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Influence of Electro Polishing Characteristics On
Influence of Electro Polishing Characteristics On
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To cite this article: Mubita Kapui & Ramesh Kuppuswamy (2017): Influence of electro-polishing
characteristics on needle-tissue interaction forces, African Journal of Science, Technology,
Innovation and Development, DOI: 10.1080/20421338.2017.1359446
Article views: 5
Download by: [Stockholm University Library] Date: 02 September 2017, At: 01:36
African Journal of Science, Technology, Innovation and Development, 2017
https://doi.org/10.1080/20421338.2017.1359446
© 2017 African Journal of Science, Technology, Innovation and Development
Advanced Manufacturing Laboratory, Department of Mechanical Engineering, University of Cape Town, Cape Town, South Africa
*Corresponding author email: kpxmub001@myuct.ac.za
The electro-polishing process was applied to stainless steel 304 with the aim of improving its surface texture. The electrolyte
was a mixture of H2O, H2SO4 (98%) and H3PO4 (85%) at a volume ratio of 2:3:5. Gravimetric analysis and stylus
profilometry were used to analyze the samples. It was observed that the material removed during the electro-polishing
process could be controlled to an error limit of 6%. The surfaces obtained showed improved cleanness and reduced
surface roughness (Ra). Hypodermic needles were then electro-polished using the same parameters with the aim of
reducing forces during needle insertion into tissue. The needle tips were analyzed using a SEM. The needles were tested
using silicone phantoms as a tissue substitute. The forces during insertion were less for all the electro-polished needles,
with the most consistent results obtained at a current density of 0.66 A/cm2. A theoretical model of the needle insertion
forces at different insertion depths was developed.
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African Journal of Science, Technology, Innovation and Development is co-published by Taylor & Francis and NISC (Pty) Ltd
2 Kapui and Kuppuswamy
various forms of tissue or phantoms. An area of significant was left on the coupons as a result of machining and hand-
interest is the modelling of these forces so as to improve ling, while the deionized water removed any acetone that
the accuracy of surgical robots and simulators (Misra did not evaporate from the coupon surface. Deionized
et al. 2010). The most common approach is to model the water was used because it has had the ions of any
forces with respect to needle displacement. Forces are mineral salts dissolved in the water removed. The ions
then modelled based on a variety of different approaches, would interfere with the electro-chemical reactions in the
including viscoelasticity (Zhao et al. 2016), fracture mech- cell which would, in turn, affect the electro-polishing
anics (Barnett, Lee, and Moore 2016) and data fitting via results. A DC power supply was used. No rotation or agi-
different methods (Maurin et al. 2004; Okamura, tation was used. The coupons were rinsed with acetone
Simone, and O’leary 2004). and deionized water after electro-polishing to remove
In some cases, the aim is to reduce the magnitude of any acid residue and products from the electro-chemical
the forces present during needle insertion. This leads to reactions from the coupon surface. The mass of the
a reduction in tissue deformation, which improves the coupons was determined before and after electro-polishing
effectiveness of treatments such as prostate brachytherapy. by weighing them using an electronic balance. The exper-
Abolhassani, Patel, and Moallem (2004) applied different iment had two independent variables, each with three
rotations to needles with the aim of reducing insertion levels. The variables were the electro-polishing current
forces. It was found that both maximum and friction and electro-polishing time. The experiments were
created using a 32 factorial design. The experiment par-
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|y′′ |
k= (2)
(1 + y′2 )3/2
4p2
k = Ra (3)
l2
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2E tan a 2
F1 = x (8)
p(1 − n2 )
where Ria and Rfa are the initial and final arithmetic mean
Fc = Fmax − F1 max − Fr (10)
roughness values of the stainless steel 304 coupons. The
results are shown in Figure 3.
where Fmax is the maximum force measured during needle
It is observed that the electro-polishing current and
insertion.
time have a significant impact on the surface texture. At
EW .I.t
m= (11)
F
a current density of 0.16 A/cm2, the change in surface density of 0.66 A/cm2 are favourable and show an
texture is not consistent. This is likely because the almost linear trend.
current is below the threshold value required for the Figure 4 shows SEM micrographs of the needle bevel
electro-polishing process to take place. It is widely edges after being electro-polished using different parameters.
accepted that four different mechanisms take place on a It is observed that the bevel surface of the standard
stainless steel surface when exposed to varying currents needle has more scratches, striations and foreign particles
in an electrolytic cell (Chen, Tu, and Huang 2005). than any of the electro-polished needles. The reduced
These are oxidation, passivation, diffusion limited roughness and improved cleanness of the electro-polished
current and oxygen evolution. Past studies agree that surfaces agrees with the results obtained in previous
electro-polishing occurs in the diffusion limited current studies (Awad et al. 2012; Nazneen et al. 2012; Latifi
region (Magaino, Matlosz, and Landolt 1993; Matlosz, et al. 2013).The smoother and cleaner surfaces reduce
Magaino, and Landolt 1994; Chen, Tu, and Huang 2005; the amount of friction present at the needle-tissue interface
Nazneen et al. 2012). The results obtained for a current during needle insertion. It can also be seen that the bevel
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Figure 4: SEM micrographs of bevel edges for needles electro-polished at different parameters (magnification: 1500×).
6 Kapui and Kuppuswamy
thickness reduced with an increase in electro-polishing currents. From Figure 5(a), the maximum forces decrease
time at each of the currents. This leads to the sharpening in a non-uniform way with an increase in electro-
of the needle cutting edges resulting in reduced cutting polishing time. While the decrease in force for the times
forces during needle insertion. While the needle tips of 5 and 15 minutes is within an expected range, the
showed improvement with increased electro-polishing time of 10 minutes produces a much lower force value
current and time, the maximum useable parameters were than expected.
limited by the small mass of hypodermic needles. The The erratic nature of the force data obtained for a
removal of too much material from the needle surface current of 0.2 A is not unexpected, as the surface texture
resulted in the needle wall rupturing. This is followed by results presented earlier were also inconsistent. This
the complete dissolution of the needle in the electrolyte. could possibly be explained by the fact that both the
Such a situation is easy to avoid as the amount of material cutting and friction forces have a large impact on the
removed can be controlled by controlling the electro-pol- overall force during needle insertion (Okamura, Simone,
ishing parameters. Consequently, electro-polishing for and O’leary 2004). The electro-polishing process is
more than 10 minutes at a current of 0.82 amps should known to produce sharper cutting edges on micro-
be avoided. needles when applied in a controlled manner (Gill and
Prausnitz 2007). It has also been shown to increase the
Needle insertion forces hydrophilicity of stainless steel surfaces (Latifi et al.
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The forces present at the needle-tissue interface during 2013). This leads to reduced friction at the needle-tissue
needle insertion into the phantom were captured and interface because of the increased lubrication. These
plotted against time as shown in Figure 5. additional factors could likely play a role in the relation-
It is observed that the maximum forces present during ship between the electro-polishing time and the insertion
needle insertion are reduced for all electro-polishing par- forces at a current of 0.2 A. The large drop in force,
ameters. Despite this, the reduction in forces is not however, cannot fully be accounted for. This discrepancy
uniform and differs for each of the electro-polishing is not present at higher currents.
Figure 5: (a) Insertion forces at J = 0.16 A/cm2. (b) Insertion forces at J = 0.66 A/cm2. (c) Insertion forces at J = 1.70 A/cm2.
African Journal of Science, Technology, Innovation and Development 7
Friction force
The frictional shear stress for the different electro-polish-
ing conditions is shown in Figure 6.
It is observed that the stress reduces uniformly as the
Figure 6: Frictional shear stress at needle-tissue for different
electro-polishing parameters.
electro-polishing time is increased at a current of 0.82
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Table 2: Needle friction and cutting forces per unit insertion Abolhassani, Niki, Rajni Patel, and Mehrdad Moallem. 2004.
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