CEE 306 - Lecture 02 - Aggregate Gradation

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AGGREGATE COMPOSITION

AND GRADATION

CEE 306
CIVIL ENGINEERING MATERIALS

CHANG-SEON SHON, PH.D., ASSOCIATE PROFESSOR


DEPARTMENT OF CIVIL & ENVIRONMENTAL ENGINEERING
NAZARBAYEV UNIVERSITY

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AGGREGATE COMPOSITION

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DEFINITIONS
• Aggregate - fragments of rocks, combination of
minerals
– Portland cement concrete (PCC): 75%
– Asphalt concrete (AC): 90%
– Granular Base, Subgrade
– Mortar, Plaster, Grout
– Railroad Ballast
– Foundation / Fill

• Rock - aggregation of minerals

• Mineral - naturally occurring, inorganic crystalline


substances 3
CEE 306: Civil Engineering Materials Lecture 02

EXAMPLE OF AGGREGATE USES

• Under foundations and pavements


– Stability
– Drainage
• As fillers
– Portland Cement Concrete
• 60-75% of volume
• 80-85% of weight
– Hot Mix Asphalt
• 80%-90% of volume
• 90-96% of weight

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SOURCES
• Natural • quarries = crushed
– igneous
– sedimentary • alluvial deposits = gravel &
– metamorphic sand

• Synthetic
– byproduct (blast furnace
slag)
– lightweight (expanded shale,
clay, slate)

• Recycled

Recycled
Concrete
Aggregate
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SOURCE:
MANUFACTURED AGGREGATE (CONT’D)

• FLY ASH & BOTTOM ASH AGGREGATES

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SOURCE:
MANUFACTURED AGGREGATE (CONT’D)

• SLAG AGGREGATE

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ROCK CYCLE

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ROCK TYPES

Igneous Sedimentary Metamorphic

solidification of weathering & transformation of


Origin molten magma erosion of rocks rocks

crystallization of accumulation/ mineralogical,


minerals from textural & structural
Process liquid with consolidation of change of rocks due
decreasing temp. weathering & to heat/pressure/
Intrusive/Extrusive erosion products recrystallization

granite, basalt, limestone, marble, slate,


Example andesite sandstone, gravel metaquartzite

WEAKER STRONGER
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PROPERTIES OF ROCKS

The Science and Technology of Civil Engineering Materials, Young, Mindess, Gray, Bentur, 1998,
Prentice Hall

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AGGREGATE TYPES

Aggregate = Combination of Minerals

• Sandstone (quartzite) – mainly quartz


• Limestone – mainly calcite
• Dolomitic Limestone – 10-30% dolomite + 90-70%
calcite
• Gravel – accumulation of different rock type
– SRG (siliceous river gravel): Quartz-rich rock
– CRG (calcareous river gravel): Calcite-rich rock
• Granite – quartz, feldspar, mica, hornblende,
pyroxene, etc.

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MINERAL TYPES

Group of rock-forming Example Formula/Elements


mineral
Silicate Quartz, Chert, Opal SiO2
Feldspars Orthoclase, Albite KAlSi3O8, NaAlSi3O8
Hornblende Ca/Na/Al/Fe/Mg/SiO2
Mica Al/K/SiO2*nH2O
Pyroxene (Fe,Mg)SiO3
Olivine (Fe,Mg)2SiO4
Carbonate Calcite CaCO3
Dolomite CaMg(CO3)2
Sulfate Gypsum CaSO4⸱2H2O

Opaque Magnetite Fe3O4


Hematite Fe2O3

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MINERAL IDENTIFICATION

• Hardness • Specific Gravity


– Mohs scale
• Crystal Structure
• HCI (hydrochloric acid) Reactivity – X-ray diffraction
– carbonate reactivity (XRD)

• Cleavage / Fracture • Other


– preferred plane surfaces / – color / striations
shape – light transmission
– between close-packed

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TUFF (TUFFACEOUS SANDSTONE)


XRD PATTERN

Image source: http://theloggingroadcyclist.com/?m=201312

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INDIRECT MINERAL COMPOSITION BY
COMPOSITE COTE
• Series Model
αc = α2V2+α1V1
Mineral CoTE
(10-6 / oC)
Calcite 05.58 • Parallel Model
Dolomite 09.62
 2 E2V2  1E1V1
Quartz 13.00 c 
E2V2  E1V1
Albite 06.52
Magnetite 06.86
Pyroxene 12.11 • Hirsch Model
ac  x  iVi  1  x   
  iVi Ei 
 
 V E i i 
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EFFECT OF PARENT ROCK ON PCC


/ AC PROPERTIES
Parent Rock PCC: Portland cement concrete
AC: Asphalt concrete

Prior Exposure &


Microstructure
Processing Factor

Mineralogical
Composition
Particle Characteristics Porosity / Density
Size
Shape
Crushing Stength
Texture
Abrasion Resistance
Elastic Modulus
Soundness

Properties of Plastic Properties of Hardened


Concrete Mix Concrete Concrete
Proportioning Consistency Ultimate strength
Cohesiveness Abrasion resistance
Unit Weight Dimensional stability
Durability
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AGGREGATE GRADATION

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AGGREGATE TYPES/CLASSIFICATION
• Source
– Natural
– Manufactured
– Recycled aggregate
barite
• Bulk density (DRUW)
– Normal-weight : 1522 – 1682 kg/m3 (95-105 lb/ft3)
– Lightweight: 160 – 1121 kg/m3 (10-70 lb/ft3)
– Heavyweight: > 2403 kg/m3 (> 150 lb/ft3 ) e.g. barite
• Size – coarse > #4 (4.75mm)
– Standard sieves – fine < #4 (4.75mm)
– Gradation – filler < #200 (0.075mm)
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AGGREGATE TYPES/CLASSIFICATION
(CONT’D)
• Shape
– Angularity – sharpness of edges & corners
• Rounded, sub-rounded, sub-angular, angular
– Sphericity – surface area to volume
• Equidimensional, flaky, flat & elongated
• Texture
– Very rough, rough,
smooth, polished

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AGGREGATE CLASSIFICATION BY WEIGHT


(CONCRETE MADE OF AGGREGATE)
• Normal weight aggregate (ASTM C 33)
– Most common aggregates such as sand, gravel, crushed stone
– Produce normal-weight concrete − 2200 to 2400 kg/m3 (140 to 150 lb/ft3)

• Light weight aggregate (ASTM C 330)


– Expanded shale, clay, slate, slag
– Produce structural lightweight concrete − 1350 to 1850 kg/m3 (90 to 120
lb/ft3)
– Pumice, scoria, perlite, vermiculite, diatomite
– Produce lightweight insulating concrete − 250 to 1450 kg/m3 (15 to 90
lb/ft3)

• Heavyweight aggregate (ASTM C 637, C 638)


– Barite, limonite, magnetite, hematite, iron, steel punchings, or shot
– Produce high-density concrete up to 6400 kg/m3 (400 lb/ft3)
– Radiation Shielding
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AGGREGATE CLASSIFICATION BY
SIZE/SIZE DISTRIBUTION

• Boulder are typically defined as aggregate than 75 mm (3


in.)
• Coarse aggregate (C.A.)
– Aggregate larger than 4.75mm (#4 sieve, 0.2in.)
– typically between 9.5 and 37.5 mm (3/8 and 1½ in.)

• Fine aggregate (F.A.)


– Aggregate smaller than 4.75mm & larger than 75 µm (#200 sieve)
– F.A. content usually 35% to 45% by mass or volume of total
aggregate

• Size, shape, & surface texture of aggregate can affect


the performance of concrete / asphalt concrete
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MAXIMUM AGGREGATE SIZE &


WATER REQUIREMENT (ABSORPTION CAPACITY)

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MAXIMUM AGGREGATE SIZE &
CEMENT REQUIREMENT

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RECYCLED-CONCRETE AGGREGATE:
WATER ABSORPTION

Virgin
aggregate

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PROPERTIES OF AGGREGATES

•Physical
•Size / Gradation •Mechanical
•Shape •Modulus of elasticity
•Texture •Compressive strength
•Specific Gravity
•Absorption •Durability
•Moisture •Physical
•Porosity •Chemical
•Void Content
•Dry Unit Weight

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CEE 306: Civil Engineering Materials

SAMPLING AGGREGATES
• Random and representative of
entire stockpile
– Sample from entire width of conveyor
belts at several locations
– Sample from top, middle, and bottom
of stockpile at several locations around
stockpile diameter
– Use larger sample for testing larger
max. size Sample Splitter

• Sample splitting or quartering


– Reduce sample size from large
stockpile to small 1-5 kg sample
Quartering
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SAMPLING AGGREGATES (CONT’D)
• ASTM C702/702M-11 Small Sample Splitters
for Fine Aggregate

Quartering on a Hard, Clean Level Surface

Large Sample Splitter for


Coarse Aggregate
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CEE 306: Civil Engineering Materials

AGGREGATE SIZE/GRADATION

• Particle size distribution determined by sieve


analysis (ASTM C136, C117, D546)
– % passing by wt
• Plots
– Standard chart
– 0.45 power chart
• Specifications
– Specific to application
– Usually require blending
– Government, voluntary, private

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SIEVE ANALYSIS

Individual Sieve Stack of Sieves

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AGGREGATE SIZE DEFINITION

• TRADITIONAL 100%
– MAXIMUM SIZE AGGREGATE (MSA)
• THE SMALLEST SIZE OF SIEVE OPENING THROUGH WHICH THE ENTIRE AMOUNT OF
AGGREGATE COMPLETELY PASSES
5 ~ 15%
– NOMINAL MAXIMUM SIZE AGGREGATE (NMSA)
• THE SMALLEST SIZE OF SIEVE OPENING THROUGH WHICH MAJORITY OF
AGGREGATE PASSES
• IT IS ALSO ONE SIEVE SMALLER TO MAXIMUM SIZE OF AGGREGATE

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Aggregate Size Definition (Cont’d)

100 • SUPERPAVE 100


100 99
91 • Nominal Maximum Aggregate Size 89
73 – one size larger than the first sieve to 72
65 retain equal & more than ≥ 10% 65
48 • Maximum Aggregate Size 48
36 – one size larger than nominal 36
22 maximum size 22
15 15
9 9
4 4
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AGGREGATE SIZE DEFINITION (CONT’D)

traditional Superpave (AC)

max agg size smallest w/ one larger than


100%Passing nom max

nominal max largest w/ one larger than


agg size some %Retained first w/ > 10%R
(≤10%)

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Aggregate Size Definitions (Cont’d):
EXAMPLE
Values indicate
Gradation % passing

Sieve Size No. 1 No. 2 No. 3


19.0 100 100 100
12.5 95 90 85
9.5 85 75 75
4.75 75 72 65
2.36 60 60 60
1.18 50 50 55
0.60 30 30 40
0.30 20 20 30
0.15 10 10 10
0.075 5 5 5
Max Agg Nominal Max >10% Retained
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CEE 306: Civil Engineering Materials

SIEVE ANALYSIS

• A SIEVE ANALYSIS TEST WAS PERFORMED ON A SAMPLE


OF FINE AGGREGATE AND PRODUCED THE FOLLOWING
RESULTS:

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SIEVE ANALYSIS (CONT’D)

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SIEVE ANALYSIS (CONT’D)

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ASTM GRADATION SPECIFICATIONS

• PORTLAND CEMENT CONCRETE REQUIRES SEPARATE


SPECIFICATIONS FOR COARSE AND FINE AGGREGATES

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ASTM GRADATION SPECIFICATIONS


(CONT’D)

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STANDARD GRADATION CHART:
GRADATION LIMITS

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STANDARD GRADATION CHART

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Fineness Modulus (FM)

• SPECIFIC SIEVES – ONLY FULL SIEVES


– NO. 100, NO. 50, NO. 30, NO. 16, NO. 8, NO. 4, 3/8” (9.5MM),
3/4” (19MM), 1.5” (37.5MM), 3” (76.2MM), AND 6” (152.4MM)
– FOR FINE AGGREGATE, DOES NOT INCLUDE SIEVES LARGER THAN
9.5MM, NO.200 SIEVE, AND PAN
• ADD CUMULATIVE % RETAINED VALUES FOR SPECIFIC SIEVES &
DIVIDE BY 100
• INDICATION OF AVERAGE PARTICLE SIZE
• FM INCREASES FOR COARSER GRADATIONS (THE HIGHER THE
FM, THE COARSER THE AGGREGATE)

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FINENESS MODULUS (FM)


FM Calculation Example (Total materials: 523g)
Sieve # Wt sieve Wt sieve+Mtls Wt Ret % Ret % Cum Ret FM

3/8” 0 0 0
No. 4 10 2 2
No. 8 68 13 15
No. 16 131 25 40
No. 30 78 15 55
No. 50 115 22 77
No. 100 105 20 97
Pan 16 3 100
Total 523 100 286 2.86

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AGGREGATE GRADATION:
0.45 POWER GRADING CHART

• USE 0.45 POWER GRADATION CHART


• BLEND SIZE DEFINITIONS
– Maximum size
– Nominal maximum size
• GRADATION LIMITS
– Control points
– Restricted zone

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0.45 Power Grading Chart


(Cont’d)

.
=

Max size P = % finer than the


sieve
d = aggregate size
being considered
D = maximum
maximum density line aggregate size to
be used

Federal Highway
Administration (FHWA),
1988
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TYPES OF GRADATION
* Uniformly graded (one-size gradation)
- Few points of contact
- Poor interlock (shape dependent)
- High permeability

* Dense / Well graded


- Good interlock
- Low permeability

* Gap graded (horizontal section of curve)


- Only limited sizes
- Good interlock
- Low permeability
* Open graded (missing small aggr.)
- Good interlock
- High permeability
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TYPES OF GRADATION ON 0.45


POWER GRAPH

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GRADATION CHART

TOTAL PERCENT PASSING

SIEVE NO.
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SUPERPAVE
(AC)
GRADATION
SPECIFICATION

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REDUCTION OF VOIDS

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EFFECT OF FINES ON THE RELATIVE


PROPERTIES OF AGGREGATE BASED
MATERIALS
Characteristics No Fines Well-Graded Large Amount of Fines
(Open or (Dense) (Dirty or Rich)
Clean)
Stability Medium Excellent Poor

Density Low High Low

Permeability Permeable Low Impervious

Frost No Maybe Yes


Susceptibility
Handling Difficult Medium Easy

Cohesion Poor Medium Large

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EXAMPLE USING OPEN GRADED AGGREGATE

Porous asphalt concrete Pervious concrete

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Blending Stockpiles (Aggregate)

• REASONS FOR BLENDING


– OBTAIN DESIRABLE GRADATION
– SINGLE NATURAL OR QUARRIED MATERIAL NOT ENOUGH
– ECONOMICAL TO COMBINE NATURAL AND PROCESS MATERIALS
• METHODS OF BLENDING OF AGGREGATES
– BASIC FORMULA
– TRIAL AND ERROR

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Blending Stockpiles (Cont’d)

• BASIC FORMULA FOR COMBINING STOCKPILES TO ACHIEVE


A TARGET GRADATION IS:

P = Aa + Bb + Cc + ….
where:
P = % material passing given sieve size for blended aggr. A, B, C,....
A, B, C, .. = % passing given sieve for each aggr. A, B, C,....
a, b, c, … = proportions (decimal fraction) of aggr. A, B, C, … to be used
in blend

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Blending Stockpiles (Cont’d)

• PLOT INDIVIDUAL GRADATIONS


• PLOT SPECIFICATION LIMITS
• CAN BE USED FOR INITIAL ASSESSMENT
– CAN BLEND BE MADE FROM AVAILABLE MATERIALS?
– IDENTIFICATION OF CRITICAL SIEVES
– ESTIMATING TRIAL PROPORTIONS

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BLENDING STOCKPILES (Cont’d)
All possible combinations fall between A and B
Percent Passing, %
100
90 Gradation B
80 Control points for
70
12. 5 nominal max. size
60
50
40 Gradation A
30
20
10
0
0.075 0.3 1 .18 4.75 9.5 12.5 19
Sieve Size, mm
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BLENDING STOCKPILES (Cont’d)


No possible combination of A and B will meet spec
Percent Passing, %
100 Gradation B
Gradation A
90
80
70
60
50
Control points for
40
12. 5 nominal max. size
30
20
10
0
0.075 0.3 1 .18 4.75 9.5 12.5 19
Sieve Size, mm
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BLENDING STOCKPILES (Cont’d)
All poss. combinations pass through cross-over point
Blends containing more A than B will be closer to A
Percent Passing, %
100 Gradation A
90
80
70
Gradation B
60
50
40
30
20 Control points for 12. 5
10 nominal max. size
0
Sieve Size, mm
0.075 0.3 1 .18 4.75 9.5 12.5 19
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Trial and Error Steps

• SELECT CRITICAL SIEVES IN BLEND


• DETERMINE INITIAL PROPORTIONS WHICH WILL MEET
CRITICAL SIEVES
• CHECK CALC. BLEND AGAINST SPECIFICATION
• ADJUST IF NECESSARY AND REPEAT ABOVE STEPS

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Blending of Aggregate:
Example
Material Agg. #1 Agg. #2
% Used Blend Target
U.S. % % % %
Sieve Passing Batch Passing Batch
3/8” 100 100 100
No.4 90 100 80 – 100
No.8 30 100 65 – 100
No.16 7 88 40 – 80
No.30 3 47 20 – 65
No.50 1 32 7 – 40
No.100 0 24 3 – 20
No.200 0 10 2 - 10

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Blending of Aggregate:
Example (Cont’d)
Material Agg. #1 Agg. #2 First Try

% Used 50% 50% (remember trial & error)


Blend Target
U.S. % % % %
Sieve Passing Batch Passing Batch
3/8” 100 50 100 50 100 100
100 * 0.5 = 50
No.4 90 45 100 50 95 80 – 100
90 * 0.5 = 45
No.8 30 15 100 * 0.5 = 50
30 15 65 65 – 100
No.16 7 3.5 788 * 0.5 = 44
3.5 47.5 40 – 80
3 * 0.5 = 1.5
No.30 3 1.5 47 23.5 25 20 – 65
1 * 0.5 = 0.5
No.50 1 0.5 32 16 16.5 7 – 40
0 * 0.5 = 50
No.100 0 0 024 * 0.5 =12
0 12 3 – 20
No.200 0 0 10 5 5 2 - 10

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Blending of Aggregate:
Example (Cont’d)
Material Agg. #1 Agg. #2
% Used 50% 50% Blend Target
U.S. % % % %
Sieve Passing Batch Passing Batch
3/8” 100 50 100 50 100 100
No.4 90 45 100 50 95 80 – 100
No.8 30 15 100 50 65 65 – 100
No.16 7 3.5 88 44 47.5 40 – 80
No.30 3 1.5 47 23.5 25 20 – 65
No.50 1 0.5 32 16 16.5 7 – 40
No.100 0 0 24 12 12 3 – 20
No.200 0 0 10 5 5 2 - 10

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Blending of Aggregate:
Example (Cont’d)
Material Agg. #1 Agg. #2
% Used 50% 50% Blend Target
U.S. % % % %
Sieve Passing Batch Passing Batch
3/8” 100 50 100 50 100 100
No.4 90 45 100
100 Let’s Try50 50 95 80 – 100
No.8 30 15 100
100and get 50 50 65 65 – 100
No.16 7 3.5
100 50 44
a88little closer 47.5 40 – 80
88 44
No.30 3 1.5 to47the middle23.5
of 25 20 – 65
47 23.5
No.50 1 0.5 the32
target values.
16 16.5 7 – 40
No.100 0 0 24 12 12 3 – 20
No.200 0 0 10 5 5 2 - 10

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Blending of Aggregate:
Example (Cont’d)
Material Agg. #1 Agg. #2
% Used 30% 70% Blend Target
U.S. % % % %
Sieve Passing Batch Passing Batch
3/8” 100 30 100 70 100 100
No.4 90 27 100 70 97 80 – 100
No.8 30 9 100 70 79 65 – 100
No.16 7 2.1 88 61.6 63.7 40 – 80
No.30 3 0.9 47 32.9 33.8 20 – 65
No.50 1 0.3 32 22.4 22.7 7 – 40
No.100 0 0 24 16.8 16.8 3 – 20
No.200 0 0 10 7 7 2 - 10

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Blended Aggregate Specific Gravities

• ONCE THE PERCENTAGES OF THE STOCKPILES HAVE BEEN


ESTABLISHED, THE COMBINED AGGREGATE SPECIFIC
GRAVITIES CAN ALSO BE CALCULATED
• COMBINED SPECIFIC GRAVITIES

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SUMMARY

• Aggregate composition
– Definition, sources, types, properties
• Aggregate gradation
– Shape and texture
– Types of gradation: Uniform, dense, gap, and open
gradations
– Sieve analysis
– 0.45 power chart, maximum aggregate size, nominal
maximum aggregate size
– Blending stockpiles
– Fineness modulus
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