TOCYJAPCTBEHHBI CTAHJIAPT PECIYBJIMKH KA3AXCTAH Meron onpesexenus KMHeMaTHYeCKOH BASKOCTH MpOspayHElx M HeNpOSpAayHEAX. sxWIKoCTeit (pacueT AMHAMHIeCKOH BASKOCTH) CT PK ACTM J 445-2011 ASTM D 445:2011 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity) (IDT) ananne ofpuunanenoe Aannoxit rocyaapersennoni cranaapt KasluCr ocuopan ua ASTM D 445:2011 «Standard ‘Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)», astopexoe mpaso npananieanT ACTM Murepremnen, 100 Bapp Xap6op pain, Bec Kouexten, Ulrat Muncenspanus, 19428, CUIA, Mepensaaeres ¢ paspenennem ACTM Hurrepnemmes. Komurer rexumseckoro perysmposanus a MeTpostorHn Munucrepersa muaycTpHl H HoBBIx TexHoaormii PecnyOamKu Kasaxcran (Toceransapr) AcranaCT PK ACTM 11 445-2011 Tpeaucaosue 1 NOATOTOBIEH HM BHECEH PII «Kasaxcranckuit wnereryr cranaaprasannn 1 cepruduxanniny x TOO «Kaz Business Solutions». 2 YTBEPAKIEH HM BBEJEH B JEMCTBHE Tpuxasom Mpeacenarenx Kowurera ‘TeXHHYECKOTO perysTHPOBAHHS H MeTPOIOTHH MHHHCTepCTBA HHAYCTPHH H HOBEIX TexHONOTHii Pecny6anxn Kasaxcran or «12» anrycra 2011 roga Ne 411-07. 3 Hacroammii cranzapr ugentayen ASTM D 445:2011 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity) (Meroy onpesenenus KuHeMaTH4ecKol BsSKOCTH NpospavIx K HeMpospasbM xHAKOCTEH (pacuer AMHaMMdeckoii BASKOCTH), ABTOPCKOe MpaBo MpHHaanexuT ACTM MxtepHemmen, 100 Bapp XapGop JIpaiin, Becr Kouexmen, Uirar Munceusnanus, 19428, CLA. Tepesanaeres ¢ paspemennen ACTM Mutepremien. ASTM D_ 445:2011 paspaGoran nokomuretom D02.07 Kownrera ASTM D02 «Hebrenposyxrt a emasounse MaTepHarteD>. B pasjene «Hopmarasnsie ccbuik H TeKcTe cTaHapra CCbUIOBIe MexyyHAposHDIe cranaapras axtyaausupoparisl, Tlepenoy ¢ atirsuticxoro sauiKa (en). Crenens coorsererans — nnentias (IDT). 4 CPOK NIEPBOM N1POBEPKH 2016 rox MEPHOJM4HOCTE MPOBEPKH Saer 5 BBEEH B3AMEH CT PK HCO 3104-2008 Huopmayun 06 usmenenuax x nacmonyeny cmandapmy nybruxyemca @ eocez0du0 wsOasaenon unbopmayuonnom ykasamene «Hopmamuantie doxymenme no cmandapmusayuu», @ mexcm usmenenuit u nonpasox - 6 ecemecauno usdasaeMbrx uniopmayuonnex ykasamensx «ocydapcmaennsie cmandapmeiy. B cayyae nepecmompa (samen!) wiu ommenes wacmosuyezo cmandapma coomsemcmaywoyee yaedourenue Gydem ony61uKosano 6 ewcemecnuno usdasaemon unipopayuonnom yasamene «IocyOapemsenneie cmaxdapme.» Hacrosuusii cranaapr He MOxkeT GkIT MOMMOCTSIO WK YACTHUHO BocnpoHsBeneH, ‘THpaKMpOBAH H pacnpocrpanien B KavecTBe O*pHUANEHOTO HsAaHHs Ges paspemensix KommTera ‘TexHMecKoro perysupoBaHua u MeTponorMu MuHucTepcTsa MAAYCTPHH UM HOBEIX TexHOmOrHit Pecny6mmn Kasaxerant 1CT PK ACTM 11 445-2011 TOCYJAPCTBEHHBIM CTAHJIAPT PECIYBJIMKH KA3AXCTAH Merog onpenenenus KuneMaTH4ecKoii BAIKOCTH NpOIpadHLIX M HeNpospayHEr sxWAKocTeit (pacer AMHAMHYeCKOil BASKOCTH) Hara spexenus 2012-07-01 1 OGaacte mpumenenusa Hacrosuuit crantapr yeranapnunaer MeTox onpeneseHis KHHEMATHHeCKOHt BASKOCTH, ¥, 2kUAKUX HepTENPOAYKTOR, MPOSpAYHIX HM HeNpOspAayHAX 2«AKOCTE!, NyTeM HIMepeHHA RPeMeHH cTeTeHA OGLeMa -AWJKOCTH TION nOgAeliCTRHeM CHLIM THKECTH depea TpaAyNponauuoiit CTCKIANUEI KAMMUUINpHBl BUCKOSHMETp. J[MNAMUNeCKYIO BxSKOCTD, 1] PACCHHTEIBAIOT YMHOKCHHEM HSMePeHHOH KHHEMATHICCKOH BASKOCTH V, Ha IMOTHOCTH, /, sennkocrn. TIPHMEYAHME 1 Onpexexerne xumewariecxolt nxaxocra mpospasnnax xauuKocrelt w KHNeMaTHNecKOl sraxocr# Gurrywon npusexenai 8 ASTM D 2170 x ASTM D 2171 TIPHMEYAHME 2 ISO 3104 coormeverayer nacrosuteny craniapry. Pesyimsrarsi, TONYCHHBIC HACTOSINNM CTAHAAPTOM, saBHCAT OT cHolicTB OOpasna H MpeAHASHAYCHEI {UK MPHMEHEHHS K XKHAKOCTIM, Y KOTOPSIX HAlIpHKeHHE CABHFa M CKOpOCT caBHra MponopunoHamsusl (PEM MOTOKA HsioTOHA). EciM BASKOCTS 3HAYMTE:BHO HSMCHSETCR 1B 3ABMCHMOCTH OT CKOPOCTH CIBHTa, TO Ha BHCKOSHMETpAX ¢ pasHBIMH J}HaMeTpaMH KAMHULIPOB MOTYT 6nITE TonyeHBI pasHBIe pesymétarsr. [pouexypa MpOBMACHHA UCTBITAHMS H 3HAICHAS TOSHOCTH BKTMOYIOT ONpENeTeHHe KHHEMATHYECKOH BISKOCTH H IHAYeHHH npeNHsHOHKOCTH JUS OCTATOSHBIX AHAKAX TOILIHB, KOTOPBIC B TEX 2K€ CAMBIX YCHOBHEX OCHAPYAHBAOT cROlicTBA HeHBIOTOHORCKHX 2kH,TKOCTEI. Auanason KunemarH4ecKoi BaSKOCTH, OxBaveHHbIM HACTOSIILAM CraHaproM, cocramsseT or 2 mw/c 70 300000 mar/c (cm Ta6n. Al.1) mpH Bcex Temmepatypax no 6.3 n 6.4. TipenuswonHocrs MoxeT GsiTh OnpemeneHa TOMBKO AIX Tex MpoayKTOB, KHHEMATHYeCKAS BASKOCTS H TeMMepatypa KOTOPBIX HAXONATCS B [HaNasOHaX, MPHBCHEHABKX B Payee 17. 3uayeHns, ycTaHoBieHHBe B enMAMuax CH, AOKHBI CUMTATBCA CTaHAapTHEIMH, Eguuuueii CH, ucrompsyemoi B HacTosiem MeTone ucmBITaHHii gna KuHeMaTHuecKoli BASKOCTH, sBaeTcA MM’/c H cauHALeK CH, HcrombsyeMoH B HaCTOSIIeM MeTONe HembITaHHit Aa MHammaeckoi © Ba3KocTH, sBaaetca Milac. [na cCBIIKM = Tomb30BaTent Tmat/e = 10% w/e = 1 cCra 1 Mllac = 1 cll = 0,001 Mare. TIPMMEYAHVE Pryrs onperexena wniormwn nexoNcTaanst Kak onactiait MaTepiian, KoTOpui MoxeT "pupecrit x nompeactemmio Heurpancuol nepaol cuCTeNL, NOWEK H NeveN, Pryrb HaH ee Henapeua MOryT Orb OMACHBIMH JIM 310POBLK K KOPPOMPYWOWHMM JUL MarepHaton. Culeayet CoGmOJaTb Mepbi IpeOcTopoxHOCTH "MpH Obpantenste pryTBio H TpORYKTaNGE, cOnepIKAIIUING PT. Hactosmmtit cranjapr He mpeqHasHaveH gna Bcero, 4TO KacaeTca GesorlacHOcTH, ecm TONBKO 3TO He cBsBAHO C ero McHOMOBANMeM. TloX OTBETCTBCHKOCTHIO MoMKSOBaTeNS HACTOMeTO CTAHMApTa, YcTAHOBHTs HEOGXOAHMYIO GesONACHOCTh HM MHCTPYKUMH 10 SMpaBooxpaxeHMio, HM ONDeyeNNTs MPUMeHMMOCTE perysMpyrOMMe orpamwseHHx 0 ero eHOMBaOBaHtAs. 2 Hopmarupnise cena Jax mpymenenus wactommero cranjapra HeoGXonHMEI crenyIoMHe ccsLIONHBTe HOpMaTHBHBIe AOKYMeHTEI: Wananne opanuansoeCT PK ACTM 1445-2011 CT PK 1.9-2007 Tocynapernennas cucrema TexnHueckoro perynmponanna PecryGnnKH Kasaxcran, Tlopaaox mpuMenena MexayHaponHBix, perHonamDHBIX HM HaLKOHaTbHBIX CTAHJapTOR HHOCTPAHHKX FocyapCTs, APYTHX HOPMATHBHBIX AOKYMeHTOB 110 CTaHapTHsaMHH » PecnyOmmxe Kasaxcran. ASTM D 446-07* Standard Specifications and Operating Instructions for Glass Capillary Kinematic Viscometers (Crenmuxanun # mHeTpYKUMM mo SKCrITyaTALMH JAK CTeK ASI AMIHIMISPHSIX KMHEMATHSICCKHX BHCKOSMMETPOB). ASTM D 1193-06* Standard Specification for Reagent Water (Cneunpuxauum aa peaxrupuolt noms). ASTM DI1217-93(2007)* Standard Test Method for Density and Relative Density (Specific Gravity) of Liquids by Bingham Pycnometer (Metoa ucnurranuit ua niorHocts 1 OTHOCHTENBHYIO THIOTHOCTE (yAesBHYIO Macy) aHKOCTeH NMKHOMeTpOM BuHreMa). ASTM D1480-07* Standard Test Method for Density and Relative Density (Specific Gravity) of Viscous Materials by Bingham Pycnometer (Mero uenrranuii wa mioTHOCTS 1 OTHOCHTeNBHYIO MLIOTHOCTS (ysIeMBHYIO MMIOTHOCTS) BAIKUX MaTEpHAsIOB MHKHOMETPOM Burena). ASTM D 1481 02(2007)* Standard Test Method for Density and Relative Density (Specific Gravity) of Viscous Materials by Lipkin Bicapillary Pycnometer (Merox nemsrramnit Ha THOTHOCTS M OTHOCHTEMBHYIO THIOTHOCTS (YAENBHYIO TOTHOCTS) BAIKIX MaTepHATOR Gukamasuispinim nuxtomerpom Jhamsta), ASTM D 2162-06* Standard Practice for Basic Calibration of Master Viscometers and Viscosity Oil Standards (IIpaxruxa 110 ocHoBHO# KaTH6poBke KOHTPOMIBHBIX BHCKOSHMETPOB It crangapton masKux macen). ASTM D 2170-10/D2170M* Standard Test Method for Kinematic Viscosity of Asphalts (Bitumens) (Meron nemsrrannii Ha knnemaTHueckyIo BsaKOCTe accbanuToR (6uTyMOR). ASTM D 2171-10* Standard Test Method for Viscosity of Asphalts by Vacuum Capillary Viscometer (Meron HemBraxnii Ha KHHeMaTHYeCKyl0 BASKOCTS acibaNbTOB BakyyMHBIM KAMMILISpHEIM BHCKOSHMETPOM). ASTM D 6071-06* Standard Test Method for Low Level Sodium in High Purity Water by Graphite Furnace Atomic Absorption Spectroscopy (Merox wemsrranuii ax ompenenenus HHSKOTO YPOBHS HATPHA B BORE BKICOKOH IHCTOTH C TOMOMTEIO CTeEKTPOCKOMHH aTOMHOTO nloraomenus ¢ rpaipuronoii 1e4610). ASTM D 6074 08* Standard Guide for Characterizing Hydrocarbon Lubricant Base Oils (CnpasosHHKk 10 xapakTepHCTHKaM yrieBOOPOAHBIX CMa304HBIX 6a30BBIX Macell). ASTM D 6299-10e1* Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance (fIpaxraxa 10 MpwMeneHmo craTHCTHHeCKHX MeTO/OB TapaNTHH KaecTBa HM MCTOROB KOHTPOUBHBIX KapT JULM OUeHKH XapakTepHCTHK auANMTHYeCKOlL cHcTeMBI HaMepeHtt). ASTM D6617-08 Standard Practice for Laboratory Bias Detection Using Single Test Result from Standard Material (IIpaxraxa no xaGoparopHomy onpenentcumo cucremarHiecKoit orpeuiHOCTH, HcHOmbaya pesysIbTaT OTAEMBHOTO HCHMTAKHS 13 CTaHAapTHOrO MarepHalta). ASTM E1-07* Standard Specification for ASTM Liquid in Glass Thermometers (Cneundukanns ana crexnamebix xnsiKkocTHBIx TepMomerpos ASTM). ASTM E 77-07* Standard Test Method for Inspection and Verification of Thermometers (Meroy nemurrannit u1x Koutpons # nponepxx TepmoMerpos). ISO 3104:1994* Petroleum products — Transparent and opaque liquids -- Determination of kinematic viscosity and calculation of dynamic viscosity (He(renpoxykrst. Mpospasmsie Herpospastiiie 2xH1KOCTH. OntpedesleHie KUHeMaTHMecKOl BEIKOCTH H pacer AUNAMHECKOH * Tipincessercx » coornercrmum ¢ CT PK 1.9 2CT PK ACTM 11 445-2011 ‘BasKocTH). ISO 3105:1994* Glass capillary kinematic viscometers -- Specifications and operating instructions (BuckOsHMeTpA CTEKINHHBIE KANIMIAPHBIe JUIA OMpeeNeHHs KKNeMATHYECKOH BaSKOCTH, TEXHHYeCKHe YCTOBHK H MHCTPYKUHH 110 9KCTLTyaTANH). ISO 3696:1987* Water for analytical laboratory use -- Specification and test methods (Boxa gua xa6oparopuoro anannsa. Texnmrieckue rpeGonanns a Meroe HemBrratsuii). ISO 5725 (ace vacra)* Accuracy (trueness and precision) of measurement methods and results (Tounocrs (mpaniitaiiocTs 1 mpeuuaHOHHOCTs) MeTOOR H peaysibraroR HaMepeHii). TSO 9000:2005* Quality management systems -- Fundamentals and vocabulary (Cranmaprst 10 MeHeZKMeHTY KavecTBa H TapaHTHH KavecTBa. PyKOBO,SIIMe TIpHHUMMTst oruocurenbiio siiGopa HcTIOMEI0BaNHs), ISO 17025:2005* General requirements for the competence of testing and calibration laboratories (OGmme TpeGonanHx K KOMMETeHTHOCTH HCTBITATeBHEIX H KAsIHOPOBOMEIEIX siaGoparoputi). NIST Texrmseckoe mpumesanne 1297*, Guidelines for Evaluating and Expressing the Uncertainty of NIST Measurement Results (Pyxogoacrso no oueHKe u BBIPaxeHHIO neompeytesieunocrH peaystsraron waMepenuii NIST). NIST GMP 11* Good Measurement Practice for Assignment and Adjustment of Calibration Intervals for Laboratory Standards (O6menpunsrax mpaxruka w3MepeHMii 10 ycTaHoRICHMIO 1 PEYsINPOBKe MEXKAJINGPOBONELIX HHTepRALOB JUIX sLAGOpaTopHBIX craLaproB). NIST Cnenmansnax ny6maxanus 819* A procedure for the effective recalibration of liquid-in-glass thermometers (Pykonogcrao no oKCILIyaTaNNH MexayHapoqHoli cucTemBi exam (CH). TIPHMEYAHHE TIpu nomssosanuu Hacromman crartaprom uenecooGpasHo mposepurs aelicrawe COBLIOMHKIX CTUHAPTOB MO CKCTOTHO WIABACMOMY HACPOPMaIIHOHHOMY ykasaremo «HOpMaTHBHBIe AOKYMCHTSI MO CTaNIapTinayHio 110 COCTOSMINO Ha TeKYUMH TOR M COOTBETCTBYIOMINM exeMeCsTIHO HaIABAeMEM uudopwanuonmim yxasareniM, onyGuKosanMuM 8 TexyuleM roxy. EciM ccsuiowuill noKyMeHT saneueH (wanexex), TO PH MONKSORAMMM ACTOR CTaHlapTOM cieAYET PYKOBOACTHOBETHCR aAMENEHTIKIM (wamenensium) noxymenrou, Eoan ccnmtoum JoKyMenT onMetien Ge3 3aMetIL, TO NOLOXEHHE, B KOTOPOM JANA (Conta Ha Hero, npumexterca B aCTH, He sarparumarouiell sTy ecuLaKy. 3 Tepmunut « onpenenenmst B wactosmem craujapre mpumeusiores cienylolue TepMHHL ¢ cOOTBETCTByIONIMMH ompeeeHnan 3.1 Apromaraeckuii nuckosHMerp (automated viscometer) — MpxGop, Koropssit NAaCTHYHO WIM MOJHOCTHIO MeXaHHSHPOBA OAMH WIM HECKONKO 9TalloB Mpouemypst, oGosravermx B Pasene 11 nm 12 6e3 HIMCHCHHS NpHHTMTA HIM MeTONA OCHOBHOTO pysHOrO mpuGopa. Bwxubie smeMeHTst mpuGopa OTHOCHTeMbHO pasMepoB, KOHCTPYKUMM 1 KCILIYaTANMOHHBIX XapakTepHCTHK TaKHe KE, KAK H IPH Py'4HOM MeTO/Ie. TIPMMEYAHVE Anrowarieckie HCKOSNMeTplt HMCIOT BOMOXHOCTA MORETHPORANS TeKOTOPAIE conepanuili Merona HeMErraKMs no Mepe COxPAIHIIX HI HewesttoneHiX HeOGXOREMOCTH PYSHOTO RMEHIATEMCTBA ‘WM MuTepnpeTanmH. 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B bree omen ewrtene, KintewariciecKaa nxxKoerH Mpencranraer cOBoH oTHOMeNe NEA epenavc FAYE rr coxpantenenc mamymaca, TIPAMEYAHHE 2 Jlax noroka, 1ocTymaroulero CaMOTEKOM, NO/| 34 AHHHIM THAPOCTSTHYCCKUM JaBICHHEM, ruxpoctanicexni Hanop >xEAKOCTH MPOFOpMWOHANER ee MIOTHOCTH p, CIM THOTHOCT BoxYxA smnAeTCR emararesoNoH To cPARHCHINO € TIOTHOCTO AIKOCTH. JX KAROFO-IHGO KORKPETHOTO BACKONMETPS, a xotopuii pacnpocrparinerca tacromnci MeTox wemurantti, spewn crora dukcuposartioro oGbeMa ‘xiIKOCTI "MpaMo Mponopumonato ee KHMeMaTHTecKoll BAAKOCTH V, TEV 1Vp Hy ARUACTES INHANGTECKOH BEOCTHIO, 4 Cyumocre Merona 4.1 Cynuocrs Merona sakioyaeres B MSMepeHMM KAIHOPOBAKIIM creKmHIIbIM BHCKOSHMCTPOM BPEMCHH VCTEHCHHE, B CEKYHAAX, OMpenereHHOTO OOKeMA uCTEITYeMOit {AWJIKOCTH TOK BIMAHHEM CHIBI THKECTH MpH NOCrosHHOl Temmeparype. 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JhoGoli suckosumerp, yerpolicrao jnx waMepeHHA TeMtteparypst, TepMOPErYAATOP, BANA C PerysINPOBANHEM TeMIIePATypsI HLT CHETIHK BPEMCHH, BXOMAINHC B ABTOMATHECKYIO YCTAHOBKY, OKHBI COOTHETCTBOBATH TPeGOBAHHAM JUIK AAHHBIX SNeMeHTOB, KaK yoranoneno B Pasyese 6 uacrosmero Merona Honbrranus. JJonyeKactex wpems ucreyenHs mene 200 c, TeM He MeHee, B cooTBereTBHH c Pasqen0M 7 TIO pacieTy KHHEMATHYECKOii asakocta ASTM D 446 zomiuo npumenstaca ucnpanicHe KueTiecKoii aHeprun, TlonpapKa a KHHeTHeCKyIO IHeprio (KoxhhULMEHT cKOpOCTHOTO Harropa) He LODKHA MpenEIMATs 3,0 % OT H3MepeHHOit Ba3KOCTH. ABTOMATHYECKag YCTAHOBKa 7OWKHA OBITS cMOCOGHA oMpesenaTs KUHEMATHMIECKYIO BSIKOCT MPHSHANHOTO GTaLOHa BABKOCTH B PAMKAX, YeraHOBNeHHLKX B 9.2.1 a Pasgene 17, Tosnocrs owKHa GBT CTaTHCTHYeCKH 9KBHBANCHTHA TOWHOCTH pysHOli YoTAHOBKH 11H MpeHOCKOAHTS ce (HMETS MEHBIIYIO KSMEH"HBOCTE). MIPHMEYAHHE Toxoers u cnctewanmeckas rorpentoerb iswepemiti raniewaririecxo BASKET 2 Bpemenm wcrevenmix wenee 200 ¢ me AomaHa onpenezarscs. Henmectio HacYeT Toro, TO TONHOCTD, yeranonnenuas 8 Pasgene 17, aeiicranrenbia ja uaMepettit KuNeMaTiecKoli BEIKOCTH CO BPEMCHEM HCTEICHUS exee 200 c. 6.2 Ilrarnest ana Buckosumerpos: Jit BkmOucHHA B paGoTy BCEX BHCKOSHMCTPOB, KOTOpMe MCIOT epXHI MEHMCK HeMOcpeNCTREHHO Ha] HUXHMM MeHHCKOM, 8 TOMBCLIMBAHHA HX BepTHKATEHO B Mpenenax 1 ° Bo BCEX HAMpABNeHHsX, HCMONESYIOT INTATHDEI JU BUCKOSHMeTpOB. Te BHCKOSHMETPBI, eH BEPXHHI MEHHCK CMEIILeH HETIOCPeACTBEHHO Hal HICKHNM MeHHCKOM, JOIKHBI MOAReLIMBATECA RepTHKATEHO B Mpenemax 0,3 ° BO Bcex nanpannenax (em. ASTM D 446 x ISO 3105). 6.2.1 BHCKOSHMETpsI JOKHBI YCTAHABIMBATSCH B BAHHE TOCTOSHHOI Temmepatypst TEM 2ke cnlocoGOM, KAK H MpH KATHOPOBKe M yeraHonKe CormacHo cepracbiKary © KanHOpoBKe. CM. ASTM D 446, cm. uncrpyxuum no oKcryataumm B IIpunoxenusx Al-A3. [lia Tex BHCKOSHMETPOB, KOTOPHIE HMeIOT KOmeHOOGpasHyt0 TpyOKy (em. ASTM D 446) yaepaumarorcs REPTUKANSHO, BepTUKAIGHOe BAIPABHHBAHMe LOTAHO NONTREpANATECA ucHOABIOBANKEM (1) lnTaTmpa, oGccneqMBaromero yilep>KHBAHMe KONeHOOOpasHOH TpyOKM B BEPTHKATbHOM noxoxeHHH, 11H (2) MYMIpsKOHOTO YpORHS, YCTAHOMMEHHOTO Ha CTePAHE, MpeTHAsHayeHHOM JA YeTaHOBKH B KONeHOOSpasHylO TpyGKy, WK (3) OTRCCHOM THHHM, NOABeMeHHOH B LeHTpe KoneHooGpasHoit TpyGKH, IK (4) APYCHX BHYTPEHHHX CpeCTE KPEMLIEHHA, MpeAYCMOTPEHEBIX B BaHHe C MOcTOMHHOM Temmepatypoil. 63 Banya ¢ perysmpyemoi renmepatypoli: Menomsyior wanny ¢ mpospaynoii 2KUIKOCTIO JOcTaTONHOH rnyOHHB!. UTOGEI B MOMEHT H3MEPeHHA BPeMeHH HCTeYeHHA m06am MacTh OGpaiya B BHCKoINMeTpe Gia Ha paccTosHHM He Mewee 20 MM OT TIORepxHOcTH 2xWIKOCTH naKHEL H He MeHee 20 MM JO Ja BANE 6.3.1 Tepmoperynstop: Jinx Kaxnoii cepun H3MepeHHit BpeMeHH HCTeTeHHS perymHpoBKa TeMMepaTypH HIKOCTH BANE B HETTepEAe OT 15°C 20 100 °C, HowKHA GuITh TaKOH, OOH TemMlepatypa B BAHHe He MeHsIack Gone ¥eM Ha + 0,02 °C oT BHGpaHHOlt TeMTeparypst 110 summue BucKOSHMeTpa, JLis TeMHeparyp BHE YKasaHHOFO HHTepBalta H3MEpeHKe TeMMepatypEt HE TomxHO npeBsimtaTs + 0,05 °C. 6.4 Verpolicrno jus HaMepenus TeMMIeparyphi B JUarasone or 0 10 100°C: Henomsyior mmGo OTKaNHOpoRanuste cTeKIMHHMe -KHAKOCTHMe Tepmomerps (IIpunoxenne A2) c ToMHOCTHIO Hocse HoMpanKH +0,02 °C wm ¢ eme Gommmel TouHOcTHIO, mHG0 sOG0H Apyroi TepMoMeTpHIecKHi MpHGop pasHoii KH Gostee BEICOKOt ToHHOCTH. 64.1 Ecnn ucromsyrores orkanOponaniute CTeKAMHHMIC XKUAKOCTHSIC TepMOMeTpsI, peKoMensyerea mpuMeHeHHe jlayx Tepmomerpos. J[sa TepMoMeTpa jONKHKI cOBTaTaT ¢ TOSHOCTBFO 10 0,04°C.CT PK ACTM 1445-2011 6.4.2 Bue amarasona or 0 70 100 °C, Hcrtomayror HGO OTKATHOPOBAHHBIe CTEKISHHBIE XKHAKOCTHBIC TepMOMETPSI ¢ TOHHOCTEIO TocHe MOMpasKH +0,05 °C um c eme Gommeit TouHocTHIO, MHG0 mOGOK Apyroli TepMoMeTpHecKHA mpAGop paBHoli WIN Gonee BEICOKO! Tounocrm. Koraa 8 ool H Toi 2e BaKHe HeTONEsyIor ja yerpolicrBa JUIN HsMepeHHs ‘Temnepatypst, OHM OmKHEI CoBNaTaTS C TOUHOCTHIO 0 £0,1 °C. 6.4.3 Tipa ucnomssoBaMHH CTeKIAHHBIX %KHAKOCTUBIX TepMOMeTpoD ¢ UeHOl jeTEHHs 0,01 °C, raxux Kax 6 Ta6mmne A2.1, HonombsytOT yBesIHUHTEMBHOE YCTPOHICTBO LIA TOTO, NTOGEI yOcaurscs, TO peGyemas Temmeparypa HCHLITaHHA COOTRETCTAYeT — HOSMOXKHOCTEM Peryamponanuia vemmeparypst mo 10.1. Pexomewmyeres, nepHouMeckH perHeTpHponaTt ToKasanHa TepMoMerpa (i moOsle MOMpaBKH Ha MlOKAIAHNA TepMoMeTpa) C TIENBIO TIOKAIa coomercraua TpeGonanmim wacrosmero Merona ucuurranni, Jlannax uerpopmauna MoxeT HCIIOMESOBATHCA TIpH pacteTax TOIHOCTI H IpeMHESHOHHOCTH HCTBITAH. 6.5 CaeraHx spemenn: Mcnomayror mo6oe yerpoiicrso juin WaMepeHH BpemenH c TouHocrBio Ao 0,1 ¢ HI ¢ Combined ToAHOCTEIO HMeiOUIee HorpemmHocre HaMepeHK + 0,07 % (em. Mpssioxenme A3) mph mponeneHnn HemstranHit 10 MAHHMAIBHOMY 1 MaKCHMANBHOMY uiTeppanam mpeqiionaraemoro BpeMeHH cTeveHHA. 6.5.1 Moryr Metlomaonarses oneKrpHYecKHe CHeTSHKH BpeMeHH, eCIH HacTOTa TOKA peryaupyerca ¢ TosHOCTHIO 0,05 % Hm ene TouHee. IlepeMeHHBi TOK, B COOTBETCTBHH c HCKOTOPHIMH KOMMYHATKHSIMH CHCTeMaMM 9u1¢KTpoCHAGxCHHs, KOHTPONMpyeTeR cKopee NepHosHeckH, eM nocrosuHo. Korga upupogsrea B gelicraHe onexrpuveckHe c4eTHHKH BPeMCHH, TAKA PeryTHPOBKA MOXCT CTATS MIpHIHHOM GONbIIHX ONTHGOK B HSMepeHHAX BpeMeHH HeTeVeHHa KUHeMaTHMeCKO!i BAIKOCTH. 7 PeaxTapet M MaTepHastet 7.1 Oxumaoumii pacrBop xpomosoli cMecH, WAH He conepxamit xpoM, cHbHO OKACMOMIMH OMMULAIOMIMIi aCTBOP KUCAOTBI. TIPHMEYAHHE Xponosas xuciora otacka Jia suoposss. OHa TOKCHHG, MpHSHAHA KaHUcpOreHHOl, xpaiine xoppoamitiax WoremmamKo onacia mp maaxwoxelicroxn ¢ opranimieckaun vemecrant. Tipit HCHONGIORAHIOE, HANCRALOT HA THO SANUNTHIO MACKY HE HOSHOCTHIO AKPSIBLOMY:O TEO ANUTHYIO OCH, skmowax coorserersyioume nepsarea HoGeraior RasIXaHUs mapa. HItONSIORSHIy:0 XPOMOBYIO KUCIOTY YARIOT OcTOpOxHO, TAK KAK OHA TO-MpexHeMy ocraeTes onacHOl. He cOxepKAUIHH XPOM, CHIIHO OKHCAAOMUA oumuaouut pacrop Tarxe suisercx xpaiie Kopposuiiiim uM MOTeNMULANGNO OnACAN pM KOMTaKKe ¢ OpraHuHeCKHIMN REULECTRAMIE, HO HE COAEPRUET XPOM, KOTOPHIli co3Ager AONOMHITEAHKIe pOGrews orwocurensio yaaseus). 7.2 Pactsopurems oGpastta, NomHOcTs10 ementusarontntics ¢ OGpastio. Dumsrpytor meper ucnonBs0BaHHeM. 721 [ia Gomsmmncraa o6pasyon B KayeCTBe § pacTROpHTeN O,XOAHT. Gsicrpoucnapsomuiica sipup 11m marpons. OcrarounBle TOMIMBA JK ysQeHUA accbanbTOBBIX CoemUHeHHi MeOGXONMMO NpesBApHTeNbHO MPOMBITs apOMaTHYECKHM PACTHOPHTeIIeM, TAKHM Kak TOYO WIH KCHION. 7.3 Bucsrxaommit pactnopurens - neryunii pactsopuremb, cmemmparomniican ¢ pacrpoptresiem oGpasua (cM. 7.2) Bosoli (cM. 7.4). Dunbrpylor Hepes, HCOMBIOBAHHEM. 7.3.1 Tloxxonmr anerou. TIPAMEYABME Ypesssrsaiiio orneonacen. 7.4 Boga, AcHOHM3MpoRAaHHas WIM JMCTHLIMpoBaHHas, cooTBeTcTByIomas ASTM D 1193 uum Knaccy 3 ISO 3696. Oussrpyior nepen ncrionba0nanueM.CT PK ACTM J 445-2011 8 Cranaaprueie o6pasmer paskocTH 8.1 Ip mpHMedeHMm Macrosmlero MeToxa AONKHEI HCTOMsORATKER craHytapTHBie o6pasuist BaSKOCTH B coorBercrBMHM ¢ ISO 17025. Cranapriste oSpasnst KHHeMATHeCKOHi RAGKOCTH OMAHA NPOCHEKHBATKCA —OCHOBHAIMH —MIpoueypaMH BUCKOIMMerpa 110 ASTM D2162. 8.2 Heompeneneniocrs cranmaprHbix OGpasii0B BASKOCTH AOIKHEI OBITS YcTaHOBEHEL juix KaxkOrO NOATREpHAeHHOTO sHaIeHHE (k= 2,95 %) no ISO 5725 usm NIST 1297. 9 Kann6ponka 1 mponepa 9.1 Bucxosmmerpst: Mcrombsylor ToxbKo OTKANHOPOBAHHBLe BHCKOSHMETpH, TepMOMETPEI 1H TaiiMepsi, Kak OMHCaHO B paszemte 6. 9.2 Craxgapranie oGpasutt axakocra (cM. TaGauuy Al.2) mpenmasnavenst 218 KoHTpOnE pH mposeientHH staGoparopHErx HermrTanHii, 9.2.1 Ecam ompexenenHas KMHeMAaTHYeCKat BA3KOCTS He coOTBETCTByeT MpHEMIeMOMY Homo JONYcKA, KaK BTIHCTeHO Ha A4, HOATREpANIeHHIOTO sHANCHHK, HepenpOREpsIOT KAKU STAN MpOUeNyPH, BNHOGAL KATHOPOBKY TepMOMeTpAa H BHCKOSHMeTpa, YTOGsI ONpeMeNHTs HCTONHMK onHOK. B Al mpunenenst AeTamt AelicTRUTesIBHBIX STANOHOB, TIPHMEYAHHE B npeysarynm nonpocex Metoxa wemuraxnti D 445, ncnomssarnes orparnienna 40.35% momepaxenoro suavenua, Jame ax nonepxana orpaeuenx = 0,35 % we Moryt Gums posepen.B Tpiotoxcmn Ad npexyesarpunaiores HBICTPYKIINH, no onpeenestito nana xonycxa. Tone AoMyeKA OG be MELIET HSMEHSHBOCTE IPHSHAHHOTO 3TAIOHA BASKOCTH H HEOMPECIEHHOCTE JaGopaTOpHOTO MCHONBIOBAHHA nprouanuoro sraiowa uxraxocri. 9.2.1.1 B xaecrne ansreparunsl k pactery a IIpaioxenun A4, Moryr HenombaonaTEcs. noxoxue roast jonyeKa ws TaGsmttst 1 9.2.2 TIprimiamn HanGoree pactipoctpaHeHHBIX HCTOUHHKOB OUINGOK ABAAOTCR YACTHUBI MLUIM, OCEBIIHe B KANIMILISPe BHCKOSHMETPA H OWINGKH IPH HIMepeHIEM TestepaTypss. TipapnbHetit pesymstar TOMyYeHHBIit Ha CTAHAApTHOM OGpasiie, He HCKMOGAET BOIMOKHBX HeTONHHKOB OMHGOK. 9.3 TMocrosuuas auckosumerpa, C, saBucuT OF YeKopeHix cBoGosHOrO HaeHHs B MecTe TOBEPKH BHCKOSHMeTpA H, MOITOMY, JOIDKTA YkaSEIBATECK TIOBepOTHO! sAGOpaTopHel BMeCTE C noctosuHo# suckosumerpa. Kora cua taxecta, g, otamuaetcn Gonee em Ha 0,1 %, MOcTosnHy10 BucKOsHMeTpa Koppextupyror no Popmyste (1): Ca= (gi/g2)*Ci, a) Tae, HEAeKeEI 1 H 2 oGosHataIoT NoBepOFHYIO H HeMBITaTeNBHYIO NaGoparopmo. 10 OGmue rpeGonanus K mponexenmo nemurrannit 10.1 PeryaMpytor m TOAMep:KHBAIOT BaHHY BUCKOSHMeTpa mpH TpeGyemoii Temmepatype HOHBITaHMA B Mpenenax, AaMMEIX B 6.3.1, yHHTHBAR ycuOBHs, mpecraBTeNHne B Tipunoxenun A2 H nonpasKku, npHUBeeHEBIe K KARHOPOBOSHEIM CepTH(HKaTaM TepMOMeTpOB. 10.1.1 Tepmomerpst 7omKHEI YAepAHBATECH B BEPTHKATGHOM TOTOKCHMM B TEX xe YeHOBHAX HOTpY:KEHMA, KaK H IPH KALHOPOBKe. 10.1.2 Uro6s nomysHT HanGosee TOUHBIe W3MepeHHA TeMMepaTypsl, PeKOMCHILYCTCA HCHONBIOBATS Ba TepMOMeTpa C jelicTBYIOLIHME KATHGpOBOHEIMH cepTacbuKaTaMu (cM. 6.4). 10.1.3 Toxasanus jomxuDI paccMarpunarsex OITHYeCKHM YCTPOlicTBOM ¢ JIKESAMH, JANOMIHM TATHKPATHO’ YBEAHYEHHE H HCKTOYAIOMVMH OIHGKH YFIOBOTO CMEMIEHRR MexTY BIJIUMEIM H PeaITbHEIM HampansieHHem HI00paKeHHs.CT PK ACTM Ji 445-2011 10.2 Bepyr yncrstii, cyxoii, Kkanw6ponannntii BUcKO3HMeTp, c qMalla30HOM, OXBATEIBAIONIMM TIpesMOMAPAeMYIO KHHEMATHIECKYIO BASKOCTS (GombITOH KAMOUINp LIK BABKOI 2KWIKOCTH M MAIEHBKHIL KAMMULISP [U1 MasIOBASKO! *KUAKOCTH). BpeMs HCTEMEHHA JL PYSHBIX [BHCKOSHMETPOB J1OIDKHO GxITS He Meee 200 c no ASTM D 446. Bpems neresenms Meee 200 ¢ AOMYCTHMO JK ABTOMATHYECKHX BHCKOSHMETPOB, ECiIH OHH OTHeNAIOT TpeGoHAHHAM 6.1.2. 10.2.1 Oco6se aeram onepaunu pasmrHaloTes IX PAsHBIX THIIOB BUCKOSHMErpOB, nepewicnennix a TaGanue Al.l. Mnctpyximm mo 9KcnyaTaNHH jx pasHbIx THTIOB uckosmmerpon arores n ASTM D 446. 10.2.2 Benn Temmepatypa MembITaHHs HIKE TONKH POCKL, HaMONHSIOT BHCKOSHMETP cnoco6om ro 11.1, Bo w36exaHHe KOHCHCaTHH BNarH Ha CTeHKAX KANWLIspa M pacutMpeHHoit SACTH BHCKOGHMETPA, 3AKPLIBAIOT CTeKIAHHLIe TPYOKH BUCKOSHMeTpA PeIMHOBLIMK IPOGKAMH JuWK YOepKaHUA Ha MecTe HCHBITYeMOrO OGpasita, H MOMeMIaIOT BHCKOSHMETp B BaHHY. JlaioT BHCKOSHMCTPY lOCTH4G TeMIepatypHI BAHHBI H yAaLAIOT MpoGKH. [pH pysHom onpesenenHH BASKOCTH, He HCHOAESYIOT BUCKOSUMETPKL, KOTOBIe He MOTYT GIT HIBEYEHE! H3 BAHHBL 1 ‘arpy3ku HerIBITYeMOrO OGpastia. 10.2.2.1 Jlonyckaetcs, Ho He TpeGyercs, HcnomssosaHMe cna6o HamomHeHHEIX OcCYIIMTENbHGHX NATPOHOR, MpHKPeILIeHHMIX K OTKPKITHIM KOHIaM BHCKOSHMerpa. TIpH CTONSSOBAHHH, OCYIIMTeNbHBIE TIATPOHBI © OIDKHBI © COOTBETCTBOBATh _KOHCTPYKUMH BUCKOIHMETpa H He OrpaHHsHBATe HOTOK OGpasiia aBIeHHEM, OGpasyeMBIM B MpHGOpe. 10.2.3 BucKosUMerpul, HcHONbsyeMBle JUIK HCIIKITAHUA CIIMKOHOBEIX, (pTOpyrneponoB i APYTHX -KANKOCTEH, TPYAHOYAMHMEIX ¢ TOMOMTSIO OFMINAIOMIeTO PaCTROPHTEsLA, MOryT HCHOMLIOBATHCH TONBKO UIA OMpEMeIeHHA BAIKOCTH STHX -AKUsKOCTell. OTH BHCKOSHMETpHL OWKUBI HONBEpratseA KATHOPOBKe wallle, HEM OGBISHBIe BUCKOSMMETpBI. PACTROPHTeNb HOCTe MPOMBIBKH STHX BHCKOSHMETPOB He OTKCH HCNONBSOBATCR ;LIR ONHCTKH -APyTHX ‘BHCKOSHMETpOR. ‘Ta6anua 1 - Mpumepnoe nose jonyexa Baskocte mpencramnennoro Toxe xonyexa emecrBa, Mat /c <10 20,30% 10-100 20.32% 100 - 1000 20.36% 1000 - 10 000 20.42% 70 000 - 100 000 20.54% > 100 000 20,73% 11 Onpeseaenue kunemarnseckoit BaskocTH mpospaytenx amIKocTelt 11.1 Buckosumerp sanommmor vembyemsimM o6pasiiom B cooTBeTcrBHH ¢ opMoit anmapara aHalorHsHO TOMY, KaK 9TO OCYUIECTRAEIOCs IPH KanHOpouKe BUCKOSHMETpA, 1 noMenmaior B Gamo. Een 8 oGpasue conepxarca TRepabe YACTHUGI, TO MPH 3arpy3Ke ero ¢buaurpyior epes caro c pasMepom oTBepeTHit 75 MKM, CTEKAHHEI HM GyMaKEBI baAETp (ca. ASTM D 446). TIPAMEYAHVE Yro6u enecri x varumyiry arperponanie OTeNMATSIX NACTINL, MPOXOAAIIUEX Neped quonrp, pexomenyercs, "ro6it MpoMeRyTOX BpEMeNH MexAy QUILTPORANEM 1 SANONTEEHILeM COXpANLICH ENB. 11.1.1 Kak mpapisto, BHcKosHMeTpst, HeromayenniIe jx mpospasmix -KHAKOCTeH, OTHOCSTCA K OHOMY H3 THTIOB, NepeucmeHHEIX B TaGanue Al.1, An B. 11.1.2 Jax mposyKros, monenenme KOTOpKIX anaorHHO remo, WIMepeHHs jOsDKUIL MPOBOHTECK MpH OCTATONHO BBICOKHX TeMMepaTypax [UIA OGecHeseHHX cBOGORHOrO 8CT PK ACTM 11 445-2011 HCTCHOHUA H TOTYHEHUS HCHTHSHBIX pesysISTATOR MIpH HCTIOTEIORAHHH BHCKOSHMETPOB c pASMHSHIM AHAMeTPOM KATHULIEpOB, 11.1.3 Hamomnenmeti BuckosHMeTp BBLIEpAUBAIOT B BAHHE 0 TEX Mop, MOKA OH He mporpeerca 10 Temmeparypt Hermbrrannx. Eom ota Gans HCMOMbayeTCH JULA HECKOSTBKHX BUCKOIUMETPOR, HENLIA NO'PYAATS WIM BMIHUMATE BUCKOSHMETPH 13 BAHHML, OKA XOTA OH MMH BHCKOSHMETP HAXOAHTES B pAGONEM COCTOSHHH. TaK KAK BpeMs HaXORACHES B Bante GyseT MEHATSCA B SABKCHMOCTH OT OOOPYsOBAHHs, TeMIIEPATYPKI H KUHEMATHIECKHX BAIKOCTEH, RPeMs TeMIepaTypHoro panHORecHA JOCTHTACTeR IKCHepHMCHTAMBHO. 11.1.4 Tax kak 970 Bpesis Gysler KoeGATbe [UIA paaHIX HIMEPHTeNBABIX MpHGOpOB, pastiolt TemmeparypsI H pasHoii KMHEMATHYeCKOii BAIKOCTH, YCTAHARTHBAIOT BpeMa jOCTIKEHA GevortacHoro pantionecws OMEITHEIM yTeM. 1.1.4.1 Tpwmara smnyr Oyler AocTaTOIHO, 34 HCKIONEHHEM B OTHOMIEHHM caMoit BBICOKOH KMHEMATHYCCKOM BA3KOCTH. 11.1.5 B tex cnysasx, Korga 9Toro TpeGyer KOHCTpYKUNA BUCKOSHMeTpa, HocHe Toro Kak o6pasen OCTHTHeT TeMTIepaTypHOrO paBHOBCCHS, CTO OGHEM AOBOAAT 10 OTMETKH. 11.2 Mcnompsys scacsizanue (ecau oOpazex He comepxKAT neTySHx BemlecTs) Hau jaBNeNHe, YCTAHABINBALOT BEICOTY crONGHKa OGpama B KAMWWULIPe BUCKOSHMETPA 10 ypoBts, HAXORAMIETOCS MPHOTHSHTETSHO Ha 7 MM BBIMIe MepBOll BPeMeHHOH METKH, ECHH B HACTPYKUMH To SKCILIyaTALLMH BUCKOSHMeTpa He yeTaHomMeHO pyroe 3HayeHHe. [pu caoGomHOM HcTeTeHHH oGpasua ompeesmor ¢ TowHocTEIO 110 0,1 ¢ BpeMs, HEOGXOMUMOe LIA MepeMeMtenHa OT HepBOli jlo Bropow Merku, Ec BpeMs HCTeveHHa MeHbINe ycTAHOBNeHHOTO MHHHMyMa 10 10.2, ToAGupalor BHCKOSHMeTp ¢ MEHBIIHM AHAMeTPOM KAIULLEpa K NOBTOpsIOT onpenesEHUe. 11.2.1 Hosropsior ompexenenne, onmcanoe » 11.2, six Homy4enus Broporo sHavenHs BPeMeHH HeTeNeHHA HeMITyeMoro OGpastia. PerHCTpHpytOT o6a sHaTeHTA. 11.2.2 Ms aayx wamepenmit apemenu 1oToKa, paccHTEIBALOT Ba OMPeAeNeHHLX SHAEHHS KUHeMATHTIeCKOii BASKOCTH. 11.2.3 Ee0m fBa 3HaveHHa KMHEMATHYECKOH BASKOCTH, BBITHCICHHEIC 13 HIMepeHHit BpeMeHH HeTeveHHA OGpasia, cornacylores c ycTaHoRIeHHOli nemuHHO! OnpenesieMocTH 110 17.1.1, TO paccuustBalor cpemiee apH>MenHiecKoe sHaveNHe s1ByX HaMepeHAli, TOOK PACCUHTaTS pesyTbTaT KMHEMATHYeCKOH BASKOCTH. ZanHcHIBAIOT pesymbTaTst. Ecmm xe pa HIMepeHHA He COrAcyloTes, culeAYeT HOBTOPUTE OMpeTeMeHMe NOCHE THATENLHOH ONKCTKH H CYLIKH BHCKOSHMeTpa H GuISTpaNUH no 11.1 HeMBIyeMoro OGpasita, 10 COOTBETCTBHA yorantosnentoit onpesiextemocrH snaterit KHMeMATHYeCKOIt BASKOCTH. 11.2.4 Ecam nemecrno WH TeMmepatypa, HIM H TO H Zpyroe, He MpHBOAATCA B cHUcKe B 17.1.1, nemomssytor 1,5% B Kasecrse oMeHKH ompestentemocTH. 12 Onpenesteune kunematuseckoii nsxaKocTH HeMpospasmnix aHAKOCTEH 12.1 Oammenmiie uummgponanmie u TeMHBe CMAIONHEIe Maca NOATOTARIHMBAIOT B coomercrpu ¢ 123 jaa NOny4eHHs mpexcrasHrensHoro oGpasua. Ha KuseMaTHuecKy10 BASKOCTb OCTATOUHEIX TOILTHB (Ma3YTOR) H PYTHX HapadMHHCTSIX MONYKTOB MOXET TOBIIHATE enmionas o6paGorka x selicraus, nooromy 8 12.1.1-12.2.2 omsicaHa npoueaypa, KoTopas cnojuT 970 BIHSIIHE 10 MHEMyNa. 12.1.1 BacKosuMerpst, HoromEsyeMbIe I HEMPOspayHEIX KUTKOCTEH, ITO BACKOSHMETPEI oGparnioro noToKa, mpusenexuete » TaGamue Al.1, C. 12.1.2 Memurryemstit oGpasen, narpenaior B KonTelinepe B Tesennu 1 aca npu (60+ 2) °C. 12.1.3 TmaremsHo nepememmeaior o6pasey, NOAXOAMMeH MaIOIKOH COoTBETCTBYIOMICH JME, OcTaRAX MO KOHTeliMepa, TpoxomKaloT MOMeMIMBaHHe, OKA Ha MAnONKy He Mepecrauter HasIHHaT» 0C40K HIM BOCK.CT PK ACTM 1445-2011 12.1.4 Copa morHo Hajlenaior KoNMayOK Ha KONTelHep M 9HeprHHO BOTPSXHBAIOT B Tesenne | MoH su TomHOTO nepementaBarms, 12.1.4.1 J[ax oGpasios ¢ BBICOKHM cosepxaHMeM napadHHOB Wi BEICOKOH KMHEMATHYCCKOH BASKOCTEIO HEOGXOAMMO YBCIHYMTS TeMMeparypy Harpewa wEmTe 60 °C JK AOCTIOKEHHA TUaTeNbHOTO NepemeumMBaHHs. OGpazen OMKEH GuITE AOCTATONHO >KUAKEM, ‘sr06st ero GsuI0 yOGHO MepeMentarh H BETpAXHYTS. 12.2 Cpasy 2xe nocae auinomienns 12.1.4, HaMBaIoT KoAHuecTRO OOpastia, LocTaTouHe sroGst sanomuTs qua BucKosMMeTpa, B 100 Ma creKasHHY:O KOIGY M HE TLIOTHO 3aTHIKAIOT mpo6xol. 12.2.1 Torpyxaror KoaGy B BaHHY c KHTSUTeit Boploit Ha 30 ME. TIPAMEYAHHE Co6moxars ocropoxocrs, Tax ax up warpesatou wenpospasnnx xuupKocrelt © Gosmmim conepwartieN Om AO BIICOKIX TeMTeparyp, MoxeT MpoWOlTH ciUMIOe aNesartoe nepestBanKe (sui6poc) xemsmeti xaxaKocrs sepes Epa 12.2.2 Vapnexaior Kon6y u3 nantibl, MIOTHO sareiKAOT mpoKOli M BCrpsxHBAIOT B Tesenne 60 c. 12.3 Tpe6yercs wa onpenexcHus KHHeMaTH4ecKOii AxIKOCTH HeMEITyeMOro Opasua. Las TeX BHCKOSHMETPOR, KOTOPHIE TPeGYIOT TlOMKOH ONMCTKK TlOCHe KAaXKNOTO HIMEPCHHLA APEMCHHL HicTeveHHs, MOrYT HeMONB3OBATKCR RA BHCKOSHMeTpa. OJIKH BCKOSHMETP MOxHO HCHOMEOBaT AIK ABYX OMpeeneHMik BPeMeHH HCTeeHHA nocsefOBATeMBHO TOrAA, KOTTA JAHHBIL BHCKOSHMeTP He Tpe6yeT O¥MCTKH MocHe KaxgOrO HsMepeHus, HanomKnTs BHCKOSHMETPBI B MOpAsKe, OSycAOBTEHHOM HX KOHCTpyKuHelt. HanpuMep, sux BHCKOSHMETPOB ¢ MomepewHot umm BS U-o6pasnoli tpy6xot ans HempospayHErx 2KHAKoCTell, puETpyoT odpasent sepes (baBTP ¢ MOpaMH 75 MKM B BA BHCKOSHMETPA, MPe/IBApHTeNBHO MOMEIICHHBIX B anny. Jina oOpasyop, MoaBepraemBiX HarpeBy, HCTIONB3yIOT MpexBapHTemBHO Tosorperstit usurp 1x npenorapamenns sa6uBKH hasTpa. 12.3.1 BuckosHMerpst, KOTOpse HANOIIHAIOTCR 10 TOTO, KaK HX BBOIST B BaHHY, MOryT norpeGonaTs mpeqBapHTembHOrO HarpenaHM B TIeYH 0 HaNomHeHHa O6pasyoM. 370 OcyUlecrBAsercs {UIA TOTO, ¥TOGH He AONYCTHTS OCTEIBAHHS OGpazlla HUKKe TeMMteparypsL wemsrranns, 12.3.2 Yepes 10 sax peryampytor oGsem oGpaauia (B Tex cay4asx, Kora 3Toro TpeGyer KOHCTPYKIIMA BHCKOSHMeTpa), ¥TOOM OM coBMamal ¢ MeTKOl OGbeMa, KaK YyKasaHO B TpeGonarHsx sucKosHMetpa (cM. ASTM D 446). 12.3.3 3anonHeHHEIe BHCKOIMMeTPEI BLYLepAHBAIOT B BAHHE 0 Tex Op, nOKa He GyneT ocTurnyra Temmeparypa ucustranna mo 12.3.1. Een Mcnombsyerca ofHa BaHHa Is HECKONBKWX BHCKOSHMETPOB, HENEIK TOTpyKATb, HIBICKATS WIK MPOMBIBATS BHCKOSMMETP, loka XoTa Get ORME BHCKOSHMeTp HcONbAyeTCs [1s HIMepeHHs BPeMeHH UCTeHeHHA. 12.4 Jlux coGoano rexymtero oGpasiia, Bpems, TPeGyeMoe LIK MPOXOAIeHHA c MepBOI j10 BTOpO# OTMETKH, H3MEPHIOT C TONHOCTEIO 0 0,1 c. 3AMHCEIBAIOT pesyTBTaT HIMepeHHit. 12.4.1 B caysasx ¢ oGpasnama, TpeGyromumu Tepmusecky!0 OOpaGorKy, OMMcaHHyt0 B 12.1-12.2.1, sapepmaior HaMepeHiix BPeMeHH TloTOKa B TeveHUH 1 vaca sanepmIeHHs 12.2.2. Banncumaror usMepeHHoe BpeMa HCTeNeEHHS. 12.5 Bsraucimor KHHeMaTHYecKyi0 Ba3KOCTb, Vv, B MM/c, #3 K@KJOTO HIMepeHHOTO BpeMenH noToKa, Hx CHHTaIOT ABYMA ONPECNEHHGIMH 3HaYeHHSIMH KUNEMATHYCCKOH BESKOCTH. 12.5.1 Jas octaTouHEIx KHAKHX TOTMIME (MazyTOR), ECM Ra 3HAYeHMA KUHEMATHUECKOIt BSSKOCTH BLMHCKEHHDe M3 HSMepeHHii BpeMeHK HCTeYeHHs OGpasia, HAXOLeTeK B Mpenestax YeTaHOBEHHOTO SHANA ompenesxemocTH 110 17.1.1, paccHATBIBAIOT cpenHee apMerH4eckoe sHayeHHe AByX WIMCPeHHi, IK BRIIMCICHHA KHHeMATHICCKOH BAIKOCTH. Banucsimaior pesynbrat. Eck 18a OnpenereHHs He Cormacylores, TO OnpeseneHHe HOBTOpAIOT Tlocde THareNbHOH ONHCTKM HM MPOCYIIKH BHCKOSHMeTpa H GHNTPOBAHHA uCTBITyeMorO oGpaaua, noKa 3HaeHHA KUHeMATHUeCKOli BAIKOCTH He OYAYT COOTHETCTHORAT YcTAHOBIEHHO! 10CT PK ACTM 11 445-2011 ompeytensemoctu, Ec Bemtectso W/MuH Temmepatypa, He mpHBogiates B cmcKe 17.1.1, TO IR Tenmeparypsr Mexury 15 °C # 100 °C, neromssyror B KayecTe ouenkn onpentensemocTH. 1,0 %, Jus Temmleparypst 34 NpesesaMH AaHHOTO slHarIasOHA - 1,5 %. HeoSxoaMMo OGpaTHT® BHAMAHHE Ha TO, TO HOMBITYeMBIe BeMecTBA He ykasannEte B 17.1.1 MOryT GbITb HeNbIOTOHOBCKHMH. 2KUAKOCTAMI H CONEPAATH THEPAKE LACTHIBL, 13 Ounerka puckosumerpa 13.1 Mexay mocmezonarenbibinH OnpeveneHHIMH KHHeMaTHYeCKOH Ba3KOCTH, BHCKOSHMETP THIATETSHO ONMINGIOT HeCKONBKO paz PACTROpHTeNeM, a 3aTeM ocymaroT slerKOMCHapsioMlMeR pacrnopHTenem m0 7.3, CyulaT BHCKOIUMerp UpoMycKanHeM cs1aGoro MOTOKa MpopuISTPOBAHHOTO cyxoro BOSYXA B TeveNNe 2 MHH WK AO MOmHOrO yawIeHHA cue1on pacrsopaens. 13.2 BHckosHMerp mepuoguveckH NCTAT ONMINIOMMIM pacTBopHTeNeM B TeveHHe HECKONGKHX "ACOB JU Y/AICHHX OpraHnYeCKHX OTOKCHHi, 3aTeM TMATEsIBHO MIpOMBIRAIOT Bono% no 7.4 MH JerKOMCHapsrOWMMca pacTBopuTenem 0 7.3 HM BBICYIUMBAIOT Mpodpi.1srponaimHKIM CYXHM BOSTYXOM HIM OX BaKyyMoM. Heopranuyecke oToxeHHA YAANAIOT COMAHOH KHCHOTO! Mepex HCTONKIOBAHHEM XPOMOBO! CMeCH, OCOGeHHO ecm mpenmonaraeres mpucyrerane coneli Gapas. TIPAMEYAHME 1 em. 7.1 TIPAMEYAHVE 2 Baxcio, sro6sr ne veromss0santich menOsIIbie OXMIUIIOMNHE PACTROPH, TAK KAK MOCYT porroliru aeuciis KaniGponke BucKosuNerpa, 14 Pacuer 14.1 Burineamor kaauloe OnpenesleHHoe sHaveHHe KHHEMATIIECKOH BESKOCTH, Vy H V2, H3 HSMEPEHHOTO BPEMEHH HeTeIeHHA, 1) M fz, H MOCTOSHHYIO BACKOSHMETpA, C, C MOMOMTBIO opmyast (2): vi2=C tha, Q) rae, V1.2 = SHA4CHHA KHHEMATHMCCKOH BAIKOCTH JULI V; H V2, COOTRETCTREHHO, MM"/c, C= kanu6posounas MocrosmHas BuckosuMeTpa, MMZ/c?, 11 = BMepeHHOe BPEMs HCTEEHHK UIA t) H 12, COOTBETCTHEHHO, C. PaccuHTIBaloT pesyiIbTaT KHHeMaTHYecKOl BAIKOCTH, V, KAK CpemHee HHCHO Vv; H v2 (CM. 11.2.3 4 12.5.1). 14.2 PaccaHTEIBaIOT THHAMHYECKY!O BESKOCTS, 1, H3 BEIIHCHeHHOH KHHeMaTHIecKOii BAIKOCTH, V, HIMIOTHOCTE, p, ¢ HoMOMtEI0 Dopstysts (3) n=Vvxpxl0", 8) 11= auHaMdeckas BasKoCTS, MITac, p = wioTHocTs, Kr/M’, IPH TeMNepaType, KOTOPat HCHOMBSOBATACh JIA ONpeneneHHA KMHEMaTHYeCKOli BY3KOCTH, H KuHeMaTH4eckas BASKOCTE, MM"/C. 14.2.1 [notHocts o6pasya Moxer GxITS ompeylemeHa MpH Temmlepatype HCTIIBITAaHHA ALA OMpes(esteHHa KUHEMATHYECKO! BASKOCTH JHOGHIM HOJXO;AILUM METOOM, TAKMM KaK MeTost nemsrranni D 1217, D 1480 wom D 1481. 15 Butpaxenue pesysbTaron 15.1 [poroxosmpyror pesysbraret HCCTeAOBAHHA KHHEMATHYECKOH HI AMHAMHTECKOL BASKOCTH, KIM M'TOFO H APyTOrO, o YerEIpeX sHaNaITEX UMP, BMecTe ¢ TeMmepaTypol MeMBTTANHA. iCT PK ACTM 11 445-2011 16 3anncs pesyabratoe memerrannit 16.1 3anucsinator caenyromyto uncbopwanuto: 16.1.1 XaparrepHeraxa MemBIryemoro mposykcra; 16.1.2 Ccninka Ha Hacrosmmit cranjapr; 16.1.3 Pesyasrar uensrranns 10 Pasaeny 15; 16.1.4 JhoGoe oTknOHEHHe, O cOrmAMeHHIO HH HHBIM O6pas0M, OT yeraHORTeHHOH mpouenypst; 16.1.5 [lara mponenenua uemerranus; 16.1.6 Haspanne anlpec HcmBITaTenbHoit maGopaToprM. 17 Tipennsnonnocrs. 17.1 Cpasnenue onpedenenmerx snavenutt: 17.1.1 Onpedersenocms (d): Pasiana Mexiy nlocenoBarembHBIMK OMpeneserHsiMe, S3HAYEHHAMH, TOYYeHHBIMH OLHHM H TEM 2Ke OMepaTOpOM, B OMHOI H Toi xe AaGopaTopHH, c HCTIOMBSOBANIHeM OMHOTO H Toro xe OBOPY.ONAKHS JIA PALA OEpANLH, CHOAAILUUXCH K OKOMY PeayABTATY, B OGHIEM, IPH HOPMAIBHOM H COOTBETCTBYIOUIeM IIPOBEACHHH HACTOAUeTO MeTOAA MCTBITAHNA, OIDKHA TIPCAMMATS YKASAHHMC IHANCHH TONMBKO B OHOM CHY*Ae HE RANNATH: Basonnie nacna mp 40 u 100°C? 0,020 y (0,20%) Komnaynmposannere Maca mp 40 4 100°C!” 0,0013 y (0,13%) Komnayxamposanusie Macna mpu 150°C"! 0,015 y (1,,5%) Hedranoit napadun (Heiranoii sock) mpa 100°C? 0,0080 y (0,80%) Tonosnsiii Masyt mp 50°C? 0,017y ‘Tonouri masyt npa 80 a 100°C? 0,011 (y+8) (1,7%) Tipcann mpa 100°C'* 0,00106 y"" Tasopoe Macuio px 40°C'> 0,0013 (y+1) Tomaso sna peakTupuEtx naurateneli pu -20°C'* 0,0018 y me: ¥ 9T0 epee cpasiiHBaeMErx OMpeMENeHHEIX sHAeHHit, 17.2 Cpasnenue pesynemamos: 172.1 Hosmopsemocmy (r): Passa Mexay nocaexonarenbiniMN pesynbrarans, TOMY4eHHBIMH ONHHM H TeM Xe oMeparopom, B oMHo H Toi xe naGoparopHH ¢ HCTIOMESOBAHHEM OsHOTO H TOTO XE OGOPysOBAHHK TPH MOCTORHHE yonOBHsX paGorE! Ha WACHTHSHOM HcHEITYeMOM MaTepHane, B OGULEM, IPH HOPMAIBHOM M_ CooTRETCTRYIONIEM MpOBeNeHHH HaCTOAMerO MeTONA MCTSITANHA, BEPOsTHO, GyseT MpeBeMMATs mpHBenenAMEIe JHANEHUA TONBKO B OHOM cysae M3 ABATNATH: Basonnie wacia mp 40 4 100°C? 0,011 x (0.11%) Komnayxupopanneie Maca mpi 40 4 100°C! 0,0026 x (0,26%) Komnaynamposannere macaa mp 150°C? 0,056 x (0,56%) Hedranolt napadun mpu 100°C? 0,0141 x'? Tonounsrit masyr mp 80 1 100°C’? 0,013 (x+8) Tonoutit Masyt mpu 50°C"? 0,015 x (15%), Tipucagxn npa 100°C'* 0,00192 x!" Tasopnte macaa npn 40°C'> 0,0043 (x+1) ‘Tonmmso ans peakupunix yeurareneit upu -20°C'* 0,007 x (0.7%) Tile: X 9TO cpeytHee cpaBHABAeMBrX pesysIbTATOR. 17.2.2 BocnpoussoxuMocrs (R): Pasnata MeaUY ABYMA OTACIBHBIMH H HesaBHCHMBIME PesyTETaTaMH, MOMyYeHHEIMK PASHEIMH OMepaTopaMH, PAGOTAIOMMMH B PAsHEIX TaGopaTopHsX Ha HOMMHAILHO WICHTHAHOM HCHBITYeMOM MarepHale, B OGUIEM, IIpH HOpMalIbHOM H 12CT PK ACTM 11 445-2011 coormerernyiomle mponeyieHuH HACTOsIHeTO MeTOsA HCMATAHH, ReposTHO, Byer MpenBIINaT SHANeHHs, YRAIAHTIBIE HHO, TOOIBKO B OAHOM CHysae HS BANMATH: Basopste wacita mp 40 w 100°C” 0,0065 x (0.65%) ‘Kommaynmposantsie Maciia npu 40 1 100°C’? 0,0076 x (0,76%) Konmaysamporannsie macna mpu 150°C"! 0,018 x (1,8%) Hedyranoii napadun pu 100°C? 0,0366 x'? Tonounsiit masyT mp 80 1 100°C? 0,04 (x+8) Tonownstit masyt mpu 50°C? 0,074 x. (7.4%) Tipucanxn npu 100°C'"* 0,00862 x!" Tasosie macna mpu 40 °C'> 0,0082 (x+1) Torumuo jus peakrHaHErx Baresi mpu -20 °C'® 0,019 x (1,9%) THE: X 9TO CpesHee CpABHUBAEMBIX Pesy:TbTATOB. 17.3 Tosnocts sua orpaSorarnsrx Macen He ONpentensetes, HO Mpesmomaraercs, 4TO ona xyake, HeM Jui COCTaBHBIX Mace. 13-sa Kpaliitelt HIMeH¥MBOCTH TAKHX OTpaGOTAHHBIX Maced, He npestmosiaraeres, 470 Gy/et ONpeNIeARTECK TOMHOCTS OTpAGOTAHEBIX MACE. 17.4 [kaa oco6six aBTOMaTHYeCKHX BHCKO3HMETPOB TOUHOCTS He OMperenamacs. Tem HE MeHee, mpoueslen anaslHs GosbMoro HaGopa AANHBIX, BKNOYAx KAK ABTOMATHYECKHe, TAK H PYSHbIe BHCKOSHMETpHI B UNTTepBasIe Temmepatyp oT 40 10 100°C. BocnpoHsBORMMOCTS JaHHBIX ABTOMATHNeCKOTO BHCKOSHMCTPA CTATHCTHYECKM © HESHAYHTeIBHO OTMMMAeTCR OT BOCHPOHSBOAMMOCTH jaHHMIX pYy4HOTO BHCKOSMMeTpa. TaKKe MOKasaHO, TO Her CHCTEMATHYCCKOH TIOTPeUIHOCTH ABTOMATHICCKHX JAHHBIX MPH CpaBHCHHH c¢ PySHBIMH TaHHEIMH, 13CT PK ACTM 1445-2011 Tpuaoxenue A (06s2amensioe) AI Tamer sHexosHMerpon H yTBepxACHHEIe ITANOHEI BASKOCTH ALI Tamer suexosumerpos ALJ. B TaGamne Al.1 mpencrapnen criMcok KamWUISpHBIX BHCKOSHMeTpOB, HCHOMSSYeMBIX AIX OMpeseneHHA BxIKOCTH HebTeNpoayKTOB, SKcIIyaTANNE H KaMHGpOBKA BHCKOSHMeTpOB MIpABeneHa B ASTM D 446. AL.1.2 B Ta6amue A1.2 npeactannen cIMcoK 3Ta1OHOB BASKOCTH. TaGauma AL.1 - Tamer uckosHMeTpon HaenrHpuxanus BHckosumerpa Kunemaraveckas pa3Kocr® A. Tums Ocrsanena sua mpospastisix xnutKocreit Kannou-Dencxe” o6aransii ‘or 0,5 0 20000 Halinpyxe 07 0,6 10 3000 BS/V-o6pasnas Tpy6xa® ‘or 0,9 70 10000 Musuariopa BS/V/M or 0,2 n0 100 SIL® 07 0,6 0 10000 Tloaymuxpo Kaxou-Mantunr or 0,4 0 20000 Thauxesye” of 0,6 20 17000 B. 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