Alakalinity

SOHAR IWP
Contract nº: Purchase order Nº
1890 PO-085B
Description SPECIAL ANALYZERS
Document type: Equipments/ TAGS Nº
MAN AIT-L1L08-04, AIT-L1L08-14
Purchaser Document number Title Rev

User Manual Titrilyzer Alkalinity
SIWP-Z0-MAN-0002-0085B 02
Contractor review and comments do not indicate either responsibility or liability for accuracy and
completeness of this document or to alter any contractual terms and conditions
REVIEW RESPONSIBLE PURCHASER
Reviewed with
Rejected
comments
Void Reviewed
without
comments
Vendor Logo Vendor Document Document Title: Rev: 02

number:
User Manual Titrilyzer Alkalinity
1090 User Manual
Titrilyzer Alkalinity R2 Date:
10/08/17
SOHAR IWP
NOTES:
(1) Purchase order nº as shown on purchase order
(2)
DOCUMENT TYPE (DCT) CODE
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Meeting Minutes MOM
Non-Conformance Report NCR
Notice NOT
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Application Manual
EnviroLyzer® Alkalinity
Series of on-line Alkalinity Analyzers
Serial number: 012.1090.1704.048

User’s Manual
EnviroLyzer® Alkalinity
Series of on-line Alkalinity Analyzers
© 2014 – AppliTek NV – Printed in Belgium
All rights reserved. No part of this manual may be reproduced, stored in a retrieval system or
transmitted in any form or by any means - electronic, mechanical, photocopying, recording or
otherwise - without the prior written permission of AppliTek NV.
The content of this document is entirely a non-binding external opinion. AppliTek NV nor any
of its employees can be held liable for damages to people, third parties, goods and assets,
that may result from implementing the content.
CONTENTS
Preface – Documents and safety........................................................................................... 8
Installation of the analyzer – Overview .............................................................................. 9
1. Installation of the analyzer ........................................................................................10
1.1 Dimensions of the analyzer ...............................................................................10
1.2 Location and ambient conditions .......................................................................11
1.3 Mounting instructions ........................................................................................11
2. Power and signals ....................................................................................................12
2.1 Power................................................................................................................12
2.2 Signals ..............................................................................................................12
3. Utilities ......................................................................................................................13
3.1 Overview ...........................................................................................................13
3.2 Sample feed ......................................................................................................13
3.3 Drain .................................................................................................................14
3.4 Rinse feed .........................................................................................................14
3.5 Overflow............................................................................................................14
3.6 Reagents & Calibration/validation solutions feed ...............................................14
3.7 Instrument air ....................................................................................................15
4. Power up & components test ....................................................................................16
4.1 Analyzer design ................................................................................................16
4.2 Wet chemical components ................................................................................17
4.3 Analog output ....................................................................................................20
4.4 Analog input ......................................................................................................21
5. Analyzer method .......................................................................................................22
5.1 Specifications ....................................................................................................22
5.2 Analysis ............................................................................................................22
5.3 Validation ..........................................................................................................22
5.4 Cleaning ............................................................................................................22
5.5 Priming..............................................................................................................23
6. Reagent preparation .................................................................................................24
6.1 Reagent Consumption ......................................................................................24
6.2 Storage and quality of chemicals and solutions .................................................24
6.3 HCl solution 0.01M ............................................................................................24
6.4 Validation standard solution (M Alk) ..................................................................25
7. Start-up of the analyzer .............................................................................................26
7.1 Access ..............................................................................................................26
7.2 Prime the reagents ............................................................................................26
7.3 Method navigation .............................................................................................27
7.4 Calibration .........................................................................................................32
7.5 Cleaning ............................................................................................................32
7.6 Time List ...........................................................................................................33
7.7 Data and results ................................................................................................34
7.8 Analyzer settings ...............................................................................................35
7.9 Start-up the analyzer for on-line measurement..................................................36
8. Maintenance .............................................................................................................37
8.1 Check for leaks and abnormal conditions ..........................................................37
8.2 Check for alarms ...............................................................................................37
8.3 Prepare reagents and fill the reagent containers ...............................................37
8.4 Replace duckbills ..............................................................................................38
8.5 Run the calibration program ..............................................................................38
8.6 Run the cleaning program .................................................................................38
8.7 Replacement of the peristaltic pump tubing .......................................................38
8.8 Replace dispenser piston ..................................................................................39
8.9 Replace dispenser valve ...................................................................................39
8.10 pH electrode maintenance ................................................................................40
8.11 Shutdown of the analyzer for a longer period ....................................................40
9. Troubleshooting ........................................................................................................41
10. Spare Parts ...........................................................................................................41
Addendum 1: Analysis Procedure.....................................................................................42
1.1 Alkalinity Method – Analysis ..............................................................................42
1.2 Method Alkalinity – Cleaning (optional) .............................................................43
1.3 Method Alkalinity– Priming (optional) ................................................................43
Addendum 2: Analyzer Configuration ...............................................................................44
2.1 Digital Outputs ..................................................................................................44
2.2 Digital Inputs .....................................................................................................44
2.3 Analog Inputs ....................................................................................................44
2.4 Analog Outputs .................................................................................................44
2.5 Constants ..........................................................................................................44
2.6 Dispensers ........................................................................................................45
2.7 Results ..............................................................................................................45
2.8 Results Calculation ...........................................................................................45
2.9 Results Analog output .......................................................................................45
2.10 Result Alarms....................................................................................................45
2.11 Results Graph ...................................................................................................46
2.12 Algorithms .........................................................................................................46
2.13 Alarm and message table..................................................................................47
2.14 Group DO .........................................................................................................47
Addendum 3: Alarms and signals .........................................................................................48
Preface – Documents and safety
Thank you for purchasing this high quality analytical instrument. The analyzer is designed for
installation in industrial environments and intended for professional use. On delivery the
analyzer does not offer readily available end-user functionality. The analyzer needs to be
installed and configured by competent staff prior to use by the end user. Information about
the exact specifications, necessary connections, utilities and maintenance schedules is given
in the accompanying GENERAL SAFETY BOOK (8 languages).
General safety instructions

AppliTek and/or its affiliates use their best efforts to deliver a high quality analytical
instrument and reliable software packages. AppliTek nor its affiliates cannot be held
responsible for any damage that may result from the incorrect use of the software and
hardware, use outside the scope of the analyzer’s specification, misinterpretation of the
safety instructions, errors or deliberate modifications made to the analyzer; in addition, any
warranty issued by AppliTek becomes void.
• Knowledge of the basic safety regulations is essential for the safe handling and
disruption-free operation of the unit. Therefore, please read the entire manual before
setting up the analyzer. Pay attention to danger and caution statements;
• These operating instructions contain the most important guidelines necessary in order
to safely oversee the unit’s operation;
• All persons working on the unit should take note of these operation instructions, and
especially those relevant to safety;
• Protect the analyzer from impacts causing corrosion or preventing components from
working properly;
• Have faulty parts of the analyzer replaced immediately;
• Spare parts must comply with the technical requirements determined by AppliTek;
• When malfunctioning, take the analyzer out of operation. Repair the malfunctions
immediately. Failure to do so could result in serious injury to persons or damage to
the equipment;
• On top of this, all rules and regulations pertinent to accident prevention, which are
applicable at the measuring site, are to be followed.
• It is the operator’s responsibility to allow only those persons to work on the unit who
are familiar with the regulations concerning safe handling and have been informed
how to work with the instrument;
Safety devices
Before any initialization of the unit, all safety devices must be properly mounted and
functional. Safety devices can only be removed:
• During maintenance and repair work by trained personnel or when the unit has been
disconnected from the electrical mains.
• After the unit has been safeguarded against renewed operation.
Electrical dangers
Work on the unit’s power supply and electronics can only be carried out by a qualified
electrician. The mains switch must be switched off during work on electrical components.
8
Installation of the analyzer – Overview
9
1. Installation of the analyzer
1.1 Dimensions of the analyzer
10
1.2 Location and ambient conditions
The analyzer is designed for installation at indoor environmental conditions. Install the
analyzer where the temperature is maintained as stable as possible between 10 and 30 °C
(range 4°C) and is not subject to sudden temperature changes.
The analyzer should be installed as close as possible near the sampling point. If this is not
the case, a fast loop sampling system has to be installed because a long distance between
the analyzer and the sampling point will increase the response time of the analyzer.
Do not mount the analyzer in direct sunlight! This can affect the visibility of the screen
and the analyzer, its components and reagents.
Other points of attention are: - humidity: 5 – 95 % non-condensing

- avoid corrosive atmospheres
Variation of these conditions can seriously affect the analyzer results and damage the
analyzer and its components!
1.3 Mounting instructions
The analyzer is designed for wall mounting and intended for permanent installation. Make
sure the location is easy accessible. The dimensions of the analyzer are given on the
previous page. The indicated footprint is a strict minimum and doesn’t take into account the
space needed for tubing and cables.
The analyzer has four mounting holes for screws M8x10mm at the back of the cabinet.
These bolts are fastened into/onto the supporting structure from the inside of the electrical
cabinet at the back.
This analyzer has to be installed by qualified technical personnel to ensure adherence

to all applicable electrical plumbing requirements.
11
2. Power and signals
2.1 Power
First open the electrical cabinet door by pulling the two levers and unhook them. Make
provisions for removing power to the analyzer during servicing. The AC power cable enters
on the left side of the cabinet at the back through the upper left cable gland. The terminals for
the power and ground are located at the upper left hand corner of the cabinet at the back, as
you face the unit. Connect your wiring to the upper side of the terminals. Connect the AC
feed as follows:
- The protective ground at the yellow/green terminal block.

- The hot/line (L) and neutral (N) wire are to be connected at the circuit breaker.
Terminal North American wire color European wire color

Protective Ground (PE) Green Green/yellow
Hot/line (L) Black Brown
Neutral (N) White Blue
2.2 Signals
External 24Vdc power supply
Note: If additional AO, DI or DO connections are required, extra terminals will be present.
Connections:
AO1-AO2: Analog Outputs

4-20mA, active current, loop
powered from the analyzer
max. load 500R
FCT1-FCT5: Free ConTacts

(digital output)
Relay output, contact loading
max. 24VDC/0,5A
PCT1-PCT4: Power ConTacts

(digital outputs)
24VDC/0,5A output
INP1-INP4: INPut
(digital input)
24VDC, to trigger with external
potential free contact
24VDC, only to be
used for external
control (max load 1A)
12
CONTACT INPUT/OUTPUT NAME
AO1 AO1 Result Alkalinity STR1
AO2 AO2 Result Alkalinity STR2
FCT1 DO25 Malfunction
FCT2 DO26
FCT3 DO27
FCT4 DO28
FCT5 DO29
PCT1 DO21 SV STR1
PCT2 DO22 SV STR2
PCT3 DO23
PCT4 DO24
INP1 DI5 Air pressure
INP2 DI6
INP3 DI7
INP4 DI8
3. Utilities
3.1 Overview
Consumption/ Consumption/28 days

Comment Connection
analysis (1 analysis/15 min)
Atmospheric
Sample ~ 60 ml ~ 165 L 1/4”
pressure
Atmospheric
Rinse water ~ 100 ml ~ 270 L 1/4”
pressure
Vent / / Free 1/4”
Atmospheric
Reagents See Chapter 6 See Chapter 6 1/8”
pressure
3.2 Sample feed
The sample feed to the analyzer must be at atmospheric pressure if the analyzer uses a
peristaltic pump for sampling. The sample feed to the analyzer must be higher than the
sample flow in the analyzer. It is recommended to use a small overflow vessel (next to the
analyzer) from which the analyzer will take fresh sample. Thus the sample in the overflow
vessel should be continuously refreshed. If the size of the solids present in the sample is too
high, it is recommended to filter the sample.
Connection: 1/4” OD tubing (PFA)

Location: Bottom side of the analyzer
The analyzer is not designed for use with samples that are explosive or flammable. If a
solution other than water is used, this solution should be tested to test the
compatibility with the instrument!
13
3.3 Drain
The analyzer needs a drain to discharge both sample and reagents after analysis. A floor or
sink drain is satisfactory, but it must be unrestricted and located at a lower level than the
analyzer so that gravity will carry away the liquid. The drain must have a vent to the
atmosphere and the drain tube from the analyzer must not be submerged. Pay attention that
the drain line is never blocked. A water connection is also recommended so that the drain
sink and piping is regularly flushed with clean water in order to avoid clogging due to
crystallization. Steepness of the draining pipe must be sufficient.
Drain piping: recommended diameter of 32 mm

Although the chemical reagents are diluted, the user has to check that the external
drain/overflow system is appropriate for reagents and corrosive wastes! Used
reagents shall be treated for disposal according to national or local regulations!
3.4 Rinse feed
The rinse solution should be on atmospheric pressure. The rinse solution (permeate water)
has to be connected to the rinse valve.

3.5 Overflow
The analyzer needs an overflow tube in order to drain the analysis compartment in case of
leakage of sample fluids, reagent fluids (and combination of both) in the compartment. A floor
or sink drain is satisfactory, but it must be unrestricted and located at a lower level than the
analyzer so that gravity will carry away the liquid. The overflow tube from the analyzer must
not be submerged. Pay attention that the overflow line is never blocked. Steepness of the
overflow pipe must be sufficient.

3.6 Reagents & Calibration/validation solutions feed
Connections have to be made between the reagent containers and the dispensers, the micro
pumps and the cleaning valve. The calibration/validation solutions can be connected to the
REF1/REF2 selection valve.
Connection: 1/8” OD tubing

Location: Bottom or left side of the analyzer
Although the chemical reagents are diluted, the user has to check that the external
drain/overflow system is appropriate for reagents and corrosive wastes! Used
reagents shall be treated for disposal according to national or local regulations!
Remark : Reagents are not supplied for start-up and commissioning.
14
3.7 Instrument air
The instrument air must be dry and dust free (according to ISA-S7.0.01-1996). The minimal
pressure of the instrument air necessary for the analyzer is 1 bar (100 kPa or 15.5 psi).
Instrument air is used for purging the analyzer in order to prevent corrosion by corrosive
gases such as chlorine gas from outside the analyzer.
Remark : If no corrosive gases are present, instrument air is not needed. AppliTek is not
responsible for corrosion if instrument air is not used.
15
4. Power up & components test
The analyzer and its components must be tested before the unit can be put into online
service. Make sure that all necessary connections were made before testing the following
components. Switch on the analyzer by means of the circuit breakers lever in the electrical
compartment and (if present) the external power switch.
When connecting the power of the analyzer, the software is started up. First, the initial
startup screen appears. While this screen is visible, the parameters are loaded (loading of
methods, configuration …) and the dispensers are initialized. Next, the MAIN screen
becomes visible automatically.
Initial startup screen MAIN screen
4.1 Analyzer design
16
4.2 Wet chemical components
Menu path:
→ F2
In the Visualization (F2) submenu, the wet chemical components (reagent pumps, stirrer,
dispenser…) can be controlled manually. Press the icons on the screen to control the
components. A control panel appears on the right side of the screen. By use of this panel,
the chemical components can be controlled. Check if these components are working
properly.
1. Stirrer
Press the stirrer icon. Switch the stirrer

ON/OFF by pressing the ‘ON/OFF’ button. It
is also possible to turn the stirrer ON for a
specified time. Fill in the time (in seconds)
and press the ‘Start’ button.
17
2. Drain pump and Drain/Level valve
The drain/level valve is used in combination

with the drain pump for draining or leveling
the analysis vessel.
When the drain pump is started and the

drain/level valve is not activated, the analysis
vessel is drained.
Press the pump icon. Switch the pump

is also possible to turn the pump ON for a
The ‘Group’ function is implemented for

safety reasons. If for example a valve must
be opened before a pump is started, the
group action can be used, if programmed.
Press the valve icon. Activate/deactivate the

valve by pressing the ‘ON/OFF’ button. It is
also possible to activate the valve for a
When the pinch valve and the drain pump

are activated, the level action takes place:
the excess of sample is removed from the
analysis vessel. The level action is used to
make sure that the amount of sample in the
analysis vessel is equal for each analysis.
3. Sample pump
The sample pump is used in combination with

the Sample valve, Validation valve and
Cleaning valve for sampling. Also the external
valves have to open (EXT SV1 or EXT SV2)

The ‘Group’ function is linked to a group

action in the analysis method.
18
When the sample enters because one or
more valves are switched, it is necessary to
switch these valves on before the sample
pump is started. Press the icon of the
corresponding valve. Switch the valve
is also possible to turn a valve ON for a
Next, press the sample pump and start the

sample pump.
4. Dispenser
Press the dispenser icon.

Press the ‘Dose’ button to dose a certain
volume into the analysis vessel.
Press the ‘Fill’ button to fill the dispenser.
Press the ‘Empty’ button to empty the
dispenser.
Press the ‘Recycle’ button to recycle the
dispenser. The volume of the dispenser is
dosed into the reagent container.
Press the ‘Extract’ button to take a certain
volume from the analysis vessel.
Press ‘Stop’ to stop any action of the
dispenser.
5. Rinse

The ‘Group’ function is implemented for

safety reasons. If for example a valve must
be opened before a pump is started, the
group action can be used, if programmed.
19
Components that are not visible on the visualization screen can be controlled in the DO
submenu.
Menu path:
Select the digital output by use of the Edit

(E) button.
The value of the digital output can be toggled

manually with the ‘ON/OFF’ button. After
entering an activation time (seconds), the
‘START’ button can be pressed to activate
the digital output. The digital output will then
be active during the inserted number of
seconds. After entering a number of pulses,
the digital output will give the set number of
pulses.
Press ‘Stop’ to stop any action of the DO.

Press the arrow keys at the top of the screen
to select another DO.
Press ‘Back’ to quit the screen.
4.3 Analog output
Menu path:
Press the EDIT (E) button to control the

selected analog output.
Use a multimeter to check if the analog

output signal is working.
20
Insert a value by use of numeric keyboard
and confirm. Press Accept to update this
value.
Check if this value corresponds to the value

the multimeter is giving.
Check the ‘Installation Manual’ to make the

right connections.
4.4 Analog input
Menu path:
Check if all analog inputs are responding

correctly.
Press the EDIT (E) button to control the

selected analog input.
pH Sensor
Calibration is performed in buffer solutions

with pH value of 4 (media 1) and pH value of 7
(media 2).
- Press enter to start calibration

- Put sensor in media 1 and enter
- Stabilizing, press enter to continue
- Put sensor in media 2 and enter
- Stabilizing, press enter to continue
- Update calibration data
21
5. Analyzer method
5.1 Specifications
Specifications are subject to change without notice.
Method: Titration (pH electrode) – End point titration
Parameter: Alkalinity
Range: 10 – 200 mg/L
Precision: < 2 % of full scale range (for standard test solutions)
Analysis time: Approximately 15 minutes
Sample requirements: Atmospheric pressure, flow rate between 10 and 30 ml/minute,

sample temperature between 5 and 60 °C
5.2 Analysis
The alkalinity concentration is determined by an acid-base titration using a pH electrode. The

sample is titrated with hydrochloric acid (HCl). After the determination of the endpoint (pH 4.5),
the alkalinity concentration is calculated.
5.3 Validation
The validation method is used to verify the functioning of the analyzer with a standard
solution. The validation procedure measures a standard solution with a known CaCO3
concentration (channel 8 – VAL) to validate the analyzer.
5.4 Cleaning
The analysis vessel is flushed with the cleaning solution and a waiting time is respected.
Next, the analysis vessel is flushed with fresh sample. The cleaning can be started manually
or automatically. The frequency of the automatic cleaning can be programmed in the
analyzer. After the cleaning, the analyzer switches automatically to the analysis program. It is
recommended to perform a cleaning every single day, to guarantee the smooth operation of
22
the analyzer. The cleaning procedure should prevent any build-up of chemicals in the
analyzer.
5.5 Priming
The prime procedure can be used when starting up the analyzer or after a shutdown of the
analyzer: the reagent tubings are flushed with fresh reagent solution and the sample tubing
and the analysis vessel are flushed with fresh sample.
23
6. Reagent preparation
Warning:
Some of the chemicals used are corrosive or harmful! All operating
! personnel should wear protective gloves, goggles and acid-proof
clothing!
6.1 Reagent Consumption
In the table below, the products that are needed to prepare the reagents are listed. The
product name, the formula, the molecular weight, the CAS No. and the amount needed to
prepare 1 liter of the reagents is given. Check the consumption of the reagents (28 days) to
adapt the volumes needed.
Consumption/28 days Type of

Product Consumption
(1 analysis/ 12 min) reagent bottle
Concentration
HCl solution dependent
Concentration dependent Plastic – 10L
6.2 Storage and quality of chemicals and solutions
Quality of chemicals:
All chemicals should be of ACS grade or better. We recommend the use of pro analysis
chemicals.
Quality of water:
Use carbon dioxide-free, de-ionized water to prepare the chemical solutions and for dilution
and rinse purposes.
Waste treatment:
Used reagents shall be treated for disposal according to national or local regulations.
6.3 HCl solution 0.01M
Product Formula MW (g/mol) CAS No. 1 liter solution

Hydrochloric acid (1M) HCl 36.46 7647-01-0 10 ml
Hydrochloric acid (1M)
Hazard statement(s):
H290: May be corrosive to metals.
Preparation:
Prepare a 0.01 M hydrochloric acid (HCl) solution. Add carefully 10 ml hydrochloric acid (HCl
1M) to 500 ml de-mineralized water and dilute to 1 liter with de-mineralized water.
24
6.4 Validation standard solution (M Alk)
Product Formula MW (g/mol) CAS No. 1 liter solution

Sodium carbonate Na₂CO₃ 105.99 497-19-8 1.0599 g
Sodium carbonate
Hazard statement(s):
H319: Causes serious eye irritation
Precautionary statement(s):
P305 + P351 + P338: IF IN EYES: Rinse cautiously with water for several minutes.
Remove contact lenses, if present and easy to do. Continue rinsing.
Preparation:
1000 mg/L CaCO₃ stock solution
Dissolve accurately 1.0599 g sodium carbonate (Na₂CO₃) in 200 ml de-ionized water, using a
volumetric flask of 1000 ml. Add de-ionized water up to the mark grade.
Preparation validation standard solution 200 mg/L CaCO3 :

Take accurately 200 ml of the 1000 ppm CaCO₃ stock solution and transfer into 200 ml de-
ionized water, using a volumetric flask of 1000 ml. Add de-ionized water up to the mark grade.
This solution contains the equivalent of 200 mg/L CaCO3.
25
7. Start-up of the analyzer
7.1 Access
Menu path:
→ F1 → User → Enter Access password
Press the black box next to ‘User:’ to change the userlevel by use of the corresponding
password.
Depending on the userlevel some menus are accessible and some are not. Normally, when
the analyzer is started up, the ‘Automatic’ userlevel appears. This level is also used in
online situations. The analyzer is locked, which means that the METHOD (F4) and CONFIG
(F5) menu are not accessible. If modifications of the software are needed, higher userlevels
can be used. The access to certain crucial parameters is only given if the ‘Administrator’
password is used. Enter the password by pressing the ‘Enter Access password’ button.
Default passwords:
User Password
Automatic -
User1 a
User2 b
7.2 Prime the reagents
Menu path:
→ F1 → 1.Method → Priming
Select the method with the navigation buttons at the bottom of the MAIN (F1) screen. The
method screen appears.
26
If all wet chemical components are working properly, the reagents can be connected to the
analyzer. Press the ‘Priming’ button to fill up all tubings to the analysis vessel with reagent
Make sure there is no air present in the tubings. Also, make sure there is no air present in
the dispenser, the tubing to the dispenser and the tubing from the dispenser to the analysis
vessel.
7.3 Method navigation
Follow the procedure below to start the method. It is recommended to run the method
several times and to make sure the measurements are stable before a calibration of the
analyzer is performed. Make sure all flushing times are set correctly before the analyzer is
started for on-line measurement.
Menu path:
→ F1 → 1.Method
Select the method with the navigation buttons at the bottom of the MAIN (F1) screen. The
method screen appears.
Menu path:
→ F1 → Method → Playlist → Automatic sequence
Press the Playlist button. Press the Automatic sequence button and insert the desired
module, channel and number of analysis. Press Accept to confirm. Press Back to quit the
window without saving the changes.
Start parameters:
Module: Analysis, Preconditioning, Cleaning, Priming, Init, and Exit.

CH: Automatic sequence or channel 1 to 10
# Runs: Insert the number of runs of the module (0 = Continuous analysis)
Comment: Add a comment concerning the analysis (Optional). This comment will also be
displayed in the data table.
27
7.3.1 Single stream analysis
- Module: select Analysis
- CH: insert the number of the stream
(Sample = stream 1 – 8; REF1 = stream 9; REF2 = stream 10)
- #Runs: insert the desired number of runs (=1 for single stream analysis)
- Continuous analysis: insert 0 as #Runs in the method main screen

- Fixed number of analysis: insert the desired #Runs in the method main screen
For example:
- The third sample stream needs to be analyzed
- Insert ‘3’ as channel (CH) and 1 as #Runs
7.3.2 Single stream analysis with cleaning
- Module: select the desired module (Analysis or Cleaning)

(For cleaning, always use channel 1)
Repeat for each stream that needs to be analyzed.

28
For example:
- There one streams that need to be analyzed. After 10 analysis, a cleaning is needed.
- Insert ‘Analysis’ as Module, ‘1’ as channel and ‘10’ as #runs
- Insert ‘Cleaning’ as Module, ‘1’ as channel and ‘1’ as #runs
7.3.3 Multiple stream analysis
- Module: select Analysis


For example:
- There are five streams that need to be analyzed.
- Insert ‘1’ as channel and 1 as # runs
7.3.4 Multiple stream analysis with cleaning
- Module: select the desired module (Analysis or Cleaning)


29
For example:
- There are two streams that need to be analyzed. Next, a cleaning is needed.
- Insert ‘Cleaning’ as Module, ‘1’ as channel and ‘1’ as #runs
7.3.5 Start the method

Menu path:
→ F1 → 1.Method1 → Playlist → Start
7.3.6 Stop the method
Menu path:
→ F1 → 1.Method1 → Stop
Press the ‘Stop’ button. The method will be finished and the analyzer will stop (status will
change from ‘Run’, to ‘Stopped’ and then ‘Ready’).
30
Menu path:
→ F1 → 1.Method1 → Abort
Press the ‘Abort’ button to stop the method immediately after confirmation.
Menu path:
→ E-Stop
In case of emergency, all methods can be stopped directly by pressing the E-STOP button
(SOFTWARE emergency stop) at the bottom of the screen.
7.3.7 Remote control

Menu path:
→ F1 → 1.Method1 → Is Master
Press the ‘Is Master’ button. The following instruction screen appears. Press ‘Toggle’ to put
the analyzer in ‘Is Slave’ position. If the method is in this position, it is impossible to start the
method manually. The method can only be started remotely i.e. by a digital input, by Modbus
communication, by a sequence…
Press Abort to stop the method. Press the ‘Is Slave’ button to put the analyzer in ‘Is Master’
position again.
31
7.4 Calibration
Once the analysis results are stable, the analyzer can be calibrated.
Menu path:
→ F1 → Method → Calibrate
Press the ‘Calibrate’ button. The calibration procedure will start automatically after
confirmation. The calibration procedure consists of following steps:
- Number of runs (REF1): 1x stream 9
The concentration of the REF1 and REF2 solution and the number of runs is programmable
in the Configuration (F5) menu (See Configuration Manual for more information).
Press the ‘Calibration history’ button to get an overview of the previous calibration data.
7.5 Cleaning
Menu path:
→ F1 → Method → Cleaning
To clean the analyzer (the analysis vessel) press the ‘Cleaning’ button. The cleaning
subroutine will be executed and the analyzer is stopped.
When the analyzer is on-line, the cleaning procedure starts after the Analysis subroutine is
finished. The analyzer is started again for on-line measurements after the Cleaning
subroutine is finished.
32
7.6 Time List
Menu path:
→ F1 → Method → Time list
Press the Time list button to configure the time list. An overview of the configured time tables
is displayed. Scroll through the list by use of the arrow keys.
Press the Edit (E) button to configure the selected time table. Every time table can be turned
ON or OFF by pressing the toggle (T) button.
Make sure the ‘Direct’ button is selected to guarantee the proper functioning of the Time list.
Press Back to quit the screen.
7.1.1 Configuration of the time list

Only a configured time list can be used. Make sure the time list is turned ‘ON’ and the
‘Direct’ button is selected.
Refer to the Configuration manual for additional information about the configuration of the
time list. Press Accept to confirm. Press Back to quit the screen.
Example:
An automatic calibration on stream 1 of
method 1 is needed, every day at 12 o’clock.
- HH: 12
- Channel: 1
- Start function: Calibration
- Index: Method1
33
7.7 Data and results
Menu path:
→ F3 → Database
The analysis results of every method are displayed in the ‘Database’ submenu. A method
can be selected by use of the arrow keys at the right side of the screen. Press the Edit (E)
button to view the result for the selected method. The arrow keys on the right side of the
screen can be used to scroll through the list.
The file can be exported to a memory stick by pressing the ‘Export’ button. The data are
exported to a CSV-file that can be opened for example in EXCEL.
Menu path:
→ F6
The course of a titration can be followed in the F6 submenu. Select the titration algorithm by
use of the dropdown menu. The graph can be appointed by use of the alphanumeric
keyboard. The screen can be copied to an USB stick by pressing the Export button. Press
the orange arrow key to view the titration data table. The titration algorithm can be selected
by use of the dropdown menu.
34
7.8 Analyzer settings
Adjustments to the analyzer configuration are made in the Configuration (F5) menu. We
recommend you to read the instructions very carefully before making adjustments to the
analyzers configuration: the functioning of the analyzer may be disturbed!
For more information about the analyzer settings, refer to the Configuration Manual.
7.8.1 Adaptation of flushing intervals

Menu path:
→ F5 → Software → CH Interval
The time set in a channel interval is channel dependent. Change this time in order to
extend/reduce for example the flush time of the sample through the analysis vessel.
Repeat for every channel (sample stream) if necessary.
7.8.2 Adaptation of constant values

Menu path:
→ F5 → Software → Constants
Constant values are used in the calculation of the results. Change these values if necessary.
7.8.3 Adaptation of Sample Group DO times

Menu path:
→ F5 → Software → Group DO → E (Edit)
Group actions are implemented to run several actions simultaneously. Be careful when
changing the ‘group DO’ settings, the functioning of the analyzer may be disturbed.
35
Select the ‘group DO’ by use of the arrow keys and press the Edit button to change the
settings.
The times are entered in millisecond (ms). To avoid problems with analyzer functioning, only
change the time with the greatest value. Press Accept to save the settings. Test the changes
before starting the analyzer for on-line measurements.
7.8.4 Adaptation of algorithms

Menu path:
→ F5 → Software → Algorithms
Settings for algorithms are configured in the AppliTek lab with standard solutions.
Depending on the problems that occur in the field, other settings need to be adapted.
For more information about the algorithm settings, refer to the Configuration Manual.
7.9 Start-up the analyzer for on-line measurement
The analyzer is now set-up and ready to go online. Make sure all analyzer components are
working properly and all settings are correct before the analyzer is started.
36
8. Maintenance
Task Daily Weekly Monthly Quarterly Annually
Check for leaks and abnormal
X X X X X
conditions
Check for alarms X X X X X
Prepare reagents and fill the
X X X
reagent containers
Run the calibration program (X) (X) X
Replace all peristaltic pump
X X
tubing
Replace the pH electrode X
Replace the duckbills of the
X
micropumps
Replace valve and piston of the
X
dispensers
Replace all pinch valve tubing X
Perform a regular inspection of the analyzer to ensure proper performance.
8.1 Check for leaks and abnormal conditions
It is recommended that the instrument and preconditioning system is inspected visually on a

regular basis in order to guarantee the correct functioning of the system and to check the
integrity of the output.
• Check for alarms on the instrument display

• Check all the components in the analysis compartment, the outside connectors and tubings
for leaks.
• Confirm sample flow by checking the constant delivery of the sample
• Check the liquid levels in the reagent and standard solution containers
• Check if all the components in the analyzer cabinet are functioning (pumps, valves,
dispensers, photometer/electrode and stirrer). The photometer/electrode can be checked
by checking if the measurement values are normal. If not, double-check by performing a
calibration.
• Check the air pressure.
8.2 Check for alarms
Check the alarm page on the touch screen PC for alarms.
8.3 Prepare reagents and fill the reagent containers
Use reagents supplied by AppliTek or a qualified company or prepare them yourself by

following the instructions in chapter 6. Refill the reagent containers with the fresh made
reagents or use supplied reagents. Make sure that the tubings reach the bottom of the
reagent containers.
Never pour the fresh reagents in containers with old reagents! Dispose the old
reagents before pouring new reagent into its specific container.
37
8.4 Replace duckbills
• Open the electrical cabinet of the analyzer.

• Disconnect the micropump and remove the old duckbill valves. Keep in mind their original
position.
• Place the new duckbill valves in the same position as the previous duckbills. Be careful the
duckbills are tightened well when reconnecting the micropump.
8.5 Run the calibration program
Refer to chapter 7.4 if analysis results are not as expected.
8.6 Run the cleaning program
Refer to chapter 7.5 to perform a manual cleaning.

Refer to chapter 7.3 to program the automatic cleaning procedure.
8.7 Replacement of the peristaltic pump tubing
• Unfasten the wingnuts that fix the peristaltic pumps onto the electric motor coupler.
• Remove the pump head.
• Separate the front pump half from the back half. Hold the pump axle and the back pump
half together (1a).
• Remove the tubing. Keep in mind the length of both endings coming out of the pump head.
• Cut new tubing of the same size at the same length of the old one.
• Assemble the tube in the exact same way the old one was placed and push it down the
back pump half in front of the pump axle rollers. Then twist the pump axle a bit while you
keep pushing the tubing down so it is pressed between the pump housing and the pump
axle rollers (1b +1c).
• Join the two pump halves and make sure the tubing is not squeezed between the two
halves (1d).
• Place back the pump head and align the pump axle with the motor axle by pushing it
against the motor axle while turning the pump axle with a screwdriver.
• Fasten the wingnuts.
• Activate the pump and check if it is running properly.
38
8.8 Replace dispenser piston
• Flush the dispenser piston with DI water (to remove the reagent
• Empty the dispenser.
• Put the dispenser in the middle position (first fill and then dose 2.5 ml).
• Remove the piston pin at the base.
• Carefully unscrew the piston from the luer lock fitting while pulling down slowly.
• Replace the old piston with a new one. Screw the piston onto the fitting while pushing
upwards slightly.
8.9 Replace dispenser valve
• Clean the dispenser with DI water (to remove the reagent).

• Fill the dispenser with air (remove the DI water).
• Power down the analyzer.
• Remove tubing and piston.
• Remove the valve by loosening the two screws on the valve.
• Install the new valve by aligning the D-coupler on the valve stem with the D-hole in
the encoder.
• Rotate the valve body so that the luer lock fitting is oriented towards the bottom of the
pump.
• Gently put the valve in place ensuring the locating pins on the frame side of the valve
body in the holes and replace the screws.
• Power up the analyzer and refill the dispenser with reagent.
• Start the analyzer and check for leaks.
39
8.10 pH electrode maintenance
Electrode preparation
The electrode is delivered ready for use. Please check visually for broken parts. For
electrodes with detachable cable connect electrode head with cable connector by twisting
clockwise. Connect other end with the pH meter. Next remove the wetting cap and rinse with
distilled water. Eliminate any air bubbles inside the glass membrane space (internal
reference electrolyte) by smoothly shaking the unit in the vertical plane (as for a fever
thermometer). The electrode is now ready for calibration. Please follow the calibration
procedure, described in chapter 4.4. After calibration the electrode is ready for measurement.
Practical hint: After rinsing do not rub the glass membrane, since this can increase response
time or damage the electrode.
Electrode storage
Rinse or clean the electrode after use and replace the wetting cap, partly filled (1/3) with
reference electrolyte.
Electrode Refilling
Open the safety cap of the filling hole. Refill the electrode with the recommend reference
electrolyte, if necessary. The electrolyte level of a correctly filled electrode is approximately
10 mm below the filling hole.
Replacement of the pH electrode
Each sensing module will last approximately six months with normal laboratory use, but the
actual lifespan of the sensing module will depend on the type of samples that the electrode is
used in.
In time, the electrode slope will decrease and readings will start to drift, indicating that the
module should be changed. Make sure that the difficulties are only or in fact caused by the
sensing module before replacing it.
Every electrode is application specific. For detailed information refer to the application
manual of the electrode.
8.11 Shutdown of the analyzer for a longer period
If the analyzer is stopped for a longer period (more than 3 days), it is recommended to rinse
the sample tubing, the reagent tubing, the dispensers and the analysis vessel with de-
mineralized water or a cleaning solution. In order to increase the lifetime of the electrodes, it
is recommended to take out the electrodes and store them with the original electrode cap. To
prevent evaporation of the electrolyte in the electrode, the electrode cap has to be filled with
electrolyte. Storage of the electrodes in de-mineralized water will significantly decrease the
lifetime of the electrodes.
40
9. Troubleshooting
If analysis results are unstable the following items should be checked:
a) Micropumps: make sure the reagents are dosed correctly and that no air is present in the
tubings
b) Peristaltic pumps: check if the drain and sample pump are working correctly
c) Valves: make sure the sample/Validation/Rinse/Clean valves are working correctly

make sure the drain/level valve is working correctly
d) Stirrer: check if there is a magnetic stirrer bar in the analysis vessel and if the solution is
stirred during analysis
e) Dispenser: Make sure the dispenser piston is filled with liquid and that no air is present in
the tubings
f) Check the positioning of the tubings inside the analysis vessel

• The tubing from the dispenser (HCl) should be positioned in the liquid after leveling
• Other tubings should be positioned above the liquid level.
g) Check the reagents. Prepare a new set of reagents when the reagent containers are
empty. Flush/Prime all tubing before performing a measurement.
h) Check the electrode.
10. Spare Parts

See Material Date Sheet with corresponding analyzer serial number.
41
Addendum 1: Analysis Procedure
Remark:
Adjustments to the methods are made in the METHOD (F4) menu. We recommend you to
read the ‘Configuration Manual’ carefully before making adjustments to the method: the
functioning of the analyzer may be disturbed.
1.1 Alkalinity Method – Analysis
Streamselection Channel DO
Channel 1 SV STR1
Channel 2 SV STR2
Channel 8 Validation (Validation)
Nr Step Name Interval Volume Pulses

1 PROGMOD4: analysis
2 Streamselection ON 1000 ms
3 HCl Fill 1s
4 Drain Group 16000 ms
5 SP CW ON 50 ms
6 DP CCW ON 50 ms
7 Flushing M Alk Variable: Flushing
8 SP CW OFF 50 ms
9 Waiting 5s
10 DP CCW OFF 50 ms
11 Sample Group 13000 ms
14 Waiting 3s
15 Drain/Level ON 50 ms
16 Level Group 11000 ms
17 Drain/Level OFF 50 ms
18 Streamselection OFF 50 ms
19 Stirrer ON 50 ms
20 pH Meas. 5s
21 Algorithm M Alk 1800 s
22 Waiting 1s
23 Algorithm check Calc. 1s
24 pH Calc. 1s
25 ml infl. pH 4.5 Calc. 1s
26 CaCO3 Calc. 1s
27 Write to database 1s
29 Rinse Group 11000 ms
32 Waiting Variable: Waiting
42
33 Sub procedure 1000 0s
34 CaCO3 Calc. 1s
36 Streamselection OFF 50 ms
39 Waiting 1s
1.2 Method Alkalinity – Cleaning (optional)

41 PROGMOD3: Cleaning
42 Clean ON 50 ms
43 DP CCW ON 50 ms
44 SP CW Interval 10 s
45 Waiting 3s
46 DP CCW OFF 50 ms
50 Stirrer ON 50 ms
51 Waiting 60 s
52 Stirrer OFF 50 ms
54 Clean OFF 50 ms
59 Waiting 1s
1.3 Method Alkalinity– Priming (optional)

60 PROGMOD3: Cleaning
61 DP CCW ON 50 ms
62 HCl Fill 35 s
63 HCl Empty 35 s
64 HCl Fill 35 s
65 HCl Empty 35 s
66 Waiting 5s
67 DP CCW OFF 50 ms
71 Waiting 1s
43
Addendum 2: Analyzer Configuration
See also ‘Material Date Sheet’ with corresponding analyzer serial number.
Software V 3.06.70
2.1 Digital Outputs
Nr Name
1 SP CW
2 SP CCW
3 DP CW
4 DP CCW
6 Drain/Level
7 Stirrer
12 Validation
14 Clean
15 Rinse
16 Sample
21 SV STR1
22 SV STR2
25 Malfunction
2.2 Digital Inputs
Nr Name
1 Air pressure
2 INP2
3 INP3
4 INP4
2.3 Analog Inputs
Nr Name
1 pH
2.4 Analog Outputs
Nr Name
1 Result Alkalinity STR1
2 Result Alkalinity STR2
2.5 Constants
Nr Name Value
1 SV (ml) 25
2 Conc HCl (M) 0,010
3 MW CaCO3 (g/mol) 100
44
2.6 Dispensers
Nr Name Speed Steps Volume

1 HCl 45 6000 10
2.7 Results
Nr Name Unit
1 ml infl. pH 4.5 ml
2 CaCO3-M Alk mg/L
3 Algorithm check N.A.
4 pH N.A.
2.8 Results Calculation
ml Infl. pH 4.5
1 M2 End of calculation
Algorithm check
1 IF M-Alarm2 = 1 THEN GOTO R3
2 0 End of calculation
3 IF 0 = 0 THEN goto subprocedure 1000
4 1 End of calculation
CaCO₃
1 M2 * Conc. HCl (M)
2 R1 * 50000
3 R2 / SV (ml)
4 R3 End of calculation
pH
1 M1 End of calculation
2.9 Results Analog output
Result Channel Analog output Value 4mA Value 20mA

Alkalinity 1 Result Alkalinity STR1 0 200
Alkalinity 1 Result Alkalinity STR2 0 200
2.10 Result Alarms
Result Channel Low value High value

pH 0 0 14
EP pH 4.5 0 0 20
Alkalinity 0 0 1000
45
2.11 Results Graph
Result Channel Low value High value

pH 0 0 14
EP pH 4.5 0 0 20
Alkalinity 0 0 1000
2.12 Algorithms
Name: M Alk
Sensor: pH
Pauze
Pauze drift: 0
Pauze Max time: 0
Pauze Min time: 0
Initial dosing
Init steps: 3
Init time: 5
Init Volume: 0,1
Init Speed: 350
Dynamic dosing
Dyn. slope: 0.1
Dyn. speed: 350
Dyn. refill speed: 300
Dyn. min step: 0.05
Dyn. max step: 0.200
Dyn. min time: 5
Dyn. max time: 5
Dyn. drift: 0
Dyn. nr of points: 5
EP minimum: 0,05
EP peak: 2
EP filter: 6
EP threshold: 50
EP1
M-position: 11
Value 4.5
Stop
Stop volume (ml) 15
Stop at measured value: 4.3
Drift: 0
Number of EP: 1
Dosed volume after EP: 0.1
Stop time: 1800
Graph
46
Graph Low: 0
Graph High: 3000
2.13 Alarm and message table
Nr Type Apply Function Message Reset

0 None Global Emergency stop E-stop/Reinitialize the dispensers ! Automatic
1 Alarm Global DispenserHCl Dispenser HCl error Automatic
2 Alarm Global SensorpH Sensor pH error Automatic
3 Alarm Global Titration algorithmM Alk Titration Alkalinity error Automatic
4 Alarm Global M-Alarmml infl. pH 4.5 Inflection point Alkalinity not found Automatic
2.14 Group DO
Action DO1 Status DO2 Status Time (ms)

Sample 1 SP CW On Stirrer Off 3000
2 SP CW On Stirrer On 9000
Drain 1 DP CCW On Stirrer On 5000
2 DP CCW On Stirrer Off 10000
Level 1 Drain/Level Continue Stirrer Off 100
2 DP CCW On off 10000
Rinse 1 SP CW On Stirrer Off 2000
2 SP CW On Stirrer On 8000
47
Addendum 3: Alarms and signals
3.1 Alarms
Introduction
All alarms are implemented as follows:
• Closed contact: the alarm is off and the Analyzer is On-line

• Open contact: the alarm is active
Alarm list
• Malfunctioning alarm:
Every alarm activates the malfunctioning alarm output (contact is opened).
o Emergency stop
When the emergency stop is activated, the analyzer shall stop immediately.
o Sensor
When there is a problem with one of the sensors, the malfunctioning alarm is
activated. A massage appears in the message or history submenu.
o Titration alarm
When there is a problem during the titration (titration out of time, no inflection
points detected…) the malfunctioning alarm is activated. A massage appears in
the message or history submenu.
• Maintenance alarm:
When the maintenance mode is active after pressing the MAINTENANCE ON/OFF
button, a digital output is activated (maintenance contact is opened) to indicate
remotely that the analyzer is not running on-line. When the maintenance mode is
active, the analyzer is always in the local control mode: the analyzer can only be
started manually.
3.2 Signals
The standard signal is an active 4-20 mA signal.
RS232/MODBUS are optional, but can be programmed and used if the proper remote IO is
installed.
48
Warranty
1. Warranties
AppliTek NV/SA warrants that its products are free from defects in materials and workmanship (under
normal conditions of use and service) for a period one (1) year from date of shipment to original
purchaser.
2. Limited warranty and liability

On principle, the “General terms of and conditions of sale and delivery” of the company AppliTek
apply. All warranty and liability claims made for damage to persons or property are invalid when they
prove to have as a cause one or more of the following:
• Operating the unit for reasons other than its designed purpose
• Improper assembly, initializing, operating or maintenance of the unit
• Operating the unit when any safety or protection devices are defect or non-functioning
• Non-adherence of any instruction in the operating manual
• Unauthorized constructional alterations to the measuring unit
• Unauthorized constructional alterations to the utilities (for example instrument air supply).
• Incorrect maintenance of unit components
• Maintenance and repair work improperly carried out
• Catastrophes caused by outside interference, natural disaster, labor unrest, acts of war,
terrorism, civil strife or acts of any governmental jurisdiction.
Warranty also does not cover:

Freight charges on expedited or express shipment of warranted parts or product
Travel fees associated with on-site warranty repair
3. Inspection and claims

Claims for damage in shipment must be filed immediately with delivering carrier. Claims for shortages,
shipping errors or any claim that the goods do not conform with the terms of the contract must be
submitted to the AppliTek NV/SA in writing within five (5) days of receipt. If buyer fails to comply with
the term ‘within 5 days of receipt’, the goods shall be deemed to conform with contract terms, and
buyer shall accept and pay for the goods in accordance with the contract. Buyer waives any right to
revoke acceptance after such five days period. All claims must be accompanied by a copy of the
shipment note.
4. Indemnity for products manufactured according to customer’s requirements

In the event AppliTek NV/SA provides products in accordance with drawings, models or samples
provided by the customer, customer shall indemnify AppliTek NV/SA from any liability, cost or expense
suffered by AppliTek NV/SA as a result of the violation of any law or regulation or the infringement of
any industrial property right or other right of third parties.
5. Notification of product hazards and recall of products

Customer will inform AppliTek NV/SA immediately in writing about any events which indicate any
hazards connected with the product. Upon written notice of the AppliTek NV/SA about hazards in
connection with the products or unfitness for use of the products and recall of products, the customer
will immediately cease using the products for any reason, the customer, as its sole remedy shall be
entitled compensation equivalent to the current value of the used product, but in no event more than
the purchase price. AppliTek NV/SA shall not be liable for buyer’s loss of profit or incidental
consequential or special damages of any kind.
49

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SOHAR IWP

Contract nº: Purchase order Nº

Description SPECIAL ANALYZERS

Document type: Equipments/ TAGS Nº

MAN AIT-L1L08-04, AIT-L1L08-14

Purchaser Document number Title Rev

REVIEW RESPONSIBLE PURCHASER

Vendor Logo Vendor Document Document Title: Rev: 02

(1) Purchase order nº as shown on purchase order

Serial number: 012.1090.1704.048

© 2014 – AppliTek NV – Printed in Belgium

General safety instructions

1.1 Dimensions of the analyzer

Other points of attention are: - humidity: 5 – 95 % non-condensing

1.3 Mounting instructions

This analyzer has to be installed by qualified technical personnel to ensure adherence

- The protective ground at the yellow/green terminal block.

Terminal North American wire color European wire color

External 24Vdc power supply

AO1-AO2: Analog Outputs

FCT1-FCT5: Free ConTacts

PCT1-PCT4: Power ConTacts

Consumption/ Consumption/28 days

3.2 Sample feed

Connection: 1/4” OD tubing (PFA)

Drain piping: recommended diameter of 32 mm

3.4 Rinse feed

Connection: 1/4” OD tubing (PFA)

Connection: 1/4” OD tubing (PFA)

3.6 Reagents & Calibration/validation solutions feed

Connection: 1/8” OD tubing

Remark : Reagents are not supplied for start-up and commissioning.

Connection: 1/4” OD tubing (PFA)

Initial startup screen MAIN screen

4.1 Analyzer design

Press the stirrer icon. Switch the stirrer

The drain/level valve is used in combination

When the drain pump is started and the

Press the pump icon. Switch the pump

The ‘Group’ function is implemented for

Press the valve icon. Activate/deactivate the

When the pinch valve and the drain pump

The sample pump is used in combination with

Press the pump icon. Switch the pump

The ‘Group’ function is linked to a group

Next, press the sample pump and start the

Press the dispenser icon.

Press the pump icon. Switch the pump

The ‘Group’ function is implemented for

Select the digital output by use of the Edit

The value of the digital output can be toggled

Press ‘Stop’ to stop any action of the DO.

Press ‘Back’ to quit the screen.

4.3 Analog output

Press the EDIT (E) button to control the

Use a multimeter to check if the analog

Check if this value corresponds to the value

Check the ‘Installation Manual’ to make the

4.4 Analog input

Check if all analog inputs are responding

Press the EDIT (E) button to control the

Calibration is performed in buffer solutions

- Press enter to start calibration

Method: Titration (pH electrode) – End point titration