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Raw Materials Experiment Test
Raw Materials Experiment Test
with the proportions of materials in each particle size chosen based on the population balance granulation
model. The uniaxial compression method and direct shear method were applied to measure the tensile
strength and shear strength of the adhering layer tablets. Then the loss of bed voidage due to the adhering
layer deformation was evaluated quantitatively.
EXPERIMENTAL
Raw materials
To get representative raw materials to simulate the adhering layer of granules for a typical sinter blend, four
iron ores were blended with flux, coke and return fines to achieve the target blend chemistry. Table 1 gives
the target chemistry of the blend and the related composition of all components of each blend is reported in
Table 2. A total of approximately 13 kg of each blend was dried in an oven at 105 °C overnight and then
screened into 13 size fractions using a standard ro-tap sieve shaker.
In Litster’s granulation model, a parameter called the partition coefficient for each size fraction, ∂ i , is defined
according to Equation 1 below (Waters et al. 1989). The partition coefficient ranges from 0 to 1, representing
the mass fraction of particles in the ith size fraction that act as nuclei during granulation. Figure 1 shows the
measured partition curves for ore blend Y under different granulation moisture conditions. It can be seen that
more intermediate particles would embed in the adhering layer with increasing granulation moisture.
m +m
∂ i = ii n ii +1
∑ mij
(1)
j =1
where mij is the mass of particles of ith size fraction found in granules of jth size fraction.
In the present study, 7 size intervals were chosen to simulate the adhering layer of granules in a sinter bed,
i.e., -0.25 mm, 0.25-0.355 mm, 0.355-0.5 mm, 0.5-0.71 mm, 0.71-1 mm, 1-1.4 mm and 1.4-2 mm particle
size. For a typical blend and moisture condition, the mass percent of each size interval used in making
tablets was calculated from the measured dry size distribution and the measured partition coefficient values.
100 g of particles in the 7 size intervals were weighed and mixed manually, then further wetted with the
target amount of water to get the experimental moisture content. Then these particles were charged into the
specially designed cylinder or shear cell to measure their strength by the following uniaxial compression
method and direct shear test method.