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Determination of the engine power for quenching of glass by forced


convection: simplified model and experimental validation of residual stress
levels

Article in Glass Structures and Engineering · January 2019


DOI: 10.1007/s40940-018-0078-5

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Navid Pourmoghaddam Jens Schneider


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Glass Struct. Eng.
https://doi.org/10.1007/s40940-018-0078-5

RESEARCH PAPER

Determination of the engine power for quenching of glass by


forced convection: simplified model and experimental
validation of residual stress levels
N. Pourmoghaddam · J. Schneider

Received: 21 March 2018 / Accepted: 1 May 2018


© Springer International Publishing AG, part of Springer Nature 2018

Abstract This work presents a simplified model for they are quenched i. e. rapidly cooled down by air jets
the determination of the engine power as a function from both sides to an ambient temperature. This pro-
of the residual stress using quench parameters by cess is illustrated in Fig. 1. When heated in the oven,
forced convection and introduces the necessary empir- the glass is in a viscous state and when quenched, the
ical equations of integral heat and mass transfer coeffi- glass plate hardens through the thickness. First the both
cients suggested by Martin (1977). For a residual stress surfaces cool and harden. The temperature difference
dependent production of thermally tempered glasses, between the surface and the centre plane grows until
float glasses were thermally tempered due to heat treat- a maximum is reached and then the centre plane also
ment of the glass panes with different heat transfer cools down and cools faster than the surface. The area
coefficients. In the method presented, quench parame- between the two surfaces of the plate contracts and puts
ters for determining the engine power required to reach the surfaces into a permanent compressive state. Due
the target residual stresses are taken into account. The to the equilibration of the surface compressive stresses
plausibility of the model is checked on the basis of tensile stresses result in the mid-plane of the glass plate.
experimental data. The residual stress distribution is parabolic through the
thickness as it is shown in Fig. 2. The parabolic stress
Keywords Tempered glass · Residual stress · distribution is in equilibrium and symmetric about the
Quenching · Heat transfer coefficient · Cooling air mid-plane. The surface stress is approximately twice
velocity · Engine power the tensile stress in magnitude (2σm = σs ). The zero
stress level is at a depth of approximately 20% of the
1 Introduction thickness t.
The residual stresses are strongly process-related
Thermally tempered glass and heat strengthened glass and vary under different boundary conditions such as
are produced by heating and rapidly cooling float glass the cooling rate, the nozzle arrangement, the nozzle
panes. For this purpose, glass plates are fed on rolls diameter, the distance between the nozzles and the glass
into an oven where they are heated to approximately surface as well as the roller distances. The initial tem-
100 ◦ C above the glass transition temperature. After- perature as well as the cooling rate in particular have a
wards they are moved further into a quench area where significant influence on the residual stress development
during the tempering process, see e.g. Narayanaswamy
N. Pourmoghaddam (B) · J. Schneider
Technical University of Darmstadt, Franziska-Braun-Str. 3,
and Gardon (1969) and Aronen and Karvinen (2017).
64287 Darmstadt, Germany
e-mail: pourmoghaddam@ismd.tu-darmstadt.de

123
N. Pourmoghaddam, J. Schneider

Fig. 1 Sketch of the process line for tempering flat glass

the desired residual stresses in glass panes from the


tempering process.
It is important for the manufacturer to be able to
calculate the residual stress before the process for an
effective utilization of the tempering oven and also for
an accurate residual stress result. Our motivation was
to produce glass specimens with systematically varying
Fig. 2 Residual stress distribution through the thickness in the residual stresses for a subsequent fragmentation anal-
far field area of a tempered glass plate ysis (Pourmoghaddam and Schneider 2018b).
In order to study the correlation between the resid-
ual stress, particle count, particle weight and particle
The heat transfer coefficient, which describes the size, glass plates with three different thicknesses of 4,
cooling property of a surface and governs the cooling 8 and 12 mm were tempered with heat treatment condi-
process is very difficult to determine experimentally. tions for a predetermined residual stress range. For the
For this reason, many authors who have numerically different heat treatment of the specimens the engine
simulated the tempering process have always focused power of the tempering oven was estimated and var-
on the analytical or complex numerical determination ied by recalculating the air velocity and the air pres-
of the heat transfer coefficient. The tempering process sure from the iteratively determined heat transfer coef-
has been numerically calculated by several authors, e.g. ficients needed for yielding the target residual stress.
Narayanaswamy and Gardon (1969), Laufs and Sed- After the tempering process, the residual stress in the
lacek (1999a), Laufs and Sedlacek (1999b), Schneider glass specimens were measured, using a scattered light
(2001), Daudeville et al. (2002), Bernard et al. (2005), polariscope (SCALP).
Nielsen et al. (2010), Aronen (2012), Pourmoghad-
dam et al. (2016) and Pourmoghaddam and Schnei- 2 Specimen preparation for the thermal tempering
der (2018a). This work presents equations, which have
been compiled by Martin (1977) from experimental For the fracture tests we produced three series of tem-
data for the determination of the heat transfer coef- pered glass specimens of size 360 mm ×1100 mm
ficient knowing the process boundaries as described with three different thicknesses of 4, 8 and 12 mm
above. This can also be used for the determination of (see Table 1). There were 24 specimens in each series

Table 1 Series for the


Series Specimens Specimens Runs per Dimension [mm] Thickness
tempering process
per series per run series [mm]

ScA 24 3 8 360 × 1100 4


ScB 24 3 8 360 × 1100 8
ScC 24 3 8 360 × 1100 12

123
Determination of the engine power for quenching of glass

velocity w and subsequently a required air pressure P.


The engine power was then calculated considering the
experience values for the relation between the adjusted
engine power and the resulting air pressure P.

3 Heat transfer coefficient

The heat transfer coefficient, which is required for


yielding the target residual stresses (Fig. 3), was cal-
culated by means of a Finite Element simulation of
the tempering process using an infinite 2D-axisymetric
model. A FE-Model for the simulation of the thermal
tempering process and the numerical calculation of the
residual stresses has been discussed in detail by several
authors, see e.g. Laufs and Sedlacek (1999a, b), Aronen
(2012), Nielsen (2009), Pourmoghaddam et al. (2016)
Fig. 3 Eight target mid-plane tensile stresses for the heat treat- and Pourmoghaddam and Schneider (2018a). The vis-
ment of the series with three different thicknesses 4, 8 and 12 mm coelastic material behaviour of glass in the glass tran-
considering the level of strain energy for the start of crack branch- sition range is considered in the FE-Model. The struc-
ing according to Fineberg (2006)
tural relaxation is taken into account using the model
of Narayanaswamy (1971). For the simulation of the
tempering process the FE-Model of the glass plate was
divided into eight groups of three specimens for each given an initial temperature of T0 = 650 ◦ C and cooled
run of the tempering process. Hence, there were eight down to the ambient temperature of T∞ = 25 ◦ C.
runs of the tempering process per series for achieving The time increments needed for converged results of
eight different residual stresses in each series. In order the tempering process for different glass thicknesses
to choose the target residual stresses for the heat treat- were given in Pourmoghaddam and Schneider (2018a).
ment of the series, the elastic strain energy level for The resulting time-temperature relationship was put in
the start of the crack branching of glass according to terms of load steps on a structural mechanical model
Fineberg (2006) was considered. However, this level to calculate the stress response due to the tempering
of energy represents the start of local crack branching process. The different heat transfer coefficients were
by one rapidly moving tensile crack. The question was determined for yielding a residual surface compressive
how this level would influence the fracture pattern of stress as shown in Fig. 5.
a tempered glass. Therefore, in the first step the target
residual stresses were chosen above as well as below
the strain energy level of 35 J/m2 . As it is shown in
4 Cooling air velocity
Fig. 3 , eight target residual mid-plane tensile stresses
were chosen from 10 to 60 MPa for the 8 and 12 mm
The various cooling air velocities w were calculated
thick specimens and from 10 to 45 MPa for the 4 mm
using the empirical equations of integral heat and mass
thick specimens.
transfer coefficients suggested by Martin (1977). The
For the heat treatment of the series, the engine
Nusselt-number N u, the Reynolds number Re and the
power of the thermal tempering oven was varied. Thus,
Prandtl-number Pr are material dependent, dimension-
the engine power needed for the corresponding resid-
less values and can be written as:
ual stress was determined considering the procedure
sketched in Fig. 4. The engine power for the cooling hD
section of the thermal tempering oven was recalculated Nu = (1)
λ
by the determination of the required heat transfer coef- wD
ficient h, which in turn leads to a certain cooling air Re = (2)
ν

123
N. Pourmoghaddam, J. Schneider

Fig. 4 Procedure for the


determination of the engine
power of the tempering
oven

ν
Pr = (3)
a

where D is the inner diameter of a nozzle, h the heat


transfer coefficient and w is the cooling air velocity.
The material values of the cooling medium, air, are the
thermal conductivity λ, the kinematic viscosity ν and
the thermal diffusivity a at an arithmetically averaged
fluid temperature Tm = (TN + TS )/2 between the tem-
perature at nozzles outlet TN and the temperature at the
surface of the glass plate TS . The empirical equations
for the integral heat and mass transfer coefficients for
an array of round triangular arranged nozzles (ARN),
as shown in Fig. 6, in terms of the practical application
is suggested by Martin (1977) as:

N u A R N = G · Re2/3 · Pr 0.42 (4)


d ∗ · (1 − 2.2d ∗ )
Fig. 5 Heat transfer coefficient [W/m2 K] versus surface com- G=
1 + 0.2 · (h ∗ − 6) · d ∗
pressive stress [MPa] from FE simulations    −0.05
10 · h ∗ · d ∗ 6
· 1+ (5)
6

Fig. 6 Left: Nozzle configuration: a single round nozzle (SRN), and Martin 2013), right: sketch of the impinging jet flow, inner
b single slotted nozzle (SSN), c array of round nozzles (ARN), d diameter of a nozzle D and distance H between the nozzles and
array of slotted nozzles (ASN) from VDI Heating atlas (Schabel the surface of the glass plate

123
Determination of the engine power for quenching of glass

Fig. 7 a Calculated cooling air velocity [m/s] versus heat trans- L T = 5 mm (ARN) and the material values of the cooling
fer coefficient [W/m2 K], b calculated cooling air velocity [m/s] medium air W/mK, m2 /s and m2 /s for an arithmetically aver-
versus surface compressive stress [MPa], calculations in a and aged temperature Tm from the temperatures TN = 25 ◦ C and
b based on the geometry values H = 50 mm, D = 5 mm and TS = 650 ◦ C

with the validity range for G: using Eq. (8) the value for the air velocity w was varied
iteratively until the numerically determined heat trans-
0.004 ≤ (d ∗ 2 = f ) ≤ 0.04, fer coefficient h was yielded. The cooling air velocities
∗ in correlation of the target residual surface compres-
2≤ (h = H/D) ≤ 12,
sive stresses are shown in Fig. 7b. The calculations
2000 ≤ Re ≤ 100, 000
were carried out with the nozzle values L T = 5 mm,
H = 50 mm and D = 5 mm for the cooling section of
In the case of triangular arranged array of round nozzles
the thermal tempering oven.
(ARN) the relative nozzle area f can be written as:

π D2 5 Engine power of the tempering oven


f = √ · 2 (6)
2 3 LT
 D The glass plates were tempered in groups of three using
d ∗ = f = 0.9523 (7) the thermal tempering oven of the company Semcoglas
LT
Holding GmbH (December 2016). Once the cooling air
where L T is the distance between the nozzles and H velocity w for different target residual stress states is
is the distance between the nozzles and the surface of determined, the air pressure P can be calculated using
the glass plate (see Fig. 6). The cooling air velocity Eq. (9) for the total pressure with the air velocity pres-
was recalculated using the Eqs. (1)–(7). Inserting the sure and the hydrostatic air pressure:
Eqs. (1), (2) and (3) in Eq. (4) we obtain for the heat 1
transfer coefficient: P = ρw 2 + ρgh j (9)
  2
Gλ w D 2/3  ν 0.42 where h j is the distance between the pressure chamber
h= · · (8)
D ν a and the air jets, ρ the air density and g is the gravity.
In Fig. 7a), the heat transfer coefficient depending on After the determination of the required air pressure
the calculated cooling air velocity w is shown. Thereby, for each target residual stress considering the cool-

123
N. Pourmoghaddam, J. Schneider

responding heat transfer coefficients, cooling air veloc-


ities and subsequently the required engine powers are
summed up in Table 2 for the three thicknesses of 4, 8
and 12 mm. For the determination of the air pressure
an average atmospheric pressure of 1013.25 Pa and the
temperature of 25◦ C was assumed (ρ = 1.184 kg/m3 ).

6 Stress measurements

In order to check the actual stress state in the spec-


imens the residual stresses were measured after the
tempering process using a scattered light polariscope
(SCALP) developed by GlasStress Ltd. The residual
stresses in vertical and horizontal direction in thirteen
measurement points were measured at both surfaces of
the specimens, see Fig. 9. The anisotropy of the residual
Fig. 8 Engine power E P in percentage of the total power vs.
air pressure P [Pa]; points show experience values of the tem- compressive surface stresses in the area of the measure-
pering oven and solid curve show the trend line including the ment points was quite low with a coefficient of variation
corresponding function and the coefficient of determination R 2 around 3%. In Fig. 10, the optical path difference under
polarized light is shown for three different thicknesses.
It was observed that the anisotropy and the inaccura-
ing air velocity and the heat transfer coefficient, the cies in yielding the target residual stresses increased for
air pressure was matched to the empirical function of the 12 mm thick plates. In Fig. 11a, the target residual
the thermal tempering oven in terms of the correla- stresses in comparison to the average of the measured
tion between the engine power E P as the percentage mid-plane tensile stresses in the measurement points
of the total power of the thermal tempering oven and after the tempering process is shown.
the resulting air pressure in the height of the air jets. Due to the lack of accuracy of the thermal tempering
The empirical function of the thermal tempering oven oven for the low engine power range, it was not possi-
is shown in Fig. 8. The eight target residual mid-plane ble to reach the lowest target residual stress states, espe-
tensile stresses, which were plotted in Fig. 3 and the cor- cially for the 12 mm thick plates, see Fig. 11a. However,

Table 2 Target residual mid-plane tensile stresses σm [MPa] and power E P [%] as the percentage of the total power, h j = 0.65 m,
the corresponding heat transfer coefficients h [W/m2 K], cooling ρ = 1.184 kg/m3 (atmospheric pressure and 25 ◦ C)
air velocities w [m/s], air pressure P [Pa] and the required engine

t = 4 mm t = 8 mm t = 12 mm
σm h w P EP σm h w P EP σm h w P EP
[MPa] [W/m2 K] [m/s] [Pa] [%] [MPa] [W/m2 K] [m/s] [Pa] [%] [MPa] [W/m2 K] [m/s] [Pa] [%]

10 76.8 9 55.5 6.6 10 35.5 5 22.9 4.0 10 25.0 4 16.1 3.3


15 115.2 16 159.1 12.1 15 51.8 9 54.4 6.6 15 35.0 6 30.3 4.7
20 153.6 25 377.5 19.7 20 67.7 13 112.3 9.9 20 45.6 9 57.7 6.8
25 192.0 35 732.7 28.8 25 86.4 19 225.8 14.7 25 56.6 13 103.0 9.4
30 240.0 49 1428.9 42.1 30 106.1 26 410.8 20.7 30 68.5 17 178.6 12.9
35 278.4 61 2210.4 54.0 40 149.8 44 1138.1 37.0 40 94.2 27 452.0 21.9
40 335.0 78 3609.3 71.3 50 203.5 70 2891.8 62.9 50 123.8 41 1012.4 34.6
45 393.6 103 6288.1 97.8 60 264.0 102 6215.1 97.2 60 157.4 59 2068.3 52.0

123
Determination of the engine power for quenching of glass

considering the objective of yielding different residual the development of high residual stresses. The inaccu-
stresses for a reasonable fragmentation analysis, the racy due to the lower cooling rates could be due to the
heat treatment of the specimen series was both neces- inaccuracy of the fan power. The determined engine
sary and successful.
In Fig. 11b the correlation between the residual mid-
plane stress and the engine power of the tempering oven
is shown. The values given on the x-axis for the engine
power are the required fan powers of the motor relative
to the maximum power. It was observed that the accu-
racy of the residual stresses decreased with thicker glass
plates and at lower cooling rates. Especially the inac-
curacy due to the thickness was expected. For thicker
glass plates, a very low cooling rate is sufficient for

Fig. 10 Optical path difference under polarized light, a t=


3.8 mm, σs = − 91.3 MPa (rel. deviation of 1.28%), b t=
Fig. 9 Positions and directions of the residual stress measure- 7.9 mm, σs = − 91.1 MPa (rel. deviation of 1.15%), c t=
ments 12.0 mm, σs = − 97.4 MPa (rel. deviation of 2.01%)

Fig. 11 a Elastic strain energy U [J/m2 ] vs. mid-plane ten- 2006), b mid-plane tensile stress [MPa] versus engine power
sile stress [MPa]; coloured points show the average residual [%] of the tempering oven; coloured points show the measured
mid-plane stress from thirteen measurement points; hollow cir- residual stress after the tempering process,solid lines are trend
cles show the target residual mid-plane stress from Fig. 3; lines including the corresponding function and the coefficient of
U = 35 J/m2 is the start of the crack branching (Fineberg determination R2

123
N. Pourmoghaddam, J. Schneider

power for achieving low residual stresses could not be parameters for the quenching of glass plates can be
set exactly. determined from this simplified calculations.

Compliance with ethical standards


7 Summary and conclusion
Conflict of interest The authors declare that they have no con-
flict of interest.
This work comprehensively demonstrated a simplified
model for the determination of the engine power as
a function of residual stresses for quenching of glass
by forced convection. For a residual stress dependent References
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