Download as pdf or txt
Download as pdf or txt
You are on page 1of 24

【j夏 PH05288型立pH计使用说明书 上濂圃和白动化仪表设备有限公司

Table of contents
Chapter One Summary. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . l
1.1 Overview ........................................................................................l

1.2 Main features .................................................................................l

1. 3 Main data indication . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ..... . 2

1.4 Working principle. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3


1.5 Instrument composition. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
Chapter Two : Installation. .. . . . .. . .. . . . .. . .. . . . .. . . . . . . . . . . . . . . . . . . . ............ ......................6

2.1 I n s t r u m e n t i n s t a l l a t i o n . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. . . . . .. 6
2.2 pH transmitter installation. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ............ 6
2. 3 U l t r a s o n i c g e n e r a t o r c h a s s i s i n s t a l l a t i o n . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. 9
2.4 pH meter wiring . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ..... 9

Chapter Three :Adjustment. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ......................... 11


3.1 Button description........................................................................... 11
3.2 Password description ....... ·.... ·....·.... ·..........·.... ·........ ··.......... ·.... ·.. · · ·..12
3.3 Adjust. . . . . . . . . . . . . . . . . . ·•••••••••••••••••••••••••• •••••••••••••••• •••••••••••••••• ••••••••••••••• 12
Chapter Four :Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ..... 15

4.1 Secondary table maintenance. . . . . . . . . . . . ........................ ......................•••15


4.2 Electrode maintenance. . . . . . . . . . . ••••••••••••••• •••••••••••••••• ••••••••• ••••••••••••••••••17
Chapter Five : Error 18
Appendix I: Standard buffer solution . . 20
Appendix II: Pt100 Index value.. ·.............. ······.................................. · ...........· · .21
Appendix III: Factory parameter . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .......... 22
Packing list. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ..... 23
【j夏 PH05288型立pH计使用说明书 上濂圃和白动化仪表设备有限公司

Chapter One Summary


1.1 Overview
PHG-5288 industrial pH meter is a new generation of intelligent online analyzer dedicated to users by our
company.With my husband

The company's PHG-280 and PHG-281 series circulating transmitters, or matched with the PHG-271
series sinking transmitters,

Widely used in thousands of power stations, pure water, chemical industry, medicine, food, environmental
protection, light industry and other industries, the pH value of aqueous solutions is connected online

Continuous monitoring. The electrode can be selected from conventional type, pure water type, acidic,
alkaline, high temperature type (20-13o•c) and anti-fouling type especially suitable for petrochemical, light
industry, environmental protection and other departments. PHG27 1 series transmitter can also be
equipped with optional ultrasonic accessories, So as not to reduce the sensitivity of the electrode signal
caused by the pollution of the electrode by the medium under test.

The display instrument is divided into two specifications: the PHG-5288 type is an on-site installation
instrument for the secondary meter, and a high-resistance converter with a thousand receiving electrode
signals is directly installed in the secondary meter. The distance between the sensor and the secondary
meter is generally not more than 20 meters. The PHG-5288A type is a long-distance quotient transmission
instrument between the secondary meter and the sensor. The high-resistance converter is placed in a
sealed small box, installed on the spot, and connected to the secondary meter through a feeder. The
transmission distance quotient is generally not more than 200m.

1.2 Main features


. The electrode system with excellent quality, compact structure, and easy installation and


maintenance has a variety of models: conventional type, pure water type, acidic, alkaline, high
temperature (20—l30°C), anti-pollution type.


Large-screen dot matrix high-resolution background light LCD display.


At the same time display the pH value, temperature, status, fault prompt and time of the liquid
under test. .


Full Chinese character text-based human-computer dialogue, operation steps, functions,
status, and fault prompts are all Chinese characters.


Built-in electronic encryption key to avoid misoperation by Yuan Guan personnel. .


Built-in programs for a variety of special measurement objects that can be selected: normal
water quality, pure water, ammonia-containing water, and other special water quality.

Automatic correction program.

• Two-point correction: Select any two of the three standard buffer solutions of pH4, 7, and


9 to achieve the slope (S) and zero potential pH value (PH) of the pH electrode.)Automatic
correction.

ne-point correction: Select any of the three standard buffer solutions of pH4, 7, and 9 to


achieve a zero potential pH value (pH.) Automatic correction, the slope of the electrode is
the slope in the ori inal memory (S).


Automatically display the micro-parameters of each electrode: S, PH.value.

Output si nal: provide a current si nal output from a - mA or 4- mA optional isolation


soc et that can be arbitrarily e tended at the same time, provide an S4 4 computer
communication interface to realize a lon -distance connection with the computer, and the
transmission distance can reach m.
1
【j夏 PH05288型工如H计使用视 明书 上濂冒和白动化仪表设备有限公司

• The instrument has static calibration and dynamic measurement error correction.

• Industrial-controlled watchdog to ensure the normal operation of the instrument.


• Upper and lower limit alarm signal display and relay contact output.
• Error signal display and Chinese character prompts for misoperation.
• The instrument has a built-in electrode cleaning program and cleaning control signal output, and
provides ultrasonic cleaning accessories.
• Provide historical child measurement data query, store one child measurement value every hour, 24
per day, and can query data for more than one month.
• With power-off protection function: in case of power failure or shutdown, the data set internally is still valid.

1.3 Main data indication


• Working conditions

• Ambient temperature: 0 - 40℃

• Relative humidity: ≤ 90%

• Power supply: 220±22 VAC 50±1 Hz

• The temperature of the liquid under test: Conventional 0-60°C, High temperature 20-130°C

• Measured liquid pressure: ≤ 0.5Mpa

• Measurement range:

• pH: 0-14 pH

• temperature: 0-100°C
• Matching accuracy:

• pH: ±0.1 pH

• temperature: ±1°C

• Repeatability:

• pH: 0.05 pH

• temperature: 0.5°C

• Stability: ±0.05 pH/24h

• Output signal:

• Isolation current: 0-1OmA or 4-20mA, maximum load 1K or 500Ω; accuracy: Soil ±1%.

• RS-422/485 computer communication interface signal.

• Automatic temperature compensation range: Conventional 0-60°C, High temperature 20-99.9°C

• Alarm accuracy: ±0.02 pH ±1 word

• Alarm relay contact capacitance: 28V DC 5A; 250V AC 3A

• Cable connection distance from sensor to display:

• Type 5288:20m

• Type 5288A: 200m

• Power consumption: 20VA

• Dimensions:

• Display instrument: 160×160×212mm.

• Circulating pH generator: type 280 ɸ32×235mm

type 281 ɸ44×235mm


【j夏 PH05288型立pH计使用说明书 上濂圃和白动化仪表设备有限公司

• Circulating pH generator:
• Power consumption:
• Circulating pH generator:

• Power consumption:
• The temperature of the liquid under test:

• Measured liquid pressure:

1.4 Working principle


pH measurement is based on the principle of electrochemical analysis. Choose an
electrode sensitive to the concentration of hydrogen ions as the measuring electrode, usually a
glass electrode, and an electrode with a constant pH measurement potential in the solution as
the reference electrode, usually a Gan Cai or silver—silver chloride electrode.

E=E。 十 2.303 · RT/F · t::,.pH


Formula: E_____________ Electrode potential

Eo____________ Standard electrode potential

For a certain number of determined electrodes, E0 is a constant.



R_____________ Molar gas constant (8.315J· K一1· mol 1)
T_____________ Absolute temperature (Kt=273.16+t°C)

F_____________ Faraday constant (9.649X10 4c · mol 1)

It is known from Nengst's formula: we only need to measure the electromotive force of
the electrode to obtain the pH value of the solution accordingly. Corresponding to the pH value
of a certain solution, the electrode potential is related to the temperature of the solution, so the
pH meter should have an automatic temperature compensation function.For a certain
determination electrode, the conversion relationship between its pH value and E is actually
impossible to fully conform to the theoretical value of Nengst's formula. There is a conversion
efficiency problem (for example, at 25°C, D.mV / D.pH=59.16mV /pH, but in fact it cannot reach
the theoretical value).We call it the slope (S) (for example, at 25°C, D.mV /D.pH=56.20mV /pH,
we call S=95%). The corresponding zero potential pH value (pH.) There are also differences. In
order for the pH meter to adapt to different electrodes to complete its weight measurement
function, the corresponding electrodes S and PH must be obtained.Value, the pH meter can
complete this task with the help of the thousand two-point calibration function. The internal
resistance of the glass electrode is extremely high, and it is generally on the order of lOOMQ at
25°C. For this reason, the pH meter has the circuit technology of high impedance conversion
and small signal processing.The instrument processes the measured signal and performs
various functions through the CPU, and finally completes the display, current output, alarm
output, and operating status display.

1.5 Instrument composition


The type 5288 instrument consists of two parts: a 1IVV
60
pH meter (secondary meter) and a pH transmitter. It is
basically installed in place with a thousand secondary
meters, and the distance between the transmitter and
the secondary meter is not more than 20 meters.
[1::1:J PHG5288工妒 H计
The 5288A instrument consists of three parts: a
PH meter (secondary meter), a high resistance
converter (PH-260), and a PH transmitter.The distance
between the high-resistance converter and the PH
transmitter is <20 meters, and the distance between
3
09(

the high-resistance converter and the secondary meter

匾]匠]巨国]
is <200 meters.

The front panel of the PH meter consists of a


large-screen dot matrix high-resolution background
light LCD display, the size of the display is 62X42, and 拉貊和自动化仪表设备有很公司
four touch buttons (Figure 1.1).

图I.I前而板
3
【j夏 PH05288型工如H计使用视 明书 上濂冒和白动化仪表设备有限公司

Figure I.I front and board

pH transmitter thousand figure 1.2

Schematic diagram of high resistance converter


(PH-260) 1.3

4
【j夏 PH05288型立pH计使用说明书 上濂圃和白动化仪表设备有限公司

Chapter Two Installation


2.1 Instrument installation
The type 5288 instrument consists of
two parts: a pH meter (secondary meter)
and a pH transmitter. It is basically installed
in place with a thousand secondary
meters, and the distance between the
transmitter and the secondary meter is not
more than 20 meters.

The 5288A instrument consists of


three parts: a PH meter (secondary
meter), a high resistance converter
(PH-260), and a PH transmitter.The
distance between the high-resistance
converter and the PH transmitter is <20
meters, and the distance between the
high-resistance converter and the
secondary meter is <200 meters.

The front panel of the PH meter


consists of a large-screen dot matrix
high-resolution background light LCD
display, the size of the display is 62X42,
and four touch buttons (Figure 1.1).

2.2 pH transmitter installation


Figure 2.2 A schematic diagram of the flow-type installation on the instrument panel
rack.

Figure 2.3 It is a schematic diagram of a flow-type installation on a vertical or


horizontal pipe.

Figure 2.4 A schematic diagram of the connection of the inlet and outlet water pipes
of the transmitter.

Figure 2.5 A schematic diagram of the installation of the submerged transmitter.

The installation of the submersible transmitter can be installed on the vertical or


horizontal pipe on the edge of the pool using accessories such as the mounting frame
and U-shaped screws provided by the company. See Figure 2.2 and Figure 2.3 for the
installation method.

Figure 2.6 A schematic diagram of the flow-type installation on the sampling rack.
5
【j夏 PH05288型工如H计使用视 明书 上濂冒和白动化仪表设备有限公司

6
【j夏 PH05288型立pH计使用说明书 上濂圃和白动化仪表设备有限公司

7
【j夏 PH05288型工如H计使用视 明书 上濂曙和白动化仪表设备有限公司

2.3 Ultrasonic generator chassis installation


The ultrasonic generator chassis should be installed nearby with the sensor, and the
factory standard is not more than 10m. The installation of the ultrasonic generator box
can be disc-mounted (Figure 2.7) or wall-mounted (Figure 2.8).

2.4 pH meter wiring


Open the back cover of the instrument, the
instrument terminal is right in front of your eyes
(Figure 2.9), and the external cables are
introduced from the three wiring holes at the
bottom of the chassis. Generally, the power
supply cord and the input signal are connected.
Signal line (terminals 1-7), the output signal
line should be introduced from the respective
eyelets.
Terminal 1 -7 is the signal input terminal of
the pH electrode and the lead-out line of the
pH electrode are respectively numbered and
seated. Columns 8 and 9 are the output ports
of the RS-422/485 interface, and columns 10
and 11 are the input ports of the 485 interface
connected to the computer, and the length of
the feeder can reach 2km.Columns 12, 13, and
14 are the power supply, of which 12 are the
ground wires, which should be connected to
the earth. The advantages and disadvantages
of the ground wires are related to the shielding
and anti-interference of the
instrument.Columns 15 and 16 are normally
open contact outputs of relays controlled by a
thousand automatic cleaning times. Generally,
they should be connected to the power supply
of the controlled object (such as an ultrasonic
cleaner) through an AC contactor.

Columns 17-19 are the lower limit alarm relay contact output, of which 17 is the open
normal terminal, 18 is the common terminal, and 19 is the normally closed terminal.
Column 20-22 is the upper limit alarm relay contact output: where 20 is the open normal
terminal, 21 is the common terminal, and 22 is the normally closed terminal. Columns
23-24 are the current output signals, of which 23 and 24 are the “negative” and “positive"
terminals of the 4-20mA (or 0–10mA) current output, respectively.

The electrode wiring of ASI company is wired according to “B". After the electrode leads
of ASI company are lengthened, they are wired according to “A", and the other electrodes
are wired according to "A".
8
【j夏 PH05288型立pH计使用说明书 上濂圃和白动化仪表设备有限公司

The wiring of the submerged transmitter junction box shall be wired in accordance with
the color indicated in the junction box (see the figure below).

Type 5288A is used for long-distance transmission of the display instrument with a PH
sensor, a PH sensor, a high-resistance converter, and the connection between the display
instrument is consistent with the color mark on the instrument.

Note:

- After the wiring is completed, the correctness of the wiring should be carefully checked
again; the unused terminal should be left empty.

- Make the support screws of each terminal should be tightened. The wiring should be firm
and there should be no loosening.

- Order column 12 to connect to the ground, do not connect to the middle line of the power
supply.
9
【j夏 PH05288型工如H计使用视明书 上濂曜和白动化仪表设备有限公司

Chapter Three Adjustment


After the instrument is installed and wired, you can enter the operation of this chapter.The
instrument adopts the method of power-on reset, and the power supply is turned on and the
instrument is automatically reset.

After the interval of about 10 seconds, the instrument enters the measurement state, and
the screen displays.

However, because the instrument is operating according to the factory parameters, it does
not represent the actual data. The instrument must enter the correct parameters before it can
be put into operation.

3.1 Button description


"Confirm" key: It is equivalent to the "enter key" in the computer. Pressing this key in the list
function means that the list is selected; pressing this key in the data function means confirming
the parameter and entering the memory.

"Long" key: Press this key in the menu function to move the item down; press this key in the
data function to modify the flashing digits.

">” key: Press this key in the menu function to move the item to the right; press this key in
the data function to move the flashing digits to the right.

"Measurement" key: Equivalent to the "exit key" in the computer.Pressing this key in the Lai
Shan function means exiting the Lai Shan; pressing this key in the data function means
abandoning the parameter and not entering memory.

3.2 Password description


Press the ”Confirm" button in the measurement status of the instrument, and the following
screen will appear on the display:

Use “long” and “>> to enter the password

5288: Is the characteristic password of this instrument. After the password is displayed,
press the “Set” button to enter the parameter setting state.

10
【j夏 PH05288型立pH计使用说明书 上濂圃和白动化仪表设备有限公司

3.3 Adjustment
Note:

- The order is only made when the parameters are adjusted and set before the instrument is
put into operation for the first time.;

- The order is only made when the user needs to modify the parameters set last time;

- So that in case of power failure or shutdown, the data originally set internally is still valid;
however, you can check the parameters originally set (see Section 3.4) to ensure that the data
is correct.

Adjustment steps:

After the instrument is turned on, it enters the measurement state

Press the "Confirm" button to enter

Wrong

Return to the measured state

II
【j夏 PH05288型立pH计使用说明书 上濂圃和白动化仪表设备有限公司

1 常规水
Water sample Water sample There are four kinds of water samples
Regular
to choose from: conventional water,

xx:xx
selection water selection
pure water, ammonia-containing water,
Clock setting Clock setting and other water.The function of
Confirm ammonia-containing water is mainly
Electrode parameter Electrode parameter designed to measure the pH value in
setting
一一伶
setting the furnace water, water supply water,
and condensate of power plants. It is
Output Output collectively referred to as nitrogen-
selection 4-20n1A selection 4-20n1A containing water.

L 穴
Water sample Regular Water sample conventional

1
selection water

xx:xx
selection water
Clock setting pH zero
Confirm x.xxx
---+
Electrode parameter Type the clock
Electrode parameter
setting
setting
Output
Output
4-20n1A selection
4-20n1A
selection

L
-
_

Water sample conventional
slope x.xxx
xx:xx
selection water

Clock setting Confirm IpH zero xx:xx You can enter this function to check the

---+ 1
slope and pH of the electrode when
Electrode parameter checking the zero position, but do not
setting piso x.xxx modify it at will.
Output
selection 4-20mA

L 久
Water sample Regular Water sample Regular
selection selection water

xx:xx
water

Clock setting Clock setting


xx:xx
-+
Confirm
Electrode parameter There are two ways to choose from:
Electrode parameter
setting 4-20 mA and 0-10 mA
setting
Output Output
selection 4-20mA selection 4-20mA

L 久
Two-point Please put the
calibration electrode in
One point In the first
Follow the prompts

-+
calibration Confirm buffer solution

I
Static calibration,

x.xxx
dynamic measurement
Press the set button to
Correct start the calibration

i 久
Two-point Please put the
calibration electrode in
One point In the first

-+
calibration buffer solution Follow the prompts
Confirm

I
Static calibration,
dynamic measurement

Correct x.xxx Press the set button to


start the calibration

i i 久

1 1

Two-point Two-point
calibration calibration
One point One point When used to correct the flow state
calibration calibration measurement, it is inconsistent with
Confirm laboratory sampling and analysis due to
Static calibration, Static calibration,
changes in the liquid connection potential
dynamic measurement

x.xxx
dynamic measurement --+

x. xxx
of the reference electrode.

1 「
Correct Correct

12
【j夏 PH05288型工如H计使用视 明书 上濂曙和白动化仪表设备有限公司

L 久
x.xxx
Lower output Lower output
limit limit
Output upper x.xxx
x.xxx
Output upper Set the lower and upper pH limits
limit limit corresponding to 4-20 mA or 0-10
x.xxx
Confirm
Alarm lower
x.xxx
Alarm lower mA.This function is to increase the
limit 一伶

limit current output sensitivity.
Alarm
x.xxx x.xxx
Alarm upper
upper limit limit

L 久
x.xxx 1 x.xxx
Lower output Lower output
limit limit

x.xxx x.xxx
Output upper Output upper
limit limit Set the upper and lower limits of the
Confirm
Alarm lower
x.xxx x.xxx
Alarm lower pH value alarm.
limit 一伶

limit
Alarm upper
x.xxx x.xxx
Alarm upper
limit limit

J. 公
Access to
XXmonth XXyear

information |
Cleaning the
xx.xx Use the " " button to check the
historical data forward.

XXmonth XXyear
electrode
Confirm
Date setting
一伶

xx.xx
J. 公
XXhours
_
Access to Cleaning

XX
information cycle For equipment that needs to be set up
Cleaning the Cleaning minutes to clean the electrode with ultrasonic

XXminutes
electrode time waves.When the cleaning time is 0, it
Confirm
Date setting Hold time means that it is not cleaned.
一伶


Year

xx I
Access to 坐
information

Cleaning the Month


Confirm
electrode Set date
xx
f

Date setting Day

13
【j夏 PH05288型立pH计使用说明书 上濂盲和白动化仪表设备有限公司

Chapter Four Maintenance


4.1 Secondary table maintenance
Daily maintenance

• Pay attention to dust and moisture-proof, the front panel and back cover of the instrument
should be covered, and the threading holes should be sealed.

• Avoid direct sunlight.

• The ambient temperature should be 0-40°C, and the instrument should not be used in an
environment that is too cold or overheated.

• Try to avoid interference sources and strong electromagnetic field environments.

• The grounding of the instrument should be good.

• When the measurement of the instrument is inaccurate, the secondary meter and


electrode should be inspected, and the inspection method shall refer to the regular
inspection of the instrument.

Regular verification

The measurement of the instrument is not timely during use, or the instrument is working


normally for a period of time (the pH meter is generally 6 months, and the electrode is
generally 2-3 weeks), the instrument can be inspected as described in this section.

pH meter measurement accuracy test


According to Figure 4.1 wiring diagram 4.1, use the "Confirm" button and "^" to build the
instrument display menu to the "Output lower limit" column.,
Set "2.00pH"; to the "Output upper limit" column, select "12.00 pH"; to the "Water sample
selection" column, select "Regular water", to the "Electrode parameter setting" column, set
"Slope=1.000" and "pH0=7.00"; to the "Cleaning electrode" is set to not clean. Press the
"Measure" button and the instrument enters the measurement state.

Ground

Potentiometer

Ammeter

Resistance
box

Figure 4.1 PH meter simulation test wiring diagram

14
【j夏 PH05288型工如H计使用视明书 上濂冒和白动化仪表设备有限公司

Adjust the resistance box so that the temperature is displayed at 25.0°C. According to table l, the
input signal of the potentiometer is used. The display value of the pH meter should not be greater
than 0.05pH of the soil with the nominal value of the meter l, and the current output error
corresponds to the soil with the nominal value of the thousand O-l01nA file. The range should not
be greater than the soil with the nominal value of the thousand O.hnA; corresponding to a thousand
4-20mA files, the range should be less than 0.16MA of the nominal value of the thousand.


Table 1: Correspondence between the display value of the 25° CpH meter and the input signal


mV 414.12
Potentiometer output 354.96 295.80 236.64 117.48 118.32 59.16
Instrument display pH 1 2 3 4 5 6 7
Potentiometer output mV -414.12 -354.96 -295.80 -236.64 -117.48 -118.32 -5 9.16
Instrument display pH 14 13 12 II 10 9 8
If the inspection is qualified, the pH meter is qualified. If it is unqualified, the internal circuit of the
entire instrument can be extracted from the front and the relevant potentiometer can be adjusted
(Figure 4.2).

• Temperature measurement
accuracy inspection

Remove the rear panel terminals 5,


6, and 7 of the instrument, and 田祁涓度ISPAN
connect to the DC (or AC-DC) resistor 粒凇卧睾六IZERO
box. Change the value of the LCD背影兑尧度PZ03
resistance box according to Table 2, A/0量启c2V>PZOI PH扭
the nominal value of the temperature
PH零位
display is shown in table 2, and the
temperature display error should be 妞§R
full Soil with a nominal value of 0.5°
vertical connection method: use three 鼓笨位
short-term wires of the same length,
one connected to one end of the
resistance box, and the other end
connected to the instrument terminal 7; 前面板 模拟板
the other two wires are connected to
the other end of the resistance box,
and the other end of the two wires are
connected to the instrument terminal 5
and 6 respectively. The resistance
value of the resistor box is set to
109.7Q, enter the “6300" password, 图4.2印刷板上可调节的电位器示意图
and press the "Confirm” button.,

The instrument automatically enters the calibration of 25.0°C. Then press the "Test Dong" button
to make the instrument enter the test Dong state

Table 2


Resistance box II (W) 100.00 107.79 115.54 123.24 130.89 138.50
Nominal
temperature (°C) 20 40 60 80 100
If the inspection is qualified, it means that the temperature measurement of the secondary meter is
qualified. If it is unqualified, the relevant potentiometer can be adjusted (Figure 4.2)

Note:

令 The internal adjustment of the instrument should be careful! Do not adjust indiscriminately. The
operator should have a certain level of instrumentation, and carefully adjust according to this
operation manual.

令 The secondary inspection table can be inspected using the equipment in Figure 4.1, or the special
equipment for the “PHJ—02 pH meter calibration box” manufactured by the company can be used for
inspection. The equipment can be ordered from our company, and it is also suitable for routine
inspection of pH meters produced by other companies.

15
【j夏 PH05288型立pH计使用说明书 上濂圃和白动化仪表设备有限公司

4.1 Secondary table maintenance


The measurement principle of a pH meter is an instrument that characterizes the pH
value by measuring the electromotive force of the electrode, and the electromotive force of
the electrode is a measurement technology with high internal resistance and small


signal.After the electrode is running in the system for a period of time, due to the pollution of
the liquid under test, its own parameters can easily be changed, so regular correction and
regular maintenance of the electrode are particularly important.
Regular correction of electrodes

• Two-point correction
Take the electrode out of the measuring cup and correct it in any two standard solutions
in Schedule 1.The measurement error of the third standard liquid should be small, and the
nominal value at this temperature should be O. l pH.

• One-point correction

Take the electrode out of the measuring cup and correct it in any of the standard
solutions in Schedule 1.If any of the other two standard solutions is measured, the
measurement error of the standard solution should be as small as 0.1 pH of the soil at the
nominal value at this temperature.

The pH electrode should be corrected regularly. Generally, a two-point correction


should be made every 2-3 months in a relatively clean measuring solution: a one-point
correction should be made every 2-3 weeks.If the solution is dirty, the correction cycle


should be shortened accordingly.The result of its correction: the electrode slope S>90%,
and the zero potential PH value p H.It should be between pH7 and 1.

Electrode activation

For electrodes that have been left unused for a long time, they should be soaked in


steaming water or other clear water for 12-24 hours before use, so that the surface layer of the
glass electrode is activated and put into use.

Electrode cleaning

The electrode that has been used in the system for a period of time should be
cleaned.Remove the electrode from the measuring cup, wipe off the stains on the electrode
head with filter paper or mirror paper, soak in 1% HCl solution for 3 hours, then rinse with
water, and put it into use after two-point calibration.

If the S<90% or pH4 of the electrode after the two-point calibration is outside the p H7 soil l,
the electrode can be soaked in a 1% HF solution for 10-20 seconds to generate a new
activation layer on the surface of the electrode, and then rinse with clean water, and put it into
use after the two-point calibration.

16
【j夏 PH05288型工如H计使用视明书 上濂冒和白动化仪表设备有限公司

Chapter Five : Error


The device has a fault self-test function. When some faults occur in the device, the alarm of


device will light on the LCD display to prompt you. Checking reliance of ground.

When S < 90 % or pHo is outside pH7± 1 during two-point calibration, situations are possible:

• The electrode has been left for too long. Activation treatment.
The standard buffer solution is wrong or expired.

• The waiting time during calibration is too short, and the potential of the electrode has not
yet stabilized.

• The electrode is contaminated so the performance was devalued.

• The terminals of the electrode connected to the pH meter (marked G or pH) and the
terminals connected to the reference electrode (marked R or REF) may be contaminated,


thus reducing the input impedance of the instrument. Cleaning the terminals with alcohol
and then blow them dry with a hair dryer.

Pure water (conductivity <10μs.cm-1) measurement value is inaccurate

• There is a program dedicated to measuring pure water in the device. The "Pure Water" file
should be selected in the "Measurement Selection" file.


• There is air leakage after leakage in the system under test. It is calculated that when 2ppm
of CO2 is dissolved in 1 liter of pure water, the solution will change from pH 7 → pH6.

The measurement value of ammonia-containing water sample is inaccurate.

The device has special programs for measuring boiler water, bath water, and condensate


water. The "Measurement Selection" file should be select the "Ammonia-Containing Sample
Water" file.

The measurement value of the device is stable in the process system, but there is a fixed error
with the calibration value of the sampling laboratory.
This is an error caused by static calibration and dynamic measurement. When the
electrode is measured in the flow state, it will change the equilibrium potential of the reference
electrode, causing an error in the measurement value between the two. The instrument should
be statically and dynamically calibrated, for example: device measurement value is 9.95, and
the sampling calibration value is 9.75. Use the method in Section 3.3 to enter the "Static


Calibration and Dynamic Measurement Correction" column, and use the "Normal" and ">>"
keys to set "-0.20pH".
The measurement error is large:

• Cleaning the electrode

• Calibrate electrode

• Whether the ground terminal of the device and the ground wire of the electrode cup are
reliably connected to the ground.

. • The flow weight in the measuring cup is zero.

The measured value is unstable

• Checking reliance of ground


Cleaning the electrode

• The flow rate in the measuring cup changes too much


“The alarm is set incorrectly”


It means that you set the upper and lower limit alarms incorrectly, in other words, the pH
value of the lower limit alarm is higher than the pH value of the upper limit alarm, and it should
be reset.
“The wrong output range”
It means that the upper and lower limits of the pH value corresponding to the output range
setting were wrong, in other words, the pH value corresponding to the current scale is less than
the pH value corresponding to the current zero, and it should be reset.

17
压夏 PH0528竺竺计使用说明书

上濂圃和白动化仪表设备有限公司

“Wrong cleaning electrode”


It means that the cleaning time you set is wrong, in other words, T1≤ T2+ T3, it should be
reset.
“The temperature value is too high”

• Situations are possible:

• It is related to terminal blocks 5, 6, and 7, or the contacts are open, or the screws are not
tightened.

. • The secondary meter needs to be checked temperature.

"The temperature value is too low"

• Situations are possible:

• The wires or contacts related to terminal blocks 5, 6, and 7 are shorted.


• The secondary meter needs to be checked temperature.

"Temperature is out of limit"


Please check that the average temperature you are measuring may be greater than 100℃
or less than 0℃.
The pH value of environment was changed, but the displayed value stays static and the cleaning

and holding function is being performed. This is not a malfunction.

18
【j夏 PH05288型工如H计使用视明书 上濂曙和白动化仪表设备有限公司

Appendix I: Standard buffer solution

CONCENTRATION

0.05mol · Kg
一1 一
0.025mol ·Kg 1 0.01 mol · Kg一1
TEMPERATURE
(°C) Potassium hydrogen
phosphophthalate
Mixed phosphate
Sodium tetraacetate

。 4.00
4.00
PH value
6.98 9.46
9.39
5 6.95
10 4.00 6.92 9.33
15 4.00 6.90 9.28
20 4.00 6.88 9.23
25 4.00 6.86 9.18
30 4.01 6.85 9.14
35 4.02 8.84 9.11
40 4.03 6.84 9.07
45 4.04 6.84 9.04
50 4.06 6.83 9.03
55 4.07 6.83 8.99
60 4.09 6.84 8.97
70 4.12 6.85 8.93
80 4.16 6.86 8.89
90 4.20 6.88 8.86
95 4.22 6.89 8.84

19
【j夏 PH05288型立pH计使用说明书 上濂圃和白动化仪表设备有限公司

Appendix II: Pt100 Index value

oc

TEMPERATURE (Degree ) RESISTANCE (Value Q)
100.00
10 103.90
20 107.79
25 109.73
30 111.67
40 115.54
50 119.40
60 123.24
80 130.89
90 134.70
100 138.50
110 142.29
120 146.06
130 149.83

20
【j夏 PH05288型工如H计使用视明书 上濂曜和白动化仪表设备有限公司

Appendix III: Factory parameter

PRODUCT PARAMETERS

Water sample selection Regular water

Slope 1.000

pH zero 17.000

Static adjustment-dynamic adjustment l+o.oo

Alarm setting I0~14PH

Signal output
l4~201nA

Output range 0~14PH

Cleaning the electrode Without

Cleaning cylce
99 hours

Cleaning time 0 minute

Holding time
0 minute

21
【j夏 PH05288型立pH计使用说明书 上濂圃和白动化仪表设备有限公司

Packing list

口5288
Secondary table
口5288A
Instrument fixing
bracket 口2 pcs
High impedance 口 Built-in
converter
口 Built-in (Cable length_ meters)
口PH0-280
Transmitter
口PHG-281口PHG-281A口PHG-281B口PHG-281C
(Insertion depth_ meters; mouth ultrasonic
口PHG-271 generator)

Transmitter 口 Standard (5 meters)


cable length
口 mouth non-standard 5 meters

Hard tube
02
Transmitter
waterway press 口2 Hose tube
mouth
口1 Hard tube 1 hose tube

口 Through-plate type (2 nuts, 2 gaskets)

Transmitter O U type installation type 2 pcs


installation
spare parts 口 2 concave mounting clips

Port mounting plate



Electric cable □

Manual 口

Certificate of
conformity

Factory number: 口口口口口口

22

You might also like