation
Location
Conductivity meter electrodes are
contaminated;Field ambulance. Due to
hydrochloric acid with strong corrosive
characteristic, and it can produce
chemical burns to the human body, the
volatile hydrogen chloride gas have a
strong irritant and corrosive effect to
respiratory; therefore, if sprayed or
[ ]
splashed by hydrochloric acid, must
rinse with plenty of water immediately ,
then clean with 0.5% sodium
bicarbonate solution, while leaving the
leakage site. If splashed in the eyes,
you must rinse with plenty of water
immediately and sent to the infirmary
for treatment.
8.3 During the backwashing of the

SPT separation tower, if it is
found that there are large
particles of mix bed resin leaking,
shall stop the executing program
immediately, report and analyze [ ]
the reason, and report the defect
repairment if necessary.
Conductivity meter electrodes are
aging or damaged;Leakage
Control
Conductivity meter secondary meter

fault;Staff who Enter the site must wear
[ ]
anti-acid clothes, anti-acid rain boots,
wear a full face shield.
Page 246 of 278

Operation
Location
8.4 During the backwashing of the

SPT separation tower, if it is
found that the flow during the
resin stratification deviates from
the set value, the resin interface is
not clear after stratification, or
the height of the cation and anion
layers is a little larger, shall stop
the executing program [ ]
immediately, report and analyze
the reason, adjust the resin
loading amount in time and report
the defect repairment if necessary.
Conductivity meter and PLC data
communication fault;Do not act
alone when emergency treatment,
must have a guardian.
Recycling water mix bed resin has

been effective;After isolation of the
system for leaks, repair and plugging [ ]
manner in a timely, to stop hydrochloric
acid further leak.
Page 247 of 278

Operation
Location
8.5 During transferring the SPT

separation tower resin to the ART
anion tower and the CRT cation
tower, if it is found that the SPT
separation tower resin is fully
transferred to the CRT cation
tower, shall stop the executing
program immediately, report and
analyze the reason, manually
transfer the CRT resin back to
SPT for re-stratification. Report [ ]
the defect repairment if necessary,
and perform maintenance
treatments for photoelectric
switch or PLC control program.
The flow when recycling water
mix beds are operating is too
large, the recycling water mix bed
is operating overloaded;Rinse the
leak with plenty of water, fire,
diluted the industrial hydrochloric
acid leaking.
Recycling water mix bed inlet water

quality is poor: acid, Caustic
concentration is too high;To prevent
leakage proliferation, affecting the [ ]
surrounding buildings, equipment and
people, if unable to control leaks, must
be disposed of spills promptly.
Page 248 of 278

Operation
Location
8.6 During the resin scrubbing of

ART anion tower and CRT cation
tower, if it is found that have large
particles of resin leak, shall stop
the executing program
immediately, report and analyze
the reason, and report the defect
repairment if necessary. Recycling
water mix bed resin regeneration
is unqualified;Disposal of spill:
Acid leak small amounts can be
flush with water. But a lot of [ ]
hydrochloric acid leak spreading
proliferation, it is difficult to
collect processing,it can be used
embankment to intercept or
drainage a safe location. To
reduce the leakage of air to the
evaporator,it can be use foam or
other coverings to cover, after it is
formed to cover the surface and
inhibit evaporation then transfer
processing.
Possible consequencesIndustrial liquid

alkali spill emergency response
Page 249 of 278

Operation
Location
8.7 During the acid entering

regeneration of cation bed resin
regeneration tower, if it is found
that the concentration of
regeneration solution deviates
from limits (3.5 to 5.5%), shall
immediately adjust the opening of
mix bed acid metering box outlet
valve (4124VR); Wastewater
cannot be recycled, the consuming
amount of TFC demineralized
water increases.Evacuation and
isolation. during the industry
liquid alkali transport, use, [ ]
storage, once it leaked, the first
step is to evacuate non-essential
personnel, isolation leakage
polluted area. Meanwhile, in case
of protect themselves security,
local personnel should be checked
the accident site, reported to the
personnel relevant industrial
safety, medical aid, direct
leadership, etc., if necessary, call
to "119" alarm, requesting rescue
to professionals fire , while to
protect, control the scene.
Page 250 of 278

Operation
Location
8.8 Abnormality HandlingIsolation

system. Isolation system is
particularly important for the
treatment of industrial liquid
alkali leakage, especially inlet and
outlet valves of the leak system, if [8.9] [
8.9[8.10]
do not rapidly isolate systems, it ]
will result a larger amount of
liquid alkali leak. Before leave
isolation system, staff should wear
protective clothing, wear
protective equipment.
Page 251 of 278

Operation
Location
8.10[8.11] During the alkali entering

regeneration of anion bed resin
regeneration tower, if it is found
that the concentration of
regeneration solution deviates
from limits (3.5 to 5.5%), shall
immediately adjust the opening of
mix bed alkali metering box outlet
valve (4124VR); First locally
check whether the sample water
of the conductivity meter is
qualified, the flows of mix bed
inlet and outlet water are
appropriate. If not, adjust
timely.Field ambulance. Due to [ ]
NaOH with strong corrosive
characteristic, and in high
concentration conditions ，it have

a strong corrosive effect to body;
Therefore, if sprayed or splashed
by NaOH, must rinse with plenty
of water immediately, then clean
with 1% acetic acid solution. If
splashed in the eyes, you must
rinse with plenty of water
immediately, then clean with 2%
of the dilute acid solution ,and
sent to the infirmary for
treatment.
Page 252 of 278

Operation
Location
8.11[8.12] Check whether the mix bed

back-inlet valve, acid (Caustic)
inlet valve is not closed tightly [8.13] [
which leads to the infiltration of 8.12[8.14]
acid-Caustic solution and other ]
unqualified liquid, and then affect
the water quality.Leakage Control
Page 253 of 278

Operation
Location
8.13[8.15] During the acid (alkali)

entering regeneration of mix bed
resin regeneration tower, if the
regeneration program abnormal
abortion or confusion is found,
shall immediately check the level
of mix bed acid (alkali) metering
boxes and the states of acid
(alkali) inlet valves. Exclude the
danger of concentrated acid
overflowing, then report and [ ]
analyze the reasons. Re-start the
"Acid (Alkali) entering
regeneration" pogram to re-
regenerate the resin. Call the
analysts to perform the sampling
analysis, check whether the
conductivity measurements are
accurate.Staff who Enter the site
must wear anti-acid clothes, anti-
acid rain boots, wear a full face
shield.
8.14[8.16] If the conductivity meter

fault or contaminated, report the
defect to the instrument control [8.17] [
maintenance personnel for 8.15[8.18]
handling;Do not act alone when ]
emergency treatment, must have a
guardian.
Page 254 of 278

Operation
Location
8.16[8.19] During the acid (alkali)

entering regeneration of mix bed
resin regeneration tower, if the
acid (alkali) pipeline leaks, shall
immediately press the "Stop"
button" of “Acid (Alkali) entering
regeneraiton”, and report the
emergency defect. Re-start the
regeneration program to [ ]
regenerate after the defect is
eliminated. If the mix bed resin
has been ineffective, shutdown the
recycling water mix bed, perform
regeneration for the ineffective
resin.After isolation of the system
for leaks, repair and plugging
manner in a timely, to stop NaOH
further leak.
8.17[8.20] If the cause is that the resin is

not clean before the regeneration,
rescrub the resin and extend the [8.21] [
strengthen cleaning time;Rinse 8.18[8.22]
the leak with plenty of water, fire, ]
diluted the industrial NaOH
leaking.
Page 255 of 278

Operation
Location
8.19[8.23] After the resin regeneration

of anion and cation bed resin
regeneration towers, if it is found
the outlet water conductivity
during the cleaning has been high,
shall immediately report and
analyze the reasons: If the cause is
that the regeneration agent
concentration or dosage is [ ]
insufficient during the
regeneration, then re-
regenerating and re-cleaning the
resin.To prevent leakage
proliferation, affecting the
surrounding buildings, equipment
and people, if unable to control
leaks, must be disposed of spills
promptly.
First, call the analyst to perform

sampling analysis, check
whether the measurements of
conductivity meter are
accurate.Wastewater pump
outlet PH values are abnormal
Disposal of spill: NaOH leak [ ]
small amounts can be flush with
water. But a lot of NaOH leak
spreading proliferation, it is
difficult to collect processing,it
can be used embankment to
intercept or drainage a safe
location.
Page 256 of 278

Operation
Location
If the reason is the conductivity

fault or contaminated, report the
defect to maintenance personnel
for treatment;Possible
CausesAccident treatment of
ammonia leakage
If the reason is the resin has not

been scrubbed clean, then re-
start the “resin scrubbing”
program to scrub the resin and
extend the time of strengthen
cleaning; PH meter sample water
is abnormal;Ammonia leakage
[ ]
phenomenon: when ammonia
leak, emitting a lot of smoke from
the leak, the surrounding
environment has a strong
irritating odor; the equipment,
pipeline of leaks chills, severe
freezing.
If the reason is that the
concentration or dosage of
regenerated reagents is not
enough, then re-start the "acid
entering regeneration" program [ ]
to re-regenerate and re-clean the
resin; PH meter electrodes are
contaminated;Reasons for
ammonia leak
Page 257 of 278

Operation
Location
If the reason is that the anion
tower is mixed with cation resin
or the cation tower is mixed with
anion resin, then the resin should
be sent back to the SPT
separation tower for re-
stratification, and adjust the
operating parameters of the SPT
separation tower or the heights
[ ]
of the anion-cation resin in the
tower. Report the defect
repairment if necessary, and
perform maintenance treatments
for photoelectric switch or PLC
control program. PH meter
electrodes are aging or
damaged;Leaking for and liquid
ammonia cylinder damaged;
If the reason is that the resin
surface is contaminated by oil or
other organic substance, shall
cooperate with the mechanical
maintenance personnel (connect
to temporary pipeline) to perform
alkali treatment to the resin, and
[ ]
then perform times amount of
acid entering regeneration to the
resin. If is still useless, shall
consider of replacing the resin.
PH meter secondary meter fault
Leak for liquid ammonia cylinder
outlet valve blocked laxly;
PH meter and PLC data
[
communication fault;Leak for
liquid ammonia tank outlet hose
]
connection damaged;
Page 258 of 278

Operation
Location
Possible ConsequencesLeak for

the connection between outlet [ ]
hose connection and the joint of
ammonia cylinder blocked laxly;
After the wastewater pump

outlet PH meter values become
abnormal, the neutralization and
control of wastewater will
[ ]
become confused. Leak for the
joints of liquid ammonia tank
outlet pipeline and installation of
pressure meter blocked laxly.
Abnormality HandlingDisposal of
ammonia leak
check whether the Wastewater

PH meter working normal; Set
evacuees to the windward at the
[ ]
first time, and isolated until the
gas dissipated or leak under
control;
Page 259 of 278

Operation
Location
On the "#1 unit wastewater,
demineralized water unit" control
screen, click the icon "#1 unit
wastewater ". On the popped-up
"#1 unit wastewater operation"
screen, click the stop button, the
PLC will stop the neutralization Pause
and discharging of # 1 [ ][ ] 2TFC471PS wastewater
wastewater pond;At the same neutralization
time, reported to the master,
phone the fire brigade: 119
(extension) alarm, then
according program to reports to
the relevant departments and
leadership;
On the "#1 unit wastewater,
demineralized water unit" control
screen, click the icon "#2 unit
wastewater ". On the popped-up
"#2 unit wastewater operation" Pause
screen, click the stop button, the [ ][ ] 2TFC471PS wastewater
PLC will stop the neutralization neutralization
and discharging of # 2
wastewater pond;Cut off the fire
source, if necessary, cut off the
power in the pollution region;
Call the MCR, notify chemical
analysts to manually detect the
wastewater pump outlet pH for
manual comparation;Open the [ ]
nearest water source, including
Open outdoor fire water ,and
then spray ammonia leak points;
Page 260 of 278

Operation
Location
Report the emergency defect
and cooperate with maintenance
personnel to remove it.In
permitted conditions, emergency [ ]
personnel wearing dedicated gas
masks and gloves to enter local
to inspect the reasons;
In permitted conditions, taken measures
to cut off the gas supply, or after the
[ ]
dilution of residual ammonia in pipeline,
drained by the discharge pipe;
Do not use sparking tools and motor
vehicles in the leakage area, severe
[ ]
should prohibit the use of
communication tools;
Poisoning should immediately rushed
ventilation, emergency rescue and [ ]
notify the hospital.
Disposal of liquid ammonia tank leak
Ammonia cylinders are produced by
specialized manufacturers before it is in
service, and it had been tested
rigorously by security department, so
the possibility of leakage is little, should
be taken notice to avoid a violent crash [ ]
at the scene, loading and unloading of
the ammonia cylinder handling
transportation, there must be a rubber
cushion rings in cylinder, no exposure
cylinders.
Page 261 of 278

Operation
Location
Liquid ammonia tank treatment: the
possible reason make ammonia tank
outlet valves leaks is the filler of the
valve wear. Disposal is to wear full
protective clothing with breathing [ ]
apparatus, strictly close the outlet valve
with the fire water. If it still leaks, water
would need to remain until the leak is
completed.
Connecting pipe leakage process: the
pipeline behind the cylinders ammonia
leak , you must first strictly close
ammonia cylinder outlet valve, and then [ ]
deal with the leak at the connection, if
still leaks, it is required for long-term fire
water spray.
Precautions
When operator received liquid ammonia
tank, check cylinder attachment is
[ ]
intact, if there is damage to the valve
port, the connection is loose;
Ammonia cylinder pipeline connection
is completed, gently open outlet valve,
[ ]
use PH test paper (alkaline) to measure
all the joints leaks;
Strict management of liquid ammonia
tank: ammonia bottle belong to mobile
high-pressure device, ammonia bottle
must be technology checked once
every three years, if it used 12 years
should be scrapped. When found
[ ]
sidewall cracks or local corrosion, it is
deeper 10% than the nominal wall
thickness, and found scarring,
depression, drum kits, scars and heavy
leather and so on, should be prohibited
using.
Page 262 of 278
Operation
Location
Local protection equipment
configuration: there are fire water,
protective clothing, breathing
[ ]
apparatus, protective gloves, ammonia
special gas masks, emergency
medicine and other nearby.
Ammonia leak on human health
hazards
Pathways: inhalation, frostbite. [ ]
Health hazard: Inhale low
concentrations will have a stimulating
effect on the mucous membranes, if
[ ]
concentrations is high, it may cause
histolysis necrosis, and it cause
chemical pneumonia and burns.
Acute poisoning: mild manifestations is
skin, mucous membrane irritation, there
is rhinitis, laryngitis, bronchitis; may
occurs corneal and skin burns. Severe
occurs laryngeal edema, glottis narrow
airway mucosal cell shedding, airway
obstruction to make suffocation, as well [ ]
as possible occurs toxic pulmonary
edema and liver damage. Ammonia can
cause breathing to stop. If splashed in
the eyes, can cause lens opacity,
corneal perforation, and even
blindness.
Ammonia poisoning patients aid
measures
Remove victim to fresh air. [ ]
Call emergency medical service center. [ ]
If breathing has stopped, administer
artificial respiration. If inhaled or
[ ]
ingested ammonia, please do not take
mouth resuscitation.
Page 263 of 278

Operation
Location
If breathing is difficult ,then carry out
[ ]
oxygen.
Removed and isolate contaminated
clothing and shoes, and wash with [ ]
water 20 minutes or more.
Keep the patient warm and quiet. [ ]
Closely observe of the patient's
[ ]
condition.
First aid dip ammonia
Eyes: Do not rub, opened the eye lids ,
can be rinse with the flow of water or
2% boric acid solution and quickly close [ ]
and open eyes, so that the water filled
the whole eye.
For the nose, throat, drops 2% of boric
acid solution to nasal, and gargle with
boric acid solution, you can drink a lot [ ]
of 0.5% of citric acid or vinegar, avoid
ammonia proliferate in vivo.
For the skin, you should take off your
clothes, pants, shoes if it stained with
ammonia, rinse the affected area with
[ ]
water and 2% boric acid solution, ,
burned skin should be exposed to the
air and coated with drugs.
The above personnel shall be promptly
[ ]
sent to hospital for treatment.
Page 264 of 278

9. LOCAL OPERATOR SHEET

NONE
Page 265 of 278

10. ANNEXURE
ANNEXURE I
HAZARDOUS CHEMICAL CHARACTERISTICS TABLE
1) Ammonia
Ammonia,
Name Ammonia Aliases English name Ammonia
ammonia
Molecular Melting
Formula NH3 17.03 -77.7℃
Weight point
- The
0.771 Vapor 1013kpa
Boiling Point 33.35 relative
(Liquid) Pressure (26) ℃
Physical ℃ density
and The 0.597
Explosive 16%- Ignition
chemical relative （Vapo 651 ℃
limit 25% point
properties density r）
Appearance
Colorless, poisonous gas with strong pungent stench
Odor
Soluble in water to form ammonium hydroxide,
Solubility
dissolved in ether and other organic solvents.
Stability: Easy liquefaction, in temperature changes conditions,
coefficient of volume change a lot, in case of high fever, explode
within the container.
Stability
Hazard: Flammable, but only in case of fire is shown in a limited area,
and hazard
the case of the presence of oil or fuel combustion can enhance risk;
contact with liquid ammonia can cause severe burns. Solution is
corrosive.
In the Workplace air, allowable concentration exposed a short time:
（mg/m3）30
Maximum allowable exhaust emissions （ kg/h ） 4.9 （ 15m ） -
75（60m）
Environme Odor pollution factory sector standard
3
ntal values（mg/m ）1.0（A），1.5,2.0
Standards (2nd new, now) ， 4.0 （ 3rd new ）， 5.0 （ 3rd existing ） , Surface
water(With NH3-N meter, mg / L) 0.15 (class I), 0.5 (Ⅱ type), 1.0 ( Ⅲ
class), 1.5 (Ⅳ class), 2.0 (Ⅴ class)
Sewage maximum allowable emission concentration :( to NH3-N
meter, mg / L) 15 (a), 25 (two)
Page 266 of 278

Acute toxicity:
Low concentrations of inhalation tolerance:20ppm
man oral median lethal concentration (LCL0):5000ppm·5min
Rat oral median lethal concentration (LC50):350×10-6
Toxicologic Rat inhaled median lethal concentration (LCL0):2000mg/m3·4h
al Acute poisoning:
Information For the skin, mucous membranes and eyes, it is corrosive. Mildly
occurred tear, sore throat, cough, edema; moderate symptoms
intensified, difficulty breathing; severe can occur toxic pulmonary
edema, severe cough, a lot of pink frothy sputum, coma, shock; high
concentrations of ammonia can cause breathing reflex stop.
Engineering Strictly confined, provide adequate local exhaust and

Controls general ventilation.
When the concentration in air overweight, must wear
Respiratory gas masks. Emergency rescue or evacuation, should
protection wear positive pressure self-contained breathing
apparatus.
Eye
Security Masks protective glasses.
protection
measures
Body
Wear rubber acid protective clothing.
Protection
Hand
Wear rubber acid gloves.
Protection
Workspace no smoking, eating and drinking. Shower
Other after working. Maintain good health habits. Enter the
high concentration operations, should be monitored.
Emergency aid Immediately escape from the scene to fresh air, should
measures measures artificial respiration when breathing is weak or stops,
while oxygen. Keep quiet and warm. Flush eyes and
skin with plenty of water more than 15 minutes when
contaminated, timely medical treatment.
Page 267 of 278

Rapid withdrawal of staff from air leakage to windward

and isolate until the gas dissipated, emergency
personnel should wear positive pressure self-contained
Leakage breathing apparatus. Wearing chemical protective
disposal clothing (complete isolation). When disposal of Cylinder
leak ,should make the valve at the top, and close the
valve, if it cannot be closed , put the cylinder immersed
in water.
Cut off the gas supply. Water spray to cool containers.
Fire
Water spray, cut off the gas supply to ensure the safety
Methods
of personnel. Fire extinction with mist water spray
Quick method: Detection trachea

Detection scope:0.5ppm-15%
GB methods: Nessler's reagent colorimetric GB/T
14668-93
Environmental Detection limit:0.25mg/m3
monitoring methods Ion Selective Electrode GB/T 14669-93
Detection limit:0.014 mg/m3
Sodium hypochlorite - salicylic acid spectrophotometry
GB/T 14679-93
Detection limit:0.008 mg/m3
Toxic gases, flammable gases; resistant to low or
General Packaging
medium pressure cylinders tank.
Used as refrigerants and preparation of ammonium
The main purpose
fertilizers and nitrogen.
2) Hydrochloric acid
Hydrochloric Hydrochloric acid
Hydrochl English
Name Aliases acid, sulfuric
oric acid name Hydrogen chloride
acid salt
Molecu
Melting
Physical Formula HCL lar 36.46 -114.8℃
point
and Weight
chemical Industrial 31% Relativ
properties concentr 、33 e 1.12- Freezing
-17～-62℃
Quality ation %、3 Densit 1.19 Point
range 6% y
Page 268 of 278

108. Vapor
Boiling 30.66
6(20 Pressu
Point (21℃)
%) re
Appearan Colorless or slightly yellow fuming liquid ,with a pungent
ce Odor sour.
Miscible with water, soluble in alcohol and ether. Easily
Solubility
volatile at room temperature.
Corrosive to most metals, release active hydrogen when react with

metal powders; can produce highly toxic hydrogen cyanide gas when
Stability
react with cyanide; concentrated hydrochloric acid in the air, hit the
and hazard
ammonia vapor generated white smoke.
Belong to the third category of precursor chemicals varieties.
Workplace Air maximum allowable concentration（mg/m3）7.5

Maximum allowable emission concentration
3
Environme （mg/m ）150（HCLGas）
ntal Without emissions monitoring of the exhaust gas
3
Standards limits（mg/m ）0.25（HCLGas）
Drinking water quality limitsPH 5.5～8.5
Sewage maximum allowable emission concentrationPH 6～9
Acute toxicity (hydrogen chloride)：
Inhalation minimum lethal concentration （LC10 ）：1 300ppm·30
min
Inhalation minimum lethal concentration （ LC10 ）： 3 000ppm·5
min
Rats inhaled median lethal concentration（LC50 ）：4 701ppm·30
Toxicologic
min
al
Mice inhaled median lethal concentration（TC50）：2 142ppm·30
Information
min
There is irritation for eye, respiratory tract and skin.
Short-term exposure can occur sore throat, coughing, choking
feeling. Severe cases may occur laryngospasm or pulmonary edema;
contact with the skin can cause corrosive burns; etching of teeth.
Aquatic Toxicity:282 ppm·96h(Mosquito fish).
Security Engineerin Closed operation, attention to ventilation.
measures g Controls
Page 269 of 278

Respirato
Contact the smoke, wear filter respirators; Emergency
ry
rescue, should wear positive pressure self-contained
protectio
breathing apparatus.
n
Eye
protectio Wear chemical safety glasses.
n
Body
Protectio Wear rubber acid protective clothing.
n
Hand
Protectio Wear rubber acid gloves.
n
Workspace no smoking, eating and drinking. shower After
Other
working.
Inhale mist should escape the scene immediately, place to
First aid rest and keep warm; after skin contact should be stripped
measure of contaminated clothing, rinse quickly with water; if
s swallowed, then rinse, do not induce vomiting and give
medical care.
Rapid withdrawal from air leakage personnel to a safe
area, emergency personnel should wear positive pressure
self-contained breathing apparatus. Wear anti-acid. Sand,
Emergency dry lime or soda ash mixed to deal with small leak, also
Leakage
measures can be with water washing and then discharged into the
disposal
wastewater treatment system; large spills should build a
causeway or trenching to collect, transfer it to the tank by
pump, and the residue was safe disposal by shipped to
recycling waste disposal sites.
Take an alkaline substance such as sodium bicarbonate,
Fire sodium carbonate, calcium hydroxide to neutralize. Also
Methods can spray a lot of water to fight the blaze. Firefighters
should wear oxygen masks and full protective clothing.
Page 270 of 278

Quick method: Gas detector tube (hydrogen chloride)

Detection range:1～1000 mg/m3
neutralizing: pH test paper
Environmental
Silver nitrate titration method GB 11896—89
monitoring methods
Detection range:10～500mg/L
Mercuric thiocyanate spectrophotometry HJ/T 27—1999
Detection limit:0.9mg/m3（10L）
Corrosive substances; liner outside the glass but inside

wooden box, acid altar outside the wooden lattice boxes,
plastic buckets, tankers. Not mix with sulfuric acid, nitric
General Packaging
acid, not transportation mixed with alkali, metal powder,
zinc oxide, hydride, chlorate, fluoride, water flammable
materials.
Uses Chemical raw materials.
None
Page 271 of 278

Sodium hydroxide
Sodium
English Sodium
Name hydroxide Aliases liquid alkali
name hydroxide
solution
Molecular Melting
Formula NaOH 40.01 318.4℃
Weight point
The
Boiling Vapor 0.13kPa
Physical and 1390℃ relative 2.12
Point Pressure (739℃)
chemical density
properties Appearance
Colorless, oily liquid.
Odor
Soluble in water, ethanol, glycerol. Dissolution
Solubility
process releases large amounts of heat.
Hazard: alkali, reacts with the acid and emit a lot of heat, the case
Stability and of the moisture ,reacts with aluminum, zinc and tin and release
hazard hydrogen; reacts with water, emit a lot of heat, can maket
combustible material on fire, aqueous solution with corrosive .
Workplace air shortly contact allowable concentration（mg/m3）2

Drinking water quality limits PH 6.5-8.5
Environmenta
Surface water PH 6-9
l Standards
Fishery Water Quality Standards PH 5.5-8.5
Sewage maximum allowable emission concentration PH6-9
Page 272 of 278

Acute toxicity：
Rabbit oral minimum lethal dose（LDLO）：500mg/kg
Mice inhaled median lethal concentration（LC50）：40ppm·h
Toxicological With a strong stimulation and corrosive. Dust irritate the throat
Information and respiratory tract; direct contact with skin and eyes can cause
burns; swallowed can cause gastrointestinal burns, mucosal
erosion, bleeding and shock.
Aquatic Toxicity: MTL 125ppm·96h(Mosquito fish).
Engineering Closed operation, safety shower and eyewash

Controls equipment provided.
Respiratory Must wear positive pressure self-contained breathing
protection apparatus when possible exposure to dust.
Eye
Wear chemical safety glasses.
Security protection
measures Body
Wear rubber acid protective clothing.
Protection
Hand
Wear rubber acid gloves.
Protection
Workspace no smoking, eating and drinking. Bath
Other
after working .
Once contacted, flush with water, if eye contact, after
rinse with plenty of water, rinse with 2% boric acid
aid
solution; if swallowed immediately mouthwash, drink
measures
water and vinegar or 1% acetic acid, and sent to
hospital.
Rapid withdrawal from air leakage, restricting
Emergency entrance-exit; emergency personnel wear self-
measures contained breathing apparatus pressure. Wear anti-
acid; leakage process to avoid dust, try to collect,
Leakage
can also be rinsed with water, wastewater flows into
disposal
the treatment system; liquid alkali leak should build a
causeway or trenching collection, transfer to tankers
by pump, carrying the residue to recycling operation
safe disposal of waste disposal sites
Fire
Water, sand saves, prevent rain splash cause burns.
Methods
Page 273 of 278

Quick method: check trachea

The detection limit: 1-1000 mg / m3
Environmental monitoring
neutralizing; pH test paper
methods
GB methods:
Glass electrode method GB6920-86
Corrosive substances; steel drum in strict closures,

plastic bags, textile bags; liquid tankers. Dry storage
environmental requirements, to prevent moisture,
General Packaging
and isolated storage with acids, aluminum, tin, lead,
zinc, and their alloys, explosives, organic peroxides,
ammonium, and inflammable material
Uses Chemical raw materials.
Page 274 of 278

3) Sodium Bisulfite
Sodium English
Name Aliases Sodium bisulfite Sulfurousacid
bisulfite name
Molecular Melting
Formula NaHSO3 104.05 /℃
Weight point
The
Boiling Vapor /kPa
Physical /℃ relative 1.37
Point Pressure (℃)
and density
chemical Appearance Appearance is white to light yellow crystal or powder
properties Odor form, there is a strong pungent odor S02
Insoluble in ethanol, soluble in water, acidic aqueous
Solubility solution. Long place in air will oxidize into sodium
hydroxide sulfate, heat or acid will produce S02 gas.
There is a irritation for the skin, eyes, respiratory tract, which can
cause allergic reactions. Can cause damage to the cornea, leading to
Health
blindness. Can cause asthma; large number of oral cause nausea,
Hazards
abdominal pain, diarrhea, circulatory failure, central nervous system
depression.
1. Respiratory protection: the dust concentrations in the air exceeding
standard, must wear self-absorption filter respirators. Emergency
rescue or evacuation, air respirators should be worn.
2. Eye protection: Wear chemical safety glasses.
Protection 3. Physical protection: wear rubber acid suit.
4. Hand protection: Wear rubber acid gloves.
5. Other protection: Workplace no smoking, eating and drinking, wash
hands before eating. After work, take a shower. Maintain good health
habits.
1．ADI 0 ~ 0.7mg / kg (SO2 meter; including 502 and sulfites; FAO /
WHO, 2001).
Toxicity
2．LD50 115mg / kg (rat, oral).
3．GRAS (FDA, §182.3739,2000).
Closed operation, local exhaust ventilation. Prevent dust released into
the air workshop. The operator must go through specialized training,
strict adherence to rules. Proposed operators wear self-absorption filter
Handling
respirators, wearing chemical protective safety glasses, wear rubber
Precautions
acid suit, wear rubber acid gloves. Avoid generating dust. Avoid contact
with oxidizing agents, acids, alkalis. Equipped with spill response
equipment. There may be harmful residues in empty containers.
Emergency Isolation leak contaminated areas, restricting entrance-exit.
Page 275 of 278
Recommended emergency personnel wearing a dust mask, wear acid-

proof clothing. Do not direct contact with leakage. A small leak: to avoid
Treatment
dust, carefully sweep, collected in a dry, clean, covered containers.
Large Leak: recycling or collection shipped to the waste disposal sites.
1. Skin contact: Immediately remove contaminated
clothing, rinse with plenty of water. Medical treatment.
2. Eye contact: immediately lifted eyelid, thoroughly
washed with a large number of mobile water or saline at
least 15 minutes. Medical treatment.
aid measures 3. Inhalation: rapidly escape from the scene to fresh air.
Keep the airway open. If breathing is difficult, give
oxygen. If not breathing, give artificial respiration
immediately. Medical treatment.
4. Ingestion: drink plenty of water, induce vomiting.
Medical treatment.
Small openings aluminum barrel; ordinary wooden
outside ampoules; threaded glass Lid pressure bottles,
General Packaging
plastic bottles or metal (cans) outside the ordinary
wooden box.
When the ship packaging,it should be completed
and loading should be safe. During transport to ensure
that the container does not leak, did not fall, do not fall,
no damage. Do not mixed with oxidants, acids, alkalis,
Transportation food chemicals and do not mixed to transportation.
Precautions When Transport ,vehicles should be equipped with spill
response equipment. Transit should prevent exposure,
rain, high temperature. According to the provisions road
transport routes, do not stay in residential areas and the
entrance dense area .
Store in a cool, ventilated warehouse. Away from fire and
heat. Prevent direct sunlight. Packing seal. Should
separately store with oxidants, acids, bases and avoid
Storage Precautions
mixing reservoir. Should not store long to avoid bad.
Storage areas should be equipped with suitable material
to collect spill material.
Uses There is bleaching effect on food, strongly inhibited
effect on oxidase in plant foods . China provides for
candied fruit, glucose, sugar, sugar, caramel, candy,
liquid glucose, dried fruits, dried vegetables, noodles,
bamboo shoots, mushrooms and canned mushrooms,
Page 276 of 278

maximum use of 0.459 / kg; potato starch can also be

used, the maximum usage is 0.2g / kg, potato starch
residues (in S02 dollars) less than 0.03g / kg.
Used as a reducer agent, food preservatives and
bleaching agents. And organic and cotton fabric
bleaching. Used as a reducer agent in the dye, paper,
leather, chemical synthesis and other industries.
Used as intermediates of the dipyrone and
aminopyrine production for pharmaceutical industry.
Food grade product is used as a bleaching agent, a
preservative, an antioxidant. A reducer agent used in the
analysis, it is also used as a bleaching agent and a
bacteriostatic agent.
Page 277 of 278

ANNEXURE II
EQUIPMENT MAIN PARAMETER TABLE
Function: bulk chemicals are produced for use demineralized water.
V P T
Pharmacy tank Remarks
M 3
Bar ℃
0SDA501BA 20.0 Atm 40
0SDA502BA 20.0 Atm 40
0SDA601BA 20.0 Atm 40
0SDA602BA 20.0 Atm 40
Threshold Function
Sensors
VH H L VL
0SDA501MN 1.80 m 0.30 m
0SDA502MN 1.80 m 0.30 m
0SDA601MN 1.80 m 0.30 m
0SDA602MN 1.80 m 0.30 m
Page 278 of 278

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STANDARD OPERATING PROCEDURE FOR HIGH-SPEED MIX

THIS DOCUMENT IS THE PROPERTY OF PAEC. NO EXPLOITATION OR TRANSFER

KARACHI NUCLEAR POWER PLANT UNIT-2 (K-2)

STANDARD OPERATING PROCEDURE FOR HIGH-SPEED

Compiled by: Commissioning Division

Checked by Reviewed by (CZEC) QA Reviewed by

Zakir Noor Khan,

STANDARD OPERATING PROCEDURE FOR HIGH-SPEED

REVISION CONTROL SHEET

DecemberJUNEMarc M. Omer Iqbal, Zakir Noor

10. LOCAL OPERATOR SHEET.................................................................................34

1.1 REFERENCE DOCUMENTS

 Demineralized water productionCondensate water polishing system

 Demineralized water productionCondensate water polishing system

Demineralized water production (pre-treatment) running procedures A0 PRE

SDA、SED、SER System operating parameters and alarm settings (debugged

SDA、SED、SER Process control logic (debugged version) 2013.01.3

Fangjiashan demineralized water production control system manual (2013.02.05）

This procedure applies to:

 In MCR, all operations shall be performed by MCR operator.;

1.4 DEFINITIONS AND ABBREVIATIONS

CI: Conventional IslandThis is a sample table

Local pressure measurementLV AC Network 380V System

MD:TF Flow rate measurementScreening drum or screen

2. SPECIFICATIONS AND PRECAUTIONS

he bulk chemicals agent used to Fangjiashan Demineralized water production are:

ation resin regenerating agent is composed of hydrochloric acid. Concentration of of liquid

combustion, explosion, corrosion, poison, etc., Once contacted to the exposed

Cation resin regenerating agent is composed of sodium hydroxide. Concentration of liquid

PH regulating agent of SERWCD Demineralized water is composed of ammonia.

leak. And speed of forklift travel is not more than 10 km / h.

The operators have worn fully [ ][ ]

2.2 Electrical requirementElectrical

The following switchboard available

380V AC Power System [ ]

OPLow-voltage AC network 90EPYLKU DPYA

380V AC power supply system

Available220V AC Power System [ ][ ]

The following systems should

Grounding and Lightning Protection

2.3 Mechanical requirement

Demineralized water from SED

Compressed Air Production System

Mix bed recirculation pump 2TFC411CW9

At least one waste water

High-speed mix bed resin

Acid, alkali regeneration units are [ ] 2TFC441BA

Available # 1 Flushing Pump [] 1ATE411PO 1MP303

High acid storage tank

Condensate polishing demineralized

Available [] 1ATE441BA 1PB

Recycling water units are available []

Available [] 1ATE481BA 1MX101

Compressed air units are available []

Available [] 1ATE502CW 1MX301

At least two Roots fans are available []

High-speed mix beds associated

Available [] 1ATE201AR 1MX101

Available [] 1ATE203CR 1MX101

Alignment Check and

3.3 Instrument Control Power