Industrial Wastewater Treatment - Sep 2021

Prepared By : Md.
Mahbub Alam 9/26/2021
Fundamental of ETP, Operation, Process Control & Management Fundamental of ETP, Operation, Process Control & Management
Institute of Professional Learning & Development Slide 1 Institute of Professional Learning & Development Slide 2
Today’s Learning Objective Expected Outcome from the sess ion
Fundamental of ETP Operation, Process Control & Management . Introduction To ETP & Waste Management
 What is wastewater & it's sources
 Characteristics of wastewater & it's legal Requirements End of this session the


Types of wastewater treatments & it’s fundamentals
ETP operation & process control
participants will be able


Water & Wastewater Management
ETP contingency plan
to get a clear idea about
 Lab manual & practice managing wastewater
 ETP assessment guideline & documentation.
 Final Quiz from the generation point
to disposal
Prepared By : Md. Mahbub Alam 9/26/2021
Presented by Lead Facilitator

Md. Mahbub Alam
Introduction To ETP & Waste Management
Organized By:
Chemical, ETP & Environmental Expert
Md. Mahbub Alam is one of the most experienced &
Institute of Professional Learning & Development. competent Environment, Chemical & Wastewater
(IPLD) Management system practitioner as well as trainer in
Bangladesh. During his 10 years’ career in Environment,
House 31, Road 01, Sector 09, Uttara, Dhaka 1230.
Chemical & Waste Management System arena, he worked in
Contact: +8801716542764, +8801958484352. 100% export-oriented garments manufacturing factory. Now
Email: info2ipld@gmail.com, info@ipldbd.com he is working as a freelancer with a National multinational
Website: www.ipldbd.com company as a Chemical & Environmental expert & auditor.
Also Heading Business Development & Operation, as a Chief
Executive Officer at EPL Group, Uttara.
Mr. Alam delivered around 45 Public training in different
topics in Environment, Water & Wastewater, Chemical, Solid
Waste, ETP Operation, Process Control & Management.
Types of Topics Number of Training Number of Participants

12 60 1050
DELEGATE INTRODUCTION Instruction to the Delegates
Take 5 minutes time to know your nearest co- • No cell phones

participant and present information about him at • Comfort breaks as needed
• Safety considerations
least below characteristics but not limited to
• Complaints and Concerns
• Name • Be respectful and be on time
• Participation is a requirement
• Position • Class Discussion -
• Company • Group Exercises – work and contribute
with different people in different groups
• Objective from this course
Important Information Key to achieve the session Goal
10
Outline of content: What is waste water?

In simplest words, it can be said that wastewater is nothing, but the used
water of liquid waste generated by the community due to its various
activities, and contains the impurities in excess of the permitted /
 What is water & it’s sources ? regulated statutory limits.
 Characteristics of wastewater & it's legal Requirements
 Types of wastewater treatments & it’s fundamentals
 ETP Process Related Calculations
 ETP operation & process control
 Requirement of water management in Higg FEM 3.0
 Classification of ETP performance based on ZDHC & BSR guideline.
 Water & Wastewater Management
 ETP contingency plan
 Lab manual & practice
 ETP assessment guideline & documentation. Technically, However, Wastewater can be defined as any water or liquid
 Final Quiz that contains impurities or pollutants in the form of solids, liquids or
gases or their combinations in such a concentration that is harmful if
disposed into the environment.
WATER POLLUTION: Oxygen deficiency Sources of Waste water
Sources of Waste water Type of Wastewater
Depending upon the source of generation,
wastewaters are broadly classified as
1. Domestic wastewater
2. Industrial Wastewater
Type of Wastewater Outline of content:

 What is water & it’s sources ?
 Characteristics of water & it’s legal requirements
Type of Wastewater Source of wastewater  Types of water treatment & it’s fundamentals
 WTP operation & Process control
Washing water from the kitchen,  Requirement of water management in Higg FEM 3.0
Gray water bathroom, laundry (without faces and  What is wastewater & it's sources
urine)  Characteristics of wastewater & it's legal Requirements
Water from flush toilet (faces and urine  ETP operation & process control
Black water  Requirement of water management in Higg FEM 3.0
with flush water)
Yellow water Urine from separated toilets and urinals  Water & Wastewater Management
Black water without urine or yellow
Brown water  Lab manual & practice
water  ETP assessment guideline & documentation.
 Final Quiz
Fresh Water How much water do we have?
• 97.5% of Earth’s water is Salt water

• A vital resource to life on this planet
• 2.5% is Fresh Water (65% Ice and 35% Liquid Water)
• Less than 1% Accessible Fresh Water
Institute of Professional Learning & Development Slide 19 Institute of Professional Learning & Development Slide
20
Why should everybody be more Why should everybody be more

conscious about water usage? conscious about water usage?
• In many areas, as the demand for water • While efforts are made to sustain water quantity and
increases it is becoming a very scarce quality in city water supplies, Dhaka pumping has
resource. caused groundwater levels to drop more than 200 feet
over the last 50 years and these levels continue to
decline at a rate of up to 9 feet per year.
Why should everybody be more

Why should everybody be more conscious about water usage?
conscious about water usage?
Water Pollution is also a major concern.
• Causes diseases
• In many areas, as the demand for water • Kill fish and other organisms
increases it is becoming a very scarce • Makes water unfit to use
resource.
Effluent Treatment Plant ETP Process Flowchart
• Effluent Treatment Plant or ETP is one type of waste

water treatment method which is particularly designed
to purify industrial waste water for its reuse and it’s
aim is to release safe water to environment from the
harmful effect caused by the effluent.
Institute of Professional Learning & Development Slide Institute of Professional Learning & Development Slide
25 26
Legal Requirements Legal Requirements
Institute of Professional Learning & Development Slide 29 Institute

Institute of Professional
of Water Learning
& Wastewater Research & Development
Technology Slide 30
Legal Requirements Minimum Requirements

Flow Meters
• Flow meters should be installed, at a minimum at input and output points to measure water
volumes on a regular basis
Staff
• A competent employee always needs to be on site to manage wastewater treatment activities
(trained in maintenance of technical equipment -machines in production as well as abatement
and recovery devices)
Lab Equipment
• Facilities should have the following lab equipment readily available on site.
 Spectrophotometer
 COD Reactor
 BOD Incubator
 Multimeter
 Imhoff Cone
 Filtration Apparatus
Institute of Professional Learning & Development Slide 31 Institute

Institute of Professional
of Water Learning
& Wastewater Research & Development
Technology Slide 32
Minimum Requirements Minimum Requirements
Legal issues Legal issues
Conditions: Conditions:
• Flow measuring devices need to be installed at the inlet and outlet • Environmental aspects of a factory needs to be managed by
pipes of ETP and their records have to be maintained. qualified environmental personnel.
• Following treatment, the sludge needs to be processed using filter- • Effluent records should be updated daily. Summary of these records
press, and should be kept within the premises. should be submitted to DoE after every 3-months.
• After 6 months, it can be disposed during dry season, and a register • Within 3 months of clearance renewal, wastewater recycling and
have to be maintained. Bypass lines avoiding ETP is not allowed. zero discharge plans/designs needs to be submitted.
• Approved Resource Conservation Plan has to be implemented.
Minimum Requirements Characteristics of Wastewater
Zero Tolerance Activities

Industrial Wastewater Characteristics:
Can be classified under following three types:
Any facility that discharges illegally or by passes
(i) Physical Characteristics
treatment systems is considered as ‘not compliant’
(ii) Chemical Characteristics and
and the appropriate steps to address the issue should
(iii) Biological Characteristics
be taken immediately.
Characteristics of Wastewater Characteristics of Wastewater

Physical Characteristics:
Characteristics of industrial wastewater are: Chemical Characteristics: the three types are:
• Temperature (i) Organic matter

(ii) Inorganic matter and
• Odor (iii) Gases
• Color
• Solids
• Density
• Turbidity
• Taste
www.Slideshare.com
Source: www.conhoo.com Source: www.Slideshare.com
Characteristics of Wastewater Characteristics of Wastewater

Chemical Characteristics of quality Parameters: Biological Characteristics:
• pH Key Microorganisms Involved in Wastewater Treatment
• Dissolved Oxygen (DO)
• Biochemical Oxygen Demand (BOD)
• Floc Forming Bacteria (saprophytes):
• Chemical Oxygen Demand (COD Primary Facultative Heterotrophs, Soil
• Total Kjeldhl Nitrogen (TKN) and Aquatic Genera
• Chlorides • Nitrifying Bacteria: Ammonia Oxidizing
• Metals Bacteria (AOB) and Nitrite Oxidizing
• Heavy metals
• Oil and Grease
Bacteria (NOB)
• Dissolved Phosphors • Predators: Protozoa, Rotifers,
• Sulfur Nematodes
• Others • Nuisance Bacteria and Eucaryotes:
Bulking, Foaming, Overgrazing
• Others: Algae, Yeast, Viruses
(Bacteriophage), etc. www.wikipidia.com www.waterworld.com
POLLUTANT VS ENVIRONMENTAL PROBLEM POLLUTANT VS ENVIRONMENTAL PROBLEM
Pollutant Environmental Problem Pollutant Environmental Problem

Biodegradable: Microbial growth in receiving Organic compounds bodies; Toxic compounds: Toxicity to flora, fauna, humans
possible toxicity; Oxygen depletion. Toxicity to flora, fauna, humans
Cyanides:
Suspended Solids: Microbial growth in receiving bodies; Deposition of sludge Phenolic: Toxicity to flora, fauna, humans, odor
blanket; possible toxicity; turbidity
Color: Aesthetics Inhibition of algal growth
Coliform and other: Health problems microorganisms
Nitrogen: Ammonia, nitrite and nitrate
pH: Toxicity to flora, fauna, humans
Nitrate: Relatively safe for adults but quite hazardous for infants below
Oil and grease: Fouling, damages to flora and fauna 6 months pH in their stomach is about 4.0 (as opposed to 2.0 in
Nutrients: Toxicity to aquatic life; eutrophication (Nitrogen, adults). This higher pH promotes the growth of a bacterium
phosphorous) capable of converting nitrate to nitrite.
Temperature: Toxicity to aquatic life Nitrate: concentration in drinking water should be below 50 mg/L
Surfactants: Toxicity to aquatic life; aesthetics Phosphorous: Orthophosphate (PO43-, HPO42-, H2PO4-) or polyphosphates
Sulfides: sulfates: Toxicity; odor (H2S); pH Rapid oxygen deoxygenating of the water
Heavy metals: Toxicity to flora, fauna, humans depletion:
Why do we need to treat wastewater ? Why do we need to treat wastewater ?

 To prevent groundwater pollution
 To prevent sea shore • Protecting the public health:
 To prevent soil  Wastewater contains pathogenic microorganisms lead
 To prevent marine life
 Protection of public health to dangerous
 To reuse the treated effluent  diseases to humans and animals
- For agriculture
- For groundwater recharge  Hazardous matter such as heavy metals that are toxic
- For industrial recycle
 Solving social problems caused by the  Produces odorous gases and bad smell
accumulation of wastewater
Why do we need to treat wastewater ? Why do we need to treat wastewater ?

• Protecting the environment:
 Raw Wastewater leads to septic conditions in the environment and
Legal Requirements & Standards
 consequently leads to the deterioration of surface and groundwater quality Environment Conservation Act (1995) and
 and pollutes the soil. Environment Conservation Rules (1997):
Environmental Clearance Certificate must be obtained before starting activity;
 Raw wastewater is rich with nitrogen and phosphorus (N, P) and leads to
• Industrial Units and Projects are classified under 4 categories;
 the phenomena of EUTROPHICATION.  Green (no wastewater considerations)
 Orange-A (Operational information + effluent discharge arrangements)
 EUTROPHICATION is the growth of huge amounts of algae and other
 Orange-B (Washing industry must have ETP, EMP & others information)
 aquatic plants leading to the deterioration of the water quality.  Red (Dyeing industry must have ETP & Environmental Impact
Assessment)
 Raw wastewater is rich with organic matter which consumes oxygen in
 aquatic environment. Manual for Sludge Management in Bangladesh Textile Sector-
October 2016
 Raw wastewater may contains toxic gases and volatile organic matter
পিরেবশ আদালত আইন, ২০১০
Outline of content: Types of Wastewater Treatments

 Characteristics of water & it’s legal requirements Process Description Treatment Level
 Types of water treatment & it’s fundamentals
 WTP operation & Process control Removal of large solids such as rags, sticks,
 Requirement of water management in Higg FEM 3.0 Physical grit and grease that may damage equipment or Preliminary
 What is wastewater & it's sources result in operational problems
 ETP operation & process control Physical and Removal of floating and settle able materials
Primary
 Requirement of water management in Higg FEM 3.0 chemical such as suspended solids and organic matter
Biological and Removal of biodegradable organic matter and
 Water & Wastewater Management Secondary
chemical suspended solids
 Lab manual & practice Physical, chemical Removal of residual suspended solids
Tertiary/advanced
 ETP assessment guideline & documentation. and biological /dissolved solids
 Final Quiz
Types of Wastewater Treatments Types of Wastewater Treatments

1) Physico-Chemical ETP: The removal efficiency of P-C ETP has been found 2) Biological ETP: with proper maintenance and operation B-ETP can efficiently remove
to be 50% and 70% for BOD5 and COD respectively; not suitable to remove TDS. BOD, pH, TSS, Oil and Grease requirements.; require more land area for ETP installation.

3) Physico-Chemical and Biological ETP: BOD and COD removal efficiency is up to 90%
Primary Treatment
• Screening
• Neutralization
• Chemical Oxidation
• Chemical Reduction
• Coagulation
• Flocculation
• Gravity Separation
• Dissolved-air Flotation

Tertiary/Advanced Treatment
Secondary Treatment
• Media Filtration
• Aerated Lagoons • Granular Activated Carbon
• SBR • Powdered Activated Carbon
• Trickling Filters • Reverse Osmosis
• MBBR • Ion Exchange
• Activated Sludge • Electro Dialysis
• High Rate Activated Sludge
• USAB (Up flow Anaerobic
Sludge Blanket)
www.jurby.com
Types of Wastewater Treatments Function of Treatment Plant Units

Reverse Osmosis Function of ETP Process
VIDEO
Function of Treatment Plant Units Function of Treatment Plant Units

 Final Quiz

Table 1: Wastewater Treatment Levels and Processes
Treatment Level Description Process

FLOW DIAGRAM
Removal of large solids such as rags, sticks, Raw Effluent → Collection Sump Tank → Screening Unit →
Preliminary grit and grease that may damage equipment or
result in operational problems
Physical Lifting Pump Sump → Storage & Homogenization Tank →
Neutralization Unit → Cooling Unit → Distribution Unit →
Removal of floating and settle able materials Physical and
Biological Oxidation Tank → Sedimentation Feeding Tank →
Primary
such as suspended solids and organic matter chemical Clarifier/Sedimentation Tank → Post Aeration Tank → Treated
Effluent
Removal of biodegradable organic matter and Biological and
Secondary
suspended solids chemical Sludge Recirculation Pit → Distribution Unit
Physical,
Tertiary/advanc Removal of residual suspended solids
chemical and
ed /dissolved solids
biological Sludge Thickener Tank → Filter Press → Sludge Drying Bed
→ Sludge Store Room → Sludge Dumping Area

Raw Effluent:
The Process Flow diagram of Biological ETP
Oxidation
Oxidation Tank
Tank Oxidation Tank 1
Outlet Drain
Post
Aeration
Clarifier
(No aeration)
22 pH 7
pH 7
Temp 25-31 ºC
DO 1.5-2.5 ppm
HRT: 3.3 Hrs
TemppH 7 ºC
25-31
tank DO 1.5-2.5 ppm
Temp
MLSS 25-31ppm
2000-5000 C
MLSS 2000-5000 ppm
MLVSS 75% of MLSS (approx.)
FM ratio 0.01-0.15 (for extended aeration)
DO75%
MLVSS 1.5-2.5
of MLSSppm(approx.)
FM ratio 0.01-.15 (for extended aeration)
Capacity : 11100 m3/Day & HRT: 48hrs
Distributi
Recycle on Tank
Move to Tank
sludge
management
Filter Press Neutralizat
room ion Tank
Influent Thickenin
g Tank Equalization Daily monitored
generation parameters for
Tank
from 5000 m3/Day inlet
Washing & Are (Except
Yarn Dyeing Do sampling for 6&7):
inlet waste water 1. pH
qualities in every 2. DO
Bar Grit Bar Rotary Liftin 2 hrs. 3. TDS
Scree Cham Scree Screening g RT: 24 Hrs 4. EC
n ber n Chamber
Tank 5. TSS
6. COD
7. BOD
8. Color

Collection Sump Tank: Function of the Screening Unit :Screening is the first unit operation
used at wastewater treatment plants (WWTPs). Screening removes
objects such as rags, paper, plastics, and metals to prevent damage
and clogging of downstream equipment, piping, and appurtenances.
Some modern wastewater treatment plants use both coarse screens
and fine screens.
Bar Screen Rotary Screen

Screening Unit : Lifting Pump Sump:(Level Sensor)

Storage & Equalization Tank: Function of the Storage & Equalization Tank:
To reduce the temperature in Equalization tank
For homogeneous mixing
To give the optimum dosing of Acid for neutralizing
To reduce the insoluble BOD and COD in the System
To avoided the solids cloaking in the air distribution system in Equalization tank
To increase the air volume in equalization tank in wastewater treatment
To increase the efficiency of Biological system

Neutralization Tank: Cooling tower Unit :
 By piping system the
 The purpose of this tank is to blend the
neutralized effluent collected
acid that is being fed for pH adjustment of to Cooling Tower.
the waste water by completely mixing the
tank contents.  The temperature of the
 The raw effluent from storage tank will incoming effluent is high, so it
have alkaline pH & neutralized by auto
dosing 98% H₂SO₄. is need to decrease the
 A pH of 7 indicates a neutral state, neither temperature for bacterial
acid nor alkaline; above 7 is considered
alkaline and below 7 is acidic. A good growth.
range for the stream is a pH within a range  Here waste water is cooled at
of 6 to 9 & the operator must see that these
standards are met. less than 30ºc temperature by
alternative cooling fan.

Distribution Tank: Biological Oxidation Tank :

Biological Oxidation Tank : Biological Oxidation Tank
 Micro-organism formed by bacteria with protozoa. Excess bacteria are harmful
for the plant where protozoa work as removal of excess bacteria.
 When color removed by bacteria then bacteria metabolized an enzyme which
oxidized heavy metal like As, Hg, Pb etc.
 To survive bacteria we have to maintain an environment like temperature (29
to 32°C), pH (7.5 to 8.5), DO (2/3 ppm) & adequate retention hour.
 The activated sludge is a bacterial mass formed by several types of
microorganisms which grows attached to organic and inorganic particles.
 Flocculation of the bacterial cells (flock-forming bacteria) which leads to the
formation small aggregates which include also inorganic particles. Flocculation
is made possible by the production of the bacteria of a viscous extra cellular
matter which works as a binding agent (this is called microstructure). The
microstructure tends to be round-shaped.

 Fine type (9”disc) of diffuser used by this tank to survive bacteria by aeration. Biological Oxidation Tank
 Urea/DAP dosing will be done for growth of bacteria; this growth of bacteria will help
Sludge Problem Treatment Picture
to increase the biomass in aeration tank.
 The aeration tank is for a food to microorganisms (F/M) ratio of 0.15 and mixed liquor
Bulking o Disinfection
suspended solids (MLSS) concentration of 3000 mg/l. • Viscous o Increase DO
 We have to provide 48 hours retention time to remove organic dissolved substance • Filamentous o Control pH
o Nutrients balance
(ODS).
 Natural bacteria is survived by C, S, H, O, N, P where 1st four comes from dyeing; N
made by urea & P comes from DAP. o Sludge age reduction
o Mechanical removal
 Function of this tank is given below: Foaming
o Chlorination
Raw Effluent + Activated Sludge + Oxygen + Nutrient → o Adequate aeration
Micro-organism + SO2 + CO2 + NOx

Sedimentation Tank:
 After Bio-degradation, the Sediment
sludge is feeding in this tank.
 Here decoloring agent is dosing for
removing the residue color of the
biologically treated effluent.
 Activated sludge is separated by
laminar pack & taken in the
centered bottom hole by scraping
blades.
 Laminar pack used by lamella
clarifier (LC) at 600 angles.
 Treated water is going to upper U
channel & then be discharged.

Post Aeration Tank: Treated Water Discharge Point:
 The clarified effluent is collected by this tank to increase the DO & finally
discharge as treated effluent.
 Testing Parameters: pH, TDS, TSS, DO, BOD, COD, N, P, Temperature.

Process Parameters Chemical ETP vs Biological ETP
 Hydraulic load: m3/h.
 Organic load: kg BOD5/h.
 Suspended solids load: kg SS/h.
 Total Nitrogen specific load: kg TN/h.
 Hydraulic volumetric load Cv: kg BOD5/m3 of reactor*day.
VIDEO
 Organic load factor Cf: kg BOD5/kg MLSS*day.
 When the volumetric load increases, the treatment efficiency
decreases at a given constant reactor volume.
 If the organic load is kept constant, the process efficiency increases
along with the reactor volume.

Sludge Thickening Unit : Filter Press Unit :
Function of Treatment Plant Units Sludge Management

Sludge Management Unit : Sludge Management Room :
Sludge Management Sludge Management

CLASSIFICATION OF SLUDGE
Depending on the origin of the wastewater sludge can be classified as
 Category A: Municipal sludge including comparable sludge
 Category B: Sludge from industry including sludge from CETP
 Category C: Sludge from industry including sludge from CETP belonging
to the category of hazardous waste.
Category A + Category B = Category B

Category A + Category C = Category C
Category B + Category C = Category C
Category A + Category B + Category C = Category C
In view of the protection of the environment, it is forbidden to mix
Category A sludge with Category C sludge.
Sludge Management Sludge Management

Characterization of textile ETP sludge
Conditions permitting application
(2) Before applying sewage sludge on soil used for
agriculture or horticulture for the first time, the
operator of a wastewater treatment plant shall
undertake to have their content of lead, cadmium,
chromium, copper, nickel, mercury and zinc
analyzed on the basis of soil analyses performed
by a body appointed by the Director General
(DG), DoE.
(3) The soil analyses specified above shall be
repeated at intervals of 10 years.
Outline of content:

 Final Quiz
Area Topics Action Plan Time Responsible

Status
1. Develop Wastewater management policy
line
1st Nov -17 Done
Importance of Worker Safety
Wastewater Management System 2. Setting compliance obligation 1st Nov -17 Done
3. Develop a procedure for wastewater collection, treatment,

1st Nov -17 Done
process control & disposal Md. Mahbub Alam,
Plan AGM- EMS & CSR.
4. Conduct risk assessment on wastewater treatment/
1st Nov -17 Done
handling.
5. Wastewater management Objectives & Targets with KPI. 25th Nov-17 Done
1. Develop a Wastewater organizational structure with Roles,

25th Nov-17 Done
VIDEO
responsibilities & authorities.
Do 2. Implementation Wastewater Management Objectives. On going Done ETP Manager
3. Set up operational control. 25th Nov-17 Done

4. Conduct training & awareness program 25th Nov-17 Done
1. Conduct the internal audit Md. Mahbub Alam,
AGM- EMS & CSR.
Check 2. Develop the monitoring tools & checklist. 25th Nov-17 Done
Md. Mahbub Alam,

AGM- EMS & CSR.
Act 1. Develop the Management Review procedure. 30th Nov-17
Outline of content: Types of emergency situations

 Characteristics of water & it’s legal requirements  Power Failure
 WTP operation & Process control  Hydraulic overloading
 Characteristics of wastewater & it's legal Requirements  Process upsets
 ETP operation & process control  Chemicals spills
 Classification of ETP performance based on ZDHC & BSR guideline.  Equipment failure
 Lab manual & practice  Temporary unavailability of trained ETP operators
 Final Quiz
Scenario of power failure at ETP Scenario of Excess Foam at ETP
Outline of content: ETP In- House Lab

 Final Quiz
Key parameters to check are: Key parameters to check are:

• pH: Treated Water; Equalization tank, Neutralization tank, • Mixed Liquor Suspended Solids (MLSS, g/l): Indicator for the biological unit: F/M ratio.
Coagulation, Flocculation, Biological Reactor • Sludge Volume Index Test (SVI, ml/g): Indicates the performance of the biological unit.
• Temperature: Treated Water, Equalization tank; Primary/Secondary, Clarifier, Biological
• Total Dissolved Solids (TDS): Treated Water; Reactor
Equalization Tank, Primary/Secondary Clarifier • Color: Treated Water
• Total Suspended Solids (TSS): Treated Water;
Equalization tank, Primary/Secondary Clarifier
• Biochemical Oxygen Demand (BOD):
Treated Water; Equalization tank,
Primary/Secondary Clarifier, Biological Reactor
• Chemical Oxygen Demand (COD): Treated
Water; Equalization tank,
Primary/Secondary Clarifier, Biological Reactor
• Dissolved Oxygen: Treated Water
List of the Apparatus and Accessories for In-house Laboratory

Type of
Remarks
List of Parameters to be Checked at Different Sampling Points
SL. No Test Apparatus Reagents Requirements
Process Legal
Multi Meter,Hach - HQ40d, pH Standard buffer solutions for
1 pH Process Legal
2 Temperature
P aper
Multi Meter,Hach - HQ40d
calibration, pH 4, 7, 9 or10
N/A Process Legal

Unit Parameters to test for Sampling point
,Thermometers.
3 Dissolved Oxygen (DO) Multi Meter; Hach - HQ40d N/A Process Legal
Biological Oxygen Demand Sample, BOD Bottle, BOD BOD Nutrient Buffer
4 Process Legal
(BOD) Incubator, BOD Truker II P illows,P otassium Hydroxide.
5
Chemical Oxygen Demand
(COD)
COD Vial, COD Reactor,
Spectrophotometer DR-6000.
COD Vial Process Legal Equalization pH, TDS, TSS, BOD, COD,
Outflow
temperature
6 Total Dissolved Solids (TDS) Multi Meter , Hach - HQ40d N/A N/A Legal
tank
Cell, Spectrophotometer:
7 Total Suspended Solids (TSS) N/A Process Legal
DR-6000
8 Elactrical Conductivity (EC) Multi Meter; Hach - HQ40d
Filter paper, Cell,
N/A Process Legal
Neutralization Outlet, to ensure that the acid or
9 Color N/A N/A N/A pH
Mixed Liqour Suspended Solids
Spectrophotometer DR-6000.
Imhoff cone, Membrane filter tank alkali has been properly mixed
10 Paper ,Vacuum P ump,Oven N/A Process N/A
(MLSS)
Machine,Weight Machine.
Mesuring Sylinder, Membrane
11
Mixed Liqour Volatile
Suspended Solids (MLVSS)
filter Paper, Vacuum P ump,
Crucible, Desicator, Muffle
N/A Process N/A DO, pH, samples of AS for microscopic
Furnace ,Weight Machine.
12 Sludge Volume (SV) Imhoff cone
Imhoff cone, Membrane filter

N/A Process N/A
Biological examination, Temperature, MLSS, In aeration basin
13 Sludge Volume Index (SVI) Paper ,Vacuum P ump,Ovan
Machine,Weight Machine,
N/A Process N/A
Reactor MLVSS,
14 Sludge Age N/A Process N/A
COD Vial,COD Reactor,
Spectrophotometer DR-6000
SVI, F/M Ratio
15 F/M Ratio &Imhoff cone, Membrane filter N/A Process N/A
Paper ,Vacuum P ump,Oven
Machine,Weight Machine,
Cell, Spectrophotometer:
DR-6000 & Imhoff cone,
Clarifier BOD, COD, TSS Outflow
16 Return Activated Sludge Flow Membrane filter P aper ,Vacuum N/A Process N/A
Pump,Oven Machine,Weight
Machine.
17 Waste Activated Sludge Flow N/A Process N/A

Treated Water pH, TDS, TSS, BOD, COD, DO, EC Outlet
Beaker-150mL (1pc), Measuring
EDTA (Ethylene Diamine
Cylinder (1pc), Dropper (1pc),
18 Hardness Tetra Acetic Acid), N/A N/A
Stirrer (1pc), HACH Auto-
Eriochrome Black T, Buffer
titration device (1pc)
Solution of pH 10
Summary of special Sampling and Handling Requirements Records of the Daily Lab Activities….
Minimum Maximum
Determination Container Sample type Preservation
Sample size (ml) storage
Alkalinity Plastic, Glass 200 Grab Refrigerate 24 h
BOD Plastic, Glass 1000 Grab, Composite Refrigerate 6h
Analyze as soon as possible or add
COD Plastic, Glass 100 Grab, Composite
H2SO4 to pH<2; refrigerate
7d
Residual Chlorine Plastic, Glass 500 Grab Analyze immediately 0.25 h

Color Plastic, Glass 500 Grab, Composite Refrigerate 48 h
Hardness Plastic, Glass 100 Grab, Composite add H2SO4 to pH<2 6 months
Nitrogen Ammonia Plastic, Glass 500 Grab, Composite
7d

Nitrate Plastic, Glass 100 Grab, Composite
48 h

Nitrate+ nitrite Plastic, Glass 200 Grab, Composite
1-2 d

Organic Kjeldahl Plastic, Glass 500 Grab, Composite
7d
Dissolved Oxygen BOD Bottle 300 Grab Analyze immediately 0.25 h

pH Plastic, Glass 50 Grab Analyze immediately 0.25 h
Glass, Wax
Salinity 240 Grab Analyze immediately or use wax seal 6 months
seal
Temperature Plastic, Glass Grab Analyze immediately 0.25 h
Analyze same day, store in dark upto
Turbidity Plastic, Glass 100 Grab, Composite
24 h, refrigerate
24 h
Analytical Lab
S ampled By:
Microscopic Examination of Oxidation Tank (1 & 2) Activated Sludge.
Des ignation: Date:
Micro Organism at Biological ETP
S ample Location : Oxidation # T-1 or Oxidation # T-2 S hift # Water Temp: ºC Time:
S lide #1 Count S lide #2 Count S lide #3 Count Comments

Dominant
S L. No Micro - Organis m Group Pres ence: Presence: Pres ence: Bugs Recommendation
Yes/No Yes /No Yes /No
1 Amoeboids
2 Flagellates
3 Spirillum
4 Fre e Swimming Cilliate s
5 Euplotes
6 Colpidium
7 Paramecium
8 Crawling Ciliate
9 Aspidisca
10 Aspidisca lynceus
11 Aspidisca sp
12 Stalke d Cilliate s
13 Vorticella campanula
14 Vorticella Convallaria
15 Stentor
16 Carchesium
17 Epistylis stalks
18 Opercularia
19 Rotifers
20 Digononta
21 Monogononta
22 Nematodes
23 Aeolosoma
24 Filamentaous
25 Water Bear
26
27
28
P repared By: Checked By:
Outline of content: ETP Assessment Guideline & Documentation.

1. ETP Proposal detail – which will contain design basis, flow rate
 Types of water treatment & it’s fundamentals 2. Design Basis: Why the technology is used? –Flow Rate (How you determine flow rate
 WTP operation & Process control considering future expansion plan), Raw water Pollution Load (Inlet waste water test
report), Capacity (Both ETP and production), HRT (Hydraulic Retention Time) and
desired Waster water characteristics while discharged
 Characteristics of wastewater & it's legal Requirements 3. Civil design with calculation: Volume, HRT (Hydraulic Retention Time), Flow rate,
 Types of wastewater treatments & it’s fundamentals Chemical dosing (if applicable)
 ETP operation & process control 4. Operation manual – In detail with emergency plan
 Requirement of water management in Higg FEM 3.0 5. Drainage layout – including rainwater and production water
6. ETP Log sheet – How facility should maintain with time and date
 ETP contingency plan 7. Outlet Waste Water Test report by 3rd Party.
 Lab manual & practice 8. Production data – last four months
9. Water consumption and discharged Data – last four months
 Final Quiz
Institute of Professional Learning & Development Slide 109 Institute of Professional Learning & Development Slide
110
Outline of content:
 Final Quiz

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Prepared By : Md.

Mahbub Alam 9/26/2021

Today’s Learning Objective Expected Outcome from the sess ion

Presented by Lead Facilitator

Types of Topics Number of Training Number of Participants

DELEGATE INTRODUCTION Instruction to the Delegates

Take 5 minutes time to know your nearest co- • No cell phones

Important Information Key to achieve the session Goal

Outline of content: What is waste water?

WATER POLLUTION: Oxygen deficiency Sources of Waste water

Sources of Waste water Type of Wastewater

Depending upon the source of generation,

wastewaters are broadly classified as

Type of Wastewater Outline of content:

Fresh Water How much water do we have?

• 97.5% of Earth’s water is Salt water

• Less than 1% Accessible Fresh Water

Why should everybody be more Why should everybody be more

Why should everybody be more

Effluent Treatment Plant ETP Process Flowchart

• Effluent Treatment Plant or ETP is one type of waste

Legal Requirements Legal Requirements

Institute of Professional Learning & Development Slide 29 Institute

Legal Requirements Minimum Requirements

Institute of Professional Learning & Development Slide 31 Institute

Minimum Requirements Minimum Requirements

Legal issues Legal issues

• Approved Resource Conservation Plan has to be implemented.

Minimum Requirements Characteristics of Wastewater

Zero Tolerance Activities

Characteristics of Wastewater Characteristics of Wastewater

• Temperature (i) Organic matter

Characteristics of Wastewater Characteristics of Wastewater

POLLUTANT VS ENVIRONMENTAL PROBLEM POLLUTANT VS ENVIRONMENTAL PROBLEM

Pollutant Environmental Problem Pollutant Environmental Problem

Why do we need to treat wastewater ? Why do we need to treat wastewater ?

Why do we need to treat wastewater ? Why do we need to treat wastewater ?

Outline of content: Types of Wastewater Treatments

Types of Wastewater Treatments Types of Wastewater Treatments

Types of Wastewater Treatments Types of Wastewater Treatments

Types of Wastewater Treatments Types of Wastewater Treatments

Types of Wastewater Treatments Function of Treatment Plant Units

Function of Treatment Plant Units Function of Treatment Plant Units

Function of Treatment Plant Units Function of Treatment Plant Units

Treatment Level Description Process

Function of Treatment Plant Units Function of Treatment Plant Units

Function of Treatment Plant Units Function of Treatment Plant Units

Bar Screen Rotary Screen

Function of Treatment Plant Units Function of Treatment Plant Units

Function of Treatment Plant Units Function of Treatment Plant Units

Function of Treatment Plant Units Function of Treatment Plant Units

Function of Treatment Plant Units Function of Treatment Plant Units

Function of Treatment Plant Units Function of Treatment Plant Units

Function of Treatment Plant Units Function of Treatment Plant Units

Function of Treatment Plant Units Function of Treatment Plant Units

Function of Treatment Plant Units Function of Treatment Plant Units

Function of Treatment Plant Units Function of Treatment Plant Units