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NpH TerAneparype 15 °C. Aina naparbunostix yrnesonoponos M o6pasuos BASKNX Hec>renpoAyKTOS ANA OGecneYeHUA asona aHann- aupyemoro oOpaaua 8 2kHAKOM COCTOSHINK TpeOYeTCA s¥eliKa, PADOTAOUIAA NH NOBLILICHHO! TeLaneparype Tipn axannae napadunoauix yresogoponoe M anaKux Hedbrenpoaysroe cneayer OOpariTeca K MHCTPYKUNH waroTosnTena npuSopa ana pykoso”cTBa K Mepam npenOCTOpoxHOCTH. VNcbopMauiiA O pesynsTarax Mexia Soparopiex uccnenoBeHnh, nposeneHHbix # 1999 r., npuBeqeHa e pasnene 15 W npHMeNaHAN 8. 1.2 Tipu paswornacnax 8 oyeHKe KavecTBa npoRYK\MM ABNAETCA MeTOR C PyNHbIM BBOAOM OBpasua NO 6.3 uni 6.4 » saeucumocrH oF Tuna oSpaaya, 1.3 HacTonui MeToA He CreayeT NPHMEHATE NPM NCHBITaHMAX OBPAs\IOB TeMHOrO YBeTA, ANA KOTO- bik HEBOSMONHO AOCTOBEPHO YCTAHOBHT» OTCYTCTBNE NYSbIPEKOS BOIMyXa B HaMepHTENsHOR sMeriKe. Dns onpenenenua nnorHoctu npoo Hed>TH vcnonbayior ACTM £4 5002. 1.4 ShavennA, yoTaHOBNeHHBIe B eAMHMYaX CHI, cHHTaIOT CTaHAApTHoiNAN, eon ApyrHe ykasaHNA OT- Cyrcrayior. FIpHisTbimM eANHHYaMH USMEpeHHIA NNOTHOCTH FENRIOTCA fpaMMe! HA KYOMYECKHA CaHTHMETp (cices?) wn kunorpammel Ha KyOuYecKHit MeTp (Kr/t4. 1.5 B HacToRUjeM crangapre He npenycMoTpeHo paccMoTpeHNe BCex BoNpOCOB OBecnevenuA Ge2- onachocrH, CesgaHHBIX C ero HCnonb20BaHHeM. MonbsoBaTens HacTOsUJero Crakgapra HeceT oTBercraeH- HOCTE 2a YoTaHOBNeHMe COOTBETCTayIOUNX NpaBHIN NO TexHHKe GesONACHOCTH H OxpaHe 3qOpOBLA, a TAIKE onpenenser YenecoobpasHocrs NPHMeHEHHs 2aKoHOAaTeNbHBIX OrpaHMeNHI nepeg ero MCnoNbaOBAHHEM Konxperiaa nacbopmayis no Texinke GesonacHocTa npuBenena 8 7.4, 7.5 0 10.3. Visnanne ocpaynansioeTOcT P 67037—2016 2 Hopmaruenpie ccbinkn B nacronujen cranaapre vcnons208aHb HOpMaTHBHbIe CcbInKN Ha cnegyIoUNNe craHAApres 2.4 Crawaapte ACTM') ASTM D 287, Test method for API gravity of crude petroleum and petroleum products (hydrometer method) [ACTM f] 287, Meron onpegenesiss nnorHocrH 8 rpaaycax API HedTu m HecbrenpogykTos (apeone- Tpusecxnit meton)] ASTM D 445, Test method for kinematic viscosity of transparent and opaque liquids (and calculation of dynamic viscosity) |ACTM | 445, Meron onpegeneHus kiHeMaTHMeCKOl R2KOCTH NpoapavHkix M Herpoapas- Hbix aknaKOCTeIt (HM BbINCEHKE AAHAMMYECKOH BRIKOCTH)] ‘ASTM D 1193, Specification for reagent water (ACTM J] 1193, Cneuncbuxayia Ha peaxTue Bony) ASTM D 1250, Guide for use of the petroleum measurement tables (ACTM f] 1250, Pykosoqcrs0 no nc- nonbsoBaHnio TaGniny HaMepeHnit HecbTenpoayKTOs) ASTM D 1298, Test method for density, relative density (specific gravity), or API gravity of crude petro- leum and liquid petroleum products by hydrometer method) [ACTM £1 1298, Meroa onpegenenia nnotHocTH, OTHOCHTeNbHOM nnoTHOCTH (yseNbHOrO BEA), HH MNOTHOCTH B rpagycaX API caIpol HECbrH M HaIAKHX Hed>Te- npoayktos apeomerpueceita MeToAOM) ‘ASTM D 4057, Practice for manual sampling of petroleum and petroleum products (ACTM 4057, Npax- ‘THka pysHoro orGopa npob HedbrH H Hec>renpoaykros) ‘ASTM D 4177, Practice for automatic sampling of petroleum and petroleum products (ACTM & 4177, Mpaxruka asroarmeckoro orGopa npoO HedprH u Hec>renponykroB) ASTM D 4377, Test method for water in crude oils by potentiometric Karl Fischer titration (ACTM 1 4377, Meroa onpenenenna Bont 8 cuipoit Hedbru noreHuMoMerpH4ecknm THTpoBaHMeM no Kapny Suuepy) ‘ASTM D 5002, Test method for density and relative density of crude oils by digital density analyzer (ACTM 1 5002, Meroa onpegeneHus nnorHocTa 4 OTHOCHTeNSHOM MNOTHOCTH CBIpOA Hec>TH Yi>poBLIM nnorHomepon) ASTM D 5191, Test method for vapor pressure of petroleum products (mini method) [ACTM f] 5191, Meron onpenenenna naeneHia HacbiuleHHbIx napos HecbTenponyKToB (\4iHH meTOA)]| ASTM D 7042, Test method for dynamic viscosity and density of liquids by Stabinger viscometer (and the calculation of kinematic viscosity) [ACTM | 7042, Meron onpeneneHita aMHaMMeCKOM BRSKOCTH M NNOTHOCTH orgKOCTe!t BHCKOSHMETPOM LlraBnArepa (M BLIMNCTeHMe KHNeMaTHMYECKOH BAIKOCTH)] 3 Tepmuni v onpenenenus 3.1. B Hacronujem cratinapre npuntenenbi cneayiouye Tepmnibl ¢ cooTBeTCTayIOUIMMH OnpEAENeHUAMAM: 3.1.1 mnoTHocTs (density): Macca sewecrea Ha eanHHUy OOeMa NpK ycraHoaneHHoll TeMnepatype. 3.1.2 oTHocuTenbHan nnoTHocTe (relative density): OrHoweHHe nmoTHocTH BeWlecTBa NPM yCTaHOB- ennoi Temneparype k nnoTHOCTH BonbI NpH YcraNoBReHNo!t TeMneparype. 3.2 Tepnmisi, xapakrepHbie Ana HacTosuero craHaapTa 3.2.1 actpoiixa (adjustment): Npoyeaypa npneneHna paGounx xapakrepucrHK npHGopa 8 COcTOR- tne, coorseToTByioujee ero cron’soBaHiO, YoTAHOBKa MH KOppeKTHPOBKa NOCTORHHEIK NnoTHOMepa 3.2.1.4 Mloncnenme — Ana HexoTopnx uMt>postix nnoTHoMepos MOXeT TpeGoBaToCA HaCTpOriKa, a He kanm6poskn npxBopa, Pon wacrpolixe nnoTHOMePOS ANA YCTaHOBNeHHA NHHeNHOCTH HsMepeHii 8 pabouent AwanasoHe Tenneparyp WcnonbayioT Boanyx M CBEMeBCKHNSWeHbIM PeaKTHs — Boay (NpenynpexneHMe — Obpaujerne c KHnAWe Bono HAN BoAOTK, GnusKOH K TeMnepaType KHMeHHIR, MOMeT NpeACTaBNATe onac- Hocrs. 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Temeparype 15 °C. 6 Annapatypa 6.1 LUnc>posolt nnotHomep Uvchposomt aHannsarop, cocrosuni #3 U-oGpasHo ocyxnnupyouel tpyGkn ana OSpaaua, cHotenst ‘oneKTpoHHOro BOaByAAEHIN, BBINMCNEHUA YACTOTbI H quCNneR, AHARMZATOP AOMKeN ODECNEYNBATb TONHOE vontepenme Tennepatypsi oGpasya Bo BpeMA vaMePeNMiK Mn nomAepHAHNe TeMnepaTyPHi OGpasuA no 6.2 Tip6op aonex obecneunaars npeyvsHOHHOCTe peaynkTaTos WcnkrTaHI, 6.2 LInpynayvonian Gas c nocTORHHOR TeMneparypor (np HEOGxogNMOCTH), OBecneHnEAIOUIER onnepxarne Teuneparypsr UHPKYAMPYIOUIe! OAKOCTH B JaqaHHOM ANaNazOHe C TONHOCTBIO AO # 0,05 °C NnorHomep moxer exniovare cpegctea KoHTpons TeunepaTypbt 6.3 Wnpiyts, ncronbayewble npx saoge OOpaaya Bpyunyio, eMECTHMOCTBIO He MeHee 2 cM? 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KONCTpyKuNA asToMaTHMeCKOTO AOZaTOpA AOMNea OGecNeNHBATb YeRIOCTHOCTD O6- asua Ao akanuaa, npH ero NpoBeAeHHK W NogaNy NpeACTaBHTENbHOH| NOPYMM NENEITyeMOrO Opaaua @ UMC posoii nnorwonep 6.6 Daranx Tenmeparypss (TSD), oGecresmeaiouyti KoHTpone Tennepatype! HcnBITAHHA C ToHHOCTEIO Bo + 0,05 °C. Ppu ucnonesoBaHiu @ xavecrae TSD CTeKnaHHOrO xAEKOCTHOTO TepMoMeTpa AINA yCTaHOBNe- isn COBnioneHus Tevineparypst HonITaHH OM AOMKEH Obit OrKaNHOpOsAH M rpaAyHpOBAH C TOSHOCTBIO AO 0,1 °C wockauien gepxarenen ana nprcoeanHeNHA K npHGopy. pm KanOposke TepmomeTpa Teuneparypy nasnesis niga M AepxaTena asiMMONAIOT C TONHOCTHIO AO 0,05 °C. na HepTyTHEIX TepMOMeTpOB YCTPOR- cr80 TSD cneayer xanuOposars exeroano no cepruchuunposanHoMy M npocnexasaeMouy sTanoHy. 6.7 Ynerpaseyxosan santa Ges nonorpesa, pasmeps! KOTOPO!! no3BoNAIOT NogAepANBATE KOHTeMHEpCs) 8 BanHe ana OBecreveHun adbeKrHBHOro PACCeMBAHKA H yAaNeHKA BOIAYXa MMM NySzIpeKOB BOBAEVEHHOFO rasa, 7 Peaxtueni 1 Marepwantt 7.4 Wecnonbayior peaxriebi keanncpaKaunn 4. A. a Eon Her ApyrHX ykaaHnil, peaKTUBb! OMI! CO orpercraosare cneyncuxaynn KowmTera ananwrH4ecknx peaKTHsos AMePHKAHCKOrO xMMMHeCKOrO OBLYe- crea”). Mokio Ucrionbg0BaTb peaKTHBbl ApyroH KBANM>UKAYMM MPH YCNOBMM, HTO CTeneHb SMCTOTEI peaKTHBa He ChinkaeT ToUHOCTb OnpeneneHiA. 2 Reagent Chemicals, American chemical society specifications, American chemical society, Washington, D.C. (o6pasuye ana naBoparopiix xrmkaTos), a Tanxe the United States pharmacopeia and national formulary, U.S. Pharma- copeial convention, inc. (USPC), Rockville, MD. (apwaxones CLUA W HayroHaNsHih cbapiaxononaMeCkAA CnpaBOMHH. 3TOcT P 67037—2016 7.2 Yncrora Boab! 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Cneay- Jor MHCTpyKuWiAlt MaroTOBUTeNs ANA OGecneYeHHA YeNOCTHOCTH OBpasya AO aHANMsa, a TaKKe Ans OOecneNe- HHA npeqcTasHTenbHooTH MenbITyeMoro OGPas\a npM ero BEOAe B MPHOOP. 12.2.2 Tipu avaruse o6pasyos GeHahHos UNH pecbopmynpoBaHHLX BeHSHHOB C NOMOUYLIO ABTOCAM- nnepa, yuNTbIBaA peaynbrarb! Mexkna6opaTopHbs HCCHeAOBAHN, NonyYeHHbie 8 1999 1-4, cnenyeT MMeTb “ Nonraepxgatoute Ranibie MoxHo nonyTe & ASTM Intemational Headquarters npu aanpoce vccnepoaarent- ‘oro omvera RR:002-1734 8Toct P 57037—2016 Ba UCNBITYEMBIx OOpaaya, UTOOb! HMETS BOSMONHOCT HCNOMIOBaTb HOBLIM OOpasey NPM NONyYeHHK No- TpeWMOCTH PeaynsTaTos HCNLITAHH NPOG NeTy4HKX MaTepHANOS HnK OGHAPYKEHMM NyZbIPbKOB NPM MOHATO- Pulire paGounx xapakrepuctux npuGopa. AInA OOpasyoe apyrux THnoB np McnonbeOBAHUM asTOCAMNnepa ‘ocTaTONHO oAHoro onpemeneHus. 12.2.2.1 Ecnu na6opatopa npunumaer pewenne npoBoaMTL BTOPOe onpeAeNeHNe C McnonbsoBANHeNM aBToMaTHYeckoro BEOga ANA AUCTHNNATA, 62208070 MN CMagoNHOTO Macria (cl4. npHMeUaHHe 8 u pagaen 15), oneayer nenonesoBart KpHTepM NpMeMAeMocTH Ana nnoTHocTH (0,0002 r/c), oTHOCHTeNLHO! nsoTHOCTH (0,0002) w nnotHocrn 8 rpanycax API (0,03) no 12.1.6.1 Kak ana BBoqa NpOG Bpysnylo. MpH ocbopunenmn porokona cneayer wcnonsso8ar® cpepHeapucMeTHueckne SHaYeHKA, yAOBNETBOPAIOUIME KPHTEpHAIM, YCTA- WOBNeHHbIM 8 AAHHOM pasnene. 12.2.3 Mpw onpegenenin nnoTHocTH MAM OTHOCHTeNLHOR nnoTHOCTH OGpasyOB GeHSKHOB HnK pe- chopmynnposanHeix GeHsMHOS c NOMOWIbIO ABTOMATHYECKOrO BOA cpeaHeapHDMeTHNECKOe sHAvEHHE pesynTaros Ans AByx OGpasyos, npoaHannsMpoBaHHbix no 12.2.2, He AOmKHO oTAMUaTBCA Gonee YEN Ha 0,0002 nar/om® ana nnorHocr uni Ha 0,0002— ann orHocHTenbHoll nnoTHocTH. 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OTMMaTECA Gonee eM Ha 0,05 OT x cpenHeapidmeTieckoro sHaHeHHA, 12.2.5 Perucrpupyior pesynbrarsi onpegenenna nnoTHOCTH, OTHOCHTeNbHOM MMOTHOCTA Mn NnoTHO- ovis rpaaycaxAPI, Hanpmmep c McnonssoBaHveM nevaTaloujero yCrporicTaa, No pesynsTaraM, yaoBneTEops- /OWIMM BbILWeHENOXKEHHEIM TPeOOBAHKAM. 413 Beruncnenna 13.1 Buluncnenia nnorHocTH atannsaTopom Ana eauHi4noro onpeneneHHa (Hn BBI4HCNEHHA CpeAHEApHc>MeETHYECKOrO SHAYEHHS PesynbTaTos Abyx Onpeslenennii 8 cooTBeTCTBHH c pasgenom 12) sanMcbIBAIOT MNM pacneNaTbIBaIOT 3HAYeHHE KOHEHHOTO peaynbrara onpegeneHna nnoHocTH (r/cé?, Kr/M3) un aHaeHMe OTHOCHTeNbHO; MoTHOCTH. CreayeT OT- meri, 470 1 Kr/M3 = 1000 rom. 13.2 Buiuncnenna nnorHoctn ahanuaaTopom Ges BLINMcHHTenbHoro ycrpoiicrBa Vicnonsaysi HaGniogaewoe sHavenie T ans npoOs! v sHaveHie T ana Boab! M cooTBercrayIoUMe KO- othebuiyrene! npuBopa, onpenenenibie no 10.4.3, BbIMIICHAIOT ANOTHOCTe UNH OTHOCHTENbHYIO ANOTHOCT no cbopmynan (6) u (7). 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ACTM £] 287 unw ACTM 1 1298) Ha ocHosaHau nnoTHocTd, CoTHoCHTentHoit noTHOCTH UNM ix cONeTaHIEA, ONPeRENEHHEX To HaCTORWEMY CTaHRAPTY M NPeoGpasoBaNHEK con s0BaHiten cooTsercrayiouleth bopraynis! no ACTM 1250 (uo nossonneT wcxniounTe KoxbebHUWleHT pacuinpeHMs cTeKria) ‘Ana KonKpeTHoro Tuna aHanvonpyeMod npoSks 14 Ocbopmnenve pesyntraton 14.1 Bnporoxone ucnbiraHit ykaaHieaior nnloTHOcTb, TeNInepatypy HCNLITAHW M EAKHKY! HaMepeHH (hanpumep nnorHocte npn 20 °C = 0,8765 r/cm? unn 876.5 Kr/?) 14.2 B npoToKone ana oTHocHTensHOit nnoTHOCTH yKasbIBAIOT ABA SHAYeHHA TeMnepatypbi — sHaNe- Hue Tenneparypbl HcnbITaHKA M aHaVeHHe CTaHAapTHO! Tennepatyps Ges ykagaHiA eqUHUL, (HANPHMEP, oTHocHTenbHan nnoTHOCTb, 20/20 °C = 0, x90) 14,3. 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Ta6nuya 2—Nosropremocts onpenenenua nnoTHocT# (ricu®) w oTHOcHTenBHOM nnoTHOCTH Awanason 6paseu "Yenoave nposenevin wensiTawnn Rosroprewocrs 0,71-0,78 | Gexsmnstn pecpopmynnposar~ | — Onvo onpegeneHne (py4Hon BBoq) 0,00045 ue Genanies Cpepneapnibuerniecnos sHaveHne _agyx onpenenenui (pysHok w asTomaTmeckwA eson) | 0,00031 080-088 | Dyctannares, Gasosie wacna | OnHo onpenenenue (py'moit # asTonaTH4e- Wcwtasoutie macna count e800), 0,00016 Cpenneapnebmerieckoe shaveHne _AaByx onpenenenii (pysHok u asrouarmiecsleaoq) | 0,00011 Ta6nuya 3—Mostopremocts onpeneneHia nnoTHocT# B rpanyeax API Bwanason 6paseu, Yenoane nposegenua wenerann Rosroprewocrs 51-66 | Gesamiiupedbopny- | Ogko onpenenenve (pystiol agoa) | 0,090 -upoBaniiie Gensuiet CpeaneapnaueT#uecKoe sHavehne geyx onpegenennit (pysion w azromarnueckai aaoa) 0,063 2045 | Ducrannarer, 6a20-| Ogno onpeaenenue (pysioll uw asTonaTwveckwit 8602) 0,032 aie wacna wewasounuie | CpemweapneperaMectoe sHavenMe jeyx onpenenenni aca (pysHolt w abromarnveckn 8802) 0,022 10Toct P 57037—2016 18.1.2 Bocnpousaoqumoct Pacxorkaehne pesynstaroe ayx eAHKMMHLIX H HEIABMCHNMEIX HonBITaNM, OAYHeHHEIX pasHbiMn Onepa- ‘Topann, paGoTarounan 8 pasHbix naSOpATOpHAX, Ha MeHTHYHOM MCNbITYeMOM MaTepHane & TeYeHHE AM. 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