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Quantachrome NovaWin - Data Acquisition and Reduction

for NOVA instruments


�1994-2013, Quantachrome Instruments
version 11.03

Analysis Report
Operator: quantachrome Date:2023/04/19 Operator: quantachrome
Date:2023/05/05
Sample ID: Cambi A Filename: Cambi A F.qps
Sample Desc: Comment:
Sample weight: 0.1143 g Sample Volume: 0.1271 cc Sample
Density:1 g/cc
Outgas Time: 5.0 hrs OutgasTemp: 100.0 C
Analysis gas: Nitrogen Bath Temp: 273.0 K
Press. Tolerance:0.100/0.100 (ads/des)Equil time: 60/60 sec (ads/des) Equil
timeout: 240/240 sec (ads/des)
Analysis Time: 402.2 min End of run: 2023/04/19 0:17:28 Instrument:
Nova Station C
Cell ID: 19
Data Reduction Parameters
Thermal Transpiration: onEff. mol. diameter (D): 3.54 �Eff. cell
stem diam. (d): 4.0000 mm

t-Method Calc. method: de Boer


BJH/DH method Moving pt. avg.: off Ignoring P-tags below 0.35 P/Po
HK method Tabulated data interval: 1
SF method Tabulated data interval: 1
DFT method Calc. Model: N2 at 77 K on carbon (slit pore, NLDFT equilibrium
model)
Rel. press. range: 0.0000 - 1.0000 Moving pt.
avg: off
Adsorbate Nitrogen Temperature 77.350K
Molec. Wt.: 28.013 Cross Section: 16.200 Ų Liquid
Density: 0.808 g/cc
Adsorbent Carbon

Surface Area Data

MultiPoint BET 4.390e+01


m�/g
BJH method cumulative adsorption surface area 2.068e+01
m�/g
BJH method cumulative desorption surface area 3.404e+01
m�/g
DH method cumulative adsorption surface area 2.107e+01
m�/g
DH method cumulative desorption surface area 3.485e+01
m�/g
DFT cumulative surface area 3.360e+01
m�/g

Pore Volume Data

Total pore volume for pores with Radius


less than 972.25 � at P/Po = 0.990039 8.345e-02
cc/g
BJH method cumulative adsorption pore volume 6.986e-02
cc/g
BJH method cumulative desorption pore volume 7.561e-02
cc/g
DH method cumulative adsorption pore volume 6.828e-02
cc/g
DH method cumulative desorption pore volume 7.425e-02
cc/g
HK method micropore volume 1.787e-02
cc/g
SF method micropore volume 1.309e-02
cc/g
DFT method cumulative pore volume 6.811e-02
cc/g

Pore Size Data

Average pore Radius 3.801e+01



BJH method adsorption pore Radius (Mode Dv(r)) 1.889e+01

BJH method desorption pore Radius (Mode Dv(r)) 1.891e+01

DH method adsorption pore Radius (Mode Dv(r)) 1.889e+01

DH method desorption pore Radius (Mode Dv(r)) 1.891e+01

HK method pore Radius (Mode) 1.838e+00

SF method pore Radius (Mode) 2.261e+00

DFT pore Radius (Mode) 1.897e+01

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