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Trans Indian Inst Met (2016) 69(2):579–583

DOI 10.1007/s12666-015-0803-6

TECHNICAL PAPER

Modification of Larson–Miller Parameter Technique


for Predicting Creep Life of Materials
Amitava Ghatak1 • P. S. Robi2

Received: 15 October 2015 / Accepted: 26 November 2015 / Published online: 31 December 2015
 The Indian Institute of Metals - IIM 2015

Abstract Larson–Miller parameter is the most exten- 1 Introduction


sively used extrapolation technique for predicting creep life
of metallic materials. In this technique, the Larson–Miller Creep life assessment is a major issue for economic and
parameter (P) is empirically expressed as: P = T [C ? safe operation of components exposed at high temperature
log(t)] where the C is considered as a constant. This is and pressure in petro-chemical and power generating
under the assumption that iso-stress lines in the plot of industries [1, 2]. During the past few decades, several
log(t) versus 1/T when extended, intersects the vertical axis methodologies, such as Larson–Miller parameter (P) [3],
at 1/T = 0, which corresponds to the Larson–Miller con- Manson–Haferd parameter [4], Orr–Sherby–Dorn parame-
stant C. Analysis of the literature data reveals that the ter [5], Manson–Sucoop parameter [6] and Wilshire
intersection of the iso-stress lines at a common point is method [7–9], have been suggested by researchers to pre-
rarely met in practice. The present paper is aimed at dict the creep life of components using short-time creep
investigating the value of Larson–Miller constant C in the test data. Among these, the Larson–Miller parametric
Larson–Miller parameter technique. Accelerated creep technique of extrapolating stress-rupture data is widely
tests on micro-alloyed HP40Nb steel were conducted at used to predict the creep life of high temperature materials
constant stresses in the range 47–120 MPa and tempera- due to its simplicity of application [10–14]. The creep-
tures 650–1050 C for the prediction of creep life by rupture parameter introduced by Larson and Miller has the
Larson–Miller parameter. The results reveal that the Lar- following form:
son–Miller constant C in the expression for P is not a PðrÞ ¼ T ½C þ logðtÞ ð1Þ
constant, rather, it is a linear function of applied stress. The
authors proposed to modify the expression for the Larson– where r is the stress in MPa, T is temperature in K, t is
Miller parameter for predicting the creep life of materials. rupture time in hour. C is the Larson–Miller constant to be
determined from the experimental data. The parameter
Keywords Larson–Miller parameter  Creep life  P(r) is a function of stress. Stress versus P is reffered as a
HP40Nb micro-alloyed steel master curve. The extended iso-stress lines in log(t) versus
1/T plot is assumed to intersect the vertical axis at 1/T = 0
at the point corresponding to C. In almost all the cases, the
value of C is considered as constant. While arriving at the
master plot, the C value is generally taken as 20, though
& Amitava Ghatak depending on the material the optimized values between 10
amitavaghatak@yahoo.com and 50 have also been reported based on the material. So
1
far no justification has been provided by any reseracher for
Department of Mechanical Engineering, North Eastern
Regional Institute of Science and Technology, Nirjuli,
choosing C = 20. Since, the value of C differers for
Arunachal Pradesh 791109, India different materials, Furillo et al. [15] modified the Larson–
2
Department of Mechanical Engineering, Indian Institute of
Miller parameter to obtain better correlation of stress-
Technology Guwahati, Guwahati 781039, India rupture data and obtained the expression:

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580 Trans Indian Inst Met (2016) 69(2):579–583

 
1 The range of temperatures was chosen such that they are
logðrÞ ¼  ½T fCðT Þ þ logðtÞg ð2Þ typical for the reforming operation in petrochemical
naT
industries. The test temperature was controlled within
where n is the power-law exponent, a the constant near to ±3 C. Creep test were conducted up to the rupture of the
unity and C(T) is a constant obtained by the expression specimen. The longest rupture time was 122.7 h at
C ðT Þ ¼ log½fAexpðQ=RT Þgr=B ð3Þ 47 MPa/800 C.
It has been observed that the value of C depends on initial
microstructure, grain size, chemical composition and cold-
3 Results and Discussion
work [16, 17]. The scatter in the experimental data in
master curve results in a large error in estimating the creep
The constant C of Eq. (1) is obtained graphically by plot-
life at lower stress region. It appears that this is due to the
ting experimental creep data in log(t) versus 1/T plot.
assumption of a constant value for C. This paper aims to
Figure 1 shows the plot of log10(t) versus 1/T for constant
achieve a better understanding of the Larson miller
stresses. The Larson–Miller parametric technique is under
parameter C for the prediction of creep life of engineering
the assumption that these iso-stress lines when extended,
materials.
intersect the vertical axis at 1/T = 0 at a common point, the
Centrifugally cast reformer tube made of HP40Nb
value of which is taken as the value of C. The Fig. 1
micro-alloyed steel is chosen for the present investigation.
indicates that the iso-stress curves when extended intersect
The tube is used in petro-chemical industries for produc-
the vertical axis at different points, each point corresponds
tion of hydrogen-rich gas. The tubes are designed for a long
to different value of C. It is evident that iso-stress plots,
service period (105 h) at temperatures up to 900 C and
when extended, intersect the vertical axis at values between
internal pressure of 25–27.5 bar. Due to the degradation of
14 and 22 for the range of stresses investigated.
microstructure and properties of the material during service
The plot of C versus stress, shown in Fig. 2, indicates
often premature failure of the steel occurs by one or more
that C varies linearly with stress. Equation (1) is modified
damage mechanisms such as creep, corrosion [13, 14, 18–
20]. Accelerated creep tests for various combinations of
stress and temperatures were carried out and the data
obtained was used for the analysis.

2 Experimenal

2.1 Material

The test material, a HP grade austenitic stainless steel


reformer tube of inner diameter 106 mm and thickness
15.3 mm, was supplied by Numaligarh Refineries Limited,
India. The chemical composition of the reformer steel used
in the present study is given in Table 1.

2.2 Creep Test

Flat specimens with gauge dimensions 3 9 6.5 9 25 mm


were machined along the longitudinal direction of reformer
tube by wire-cut electric discharge machining (EDM).
Tensile creep-rupture tests were performed on constant-
stress creep testing machine at stresses of 47, 68 and
Fig. 1 Plot of log(t) versus 1/T to determine Larson–Miller
120 MPa and temperatures ranging from 650 to 1050 C. constant C

Table 1 Chemical composition of the steel (in weight percentage)


C Si Cr Ni Mo Nb Ti Fe

0.41 1.25 23.56 34.95 0.04 0.81 0.04 Balance

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Trans Indian Inst Met (2016) 69(2):579–583 581

Table 2 P values from master curves for different stresses


Stress (MPa) Larson–Miller parameter, P
Using C = 20 Using C(r)

5 26.57 33.24
10 26.26 32.35
15 25.95 31.46

P for each stress with C = 20 and C as a function of


applied stress. The coefficient of determination (R2) for
master curve with C = 20 and C = C(r) are found to be
0.94 and 0.996, respectively. Based on the R2 value, the
master curve of the investigated steel considering C as a
function of stress shows a better fit.
The P value at low stress levels are obtained by
extrapolating the master curves for both cases of C values.
The P values for stresses of 5, 10 and 15 MPa for the steel
tube are given in Table 2. The creep life of the steel con-
Fig. 2 Plot of Larson–Miller constant C versus stress for the steel sidering C = 20 and C = C(r) are determined by Eq. (5)
and (6), respectively.
t ¼ 10½ð1000  T Þ20
P
ð5Þ

t ¼ 10½ð1000  T Þð0:1119  r þ 26:937Þ


P
ð6Þ
Figures 4 and 5 show the predicted creep life of the
reformer tube considering C = 20 and C as a function of
stress. Both the figures show that the creep life decreases
with increase in temperature and/or stress.
Figure 6 compares the creep life of the material pre-
dicted for different combinations of stresses, by consider-
ing C = 20 and C = C(r). Similar comparison of
predicted creep life of the investigated steel at constant
temperatures considering C = 20 and C = C(r) is shown
in Fig. 7. At 800 C and 5 MPa, the estimated creep life of
the steel is 6.5 and 4.5 years for the case of C = 20 and
C = C(r), respectively. At 780 C and 10 MPa, the
respective creep lives are found to be 9.8 and 9.1 years.
Figure 7 shows lower creep life when C is considered as a
function of stress, compared to the case when C is taken as
Fig. 3 Comparison of Larson–Miller master curves for C = 20 and
a constant value of 20.
C = C(r) The result indicates that the creep life of the reformer
tube is very sensitive to small difference in temperature and
considering C as a function of r [i.e., C = C(r)] to obtain C value, even if C is considered as a constant. It is observed
the relationship: that the iso-stress lines in log10(t) versus 1/T plot are not
intersecting at a single point on the y-axis at 1/T = 0.
PðrÞ ¼ T ½ða1 þ a2  rÞ þ logðtÞ  103 ð4Þ
Since, the Larson–Miller constant C value depends on the
From the experimental data, values of the constants a1 and applied stress, hence, the modification is required in the
a2 in Eq. (4) for the investigated steel were obtained as Larson–Miller parametric technique. The results of the
26.937 and -0.1119, respectively. analysis indicates that the creep life prediction of the
For austenitic steels, the C value proposed by Larson material by considering C = C(r) in the Larson–Miller
and Miller for obtaining the r versus P master plot is 20 parametric technique is conservative in nature and will
[3]. Figure 3 shows the log–log plots of r versus average provide a better realistic prediction.

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582 Trans Indian Inst Met (2016) 69(2):579–583

Fig. 4 Plot of a temperature (a) (b)


versus creep life and b stress
versus creep life, for C = 20

Fig. 5 Plot of a temperature (a) (b)


versus creep life and b stress
versus creep life, for C = C(r)

Fig. 6 Plot of temperature versus predicted creep life for C = 20 and


C = C(r) Fig. 7 Plot of stress versus predicted creep life for C = 20 and
C = C(r)

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Trans Indian Inst Met (2016) 69(2):579–583 583

4 Conclusions 6. Manson S S, and Succop G, in Stress-Rupture Properties of


Inconel 700 and Correlation on the Basis of Several Time-Tem-
perature Parameters, (ed.) ASTM, of Symposium on Metallic
The modified Larson–Miller parameter is proposed to Materials for Service Temperatures Above 1600 F, ASTM-STP
predict the creep life of micro-alloyed HP40Nb reformer 174, ASTM, Philadephia, (1956).
steel. Following conclusions are obtained: 7. B. Wilshire and P.J. Scharning, Int Mater Rev, 53 (2008) 91.
8. B. Wilshire and P.J. Scharning, Mater Sci Tech, 24 (2008) 1.
• The creep-rupture data was analyzed by Larson–Miller 9. Wilshire B, and Bache M R, Proceedings of the Creep & Frac-
parameter to predict the creep life of the steel. ture in High Temperature Components-2nd ECCC Creep Con-
ference, Switzerland (2009), p 44.
• It is proposed that C in the P expression be modified by 10. A. Kim, K. Tunvir, S. Nahm and S. Cho, J Mater Process Tech,
stress dependent function rather than considering C as a 202 (2008) 450.
constant. 11. A.K. Ray, K. Diwakar, B.N. Prasad, Y.N. Tiwari, R.N. Ghosh
and J.D. Whittenberger, Mater Sci Eng A, 454-455 (2007) 124.
12. J.E. Indacochea and R.A. Seshadri, Mater Sci Eng A, 234-236
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Refinery Limited, India is gratefully acknowledged. 13. A.K. Ray, S. Kumar, G. Krishna, M. Gunjan, B. Goswami and
S.C. Bose, Mater Sci Eng A, 529 (2011) 102.
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