820-Puri Voda

Contractor: Client:
KLIMAOPREMA d.d. Bristol Myers Squibb, Bio Science

Gradna 78A Park François Aragostraat 2, 2342
10430 Samobor BH, Oegstgeest, Leiden, Netherlands
Document: Project:
4606-8006-KO-FTP-03 –Initial flush and hydrotest for system 981 EU Cell Therapy Facility
PLAN FOR HYDROTEST AND FLUSHING OF THE SYSTEM

820 –PURIFIED WATER
Attachments:
1. VECOM hydrotest plan:

a) Method Statement
b) Task risk assessment
c) Pneumatic pre-test acceptance
d) Hydrostatic test acceptance
e) Toolbox Form PRS
f) Leak report
g) Limit status check list
h) Marked-up P&ID’s
2. VECOM flushing plan:
a) Method Statement
b) MSDS for Vecinox Passivating Liquid
c) Task risk assessment
d) Emergency spill response plan
e) Waste water treatment, storage and disposal
f) Limit status check list
g) Marked-up P&ID’s
Work Method Statement
Author Nick Berens

Revision 0.0
Client Klimaoprema
Subject Pneumatic pre-testing and hydrostatic testing
Location BSM Oegstgeest
Checked by: Signature:
Nick Berens
PRS International | Industrieweg 10 | 7761 PV Schoonebeek | The Netherlands a VolkerWessels company

Table of contents
1. Purpose ........................................................................................................................................... 2
2. Responsibilities and authorities ...................................................................................................... 2
Project responsible ................................................................................................................. 2
Supervisor ............................................................................................................................... 2
Operator.................................................................................................................................. 2
3. General QHSE.................................................................................................................................. 3
Policy ....................................................................................................................................... 3
General Safety ......................................................................................................................... 4
Slips, trips and falls.................................................................................................................. 5
Manual handling and lifting .................................................................................................... 6
Barriers .................................................................................................................................... 6
Personnel protect equipment ................................................................................................. 7
Positioning of equipment........................................................................................................ 8
Equipment safety .................................................................................................................... 8
Actions in the event of an emergency .................................................................................... 9
4. Communications ........................................................................................................................... 10
Site induction and permit to work ........................................................................................ 10
Pre-job safety meeting .......................................................................................................... 10
Toolbox talk........................................................................................................................... 11
Shift Handover ...................................................................................................................... 11
Post-job safety meeting ........................................................................................................ 12
5. General Preparation...................................................................................................................... 13
Establishment of job pressure .............................................................................................. 13
Maintenance/certification/stored equipment ..................................................................... 13
Rig-up / Rig-down (General) ................................................................................................. 13
Injection manifold ................................................................................................................. 14
System over pressurization protection ................................................................................. 15
Hose over pessurization protection ...................................................................................... 16
6. Work method statement .............................................................................................................. 18
Pre-notification provided by customer................................................................................. 18
Registration ........................................................................................................................... 18
Safety distance ...................................................................................................................... 18
Pressure measurement requirement.................................................................................... 18
Pneumatic pre-test ............................................................................................................... 18
Filling of system (performed by Vecom) ............................................................................... 19
Hydrostatic test ..................................................................................................................... 19
Measuring equipment........................................................................................................... 20
Dewatering ............................................................................................................................ 20
7. Reporting....................................................................................................................................... 21
8. Disassembly / Demobilization of equipment ................................................................................ 21
a VolkerWessels company 1|P a g e

1. Purpose
The purpose of this document is to provide a written method of working for all operational personnel.
This document is to ensure that the required operations are carried out in a safe, uniform manner.
2. Responsibilities and authorities
Project responsible
• The commitment of qualified personnel

• The necessary measures regarding the execution of the work
• Giving sufficient information to anyone involved in the project on the dangers and nature of
the work to be done
• Monitoring the performance of the activities under this work instruction
• The preparation and authorization of a project specific TRA (Task Risk Analysis)
Supervisor
• Obtaining the necessary permits

• Execution of the work in a safe, efficient en qualitative responsible way
• Job reporting
• The presence and control of non-conformities from the General Information list.
Operator
• Working in accordance to the project / job specific work instruction

• Ensuring that Heath, Safety and environmental instructions are followed
• Keeping records of pump logs or other job specific Information
• Reporting all accidents and incidents
• Taking preventive measures, if necessary, by stopping unsafe work

3. General QHSE
Policy
QHSE is embedded in the while organization as an integral part of the day-to-day business and has the
full attention of the management and every employee.
Quality: To fulfil requirements, resulting from defined needs and expectations of the client.
Safety: The prevention of accidents, injuries to health or welfare of employees and damage to
machines or plant.
Environment: The fulfilment of local environmental rules and regulations and the commitment for
preventing pollution to the environment.
We implement our policy in compliance with the valid codes, specifications, legislations and
regulations.
PRS Management objective is focusing on a process approach and continual improvement by means
of key performance indicators in order to measure the effectiveness and efficiency of the process.
To achieve this aim PRS and operational divisions are fully committed:
• To ensure that all products and services are in accordance with the specified requirements of
the client: on time, within budget and in accordance with specifications and legal
requirements
• To provide safe and healthy working conditions for all employees and third parties and to use
safe working methods and practices
• To stop the work, or part thereof, when the health, safety or welfare of any employee or the
environment is endangered by PRS activities
• To promote the reporting of potential risks and to take the necessary preventive actions.
• To control and monitor the illness rate and to ensure the implementation of preventive
actions for healthy work conditions
• To ensure that all personnel do not use, transport or have in their possession drugs, alcohol,
natural stimulants or other similar intoxicating substances
• To check the fulfilment of local environmental rules and regulations and to aim for the
efficient use of consumables in order to decrease and limit waste and prevent pollution of the
environment
• To verify the management’s system against the objectives through implementation of both
internal and external audits, management reviews as well as to take preventive and corrective
measures
The management makes this policy available to all those concerned. The duty, responsibility and
authority for realizing and implementing the integrated management system is assigned to the
division directors and line staff. The control of objectives is monitored in the “Plan of Actions” as part
of the operational business program.

General Safety
Safety is the responsibility of every employee irrespective of status. Employees shall ensure that their
workplace is safe and functions efficiently and safely. Common sense should be applied for safe
working practices to be implemented and adhered to at all times. Particular attention is to be given to
worksite safety and to any safety procedures provided.
The following safety rules shall be adhered to at all times:
• Help prevent accidents and injury before they occur. Stay alert at all times. Report situations
which may cause or lead to accident or injury.
• In particular, report all unsafe conditions, tools, equipment and working practices immediately
to operational management / supervision so that they can be corrected before they can cause
accidents.
• Use the Hazard Report Form to notify management of Health, Safety or Environmental hazards
or problems that are encountered in the workplace.
• Find out and understand all relevant information involving general health and safety issues as
well as those specific to PRS project work scope without having first to be told about it.
• Alcohol and drugs (except under prescription) are prohibited. If a person is taking prescribed
drugs this information must be notified to the installation's medical person on arrival.
• Do not remove, displace, damage or destroy any safety equipment provided for use on jobs.
• Permit to work procedures shall be strictly adhered to. No work shall commence until the
appropriate permit has been obtained from a competent issuing authority.
• Watch where you walk and keep alert to the movement of equipment and other persons
around you. Use the handrail when on stairways.
• All employees shall maintain their work area in a neat, orderly, tidy and litter free condition
at all times.
All employees shall use personal protective equipment (PPE) provided for their use. Only authorized
persons shall be allowed to operate plant and power tools.
All employees shall inspect their work areas at the end of each shift and ensure that all air, water,
diesel and electrical supplies are shut off unless otherwise instructed.
No person shall stand under loads handled by power operated lifting equipment. All personnel shall
be aware of what to do in an emergency. Equipment shall not be operated unless the operator is
sufficiently trained and experienced in its use whilst unsupervised

Slips, trips and falls
Be careful when moving about any work area to avoid slipping, tripping, or falling. Be especially careful
when weather or other conditions create or aggravate hazardous situations. Look for slip and trip
hazards around the workplace, such as uneven floors, trailing cables, areas that are sometimes
slippery due to spillages (include outdoor areas).
Hazard Suggested Action
Clean spills up immediately. If a liquid is greasy ensure a

suitable cleaning agent is used. After cleaning the floor may
Spillage of wet and dry substances
be wet for some time. Use appropriate signs to tell people
the floor is still wet and arrange alternative bypass routes.
Position equipment to avoid cables crossing pedestrian

Trailing cables
routes, use cable covers to securely fix to surfaces.
Miscellaneous rubbish, e.g. plastic Keep areas clear, remove rubbish and do not allow to build
bags up.
Choose suitable footwear, particularly with the correct type

Unsuitable footwear
of sole.
Smoke /steam/ vapour obscuring Eliminate or control by redirecting it away from risk areas;
view improve ventilation and warn of it.
Slopes Improve visibility, provide hand rails, use floor markings.
Ensure mats are securely fixed and do not have curling

Rugs/mats
edges.
Slippery surfaces and change from Suitable footwear, warn of risks by using signs, locate
wet to dry floor surfaces doormats where these changes are likely.
Poor lighting Improve lighting levels and placement of light fittings.

Manual handling and lifting
Many injuries are caused by poor lifting practices.
Back injuries can be eliminated by following these simple rules:

• Assess the load and your own capability before you lift it (size, weight, centre of gravity, hand
holds, sharp edges, hot/cold surfaces, sudden internal weight shifts in liquid containers)
• Get help if necessary. If the load requires help –don’t lift it without help
• Beware of distractions (noise, other people etc.), bad lighting and physical obstructions
• Secure a good hold on the object before lifting
• Take the strain gradually
• Make sure you can see where you are going when carrying the load – slip/trip hazards in
particular
• Use teamwork when lifting with others. Lift or lower the object together
• Minimise occasions for which manual lifting is required. Use mechanical means whenever
possible
• Minimise the weight of a lift whenever possible
To make a manual lift from floor level, you should:

• Avoid lifting in an awkward or off-balance position. Never twist or bend your spine when lifting
or carrying
• Stand with feet approximately 30 cm (12 inches) apart
• Recess one foot approximately halfway behind the other
• Squat to the load or object
• Place hands on load or subject for firm grip
• Keep the back straight
• Lift by straightening the legs
• Do not lift with the back
Lifts from between knee and shoulder height are much easier than those outside this height range.
Moving loads from one level or floor to another is more hazardous. Remember a back injury is usually
for life.
Barriers
All PRS equipment and hoses as well as the system need to be barriered of in order to prevent
unauthorized personnel entering the area.
Red and white tape will be used at the entrance of the site. Warning signs displaying information on
the activities e.g.(“PRESSURE TESTING”) will be posted with the barrier tape at all access points.
Warning signs must also be posted with regular intervals around the test barriers.
Prior to the commencement of operations on any system, all relevant personnel must be informed of
the impending operations by either a tannoy announcement or by individual verbal messages. The
complete site will be cleared of “Unauthorized personnel”.

Personnel protect equipment
All PRS operational personnel are provided with full protective clothing which must be worn at all
times when working on site or when appropriate on company premises.
The minimum standard of protective clothing provided and worn includes:
• Footwear: safety boots/shoes to the newest standard.

• Hard Hat: an approved hard hat shall be worn at all times.
• Gloves: dry gloves must be worn when handling the cold transfer hoses. Loose gloves that
can be quickly shaken off, in case of accidental spillage into them, are preferred
• Safety glasses: safety glasses shall be worn at all times
• Ear protection:- ear protection shall be worn
Client requirements on personal protective equipment will be adhered to at all times by all PRS
personnel.
In the event of an emergency during operations, all equipment shall be shut down immediately. The
power supply to the leak test equipment container or lab shall be isolated and the air supply to the
diesel unit closed off.
If a system is under pressure at the time of an emergency the injection point must be closed as soon
as pumping has stopped. Non return valves shall be fitted to injection points of systems to ensure that
pressure is contained in the event of hose failure.
Work permits are to be returned to the permit office / control room unless the permit states
otherwise. Personnel shall proceed to their allocated emergency muster point in accordance with the
clients site contingency plan.

Positioning of equipment
The equipment required to perform the work scope may not have arrived on site yet or if it has, it may
require moving to an alternative position or location. In this case the supervisor must liaise with the
client representative or other similar persons to assist in this operation.
Care must be taken to ensure that the movement of any equipment is sited in accordance with normal
PRS and clients requirements (for example - on wooden slats or on plastic sheets etc.), is prevented
from damage, is sited appropriately for operational purposes and ideally in the vicinity of the following
services - tannoy announcements, air, water, fuel supply, firefighting appliances etc.
Once the equipment has been sited an inventory check and inspection must be performed on all
equipment, consumables and ancillaries to check for obvious deficiencies and damage. Any
deficiencies or damage identified must be suitably recorded and reported to the Supervisor as soon
as possible for immediate action.
The availability, calibration, condition and operability of all safety critical items (alarms, trips, shut-
downs, pressure relief valves, bunds, site services etc. must be checked and work must not proceed if
any are deficient.
All equipment, especially any that is subject to positive or negative pressure, prior to operations must
be physically checked for any obvious signs of wear and tear or damage that may, or is likely to, lead
to its failure. The use of the damaged equipment must not continue. The item must be withdrawn
from use, identified and / or segregated and the matter immediately reported to the Job Supervisor.
The matter must also be recorded so that any appropriate and if need be, immediate action may be
initiated.
Equipment safety
Access to the top of all framed units higher than 1,8 metres above deck / ground level shall involve
the wearing and securing of safety harness. PRS personnel shall wear ear defenders at all times when
running diesel powered equipment with a sound power level in excess of 85 dB(A). The pump operator
and all other PRS personnel must obey tannoy announcements and any other instructions whether
they be verbal or by audible alarm. All equipment shall be located when on-site in a manner which
leaves suitable and safe escape routes. Equipment shall be located so as to leave 2 ft gangways
between each unit wherever possible.
Hoses (hydraulic oil and high-pressure gas) shall be routed so as to:

• prevent trip hazards
• prevent damage to hoses
• protect all personnel and site equipment in the event of hose failure i.e. away from access
routes.
All equipment that is used during operations must be certified and in date. This includes but not
limited to: gauges, chart recorders, dew-point meters, pressure release valves. If no certificate can be
found and no record is on or in the equipment that must be treated as non-certified and not used.

Actions in the event of an emergency
In the event of an emergency during operations, all equipment shall be shut down immediately. The
power supply to the equipment container or lab shall be isolated and the air supply to the diesel unit
closed off.
If a system is under pressure at the time of an emergency the injection point must be closed as soon
as pumping has stopped. Non return valves shall be fitted to injection points of systems to ensure that
pressure is contained in the event of hose failure.
Work permits are to be returned to the permit office / control room unless the permit states
otherwise. Personnel shall proceed to their allocated emergency muster point in accordance with the
clients contingency plan.

4. Communications
Site induction and permit to work
All PRS operational personnel must attend the clients standard induction (if not already inducted)
courses on arrival at site.
All works must be carried out in accordance with the clients Permit to Work System. A valid permit to
work need to be signed before every shift change.
Wherever practicable, PRS personnel should receive training from the client on the clients permit
system.
All PRS crew members on any job must read, understand and be aware of all Work Permits in force
and information contained therein relating to their scope of work. Any precautions, measures or
actions to be taken as specified by the Work Permit must be adhered to at all times throughout the
duration of the work.
Any new hazards or risks that arise from changes must be identified and assessed at this time. If a
permit will expire before the workscope will be completed, the Job Supervisor shall ensure that a new
permit is raised and endorsed before the expiry time / date of the old permit.
The PRS Supervisor will hold a pre job briefing for the Work crews to discuss operational procedures,
safety issues and any site-specific hazards. This will be repeated for new arrivals to site
Pre-job safety meeting
The Service Supervisor must conduct a pre-job safety meeting for all Company personnel, customer
representatives, and all other relevant individuals on location. For offshore operations all personnel
that will be involved to some capacity on the rig floor should be included in the pre-job meeting.
The subjects covered and discussed during the briefing shall include, but should not be limited to the
following
• A review of the job procedure / work scope and timings.

• A reminder of any safety points.
• A discussion on equipment deployed.
• A discussion on personnel involved and their responsibilities.
• Any client key points.
• Contingency planning [if applicable]
• Risk Assessments
• House Keeping and general Safety
• Lighting (if night shift)
• Conflicting Activities
• Access and Evacuation
• Specific Job Hazards
• Use of correct PPE
• Weather Conditions
• Work Permits
a VolkerWessels company 10 | P a g e
Toolbox talk
When crew members attend the onsite job pre-meeting there shall be no need to conduct a
subsequent Toolbox talk. Where any crew members (including other shifts) do not attend, then a
toolbox talk shall take place for them, before work starts. The Senior Operator/Crew Supervisor/Senior
Technician/Engineer shall conduct a brief onsite meeting to discuss the particular job to be undertaken
and inform the crew of any potential hazards.
These meetings shall be repeated whenever the crew/shift changes. Any third-party personnel
involved in or affected by the work shall also be invited to the meeting. Topics covered shall include
those in the previous section. Meetings shall be recorded on the Toolbox Talk Form (Insert Ref).
Toolbox talks held shall be noted on the daily operations form. This kind of meeting is meant to give
the employee specific information about actual QHSE-aspects in a short time frame (15 minutes). This
may include:
• Risks and hazards mentioned in the Task Risk Analysis

• Past accidents and loss experience
• Content of the work permit
• Good housekeeping
• Division of waste materials
• Safe lifting
• Emergency procedures
• Environmental aspects and impacts
• Handling specific equipment/tools/matters etc.
Shift Handover
At every shift change, there shall be a time period solely dedicated for the purpose of exchanging a
written and a verbal account of the previous shift's operations. It is the responsibility of the supervisor
to ensure that there is a complete exchange of all information sufficient to allow the "oncoming" crew
to safely and competently continue with the operations. The shift handover period should include
(when appropriate) a complete "walk through" of the systems under test in order to identify strategic
areas or points
Points that need to be discussed in meeting:
• Status of the work during the previous shift

• Ongoing work in progress
• Work that needs to be done in the next period
• Status of the system (purging, pressurized etched)
• Permit status
• Changes in procedure or work scope
• Consumables status (diesel level, water, etc.)
• Any other relevant points
All above points need to be recorded on a PRS shift handover form
Post-job safety meeting
Following the end of all jobs and on return to base any health, safety or environmental issue (including
Job Performance Indicator Forms or Job HSE Audit Forms) arising from the job shall be discussed and
recorded. Corrective action arising shall be implemented and where appropriate or serious enough,
shall be notified to the HSE Manager.
Topics to be discussed:
• Work scope summary.

• Problems experienced during work scope.
• Recommendations for next work scope.
• Quality and safety performance.
• Client comments.
• Areas of improvement or concern
5. General Preparation
Establishment of job pressure
Whether generic, project or client procedures are to be used, work shall not commence before the
maximum allowable system pressure have been established, agreed with the client and stated in
writing within whatever procedure / safe working practice is to apply.
Maintenance/certification/stored equipment
All working equipment shall be properly maintained and equipment requiring certification shall always
have current certification provided by a competent and recognised authority. Faulty equipment
should be brought to the attention of the supervisor/coordinator. Any equipment belonging to
ourselves or customers shall always be stored in a safe manner.
Rig-up / Rig-down (General)
Rig-up, the area should be accessible to 40-ton truck combinations. The location of the high-pressure
pump must be in such a way that they can drive in and out easy and safe.
Ensure that the location does not stop or impede other activities of the plant/installation. Ensure
sufficient space for forklift access and egress. On larger projects allow for space to be allocated if
needed for deliveries of equipment or supplies.
Ensure that the location chosen conforms to these requirements. (If Possible)
• Stores container
• Space for equipment and delivery’s
• Ensure the location is close to all the necessary support e.g., electric, air supply, water
supply
• Installation of temporary silencer
Rig-down, upon rigging down ensure that a full site inspection has been done and that all container
and Workspaces have been cleaned and correctly stowed for transportation.
If working on an off-shore installation, ensure that the corrected paper work has been raised with the
plant for the loading of the containers on the transportation ship back to shore.
All equipment that has become unserviceable during operations should be taped red and a
maintenance sheet has been correctly filled out detailing all the information that is necessary for the
workshop to understand why the equipment is now unserviceable.
Injection manifold
Every injection point into a customer system shall be fitted with an injection manifold. All fittings shall
be rated to the same maximum working pressure as the hose. A check valve shall be fitted to all high-
pressure gas transmission hoses at the system injection point manifold on all jobs without exception.
This valve is required to prevent backflow of high-pressure gas from the system in the event of a hose
bursting. Prior to removal of the manifold care must be taken to ensure that any trapped high-pressure
gas has been vented to atmosphere.
The injection manifold shall always comprise the following, in sequence starting from the hose
coupling and ending with the crossover into the customer injection fitting:
• A "whip check" or other securing device must be used to secure the hose to the injection
manifold
• Coupling from hose to manifold
• A manifold isolation ball valve
• A check valve with the flow direction positioned correctly
• Hose bleed down or vent facility (incorporating a ball valve or needle valve)
• A pressure tapping (with ball valve)
• A main injection point isolation ball valve.
• Cross over from manifold to customer injection fitting
• A "whip check" or other securing device must be used to secure the injection manifold to the
customer system
Isolation from the customer system before and after pressurisation shall always be by use of the
main injection point valve.
Customer valves shall never be used. In the event of inadvertent closure during pump flow or before
full pump shut down all fittings will experience a transient high pressure "spike" before the hose
protection relief valve lifts and the hose protection overpressure switch trips the pump. Customer
systems must always be protected from these pressures.
Hose runs may be manifold along their length to split a single hose into a number of legs –each having
its own injection manifold.
IMPORTANT:
Care must be taken to ensure that fittings have compatible threads before mating them together. For
example, BSP and NPT threads are not to be matched together as this practice is potentially
dangerous. Jointing material should not be used with parallel threaded fittings. When pressures are
expected that are in excess of the equipment employed, appropriate and certified higher pressure
rated assemblies must be exchanged prior to use. The use of higher pressure rated equipment in lower
pressure conditions is acceptable when lower rated equipment is in limited supply.
Pressurisation of any system must be through a suitably sized customer valve or orifice. The practice
of utilising needle valves to inject through should be avoided. The limited orifice size of these types of
valves causes flow restriction and generates unacceptably high back pressures.
System over pressurization protection
Client systems may be pressurised during hydro test, leak test, pigging or purging jobs. The system to
be pressurised shall, at all times, be protected from over pressurisation. Job test or maximum
pressure shall be set following consultation with the client and system overpressure protection
devices shall be set at 10% above this pressure (where system design pressure allows).
Client system over pressure protection may be provided by use of a single or a number of protection
devices namely:
• A mechanical pressure relief valve set as above and temporarily attached to the system
(Temporary PRV).
• The temporary PRV must be sized for maximum pump flow at the above set pressure. Some
PRS departments use stand-alone overpressure manifolds (OPM) with the Temporary PRV
mounted inside.
• In addition to the over pressure protection devices there shall be a calibrated pressure gauge
(or client's own electronic pressure monitoring device) and a pressure chart recorder attached
to the system.
As part of the pre job function tests the sender and any other lines associated with the over pressure
panel shall be isolated and pressured tested to test pressure. The pre-pressurisation checklist shall
include this valve. It shall state that this must be opened along with the injection point to the client
system prior to tests commencing. These function tests shall be recorded on the chart recorder.
Note: Where maximum possible pump discharge pressure is substantially below the rated maximum
operating pressure of the whole client system, pumps, hoses, flow iron, pipes, manifold (or any other
fitting located in the line of flow) then temporary PRV's may not be practicable and need not be used.
This note applies to centrifugal pumps only. Large flooding spreads, operating at medium to low
pressures with pigs in open vented lines for example. However, the maximum pump pressure used
shall be assessed under all foreseeable emergency conditions, including accidental shut in / dead head
conditions.
Note: Wherever a secondary system such as a pressure switch is run to back up a primary system such
as a PRV, personnel should clearly understand that such systems are fitted for added assurance and
where fitted shall always be run together with the primary system and not as an alternative to it.
All relief valves shall be positioned or piped up so that discharge of vented fluids, if the valve lifts, is
to a safe location.
• For non-hazardous fluids this means positioning relief valves so as to avoid personnel or
equipment being struck by discharged fluids or debris. Positioning, selection and support of
relief valves and associated pipework shall be designed to safely accommodate any side thrust
at the point of discharge.
• For hazardous fluids this may involve a number of possibilities (recycle to pump suction,
recycle back to tank, feed off to a designated safe location agreed with the client such as a pit
or flare).
Whatever method is used, it shall be scrupulously risk assessed for safety. Return lines run for this
purpose shall not impose flow induced pressure drops that could reduce relief valve output and
protection performance. Return lines shall be suitably pressure rated and sized for vented flow.
Return lines shall be checked for leak tightness during the pre-job pressure test. Block valves
shall not be run downstream of relief valves.
Temporary PRV's shall be tested, recalibrated and recertified to the agreed job set pressure before
each job. Pressure switches (where fitted) shall be tested and set by the job supervisor before each
job and at least monthly for long duration jobs. Pump PRV's shall be tested, recalibrated and
recertified annually as part of a base programmed maintenance system. Where appropriate identical,
certified, replacement relief valves shall be fitted to operational pumps to allow this.
IMPORTANT:
No part of a customer system shall be isolated from previously arranged overpressure protection
for any reason, at any time during the job.
No one shall remove or isolate any safety device installed on PRS equipment except for the purposes
of calibration, repair or maintenance. Safety devices shall be immediately replaced by equivalent
devices in such circumstances.
Whatever device is used, interference, tampering, modifying, isolating or altering the devices during
pressurisation or depressurisation of a system shall not take place without the system being first made
safe. If there is any reason to suspect that unauthorised interference has taken place the operation
shall be stopped for investigation prior to its continuation.
If at any time there is evidence to suggest that any protection or monitoring device is not performing
as it is designed to do then work shall be halted immediately, the system under pressure first made
safe and action taken to remedy the situation. Operations shall not commence without the above
protection devices in place and working properly.
Hose over pessurization protection
During rig up, appropriate lengths of hoses or other means of conveying the pressurising fluid (treating
iron or "pipes") and associated clean connections and fittings are to be run out to the agreed injection
point. This may be a single or multipoint injection. Hoses may be for low- or high-pressure gas/liquid
duty; in every case hoses, pipes, connections and fittings must be correctly pressure rated and sized
according to the type of work scope. Check before they are used. All hoses, treating iron or temporary
pipework shall have been pre-tested prior to mobilisation and carry current test certificates. These
certificates shall be presented to the client for inspection/approval prior to use on the job.
When applicable, rubber hoses and pipes shall have visual identification as to their function (i.e. main
discharge line, to test separator 1 ..... etc.). All hoses for whatever duty shall be tagged with a label
stating their maximum working pressure. All hoses shall be tested to their MWP every 12 months, and
the tested date marked on the tag. All pipeline services hoses shall be pre-tested to job working
pressure before each mobilisation.
Where appropriate, pressure drop shall be checked by calculation. Required flow rates may demand
pump discharge pressures greater than fitting or hose ratings. Discharge of used / spent liquid or gas
into customer vent or drain systems may generate sufficient back pressure to overpressure under
specified hose. Unplanned changes to rig up may cause excess flow and pressure to occur at
unforeseen points in hose runs.
At each rubber hose connection, a safety device shall be fitted so that in the event of hoses parting
company under pressure, the hoses are prevented from "whipping" about. A device such as a "whip-
check" or another suitable device must be used. Strong rope shall also be used to tie down lengths of
hoses providing, however, that the tie-down point selected is secure. Rubber hoses shall be secured
together and tied down (where practical) at each connection point along their length.
Long hoses shall be tied down at intermediate points where appropriate. Rubber hoses shall be
secured at all interfaces with the process plant and at the pump discharge.
Rubber hoses and pipes shall be routed (whenever possible) out of all walkways. If unavoidable, they
shall be routed in such a position so as not to present a "tripping" or safety hazard. In addition, rubber
hoses must be routed (where possible) in such a manner as to minimise the effects of abrasion,
accidental damage and away from areas frequently used by personnel (e.g., exits to and from
accommodation areas, tea shacks, designated smoking areas).
All surplus rubber hoses and pipes shall be coiled or stacked neatly and in such a manner that they do
not present a "tripping" or safety hazard.
Both rubber hoses and pipes shall be protected against over pressure and unacceptable temperatures
either by being rated above max possible (normal, abnormal and emergency) pressures and
temperatures or if this is not practical, by the use of suitable PRV's (Line PRV) or pressure/temperature
switches. Requirements for safe venting/recycle of hazardous liquids and for PRV/switch testing
specified for System Protection shall also apply to Hose Protection.
All equipment test dates should be checked for expiring based on the existing labels and stickers. Of
all pump / air hoses / pig-launchers etc. must be checked if the inspection date is not expired and is
suitable for the maximum test pressure.
Also, this procedure includes project specific TRA. The procedure must be checked by all parties,
approved, and signed before the work is performed.
6. Work method statement
Pre-notification provided by customer
Before testing can take place, a pre-notification is required at an early stage. It should contain at
least the following points:
• The system number and location
• The external diameters (mm), the wall thicknesses (mm), the lengths (m) and the volume
(m³) per diameter/ wall thickness section
• The total volume
• The test medium
• Date and time start hydrostatic test
• Design pressure
• Test pressures of the hydrostatic test
• Duration of the hydrostatic test
Registration
A pressure test form is drawn up of the test, containing at least the following data:
• Client name
• Identification of the tested pipeline or system
• Information of pressure gauges and temperature gauges
• Used medium
• Date of filling
• Date and time start hydrostatic test
• Test pressures of the hydrostatic test
• Duration of the hydrostatic test
• Remarks/ Events
Safety distance
During the test, the safety of the operating personnel, the environment and the installation must be
guaranteed. Although no explosions occur when testing with liquid, the ejecting of a part or the
spraying of the test liquid in the event of a collapse can cause danger to persons. Before starting each
test, a safety distance will be calculated based on the pipeline data.
Pressure measurement requirement
• The pipeline can be approved if pressure changes can be explained from the measured
temperature measurements, taking into account the inaccuracy in the measuring equipment
• During the test, a combination of two calibrated pressure gauges should be used to verify
that the test is performed at the correct pressure
Pneumatic pre-test
Initial pressurization of any system must always be performed in a slow and controlled manner.
Injection will be halted at 1 bar(g) and visual and audible inspection checks will be carried out.
Filling of system (performed by Vecom)
To prevent air pockets in the system, the system is filled slowly via the temporary inlet and fully
vented. When the system is fully filled with water, circulation of the main systems are started, and
one by one the subsystems are put into the circulation loop.
Hydrostatic test
A minimum of 1 hour for test pressure will be recommended. During the pressure test, if necessary,
welds are soaped in order to identify leakages/ or bad welds and or connections. The strength test
should be clearly visible written down on the gauge. This should have the correct measuring range so
that the test pressure can be read clearly.
The first pressurization step is at 1 bar(g), the stabilization time will be 5 min for each step. After the
first step, the next step will be 50% of the test pressure and then steps of 10%.
Initial pressurization of any system must always be performed in a slow and controlled manner,
stopping initially at 1 bar(g) and then at pressures equal to 50% of the final test pressure, in order
to allow the system to stabilize for a 5-minute period and to check all joints and flanges for visible or
audible leakage.
This will be repeated at 50%, steps of 10% till 100% test pressure. Injection will be halted at these
points and visual and audible inspection checks will be carried out. Pressure drop time assessments
will be carried out in order to satisfy the PRS supervisor and client responsible. Once system integrity
is established then pressurization will recommence up to 100% final test pressure with all checks
carried out as previously stated.
TEST PRESSURE IN BAR(G)

16 15
14 13,5
12
12
10,5
10 9 9
8,1
7,2 7,5
8
6,3
6 5,4
4,5
4
2 1 1
0
Test 9 bar(g) Test 15 bar(g)
Start 50% 60% 70% 80% 90% 100%
Measuring equipment
During the strength test the following precision measuring equipment is used:
Item Deviation % Exactitude Range

Analog precision gauge 1 cl. 0.6 0,5 bar To be determined later
Analog precision gauge 2 cl. 0.6 0,5 bar To be determined later
Pressure recorder cl. 1.0 2 bars To be determined later
Ambient temperature recorder cl. 1.0 2℃ -20℃ / + 50℃
Contact thermometer N/a 0,1 ℃ -50℃ / + 400℃
Instruments used for measurement of pressure and temperature shall be certified for accuracy and
sensitivity. The certification date shall be within 12 months preceding the test. All instrument relevant
test/ calibration certificates will be supplied for review and approval prior the testing activities.
If the system is equipped with many valves, it is wise to use more pressure gauges to ensure that the
entire system is fully pressurized.
Dewatering
After the hydrostatic testing has been completed, the water must be removed from the pipeline/
system. The system must be drained at all possible drain points/ vents fitted on the line. During
dewatering it is important that an air vent is opened so that no vacuum is created in the system. This
drains the system and completes the test.
7. Reporting
After successfully performing the hydrostatic test. The completed system pack will be passed to the
client for comment. The completed system pack shall include the following information:
1. Chart recorder information showing temperature sequence

2. Chart recorder information showing pressurisation sequence
3. Pressure test form
4. Daily operations logs
5. Toolbox talk and pre-job safety meeting
6. Equipment and personnel schedules
7. Job site risk assessments
8. Accident / Incident Reports
8. Disassembly / Demobilization of equipment
All pump-/air Hoses must be disconnected from the system and stored in the tool container. All spool-
pieces-, blind flanges etc. should be removed and the original valves should be mounted again.
A full site check for PRS equipment should be carried out on projects or large jobs prior to leaving site
All equipment that has become unserviceable during operations should be taped red so that
mechanics back at PRS yard can easily identify that equipment for repair.
TASK RISK ASSESSMENT FORM
Hydrostatic pressure testing Job Number: 032-P23
CLIENT: Klim aoprem a DATE: 10 May 2023 TRA TEAM LEADER: Project Supervisor
ACTIVITY: Hydrostatic testing ■ NEW TRA VALIDATED BY: S. Valkem a

REVISION:
DESCRIPTION OF JOB: Hydrostatic pressure test □ REVISED TRA TEAM: S. Valkem a, R. Anbergen, N. Berens
SPLIT-UP OF JOB IN TASKS

Highest Highest Note 1:
If one (1) or more tasks have an initial risk “Upper
Task Range Medium” or “High” then TRA shall be countersigned
Task Description Initial Risk Residual Risk
No: by Client rep. prior to start of activities.
(Note 1) (Note 2)
1. Mobilisation / Transport UM L
Note 2: If one (1) or more tasks have a residual risk of
2. Installation of equipment H LM “Upper Range Medium” or “High” then TRA shall be
countersigned by Operation Manager prior to start of
3. System preparation UM L activities
4. Pressure Testing H LM Countersign CR (Note 1)
5. Rig down of the equipment UM L Date:
Name:
Countersign Operation Manager (Note 2)
Date: 10 May 2023
Name: R. Anbergen
Form : PRS-ENG-F-001 rev. 0.0 10 May 2023 Page 1/8

Hydrostatic pressure testing
CLIENT: Klim aoprem a

ACTIVITY: Hydrostatic testing
DESCRIPTION OF JOB 1: Mobilisation / Transport
DETAILED TASK RISK ASSESSMENT:

Task Job Task Hazard(s) Involved Initial Risk Control measures Residual Risk
No: Assessment Assessment
P S R P S RR
Use steel plating to prevent getting stuck or

Material damage and personnel
to supporting loads in the field.
1 Transport to and from site. injury caused by falling loads. D II UM A II L
Traffic signs at loading areas will be obeyed.
Traffic accident.
Use pre-selected routes for transport.
Traffic guidance on site, secure loads and
fasten loads properly. Use the certified
Material damage and personnel
materials to secure and fasten the loads.
2 Mobilisation / de-mobilisation. injury caused by falling loads. C II LM A II L
Competent personnel and certified
Traffic accident.
companies will be used for transport and
mobilisation.
Check for leakages prior to leaving the
workshop and/or working sites. In case of
leakages, cleaning will be done by certified
Environmental damage caused by
3 Mobilisation / de-mobilisation. C II LM personnel/companies. An emergency A II L
leakages / oil spills.
response kit will be available (oil absorption
kit). In case of a spill HSE department will be
informed.


DESCRIPTION OF JOB 2: Installation of equipm ent

P S R P S RR
For heavy lifts a crane should be used. An

banks man shall guide the load in case of
Material damage and
using lifting equipment. Lifting will only be
1 Placing equipment. personnel injury caused by D II UM C II LM
done by certified companies. All lifting
falling loads / objects.
equipment should be certified.
Standard PPE should be worn at all times.
Use of correct hand-tools, ear protection
when use of air driven torque tools, use of
Connecting equipment, hoses and Material damage.
2 E III H whip-checks on gas-hoses. Define limits and B III LM
gauges. Personnel injury, slipping or falling.
maximum forces for bolting and screwed
connections. Verify the client’s connection
and pressure rating.
Injection point to be determined and agreed
by PRS and Petrogas supervision. Use of
Material damage.
standard PPE. Verify the clients connection
3 Connecting injection point. Damaging screwed connections. C III UM B III LM
and pressure rating. W hen working at
Personnel injury, falling of heights.
heights a proper scaffolding has to be in
place.


DESCRIPTION OF JOB 3: System preparation

P S R P S RR

Material damage. Never start without a Permit to work.
W rong installation point for the Check the working area to prevent slip and
Install pressure gauge, recorder and
1 gauge, recorder and PSV. D II UM trip. Use proper scaffolding if needed. B II L
PSV.
Personnel injury, slipping or falling of Gauge, recorder and PSV position to be
heights. checked and verified by PRS and Client
supervision.
Never start without a Permit to work. Check
Personnel injury, slipping or falling of
the working area to prevent slip and trip. Use
heights.
proper scaffolding if needed.
2 Valve line up. Material damage, wrong valve D II UM B II L
Only trained PRS and Client personnel can
handling and/or valve line up.
perform the valve line up.
System partly untested.
Valve positions to be checked and verified by
PRS and PRS and Client supervision.


DESCRIPTION OF JOB 4: Pressure Testing

P S R P S RR
Chemical resistance PPE should be worn at

all times. Ear plugs must be worn when the
pump is started. Never start without a Permit
Personnel injury, slips and trips. to work. Only trained PRS personnel can
1 Connect (testing) injection equipment. D II UM B II L
Material damage. operate the pump. Put barriers (barrier tape)
and warning sings in place. Pre-work
Toolbox talk / LMRA must be held with all
parties involved.
Personnel injury caused by leaking all times. Ear plugs must be worn when the
equipment. pump is operated. Only trained PRS
Unexpected release of compressed personnel can operate the pump. Only
2 Pre-test injection hose. stored energy. D II UM authorized personnel is allowed in the testing B II L
Untrained personnel in testing area. area. Use whip-checks around all hose-
Material damage caused by bursting connections. Check material certificates and
injection hose. PSV setting. All equipment should be fit for
purpose.
all times. Ear plugs must be worn during
pumping. Only authorized personnel is
Personnel injury, release of
allowed in the testing area. Proper certified
compressed stored energy.
3 Pressurize the system. D III H gauges and recorders must be installed and D I L
Material damage caused by over-
checked prior pressurisation. The safe
pressurizing the system.
distance must be maintained during
pressurisation. Check material certificates
and PSV setting.


all times. Use proper scaffolding if needed.
Check the pressure gauge to make sure the
Personnel injury, release of pressure is bled off before disconnecting the
compressed stored energy during injection hose. All hoses should be secured.
4 Disconnect the injection hose. D II UM B II L
disconnecting the hose. Hammering The whip-checks should be in place during
hose. Spills. disconnecting the injection hose. Only
trained PRS personnel is allowed to
disconnect the injection hose. Use drip trays
when disconnecting hoses.
Personnel injury, release of soap, all times. W hen working at heights a proper
falling from heights. scaffolding has to be in place. Check the
5 Check the system for leakages. D II UM C II LM
Material damage: blow out of working area to prevent slip and trip. Only
gaskets, leaking flanges. authorized personnel is allowed in the testing
area.


DESCRIPTION OF JOB 5: Rig down of the equipm ent

P S R P S RR

W hen working at heights a proper scaffolding
Personnel injury caused by falling has to be in place. Check the working area to
1 Rig down the equipment. loads or falling from heights. D II UM prevent slip and trip. B II L
Trapped pressure. Make sure every line is bled down to 0barg
before disconnecting.
check the pressure on the gauges.
Standard PPE should be worn at all times..
Check the working area to prevent slip and
Personnel injury and material trip.
2 Load equipment. D II UM B II L
damage caused by falling loads. Secure and fasten loads properly. Use the
certified materials to secure and fasten the
loads.
P = Probability; S = Potential Severity; R = Risk; RR = Residual Risk

JOB SAFETY ANALYSIS FORM RISK ASSESSMENT

USER INSTRUCTIONS USER INSTRUCTIONS
Front page: To asses the risk value of hazards, two parameters are to be defined:
* The probability (or likelihood) of an event to occur from the hazard
1. Installation: Enter name of installation or location
* The severity of the consequences (impact) of such events (in terms of the
2. Activity: Describe type of operation worst possible case)
3. Description of job: Enter job as precise as possible The probability of occurrence is found by answering the question:
4: Date: Enter date of TRA W ITH W HAT FREQUENCY IS THE HAZARD LIKELY TO ARISE?
5. TRA Team Leader: Enter name of nominated team leader For answering this question a selection may be taken from the following
6. TRA validated by: Enter name of authorized validator (RSES) predetermined categories:
* (A) PRACTICALLY IMPOSSIBLE (1 to 3 occurrences in 100 years)

7. TRA Team :
* (B) NOT LIKELY To OCCUR (1 to 3 occurrences in 30 years)
8. Split-up of job: List logical tasks in which the job can be split-up * (C) POSSIBILITY Of OCCURRING SOMETIMES (1 to 3 occurrences in 10 years)
* (D) POSSIBILITY Of ISOLATED INCIDENTS (1 to 3 occurrences in 3 years)
9. Task No.: Enter sequence number of tasks * (E) PROBABILITY Of REPEATED INCIDENTS (Annual occurrence or more)
10. Task description: Enter task as precise as possible The severity of the consequences of an event is found by answering the question:
W HAT RATING DOES APPLY TO THE W ORST CASE POSSIBLE
11. Highest Initial Risk: List the calculated Risk (14) from page 2 per task CONSEQUENCE W HEN A HAZARD RESULTS IN AN ACCIDENTAL EVENT?
12. Highest Residual Risk: List the calculated Residual Risk (16) per task For answering this question a selection may be taken from the following
predetermined categories:
Page 2: Detailed Task Risk Assessm ent
13. Hazard(s) involved: List per task the related hazards
14. Initial Risk Assessm ent: Consider the risk with standard control measures in
place (PPE and Permit to W ork). Enter the hazard
specific Probability, Severity and Risk from the matrix.
15. Control m easures: List the agreed control measures, including those
resulting from applicable VMS Procedures and write
down the VMS Procedure Number. Attach VMS
Procedure to this TRA when needed.
16. Residual Risk Assessm ent: Consider the control measures in place. Enter the
hazard specific Probability, Severity and related Risk
from the matrix. Combination of the probability & severity results in the calculated risk as per the
Corporate Risk Management Manual “Risk Matrix” on page 2 of this form.

Date: 12 May 2023
KLIMAOPREMA
Job Number:
032-P23
HYDROSTATIC TESTING
TEST-PACK NR.: TP-KO-820-001
PROJECT NR.: 032-P23
INSTALLATION: 820 Purified water
PREPARED FOR: Klimaoprema d.d.
DISTRIBUTION: Vecom/ PRS international
A 12 May 2023 Draft for approval
Rev. Date Description of modification

Name : Name : Name :
Date : Date : Date :
Originator Checked Verification & Approval

Date: 12 May 2023
KLIMAOPREMA
Job number:
032-P23
HYDROSTATIC TESTING
Index
Pneumatic pre-test acceptance A1
Hydrostatic test acceptance A2
Toolbox form B
Leak check repair report C
Limit status checklist D
Marked-up P&ID’s E
Client: Plant/Location:
Klimaoprema Leiden
Jobnumber: Subcontractor:
032-P23 SYSTEM LEAK TEST CERTIFICATE Vecom & PRS
AREA/UNIT/SYSTEM: DESCRIPTION:
820 Purified water Pneumatic pre-testing
Discipline: CERTIFICATE Nr.:

REV.A
Pneumatic pre-testing services 032-P23-820-A1
NOTE:
(*) Checks must be carried out according to project document’s latest applicable revision.
If not satisfactory, issue a punch list.
1.0) GENERAL INFORMATION
a) P&ID references:
LEI-310-819-41-001, LEI-310-820-41-001, LEI-310-820-41-002 and LEI-310-820-41-003
Test pressure PSV setting System volume Test duration
Test medium
[bar(g)] [bar(g)] [liter] [min]
Compressed air 15 bar(g) 16,5 bar(g) 45 liter 15 minutes
c) Leak test method used:
Gross leak test with compressed air (visual and hearing)
2.0) LEAK METHOD
ACTION DONE CHECK COMMENTS
Leaktest executed and signed off
Leak medium used
Leak witnessed by
System drained N/A Done by Vecom after cleaning method
Low Point drains checked N/A Done by Vecom after cleaning method
3.0) GENERAL COMMENTS
APPROVED BY: VECOM/ PRS CLIENT THIRD PARTY
Name:
Signature:
Date:
A1 TP 820 Pneumatic pre-test acceptance Page 1 of 1

Client: Plant/Location:
Klimaoprema Leiden
Jobnumber: Subcontractor:
032-P23 SYSTEM LEAK TEST CERTIFICATE Vecom & PRS
AREA/UNIT/SYSTEM: DESCRIPTION:
820 Purified water Hydrostatic testing
Discipline: CERTIFICATE Nr.:

REV.A
Hydrostatic testing services 032-P23-820-A2
NOTE:
(*) Checks must be carried out according to project document’s latest applicable revision.
If not satisfactory, issue a punch list.
1.0) GENERAL INFORMATION
a) P&ID references:
LEI-310-819-41-001, LEI-310-820-41-001, LEI-310-820-41-002 and LEI-310-820-41-003
Test pressure PSV setting System volume Test duration
Test medium
[bar(g)] [bar(g)] [liter] [min]
Demin water 15 bar(g) 16,5 bar(g) 45 liter 60 minutes
c) Leak test method used:
Final leak test with water (pressure chart)
2.0) LEAK METHOD
ACTION DONE CHECK COMMENTS
Leaktest executed and signed off
Leak medium used
Leak witnessed by
System drained N/A Done by Vecom after cleaning method
Low Point drains checked N/A Done by Vecom after cleaning method
3.0) GENERAL COMMENTS
APPROVED BY: VECOM/ PRS CLIENT THIRD PARTY
Name:
Signature:
Date:
A2 TP 820 Hydrostatic test acceptance Page 1 of 1

Doc. Nr. PRS-OP-F-002
Toolbox Form Page: 1 of 1
Revision: A
Client: Klimaoprema Location: Leiden
Type of job: Hydrostatic testing Job no: 032-P23 Date:
Job personnel
Name Company Name Company
• Has the test pack summary information reviewed?

• Is the permit to work in place and reviewed?
• No conflict with other working parties in the area?
• Is all personnel wearing the required PPE?
• Is the “JSA” been discussed with all parties involved?
• Is PRS equipment lined-up as per procedure?
• Is the temporary PSV in place and set at the correct pressure?
• Are pressure recorder and gauges online?
• Are the trapped pressure points identified?
• Is the blow down route been verified?
• Is the valve status checklist been reviewed and signed off?
• Are all flanged connections tapped off?
• Is the pressurization checklist been reviewed and signed off?
• Is the testing area barriered off?
Supervisor: Signature: Date:
B. TP 820 PRS-OP-F-002 - Toolbox Form PRS Page 1 of 1

LEAK CHECK/REPAIR REPORT
Location: Leiden Date:
Test pack: TP 820 Test Pressure: 15 bar(g)

Leak Leak Repaired
Details of Leak Detected & Repair
nr (Yes/No) (Yes/No)
Vecom/ PRS CLIENT
Completed by: Representative:
Date: Date:
C. TP 820 Leak report Page 1 of 1

C. TP 820 Leak report Page 2 of 1
PRS International and Vecom Klimaoprema TP 820
Limit status checklist Purified water
Limit/Valve Checked?
P&ID No. Valve TAG/NUM Position
No. (Encircle)
1 N3A - Connect jumper hose OPEN YES / NO
LEI-310-820-41-001
2 N3B - Connect jumper hose OPEN YES / NO
3 MV-003 CLOSED YES / NO
LEI-310-820-41-003 4 Before MV-001 - Install blind/ cap CLOSED YES / NO
5 Before MV-002 - Install blind/ cap CLOSED YES / NO
Check performed by (date & sign):
Witnessed by (date & sign):
D. TP 820 Limit check list Page 1 of 1

Incorrect
P&ID
revision
used.
Extent of skid
needs to be
reviewed/confir
med by BMS.
If pipe is >3D the Point 4

and 5 need flushing of
that pipe piece. Else it will
be static in that piece of
pipe.
Specialists in Maintenance & Surface Treatment
Author Gert Germs

Project num ber Vecom Industrial services B.V. 2300210
Client Klimaoprema
Subject Passivation and drying of purified water piping
systems
Location of cleaning BMS Oegstgeest
Date 30-08-2023
Checked by: Signature:
L. Vroon
Type of Document Rev. Lang. Pages

W MS 03 ENG. 11
Content
Contact matrix.................................................................................................................................. 2
Chemical cleaning procedure .......................................................................................................... 2
2.1 Equipment................................................................................................................................ 2
2.2 Delivery of systems ................................................................................................................. 2
2.3 Filling of the system ................................................................................................................. 2
2.4 Leak test .................................................................................................................................. 3
2.5 Passivating the system with Vecinox Passivating Liquid ........................................................ 3
2.6 Final flush ................................................................................................................................ 3
2.7 Drying of system ...................................................................................................................... 4
2.8 Sign off list: .............................................................................................................................. 4
Chemicals ........................................................................................................................................ 8
W aste ............................................................................................................................................... 8
Safety............................................................................................................................................... 9
5.1 Personal safety ........................................................................................................................ 9
5.2 Tools ........................................................................................................................................ 9
5.3 W orking on height.................................................................................................................... 9
5.4 First aid .................................................................................................................................... 9
5.5 Eating and drinking .................................................................................................................. 9
5.6 Safety for non-Vecom personnel ............................................................................................. 9
5.7 W ork place inspection ............................................................................................................. 9
Start work meeting ......................................................................................................................... 10
W ork place inspection form ........................................................................................................... 11
SIR W ork place inspection ............................................................................................................ 12
1
Contact m atrix
Klim aoprem a
Project Manager Ivan Juric ivan.juric@klimaoprema.com +385 (0)99 7072458
H&S Manager Klimaoprema Karl Heinz Karl.Heinz@klimaoprema.com +31(0) 613 003 402
Kwakman
Vecom Industrial Services B.V.

Project Manager ad interim Jan van Vulpen j.v.vulpen@vecom.nl +31 6 12 660 659
Supervisor David Przibilla d.przibilla@vecom.nl +31 6 20 096 584
Supervisor Gert Germs g.germs@vecom.nl +31 6 10 90 93 63
Chem ical cleaning procedure
Overview of works
To enable cleaning, circulation and pressure testing of the system Vecom will build a
tem porary piping system with pum p and circulationtank (see P&ID file)
The following steps will be m ade to clean the system
1 Erection tem porary system , 2 Air test and filling with water, 3 hydrotest (by PRS), 4 Leaktest
tem porary system 5 chem ical cleaning, 6 draining, 7 flushing, 8 drying with air, 9 dism antling
tem porary system
2.1 Equipment
Description of project: The passivation and drying of purified water system
Volume of system: ± 100 Liter (Purified water piping incl. temporary cleaning circuit)
Type of material: Stainless steel
2.2 Delivery of systems
Klimaoprema will ensure the system is prepared as per Vecom engineering before the start of the
filling of the systems.
Klimaoprema will ensure the availability of sufficient water.
W aste water treatment or disposal of waste water has been arranged and approved
2.3 Air-test and Filling of the system

Before the system can be filled an air-test will be held in order to see if there are any major leaks in
the system.
2
For this the complete system (including temporary system) will be slowly pressurised with air to
1Bar(g) and inspected before filling with water may commence.
If test is successful, the system can be filled with water to perform the hydrotest of the system
To prevent air pockets in the system, the system is able to switch flow direction and by switching flow
direction air can be removed. W hen the system is fully filled with demin water, circulation of the main
systems are started, and one by one the subsystems are put into the circulation loop.
HYDROTEST: After filling of the system with water a hydrotest will be held by PRS on the
existing system (see separate Hydrotest package for further inform ation).
2.4 Leak test

After the hydrotest of the existing system is finished and before starting any chemical phase, the
temporary system is leaktested separately at a higher pressure.
The leak test is performed specifically to check if the temporary systems are free of any leaks. This is
done with demin water. Both the temporary and existing system are put under 1.5 times the pressure
that will be used during the cleaning, with a minimum of 5.0 –6.0 bar, but always at least one (2) bar
lower than the hydrotest pressure. The test lasts 15-30min.
During this time, the system is walked down to see if any leaks are noticed, and this is validated by a
visual inspection around the system and tracking of the pressure given on the manometer. A decrease
in the pressure signifies that there is a leak. Should there be any leaks, these will be taken care of before
the chemical cleaning commences.
2.5 Passivating the system with Vecinox Passivating Liquid
After the leaktest the system will be drained fully.

W hen system is empty, it will be refilled completely with Vecinox Passivating liquid.
The passivating liquid will be circulated for a minimum of 2-3 hour.
During the passivation the iron and acid concentrations are determined.
The passivation is ended when the iron and acid concentrations are stable.
Parameters:
Temperature : Ambient temperature
Vecinox Passivating Liquid : 100 % (approx.. 18 –22 % nitric acid)
During the passivation, analyses will be performed (acid and iron concentrations are measured).
Test freg. : Every 30 minutes
After passivation the solution is drained to temporary waste water storage.
2.6 Final flush
Flushing with demineralized water

The lines are filled and flushed until the difference in conductivity of the influent and effluent is less than
25 µS/cm. The flush water is collected in temporary waste water storage.
After the final flushing the lines will be fully drained in preparation for the drying step
3
Parameters for flushing:
Temperature : Ambient
pH value : < 1 pH units difference (influent and effluent water)
Conductivity : < 5 µS/cm in/out (influent and effluent water)
2.7 Drying of system
After draining of the system the final drying step will follow
This will be executed by means of compressed air (dry and oil free) according DPS procedure –LEI-
310-B-SP-103 / BP104-2
System volum e W ater W aste water

Step totals for purified water liter liter
Filling 1 100 -
Pre-flush (if deemed necessary) Est. 50 50
Draining after flush and hydrotest 100
Passivating phase 1 volume passivating liquid 100 100
Filling 1 100-
Flushing after passivation 2 200 200
Final draining 1 100
Totals 500/550 500/550
2.8 Sign off list:
All steps described in the previous chapters are set here in blocks.
Analytical measurements and times of completion are written down.
Below chapter which is filled in during the chemical cleaning phase is added to the final customers
report.
Main items Notes Verified by Verified By

Vecom (Name + Sign.)
(Name + Sign)
1. Is system erection completed Date:

and accepted
Time:
2. Air test on system completed Date:
Time
3. Filling existing system with water Date
Time
4. Hydrotest existing system Date:
completed and accepted
4
Time
5. Chemical cleaning step Start:
End:
6. Draining and flushing step Start:
End:
7. Drying step Start:
End:
8. Dismantling temporary system Start:
End:
Leak test temporary connections Notes Verified by Verified By

Vecom (Name + Sign.)
(Name + Sign)
1. Check valve list. All valves have Date:

correct position for filling the
system?
Time:
2. Vents are open before start Date:

filling?
Time:
3. Check if sufficient Demin water is

available (>600 liter)
4. Fill the system with Date:
demineralized water
Time:
5. Closed all vents when system is Date:

completely filled
Time:
6. Pressurize the system Date:

(approx. 5-6 bars) for minimal 15
minutes
Time:
7. Check for leakages Date:
Time:
8. Repair possible leakages Date:
No. of leakages:
Time:
9. Drain the complete system Date:
5
Time:
Passivation step Verified by Verified By

Notes Vecom (Name + Sign.)
(Name +
Sign)
1. Check valve list. All valves have Date:

correct position for filling the
system with passivating liquid?
Time:
2. Dose Vecinox Passivating Liquid Date:
Time:
Concentration Nitric
acid:
Temperature:
3. Check for leakages. Date:
(continuously)
Time:
4. Vent system with the vent outlet Date:

venting in a 25 liter container
Time:
5. Perform iron and acid Date:

measurements every 30 minutes
on sample point. Time: during passivating
phase.
Results:
Iron:
Acid:
6. End passivation when analyses Date:

are stable
Time:
7. Note results of last iron and acid Date:

measurements.
Time sample taken:
Iron conc.
Acid conc.
Time sample taken:
6
Iron conc.
Acid conc.
Draining Step Verified by Verified By

(Name +
Sign)
1. Drain solution to effluent storage Time:
Date:
2. Check if all drains and vents are Time:

open with PI&D
3. Draining finished Time:
Date:
Final flushing Verified by Verified By

(Name +
Sign)
1. Fill the system with Time:

dem ineralized water
Date:
2. Check vents before flushing. Time:
3. Flush system according P&ID Time:

with dem ineralized water
4. Flushing completed Time:
Conductivity in:
Conductivity out:
4. Drain the solution to the effluent Time:

storage.
Date:
7
Chem icals
Chemicals are placed either in or on top of drip trays. The following amounts of chemicals will be used
(based on a total system volume of 100 liter
Vecinox passivating liquid : 100 Liter (est.)
W aste
Vecom will arrange waste water storage. The concentrated chemical cleaning solutions and flushing
water will be pumped into a waste storage tanks (IBC).
The chemical waste water will be removed from site to a certified waste disposal company
8
Safety
5.1 Personal safety
In order to work safely on site, all personnel must wear the required PBMs. These PBMs are given by
Vecom to Vecom personnel, however, everyone involved in the chemical cleaning must adhere to
wearing these PBMs as well.
Vecom personnel wear the following PBMs during the work activities:
- Safety shoes
- Helmet (white)
- Safety goggles (with side protection)
- Overall
- W orking gloves (during the build-up and breakdown of system)
During the chemical cleaning, the following additional PBMs are used according to degree of necessity
(dependent on chemical procedure):
- Rubber, chemically resistant gloves
- Chemically resistant suit
- Face protection screen
All PBMs are kept and used according to the regulations of the supplier.
W orking in shorts (pants or shirt) is prohibited.
5.2 Tools
All the electrical tool and apparatus must be tested according to the NEN3140 standards.
5.3 W orking on height

Ladders, scaffolding and aerial platforms must be tested.
Scaffolding must only be tread upon if a green scaffolding card is present. Modifications to the
scaffolding are never done by Vecom personnel. Scaffolding can only be changed by scaffolding
contractor.
5.4 First aid

The first aid post of the client is available.
A standard first aid kit is present at the workplace or in the Vecom transport van.
5.5 Eating and drinking

Eating and drinking at the workplace is prohibited. It is solely allowed to eat and drink at the appointed
spaces (canteens).
5.6 Safety for non-Vecom personnel

During the chemical cleaning, the area where the pumps and chemicals are placed must be cordoned
off with tape and signs reading “corrosive” in every entrance and exit point of the area.
5.7 W ork place inspection

To maintain a safe work space, a work place inspection will be performed by one of the Vecom
supervisors. The inspection will be done according to the VECOM VCA-Handbook.
9
Start work m eeting
The purpose of the “start work meeting” is to ensure that all the personnel involved with the chemi cal
cleaning is well informed about the chemical procedure. Additionally, the safety, health and
environmental risks are discussed.
The “start work meeting” is given by a Vecom supervisor/operator that knows all the details of the project
and the chemical procedures.
It is imperative for the Vecom personnel to know the relevant procedure before commencing with the
chemical cleaning.
The following documents will be discussed during the “start work discussion” :
- Task Risk Analysis (TRA)
- Chemical cleaning procedure
After the meeting, a presence list is filled in and signed by all the present members.
Report “start work meeting”

…………………………………………………………………………………………………………………………
…………………………………………………………………………………………………………………………
…………………………………………………………………………………………………………………………
…………………………………………………………………………………………………………………………
…………………………………………………………………………………………………………………………
…………………………………………………………………………………………………………………………
…………………………………………………………………………………………………………………………
…………………………………………………………………………………………………………………………
…………………………………………………………………………………………………………………………
…………………………………………………………………………………………………………………………
…………………………………………………………………………………………………………………………
…………………………………………………………………………………………………………………………
…………………………………………………………………………………………………………………………
…………………………………………………………………………………………………………………………
…………………………………………………………………………………………………………………………
Name Date Signature
10
W ork place inspection form
1 Is the workplace cleaned up and tidy? YES NO
Are there any obstacles that could pose a threat of tripping?

2 YES NO
If so, why have they not been removed?
Are all emergency exits free of obstacles?

3 YES NO
If not, why have they not been removed?
Are fire extinguishers in close vicinity?

4 • Are they fast and easily reachable? YES NO
• Have they been recently tested and approved?
5 Is the work being performed according the work permit? YES NO
Are the necessary utensils against calamities present?

• Absorption granules
6 YES NO
• Drip trays
• First aid materials
7 Are personal protective utensils, in case prescribed, applied correctly? YES NO
Are chemicals stored in the prescribed manner?

8 • Are acids and bases separated? YES NO
• Are all chemicals on a liquid proof floor or drip tray?
Are the pumps, circulation tank, etc. on a liquid proof floor?

9 YES NO
If not, why not?
Name: Signature
Date:
11
SIR W ork place inspection
General information
Work permit #: Date:
Location: Object:
Documents
(SIR) Certificates of hoses and equipment available? Y N Task Risk Analysis and CTR procedure available? Y N
SDS of pollutant available? Y N SDS of treatment chemicals available? Y N
Transport/CMR documents for waste available? Y N Permit to discharge chemicals and/or contaminated Y N
water to sewer?
Applicable PPE (standard: helmet safety shoes S3, gloves (task specific) and safety glasses)
Chemically resistant clothes (coverall) Y N Chemically resistant gloves Y N
Face shield Y N Safety glasses and/or splash goggles Y N
Safety shoes or boots (S3 qualification) Y N Full face mask including (spare) ABEK filter Y N
Specific PPE needed? Which one?
Installing equipment
Utilities (water, power) available? Y N Emissions of installation subject to cleaning, known and Y N
controlled?
Floor stable and without stumbling and slipping Y N Hoses for chemical substances and hoses for pressurised Y N
issues? air are secured?
Emergency stop available and tested? Y N Storage IBC’s/tank(s) for wastewater/chemicals Y N
available?
Installation isolated and blocked according to Y N Secondary containment (chemicals, wastewater etc.) Y N
tagout-lockout standard? available?
Streaming water (hose with water tap) available? Y N Correct flange and gasket available? Y N
Installation at normal pressure (1013 mbar) and Y N Left over chemicals etc under control? Y N
approval available?
Equipment without SIR certificate and why?
ATX or EX zone, which extra measures are needed?
Electrical grounding
Earthing available and approved? Y N Earthing checked and tested? Y N
Safety precautions
Safety shower tested and accessible without Y N SIR CTO First aid box incl. SIR First Aid instruction chart Y N
obstruction? available?
Fire extinguisher available? Y N Communication with CCR available and tested. Y N
Work floor corned off with CTO safety signs? Y N
Special conditions
Is there a deviation of the SIR standards? If yes, where?
Are these deviations discussed and reported? How and by whom?
Reduction of emissions needed; if yes, which one?
Are extra measures taken; if yes, which ones?
Chemical Cleaning completed

Work floor cleaned? Y N
Work permit completed and returned? Y N
Chemicals and wastewater labelled? Y N
Are there any malfunctions known? Y N If yes, reported to?
Completed by:
Name: Date:
Signature: Time:
12
According to EC-Regulation 1907/2006 (REACH), annex II, including changes implemented by EC-Regulation 2020/878
SAFETY DATA SHEET
Vecinox Passivating Liquid
SECTION 1: Identification of the substance/mixture and of the company/undertaking
1.1. Product identifier

Trade name
Vecinox Passivating Liquid
1.2. Relevant identified uses of the substance or mixture and uses advised against
Relevant identified uses of the substance or mixture
No special
Uses advised against
No special
1.3. Details of the supplier of the safety data sheet
Company and address
V-Com Chemicals
Beugsloepweg 9
3133 KV Vlaardingen
Nederland
+31 (0) 10 316 0567
Contact person
-
E-mail
msds@blendfill.nl
SDS date
2021-07-21
SDS Version
1.0
1.4. Emergency telephone number
Contact The National Poisons Information Service (dial 111, 24 h service).
See section 4 “First aid measures”.
SECTION 2: Hazards identification
2.1. Classification of the substance or mixture

Met. Corr. 1; H290, May be corrosive to metals.
Skin Corr. 1A; H314, Causes severe skin burns and eye damage.
Eye Dam. 1; H318, Causes serious eye damage.
Acute Tox. 4; H332, Harmful if inhaled.

2.2. Label elements
Hazard pictogram(s)
Signal word
Danger
Hazard statement(s)
Vecinox Passivating Liquid Page 1 of 10

May be corrosive to metals. (H290)

Causes severe skin burns and eye damage. (H314)
Harmful if inhaled. (H332)
Safety statement(s)
General
-
Prevention
Do not breathe vapour / mist. (P260)
Wear eye protection / protective gloves / protective clothing. (P280)
Response
IF ON SKIN (or hair): Take off immediately all contaminated clothing. Rinse skin with water [or shower].
(P303+P361+P353)
IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to
do. Continue rinsing. (P305+P351+P338)
Storage
Store in a container with a resistant inner liner. (P406)
Disposal
Dispose of contents/container to an approved waste disposal plant. (P501)
Hazardous substances
nitric acid ... %
2.3. Other hazards
Additional labelling
Not applicable
Additional warnings
This mixture/product does not contain any substances considered to meet the criteria classifying them as PBT
and/or vPvB.
SECTION 3: Composition/information on ingredients
3.2 Mixtures
Product/substance Identifiers % w/w Classification Note
nitric acid ... % CAS No.: 7697-37-2 15-25% Ox. Liq. 2, H272 [1]
Met. Corr. 1, H290
EC No.: 231-714-2 Acute Tox. 3, H331
Skin Corr. 1A, H314
REACH: 01-2119487297-23 EUH071
Index No.: 007-004-00-1
-----
See full text of H-phrases in section 16. Occupational exposure limits are listed in section 8, if these are available.
Other information
[1] European occupational exposure limit
SECTION 4: First aid measures
4.1. Description of first aid measures

General information
In the case of accident: Contact a doctor or casualty department – take the label or this safety data sheet.
Contact a doctor if in doubt about the injured person’s condition or if the symptoms persist. Never give an
unconscious person water or other drink.
Inhalation
Upon breathing difficulties or irritation of the respiratory tract: Bring the injured person into fresh air. Make sure
the injured person is continuously monitored. Prevent shock by keeping the injured person warm and calm. If
breathing ceases, give mouth-to-mouth resuscitation. If unconscious, roll the injured person into recovery

position. Call an ambulance.

Skin contact
Remove contaminated clothing and shoes immediately. Ensure to wash exposed skin thoroughly with water and
soap. Skin cleanser can be used. DO NOT use solvents or thinners.
If skin irritation occurs: Get medical advice/attention.
Eye contact
Upon irritation of the eye: Remove contact lenses. Flush eyes with plenty of water or salt water (20-30°C) for at
least 15 minutes and continue until irritation stops. Make sure you flush under the upper and lower eyelids. Seek
medical assistance immediately and continue flushing during transport.
Ingestion
Provide plenty of water for the person to drink and stay with him/her. In case of malaise, seek medical advice
immediately and bring the safety data sheet or label from the product. Do not induce vomiting, unless
recommended by the doctor. Have the victim lean forward with head down to avoid inhalation of- or choking on
vomited material.
Burns
Not applicable
4.2. Most important symptoms and effects, both acute and delayed
Tissue-damaging effects: This product contains substances with skin corrosive properties. Inhaled vapour or
aerosols may produce adverse effects to lungs, -irritations and burns in the respiratory organs -as well as
coughing. Dermal contact and contact with the eye cause irreversible effects.
Irritation effects: This product contains substances, which may cause irritation upon exposure to skin, eyes or
lungs. Exposure may result in an increased absorption potential of other hazardous substances at the area of
exposure.
4.3. Indication of any immediate medical attention and special treatment needed
IF exposed or concerned:
Get immediate medical advice/attention.
Information to medics
Bring this safety data sheet or the label from this product.
SECTION 5: Firefighting measures
5.1. Extinguishing media

Suitable extinguishing media: Alcohol-resistant foam, carbon dioxide, powder, water mist.
Unsuitable extinguishing media: Waterjets should not be used, since they can spread the fire.
5.2. Special hazards arising from the substance or mixture
Fire will result in dense smoke. Exposure to combustion products may harm your health. Closed containers,
which are exposed to fire, should be cooled with water. Do not allow fire-extinguishing water to enter the
sewage system and nearby surface waters.
If the product is exposed to high temperatures, e.g. in the event of fire, dangerous decomposition compounds
are produced. These are:
Nitrogen oxides (NOₓ)
5.3. Advice for firefighters
Wear self-contained breathing apparatus and protective clothing to prevent contact. Upon direct exposure
contact The National Poisons Information Service (dial 111, 24 h service) in order to obtain further advice.
SECTION 6: Accidental release measures
6.1. Personal precautions, protective equipment and emergency procedures

Avoid direct contact with spilled substances.
Avoid inhalation of vapours from spilled material.
6.2. Environmental precautions
Avoid discharge to lakes, streams, sewers, etc.
6.3. Methods and material for containment and cleaning up
Use sand, sawdust, earth, vermiculite, diatomaceous earth to contain and collect non-combustible absorbent
materials and place in container for disposal, according to local regulations.

To the extent possible cleaning is performed with normal cleaning agents. Avoid use of solvents.
6.4. Reference to other sections
See section 13 on “Disposal considerations” in regard of handling of waste.
See section 8 "Exposure controls/personal protection" for protective measures.
SECTION 7: Handling and storage
7.1. Precautions for safe handling

Avoid direct contact with the product.
Smoking, drinking and consumption of food is not allowed in the work area.
See section 8 "Exposure controls/personal protection" for information on personal protection.
7.2. Conditions for safe storage, including any incompatibilities
Containers that have been opened must be carefully resealed and kept upright to prevent leakage.
Store in a container with a resistant inner liner.
Recommended storage material
Always store in containers of the same material as the original container.
Storage temperature
Dry, cool and well ventilated
Incompatible materials
Strong acids, strong bases, strong oxidizing agents, and strong reducing agents.
7.3. Specific end use(s)
This product should only be used for applications quoted in section 1.2
SECTION 8: Exposure controls/personal protection
8.1. Control parameters

__
nitric acid ... %
Short term exposure limit (15 minutes) (ppm): 1
Short term exposure limit (15 minutes) (mg/m³): 2,6
The Control of Substances Hazardous to Health Regulations 2002. SI 2002/2677 The Stationery Office 2002.
EH40/2005 Workplace exposure limits (Fourth Edition 2020)
DNEL
Product/substance nitric acid ... %

DNEL 2.6 mg/m3
Route of exposure Inhalation
Duration Short term

DNEL 2.6 mg/m3
Duration Long term
PNEC
No data available
8.2. Exposure controls
Compliance with the given occupational exposure limits values should be controlled on a regular basis.
General recommendations
Smoking, drinking and consumption of food is not allowed in the work area.
Exposure scenarios
There are no exposure scenarios implemented for this product.
Exposure limits
Professional users are subjected to the legally set maximum concentrations for occupational exposure. See

occupational hygiene limit values above.

Appropriate technical measures
Airborne gas and dust concentrations must be kept at a minimum and below current limit values (see above).
Installation of a local exhaust system if normal air flow in the work room is not sufficient is recommended.
Ensure emergency eyewash and -showers are clearly marked.
Hygiene measures
In between use of the product and at the end of the working day all exposed areas of the body must be washed
thoroughly. Always wash hands, forearms and face.
Measures to avoid environmental exposure
Keep damming materials near the workplace. If possible, collect spillage during work.
Individual protection measures, such as personal protective equipment
Generally
Use only CE marked protective equipment.
Respiratory Equipment
Work situation Type Class Colour Standards
- Respiratory - - -
protection is not
needed in the
event of
adequate
ventilation
Combination Class 2 Brown/Gray/Yellow/Green EN14387

Filter A2B2E2K2 (medium
capacity)
Skin protection
Work situation Recommended Type/Category Standards
Wear appropriate protection clothing, - -

e.g. coveralls in polypropylene or
working clothes in cotton or polyester.
Hand protection
Work situation Material Glove thickness Breakthrough time Standards

(mm) (min.)
Nitrile 0.4 > 480 EN374-2, EN374-3,

EN388
Eye protection
Work situation Type Standards
Wear safety glasses with side shields. EN166
SECTION 9: Physical and chemical properties
9.1. Information on basic physical and chemical properties

Physical state
Liquid
Colour
Colourless

Odour / Odour threshold

Testing not relevant or not possible due to nature of the product.
pH
1
Density (g/cm³)
1.10 (20.00 °C)
Relative density
1.10 (20.00 °C)
Kinematic viscosity
Particle characteristics
Does not apply to liquids.
Phase changes
Melting point/Freezing point (°C)
Softening point/range (waxes and pastes) (°C)
Does not apply to liquids.
Boiling point (°C)
Vapour pressure
Relative vapour density
Decomposition temperature (°C)
Data on fire and explosion hazards
Flash point (°C)
Ignition (°C)
Auto flammability (°C)
Lower and upper explosion limit (% v/v)
Solubility
Solubility in water
Soluble
n-octanol/water coefficient
Solubility in fat (g/L)
9.2. Other information
SECTION 10: Stability and reactivity
10.1. Reactivity
No data available
10.2. Chemical stability
The product is stable under the conditions, noted in section 7 “Handling and storage”.
10.3. Possibility of hazardous reactions
No special
10.4. Conditions to avoid
No special
10.5. Incompatible materials
Strong acids, strong bases, strong oxidizing agents, and strong reducing agents.

10.6. Hazardous decomposition products

The product is not degraded when used as specified in section 1.
SECTION 11: Toxicological information
11.1. Information on hazard classes as defined in Regulation (EC) No 1272/2008

Acute toxicity

Test method
Species Rat
Test LC50 (4 hours)
Result 2.65 mg/L
Other information
Harmful if inhaled.
Skin corrosion/irritation
Causes severe skin burns and eye damage.
Serious eye damage/irritation
Causes severe skin burns and eye damage.
Causes serious eye damage.
Respiratory sensitisation
Based on available data, the classification criteria are not met.
Skin sensitisation
Germ cell mutagenicity
Carcinogenicity
Reproductive toxicity
STOT-single exposure
STOT-repeated exposure
Aspiration hazard
11.2 Information on other hazards
Long term effects
Tissue-damaging effects: This product contains substances with skin corrosive properties. Inhaled vapour or
aerosols may produce adverse effects to lungs, -irritations and burns in the respiratory organs -as well as
coughing. Dermal contact and contact with the eye cause irreversible effects.
Endocrine disrupting properties
No special
Other information
No special
SECTION 12: Ecological information
12.1. Toxicity

Test method
Species Fish

Compartment
Duration 96 hours
Test LC50
Result > 100 mg/L
Other information

Test method
Species Daphnia
Compartment
Duration 24 hours
Test EC50
Result 180 mg/L
Other information
12.2. Persistence and degradability

No data available
12.3. Bioaccumulative potential
No data available
12.4. Mobility in soil
No data available
12.5. Results of PBT and vPvB assessment
This mixture/product does not contain any substances considered to meet the criteria classifying them as PBT
and/or vPvB.
12.6. Endocrine disrupting properties
No special
12.7. Other adverse effects
No special
SECTION 13: Disposal considerations
13.1. Waste treatment methods

Product is covered by the regulations on hazardous waste.
HP 6 - Acute toxicity
HP 8 – Corrosive
Avoid discharge to lakes, streams, sewers, etc.
Dispose of contents/container to an approved waste disposal plant.
Regulation (EU) No 1357/2014 of 18 December 2014 on waste.
EWC code
Not applicable
Specific labelling
Not applicable
Contaminated packing
Packaging containing residues of the product must be disposed of similarly to the product.
SECTION 14: Transport information
14.1 - 14.4
This product is within scope of the regulations of transport of dangerous goods.
ADR/RID

UN- or ID UN proper shipping name Labels Packing group Tunnel restriction code
number
2031 NITRIC ACID 8 II 2 (E)
IMDG
UN- or ID UN proper shipping name Labels Packing group EmS

number
2031 NITRIC ACID 8 II F-A, S-B*
MARINE POLLUTANT
No
IATA
UN- or ID UN proper shipping name Labels Packing group

number
2031 NITRIC ACID 8 II
14.5. Environmental hazards

Not applicable
14.6. Special precautions for user
Not applicable
14.7. Maritime transport in bulk according to IMO instruments
No data available
SECTION 15: Regulatory information
15.1. Safety, health and environmental regulations/legislation specific for the substance or mixture
Restrictions for application
Restricted to professional users.
People under the age of 18 shall not be exposed to this product.
Demands for specific education
No specific requirements
SEVESO - Categories / dangerous substances
Not applicable
Additional information
Not applicable
Sources
The Management of Health and Safety at Work Regulations 1999
Regulation (EU) No 1357/2014 of 18 December 2014 on waste.
Regulation (EC) No 1272/2008 of the European Parliament and of the Council of 16 December 2008 on
classification, labelling and packaging of substances and mixtures, amending and repealing Directives
67/548/EEC and 1999/45/EC, and amending Regulation (EC) No 1907/2006 (CLP).
Regulation (EC) 1907/2006 (REACH).
15.2. Chemical safety assessment
No
SECTION 16: Other information
Full text of H-phrases as mentioned in section 3

EUH071, Corrosive to the respiratory tract.
H272, May intensify fire; oxidiser.
H290, May be corrosive to metals.
H314, Causes severe skin burns and eye damage.
H331, Toxic if inhaled.

Abbreviations and acronyms

ADN = European Provisions concerning the International Carriage of Dangerous Goods by Inland Waterway
ADR = The European Agreement concerning the International Carriage of Dangerous Goods by Road
ATE = Acute Toxicity Estimate
BCF = Bioconcentration Factor
CAS = Chemical Abstracts Service
CE = Conformité Européenne
CLP = Classification, Labelling and Packaging Regulation [Regulation (EC) No. 1272/2008]
CSA = Chemical Safety Assessment
CSR = Chemical Safety Report
DMEL = Derived Minimal Effect Level
DNEL = Derived No Effect Level
EINECS = European Inventory of Existing Commercial chemical Substances
ES = Exposure Scenario
EUH statement = CLP-specific Hazard statement
EWC = European Waste Catalogue
GHS = Globally Harmonized System of Classification and Labelling of Chemicals
IARC = International Agency for Research on Cancer (IARC)
IATA = International Air Transport Association
IBC = Intermediate Bulk Container
IMDG = International Maritime Dangerous Goods
LogPow = logarithm of the octanol/water partition coefficient
MARPOL = International Convention for the Prevention of Pollution From Ships, 1973 as modified by the Protocol
of 1978. ("Marpol" = marine pollution)
OECD = Organisation for Economic Co-operation and Development
PBT = Persistent, Bioaccumulative and Toxic
PNEC = Predicted No Effect Concentration
RID = The Regulations concerning the International Carriage of Dangerous Goods by Rail
RRN = REACH Registration Number
SCL = A specific concentration limit.
SVHC = Substances of Very High Concern
STOT-RE = Specific Target Organ Toxicity - Repeated Exposure
STOT-SE = Specific Target Organ Toxicity - Single Exposure
TWA = Time weighted average
UN = United Nations
UVCB = Complex hydrocarbon substance
VOC = Volatile Organic Compound
vPvB = Very Persistent and Very Bioaccumulative
Additional information
The classification of the substance/mixture in regard of health hazards are in accordance with the calculation
methods given by Regulation (EC) No. 1272/2008 (CLP)
The safety data sheet is validated by
RK
Other
A change (in proportion to the last essential change (first cipher in SDS version, see section 1)) is marked with a
blue triangle.
The information in this safety data sheet applies only to this specific product (mentioned in section 1) and is not
necessarily correct for use with other chemicals/products.
It is recommended to hand over this safety data sheet to the actual user of the product. Information in this
safety data sheet cannot be used as a product specification.
Country-language: GB-en

Pre-commissioning Passivation and drying of pipework
Risk Assessments
Project:BMS Leiden
Subject
Risk Assessm ents
Purified water system s
Validation
Project: BMS Leiden
Project: Pre-com m issioning Passivation and drying of Stainless Steel pipework

Customer: Klimaoprema
Created by Checked by Approved by

G.Germs D.Przibilla l.Vroon
Document Number P/O Date

2300210 25-04-2023
Mozartlaan 3
3144NA Maassluis
The Netherlands
Revision history
Rev. Rev. Date Approved by Remarks

Data sheets 1 Eng. 1/
1
Pre-commissioning Passivation and drying of pipework
Risk Assessments
Project:BMS Leiden
Doc No. Risk Assessm ent Title Page No.
09.1 Chemical Storage 3-8

09.2 Circulation of Chemicals with a Temporary Circulation Loop 9-15
09.3 Hazardous Products Spill Response 16-19
09.4 Manual Handling 20-24
09.5 Transfer of Chemicals Around Site 25-29
09.6 Transfer of Chemicals from one Container to Another 30-36
09.7 Use of Compressed Air 37-40
09.8 Use of Hand Tools 41-44
09.9 Use of Electrical Equipment 45-47
09.10 Heating of Chemicals (with Steam) 48-51
2
Ref Num ber: 09.1
Risk Assessm ent Record

Chem ical Storage
Departm ent : CTR Date : 04-05-2023
Drafted by : G.Germ s Signature : Assessed By : Signature :
Date of Review: Type of Review (Routine (R) or Incident Based (IB): Future Review Date: 04-05-2023
Description of Task : Chemical Storage
MSDS: Vecinox passivating liquid
Personnel at Risk : Vecom Operatives
Residual Risk
Health, Safety or Environm ental Risk
Likely Effect Probability x Severity = Minim ise Risk By
(H/M/L)
Hazard Rating
Hazardous Chemicals Contact with personnel H H H W here possible, bulk and concentrate L
Adverse effect on environment chemicals shall be stored in one
Further damage to equipment location. Smaller volumes shall be
transferred into small containers for
movement around site.
All chemicals shall be stored within

secure (fenced), bunded locations.
Bunds shall have at minimum, a
volume capacity of 110% of the
largest container within it.
Storage bunds shall be inspected

daily. Liquid contents of the bund shall
be pH tested to determine if they are
rainwater or not
Probability : Severity : Risk Rating :

H = Highly Likely H = Serious / Fatal (HxH) = H (MxM) = M (LxL) = L H = Task requires im proved control
M = Probable M = LTI / MTC (HxM) or (MxH) = H M = Task requires im proved control
(LxH) or (HxL) = M
L = Unlikely L = Minor / First Aid L = Task m ay com m ence subject to
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.1

Chem ical Storage
Residual Risk
(H/M/L)
Hazard Rating
Hazardous Chemicals Contact with personnel H H H All liquids found in the bund (rainwater L
(continued....) Adverse effect on environment or not) shall be pumped directly in the
Further damage to equipment hazardous waste storage tank
Access to the chemical storage area

shall be off-limits to non-essential and
unauthorised staff
W here practicable, the chemical

containers shall be locked to prevent
unauthorised opening / decanting
Containers shall be routinely

inspected daily (logged on daily
inspection sheet) to verify that they
are not leaking and are fit-for-purpose
All chemical storage areas (including

the area around the effluent tank)
shall be fenced off and warning signs
should be placed

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.1

Chem ical Storage
Residual Risk
(H/M/L)
Hazard Rating
Chemical quantities in storage shall

be logged continuously by the Vecom
Supervisor. A physical record of the
chemicals onsite –and their
respective locations shall always be
available upon request
Vecom staff are trained in using

chemicals and have had an
awareness training
First aid kit, emergency shower and

eye flush bottles are available on
jobsite
Empty / Used Containers Contact with personnel M H H Empty containers still pose a health & L
Adverse effect on environment safety risk and should be handled with
care. The container shall be labelled
using the information of the last
product it contained and treated with
the same precautions

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.1

Chem ical Storage
Residual Risk
(H/M/L)
Hazard Rating
Containers that are no longer required

shall be collected by a registered
waste carrier and disposed of in
accordance with VLAREMA (Belgium)
Regulations 17 june 2019
Spills Contact with personnel H H H Spill-kit materials to be ready at hand L

Adverse effect on environment and sufficient in quantity to handle the
Further damage to equipment volume of chemical being stored. In
the case of an IBC storage area, the
spill-kit shall be able to absorb 1,100 lt
A leaktest has to be performed on the

system before any chemicalls are
allowed to be dosed
Vecom staff shall be competent to use

spill-kit materials and are familiar with
the approved spill-response plan

jobsite

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.1

Chem ical Storage
Residual Risk
(H/M/L)
Hazard Rating

awareness training
Incompatible Materials Adverse Chemical Reaction M H H Incompatible materials shall be kept in L

separate bunds, and never stored
directly adjacent to each other
All containers shall be accurately

labelled in accordance with CLP
regulations & GHS pictograms
Exposure to Hazardous Substances Adverse effect of health H H H Check relevant MSDS before start of L
works
Vecom First-Aider, familiar with the

treatment of chemical injuries shall be
available during working hours
Suitable and sufficient first-aid

equipment shall be available and
close-at-hand –including:
- Safety shower
- Eye wash station

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.1

Chem ical Storage
Residual Risk
(H/M/L)
Hazard Rating
Good hygiene to be adhered to at all

times especially before eating,
drinking and smoking

chemicals and have had an awarenes
training

jobsite

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.1

Chem ical Storage
Risk Assessment Title: Chemical Storage Date of Revision: April 2023
Read, understood and accepted by:
Nam e Signature Date

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.2

Circulation of Chem icals within a Tem porary Circulation Loop
Description of Task : Circulation of Chemicals within a Temporary Circulation Loop
Residual Risk
(H/M/L)
Hazard Rating
Leaking / Defective pump, hoses Contact with personnel H H H Restrict access to non-essential staff L
temporary connections Adverse effect on environment in work area using barriers and
Further damage to equipment appropriate signage
Staff to be trained, competent and

authorised to carry out chemical
circulation activities
A leaktest must be performed before

any chemicalls can be dosed in the
system
All personnel to wear PPE as defined

in relevant MSDS

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.2

Residual Risk
(H/M/L)
Hazard Rating
Chemical containers and pump(s)

must be positioned within bunded
area(s)
Leaking / Defective pump, hoses Contact with personnel H H H Spill-kit materials to be ready at hand L
temporary connections Adverse effect on environment and sufficient in quantity to handle the
(continued…) Further damage to equipment volume of chemical being circulated.
(continued…) Bulk (1,100 litre spill-kit shall be
located in the chemical storage area.
Various 50 litre spill kits shall be
positioned around the temporary
circulation loop
Staff carrying out circulation activities

shall be competent to use spill-kit
materials and are familiar with the
approved spill-response plan
Pump, hoses and gaskets to be

compatible (resistant) with the
chemicals being transferred.
Equipment subject to regular

maintenance and inspections –
including pre-use inspections.

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.2

Residual Risk
(H/M/L)
Hazard Rating
Leaking / Defective pump, hoses Contact with personnel H H H All temporary connections to be L
temporary connections Adverse effect on environment inspected by a second person prior to
(continued…) Further damage to equipment chemical cleaning –as per approved
(continued…) Vecom System Method Statement
All temporary connections shall be

fitted with a valve that can be used to
isolate the system in the event of a
leak
Temporary system shall be leak-

tested with water prior to the
introduction of chemicals. Leak-test
shall be at <10bar for >15 minutes.
Permanent manual/actuated valves

shall be locked in open position during
circulation
Vecom staff shall patrol the circulation

loop throughout the process,
inspecting temporary connections for
leaks.

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.2

Residual Risk
(H/M/L)
Hazard Rating
Leaking / Defective pump, hoses Contact with personnel H H H Vecom staff shall carry radios in order
temporary connections Adverse effect on environment to maintain communication with the
(continued…) Further damage to equipment Vecom Supervisor and Pump operator
(continued…)
The Vecom Supervisor shall carry an

additional radio in order to
communicate with Klimaoprema-Sisk
security / Response teams.
Significant spills, smaller spills that L

cannot be immediately contained or
spills that directly contact sensitive
and/or electrical equipment shall be
immediately notified to Klimaoprema-
Sisk
Sufficient volumes of mains water

shall be in position to flush the
temporary circulation loop to pH
neutral

jobsite

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.2

Residual Risk
(H/M/L)
Hazard Rating

awareness training
Retained Chemical in Temporary Contact with personnel H H H Once process is complete, vent lines L
Circulation Loop Adverse effect on environment shall be opened as to allow residual
Further damage to equipment chemicals to drain back to circulation
tank / effluent tank.
Flush temporary circulation loop with

mains water until outgoing water is pH
neutral (pH6-8) –as per approved
Vecom System Method Statement.
Each section/temporary connection of
the system shall be tested
Exposure to Hazardous Substances Adverse effect of health H H H Check relevant MSDS before start L
works
Vecom First-Aider shall be present

during all chemical transfer activities.
First-Aider will be familiar with the
chemicals and the appropriate
response in a contact situation

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.2

Residual Risk
(H/M/L)
Hazard Rating
First-aid responder shall ensure they

are wearing appropriate PPE before
handling the casualty

- Safety shower
- Eye wash station
- First aid kit
Potential exposure to material limited

to uncoupling of hoses.

Exposure to loud noises Adverse effect on personnel hearing H M H All equipment that generate noise in L
excess of 85dB to be enclosed in
sound attenuating materials to ensure
any noises are reduced to below 80dB

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.2

Residual Risk
(H/M/L)
Hazard Rating
Suitable signage advising of loud

equipment to be placed in suitable
locations
Hearing protection (PPE) to be worn

when working adjacent to any loud
equipment.
Risk Assessment Title: Circulation of Chemicals within a Temporary Circulation Loop Date of Revision: April 2023

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.2


(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.3

Hazardous Product Spill Response
Description of Task : Hazardous Product Spill Response
Personnel at Risk : Vecom Operatives / Klimaoprema and Sisk staff / Other Contractors
Residual Risk
(H/M/L)
Hazard Rating
Failed containment resulting in the Personal injury H H H Vecom staff shall be trained and L
escape of Hazardous liquids Adverse effect on environment competent in spill containment
Damage to plant / equipment methods
Communicate the Spill Response

Plan to all relevant parties
Suitable and sufficient quantities of

spill-kit materials shall be readily
available and in appropriate locations
All activities involving hazardous

liquids shall be vigilantly monitored by
Vecom staff, familiar with and trained
in the handling of them.

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.3

Residual Risk
(H/M/L)
Hazard Rating
Vecom operatives shall carry radios in

order to effectively communicate any
spill scenarios with the Vecom
Supervisor
The Vecom Supervisor(s) shall carry a

Klimaoprema-Sisk radio (in addition to
the Vecom radio) in order to
communicate with responsible parties
Spilled liquid shall be contained and

absorbed with spill-kit materials as per
the Spill Response Plan
Exposure to Hazardous Substances Adverse effect to health H H H Check relevant MSDS before start L
works
Vecom staff shall wear suitable PPE

appropriate for handling the chemical
spillage

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.3

Residual Risk
(H/M/L)
Hazard Rating
Exposure to Hazardous Substances Adverse effect to health H H H All spill-kit materials, PPE and other L
(Continued...) materials that have been in contact
with the spilled chemical that cannot
be effectively cleaned shall be treated
as Hazardous W aste and disposed of
as such
A Vecom first-aider, familiar with

chemical injury treatments shall be
available at all times


(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.3

Risk Assessment Title: Hazardous Product Spill Response Date of Revision: 25-04-2023

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.4

Manual Handling
Drafted by :G.Germ s Signature : Assessed By : Signature :
Date of Review : Type of Review (Routine (R) or Incident Based (IB) : Future Review Date : 25-04-2024
Description of Task : Manual Handling
Residual Risk
(H/M/L)
Hazard Rating
Lifting, Pulling, Pushing of Materials & Muscular-skeletal Damage M M M All work that involves lifting, carrying L
Equipment or moving objects shall be assessed
in accordance with the Manual
Handling Operations Regs 1992
All manual handling and lifting

operations shall be planned
beforehand to ensure the load can be
lifted/moved safely
Mechanical aids shall be used where

practicable. i.e. pallet trucks, hoists,
etc.

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.4

Manual Handling
Residual Risk
(H/M/L)
Hazard Rating
Lifting, Pulling, Pushing of Materials & Muscular-skeletal Damage M M M If this is not necessary or practicable, L
Equipment and the load is within your
(Continued...) capabilities, lift the load with your back
straight, knees bent whilst looking
straight forward, taking the strain on
your legs.
If the load is too heavy or awkward,

seek assistance. Do not attempt to lift
it on your own
Vecom staff shall be trained and

competent in lifting, carrying and
kinetic movement techniques to
reduce the risk of injury
Loads that restrict the vision of the

employee shall not be carried
Large awkward loads shall be moved

by a team of similar height and build

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.4

Manual Handling
Residual Risk
(H/M/L)
Hazard Rating
Adequate platforms or rest areas shall

be provided along the route where the
load is being moved to allow the
employee to rest and adjust the load
Stack loads on level surfaces. Avoid

storing equipment/materials below
waist level if possible and practical
Slips, Trips & Falls Muscular-skeletal Damage M M M Ensure that the work area is tidy and L
clear of obstructions/obstacles at all
times
Ensure safe access and egress to the

work area at all times –including
sufficient provision for lighting
Team shall be supervised and given

clear instructions where they cannot
adequately communicate (obscured
vision / high noise levels)
Sharp Edges Cuts M M M Suitable PPE used to protect against L

sharp edges, splinters, etc.

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.4

Manual Handling
Residual Risk
(H/M/L)
Hazard Rating
Trapped Fingers and Hands Cuts, Grazes, Crush Injuries M M M Always try to keep hand away from L
load edges especially in tight areas
and use handles where provided

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.4

Manual Handling
Risk Assessment Title: Manual Handling Date of Revision: 25-04-2023

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.5

Transfer of Chem icals around Site
Description of Task : Transfer of Chemical’s around Site
Personnel at Risk : Vecom Operatives / Klimaoprema/Sisk/BMS staff / Other Contractors / General Public
Residual Risk
(H/M/L)
Hazard Rating
Movement of Hazardous Materials Dropped loads M H H Forklift truck (with suitable lifting L
around Site Spilled product capacity) shall be used for moving
Adverse effect on environment materials around site
Collision with pedestrian Forklift truck driver to be trained,

Collision with another vehicle competent and authorised to operate
Collision with an object equipment
Fumes Speed during transit to be reduced to

Personal injury absolute minimum as to avoid
excessive liquid movement inside the
IBC (shifting centre of gravity).

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.5

Residual Risk
(H/M/L)
Hazard Rating
Movement of Hazardous Materials Dropped loads M H H The route that the forklift truck shall L
around Site Spilled product take between chemical storage areas
(Continued....) Adverse effect on environment shall be pre-planned, agreed and
effectively communicated to all
relevant parties
Collision with pedestrian The route shall be free of obstruction,

Collision with another vehicle surface imperfections, avoid any
Collision with an object unnecessary detours and not require
driving over drain covers
Fumes Vecom shall provide a banksman

Personal injury throughout the operation. Vecom
banksman shall wear PPE as required
for an Emergency Spill Response
Vecom banksman shall carry a radio

and remain in contact with the Vecom
Supervisor
Suitable and sufficient spill materials

shall be available and close-at-hand

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.5

Residual Risk
(H/M/L)
Hazard Rating
All hazardous materials moved shall

be positioned into a secure bunded
location
Exposure to Hazardous Substances Adverse effect to health M H H Check relevant MSDS before start L
works



- Safety shower
Eye wash station

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.5

Residual Risk
(H/M/L)
Hazard Rating



(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.5

Risk Assessment Title: Transfer of Chemical’s around Site Date of Revision: 24-04-2023

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.6

Transfer of Chem icals from one Container to Another Container
Drafted by :G.Germ s Signature : Assessed By : Signature :
Description of Task : Transfer of Chemicals from one Container to Another Container
Residual Risk
(H/M/L)
Hazard Rating
Leaking / Defective pump & hoses Contact with personnel H H H Restrict access to non-essential staff L
Adverse effect on environment in work area using barriers and
Staff to be trained, competent and

authorised to carry out chemical
transfer activities
Supervisor / standby man to over-look

transfer activities from a safe distance
(>5 metres)
All personnel (inc. standby man to

wear PPE as defined in product
COSHH risk assessment

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.6

Residual Risk
(H/M/L)
Hazard Rating
Leaking / Defective pump & hoses Contact with personnel H H H Chemical containers and pump must L
(Continued...) Adverse effect on environment be positioned within bunded area(s)
Further damage to equipment
Spill-kit materials to be ready at hand

and sufficient in quantity to handle the
volume of chemical being transferred
Staff carrying out transfer activities

shall be competent to use spill-kit
materials and are familiar with the
approved spill-response plan
Pump, hoses and gaskets to be

compatible (resistant) with the
chemicals being transferred.
Equipment subject to regular

maintenance and inspections –
including pre-use inspections.
All temporary connections to be

inspected by a second person prior to
chemical transfer

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.6

Residual Risk
(H/M/L)
Hazard Rating
Use only diaphragm pump or drum

pump for chemical transfer. Do not
decant from IBC drain valve
Have IBC of mains water within range

of the suction hose for flushing /
dilution
Adverse Chemical Reaction Excessive temperature reaction M H H W hen transferring one chemical L
- Endo/Exo-thermic product into another, follow guidance
Excessive fume generation
from Vecom Chemist
Transfer speed during blending

activities should be slow and in small
quantities to minimise reaction
Operatives should be vigilant and

aware of unusual increases in
temperature or fume generation
W here a reaction is expected, suitable

PPE shall be worn

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.6

Residual Risk
(H/M/L)
Hazard Rating
Carry out chemical transfer activities

in well-ventilated area.
Over-filling of Recipient Container Contact with personnel H H H W here there is a risk of over-filling L
Adverse effect on environment (i.e. transferring from IBC to small
container) a drum-pump must be used
Ensure transfer hose is >25% smaller

diameter than that of the recipient
containers filling nozzle
Fill no higher than the “high-level”

indicator on the recipient container
Retained Chemical in Transfer Contact with personnel Once transfer is complete, vent lines
Equipment Adverse effect on environment (remove from containers) and allow
Further damage to equipment residual chemical drain into a suitable
waste container
Flush transfer equipment through with

mains water until outgoing water is pH
neutral (pH6-8)

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.6

Residual Risk
(H/M/L)
Hazard Rating
Exposure to Hazardous Substances Adverse effect of health H H H Check relevant MSDS before start L
works



- Safety shower
Eye wash station


(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.6

Residual Risk
(H/M/L)
Hazard Rating


(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.6

Risk Assessment Title: Transfer of Chemicals from IBC to another Container Date of Revision: 24-04-2023

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.7

Use of Com pressed Air
Description of Task : Use of Compressed Air
Personnel at Risk : Vecom Operatives / Other staff
Residual Risk
(H/M/L)
Hazard Rating
Release of Compressed Air Injury to Personnel M H H Compressor shall be well maintained L

Long-Term Hearing Damage and be suitable for use
Adverse effect on Environment
Portable compressors shall have a

drip-tray positioned beneath them to
contain any fuel spillages / drips
Compressed air shall be regulated (at

the tool) to the minimum working
pressure
W hip-checks shall be used on all

connections on air-lines

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.7

Residual Risk
(H/M/L)
Hazard Rating
Release of Compressed Air Injury to Personnel M H H Air-lines shall be run in unobtrusive L

(Continued…) Long-Term Hearing Damage areas and well shielded from traffic.
Adverse effect on Environment W here practical, this shall be over-
head. W here this is not practical,
appropriate barriers and signage shall
be used
All lines shall be fitted with valves (at

the compressor side) to enable
isolation in the event of a failed
connection at the tool end
All staff shall be competent to work

with compressed air and associated
equipment
Suitable noise attenuation shall be put

in place to ensure that the noise
emissions comply with site policies
Appropriate PPE shall be worn when

in the vicinity of the source of
excessive noise

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.7

Residual Risk
(H/M/L)
Hazard Rating
Release of Compressed Air Injury to Personnel M H H Compressed air shall not be used to L
(Continued…) Long-Term Hearing Damage blow down equipment unless the hose
Adverse effect on Environment is fitted with a suitable gun/trigger
attachment –and is regulated to <2
bar.
Equipment and lines shall be

depressurised before breaking any
compressed air connections

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.7

Risk Assessment Title: Use of Compressed Air Date of Revision: 24-04-2023

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.8

Use of Hand Tools
Date of Review : 25-04-2023 Type of Review (Routine (R) or Incident Based (IB): Future Review Date : 25-04-2024
Description of Task : Use of Hand Tools
Residual Risk
(H/M/L)
Hazard Rating
Sprains & Strains Injury to Personnel M M M Always use the correct tool for the L
task in hand.
During repetitive work, share the task

or take regular breaks to do
alternative work
Cutting Tools Injury to Personnel M H H Safety glasses / face shield to be L

Flying Particles worn when using hand tools liable to
create flying particles. Screens must
be used to protect other personnel if
required

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.8

Use of Hand Tools
Residual Risk
(H/M/L)
Hazard Rating
Sharp Tools Injury to Personnel M H H Ensure sharp edges of tools are L

Lacerations protected when stored or carried.
Always keep hands behind the cutting
edge. W ear suitable PPE where
required.(working gloves class D)
Equipment Falling from Height Injury to Personnel M H H All hand tools used at height where L
there is a risk of them falling must be
securely stored with adequate
protection installed to prevent
materials falling
Lanyards to be fastened to tools whilst

working at height
Noise Injury to Personnel H H H Ear protection is to be worn where L

Long-Term Hearing Damage required.
Display signage to warn other

personnel in the vicinity

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.8

Use of Hand Tools
Residual Risk
(H/M/L)
Hazard Rating
Poor Lighting Injury to Personnel M M M W hen using hand tools, ensure there L
is adequate lighting to enable the task
to be done
Injury from Damaged Equipment Only well maintained tools that

conform to European Standards shall
be used
Prior to use, check all tools for wear

and tear. Any worn or damaged
equipment must be returned to the
stores.

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.8

Use of Hand Tools
Risk Assessment Title: Use of Hand Tools Date of Revision: 25-04-2023

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.9

Use of Electrical Equipm ent
Date of Review : Type of Review (Routine (R) or Incident Based (IB): Future Review Date : 25-04-2024
Description of Task : Use of Electrical Equipment
Residual Risk
(H/M/L)
Hazard Rating
Electrocution / Fire Injury to Personnel M H H All portable electrical equipment will L

be identified individually and is subject
Damage to property
to planned maintenance.
Damage to equipment
Operatives will be trained in the

precautions and safe use of portable
electrical equipment.
Equipment supplied to site will be fit

for its purpose with regard to voltage,
power and environmental conditions.
Suitable attention shall be paid to

site electrical requirem ents,
including arrangements for design,
testing and installation of circuits
and their protection by fuses,
residual current devices or similar.

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.9

Residual Risk
(H/M/L)
Hazard Rating
The use of electrical equipment will

be monitored to ensure safe use.
Electrocution / Fire Injury to Personnel Only trained and competent

Damage to property persons shall test, repair and
Damage to equipment maintain portable electrical
equipment.
All equipment found to be

defective will be switched off
and reported immediately.
Visual inspection of equipment will

be carried out before use.
Leads and extension cables

are to be routed so as to
minimise the likelihood of
dam age and trip hazards.

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.9

Risk Assessment Title: Use of Electrical Equipment Date of Revision: 25-04-2023

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.10

Heating of Chem icals (with Steam )
Description of Task : Heating of Chemicals with Steam
Residual Risk
(H/M/L)
Hazard Rating
Auxillary Steam Boiler Contact with personnel H H H Restrict access to non-essential staff L
Adverse effect on environment in work area using barriers and
Aux. steam boiler shall be installed

and commissioned by competent and
authorised person (typically the boiler
supplier)
Steam delivery lines to be insulated

and guarded to avoid direct contact
from other materials / personnel
Diesel tank (supply to boiler) shall be

stored within cordoned area.

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.10

Residual Risk
(H/M/L)
Hazard Rating
Auxillary Steam Boiler Contact with personnel H H H Diesel tank to be bunded L

Adverse effect on environment
Further damage to equipment
Boiler maintenance and inspection

documentation to be readily available
onsite –including any necessary
contact details for the
supplier/manufacturer as necessary
All associated electrical systems to be

tested and inspected as according to
regulations
Safety valve (pressure relief) and aux.

trip equipment to be tested and
approved prior to job commencement.
Heating of Chemicals / Temporary Adverse chemical reaction H H H Confirm temperature limits for L
System Excessive formation of vapour / respective chemical solutions and/or
steam circulation equipment with Vecom
Injury to personnel Chemist prior to job commencement.
Damage to Vecom equipment Check material compatibility of all
Damage to Client system gaskets and connections with regards
to temperature

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.10

Residual Risk
(H/M/L)
Hazard Rating
Auxillary Steam Boiler Contact with personnel H H H Ensure temperature monitoring L

Adverse effect on environment equipment is fully operational and
Further damage to equipment where applicable, calibration
certificates are available
All equipment (including client system)

that will be heated should be
cordoned off and made inaccessible
to non-critical personnel.
Ensure all Vecom staff are aware of
the locations of any equipment/pipes
that may be hot to touch
W here chemical solutions are being

heated by direct steam injection,
ensure that the liquid level is sufficient
to cover the steam pipe outlet. Steam
will condensate directly in the solution

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Ref Num ber: 09.10

Risk Assessment Title: Heating of Chemicals with Steam Date of Revision: 25-04-2023

(LxH) or (HxL) = M
(MxL) or (LxM) = M
m onitoring
Subject
EMERGENCY SPILL RESPONSE PLAN
Validation
Project: BMS
Passivating Purified water system
Project: Passivating pipework

G.Germs D.Przibilla L.Vroon
Document Number P/O Date

2300210 03-05-2023
Mozartlaan 3
3144NA Maassluis
Nederland
Revision history

HSE –Spill Response Plan 0 Eng. 1/19
Page 1 of 14
Emergency Response Plan
Rev: 0
Index
1. BRIEF SCOPE OF WORKS .......................................................................................................................... 3
2. PURPOSE OF EMERGENCY SPILL RESPONSE PLAN .................................................................................... 3
3. ABBREVIATIONS AND DEFINITIONS ......................................................................................................... 3
4. PRECAUTIONS .......................................................................................................................................... 4
4.1 GENERAL PRECAUTIONS............................................................................................................................... 4

4.2 TRANSFER & TRANSPORT PRECAUTIONS ......................................................................................................... 4
5. GENERAL RESPONSE TO SPILL INCIDENTS ................................................................................................ 6
5.1 PROPOSED QUANTITIES OF SPILLAGE MITIGATION MEASURES............................................................................. 7

5.2 SPILLS RESULTING FROM BREAKING A CONNECTION .......................................................................................... 7
5.3 SPILLS WITHIN THE CHEMICAL STORAGE AREA .................................................................................................. 8
5.4 SPILLS WITHIN THE SYSTEM AREA ................................................................................................................... 8
5.5 SPILLS ONTO THE ROAD (DURING TRANSPORT OF CHEMICALS) ............................................................................. 9
6. IMPLEMENTATION OF SPILL RESPONSE PLAN ........................................................................................ 11

6.1 LOCATION OF SPILL KITS............................................................................................................................. 11
6.2 STAFF TRAINING ....................................................................................................................................... 11
7. PROJECT CONTACTS ............................................................................................................................... 12

Appendix I: W orkplace Inspections/toolbox .................................................................................... 13
Page 2 of 14
Rev: 0
1. Brief Scope of W orks
Vecom’s activities on the Klimaoprema/Sisk/BMS site relate to the chemical cleaning of the various
pipework systems.
Large volumes of chemical, water and contaminated rinse water shall be used, generated and stored
onsite during these works.
The pipework shall be disinfected and/or chemically cleaned by creating temporary circulation loops and
pumping the various chemical products into and around the respective system(s).
The chemicals, water and waste shall be stored in a defined and barriered location controlled by Vecom,
strictly off-limits to non-authorized personnel and vehicles.
2. Purpose of Em ergency Spill Response Plan
This document describes the actions to be taken in the event of an accidental spillage of chemical or
other hazardous liquids used in the chemical cleaning activities on the Klimaoprema/Sisk/BMS site.
3. Abbreviations and Definitions
ALARP As Low As Reasonably Practicable

COSHH Control of Substances Hazardous to Health
HSE Health, Safety & Environmental
LMRA Last Minute Risk Assessment
MSDS Material Safety Data sheet
PPE Personal Protective Equipment
PTW Permit to W ork
SMS Safety Management System
SOS Safety Observation Scheme
SSOW Safe System of W ork
CLP Classification, Labelling, Packaging
GHS Globally Harmonised System
IBC Intermediate Bulk Container
Page 3 of 14
Rev: 0
4. Precautions
4.1 General Precautions
In order to minimize the possibilities of accidental spillage of chemical or other hazardous liquids,
the following precautionary measures will be implemented on site as far as possible:
a) The storage area of chemicals and chemical waste shall be located within a bunded, secure
location –away from general pedestrian and vehicular traffic –and off-limits to non-authorized
personnel.
b) Use suitable containers which are resistant to the stored chemicals or the chemical waste.
c) Label the storage containers and the chemical tanks in accordance with CLP regulations and
GHS
d) Bunds of a sufficient volume (>110% of largest container) shall be used to store chemicals
onsite.
e) Provide tightly closed lids as to avoid leakage of chemicals and chemical waste during transit
–or if accidently knocked over
f) Inspect the storage area regularly to detect if any leakage has occurred or if any of the
containers become defective on a regular basis
g) Provide adequate space for safe and easy handling and inspection of the containers
h) Maintain an up-to-date log of all chemicals and chemical waste stored at the site
i) Separate incompatible materials from one another
j) Suitable and sufficient signage shall be displayed around the storage area
k) Keep the ingress to the chemical storage area secure and restrict access. Vecom supervisors
and nominated Klimaoprema/Sisk/BMS site representative(s) as necessary
l) Ensure suitable and sufficient spill materials are readily available in the storage / work area(s)
and that staff are trained to use them effectively
4.2 Transfer & Transport Precautions
In order to minimise the chance of accidental spillage occurring during the transportation of chemicals
around site, some precautionary measures will be implemented:
a) Use a suitably sized container so as to avoid over-filling

b) Use proper, safe and suitably labelled containers
c) Provide a containment structure (bund) which is able to hold any chemicals that are
accidentally spilled.
d) Use pumps to transfer chemicals instead of decanting / pouring
e) Transfer chemicals in and out of the container using a dip-pipe –not a drain valve –wherever
possible.
Page 4 of 14
Rev: 0
f) Use suitable carrying equipment to transfer the chemical and waste containers from one
location to another
a. Forklift truck and other vehicle drivers should be accompanied by a banksman. An
appropriately sized spill-kit should be readily available along the route in order to
contain any accidental spillages. The forklift driver and banksman should be familiar
with the chemicals being transported and be competent to use any spill materials. The
banksman shall be wearing PPE suitable for handling the chemicals being transported
as per MSDS
b. Transfer of hazardous liquids from/to bulk storage tanks to/from road tanker shall be
controlled by competent tanker operator. Suitable spill materials and PPE shall be
worn by all personnel involved.
g) Chemical deliveries and waste collections to/from site shall only be carried out by competent,
licensed and responsible companies/persons.
h) Vecom Project manager or delegate to contact security before the delivery of chemicals to site
Page 5 of 14
Rev: 0
5. General Response to Spill Incidents
The general response to the spill shall be carried out to minimize the amount of hazardous chemicals to the surrounding environment. The location of the spill
is also a consideration. The general responses include the following and they are illustrated in the flowchart below:
Chemical Spillage
Scale of spillage?
Identified
Minor spill Major spill

Catastrophic spill
< 5 litres – litres
> 1,000 litres
Retrieve spill –kit

Inform Vecom Inform Vecom
materials and
Supervisor Supervisor
appropriate PPE
Vecom Supervisor to inform Vecom Supervisor to inform
Klimaoprema and Vecom Klimaoprema, emergency
nominated first aider services and Vecom nominated
first aider
Retrieve spill –kit Retrieve spill –kit
Isolate the source of
materials and materials and
the leak if possible
appropriate PPE appropriate PPE
Contain and clean the First Aider attends scene with First Aider attends scene with
Isolate the source of Isolate the source of
spillage areas using appropriate PPE & first aid appropriate PPE & first aid
the leak if possible the leak if possible
driptrays / spill kit materials materials
Cover drains and use

Dispose of Contain and clean the
spill kit materials to
contaminated items spillage areas using
direct spill to least
(hazardous waste) driptrays / spill kit
critical / sensitive areas
NO NO
Dispose of Dispose of
contaminated items contaminated items
(hazardous waste) (hazardous waste)
Safety & Environmental

representative observe the site Spill contained and Spill contained and
condition and proposes cleand –up? cleand –up?
preventive measures
YES YES
Page 6 of 14
Rev: 0
5.1 Proposed Quantities of Spillage Mitigation Measures
A sufficient quantity of spill-kit material shall be made available in order to carry out effective mitigation
measures as and when required. A 1,100 litre spill-kit shall be positioned adjacent to the IBC storage
area. The proposed quantities are sufficient for containing 110% of the largest portable chemical storage
container – and thus are vulnerable to causing environmental damage during transportation. All other
containers are considered “fixed” and will not be moved during the project. These container s are fully
bunded / contained. Spill kit materials shall be replaced immediately after use.
Smaller (50lt) spill-kits shall be positioned strategically around the temporary circulation loop to be
readily available in the instance of any leaks/drips, etc. during the chemical cleaning activities.
Spill-kit material and a drip-tray will be in position whenever a temporary connection is broken.
Two disposable chemical resistant suits (Microchem 3000 –resistant to all chemicals specified on this
project), box of disposable vinyl gloves, two pairs of nitrile gloves, two pairs of safety goggles and two
pairs of chemical resistant wellington boots shall be placed inside each 1,100 litre spill-kit.
5.2 Spills Resulting from Breaking a Connection
All temporary connections shall be flanged and left intact wherever possible. W here this is not possible
(completion of a temporary system, defective seal resulting in a leak, etc.), the breaking of connections
must follow this process:
1) Isolate valves at either side of the flange connection.

2) Position drip-tray beneath flange connection
3) Determine volume of chemical / water that could potentially be trapped in the line between the
two isolated flanges.
4) Provide sufficient spill material for this volume –and have it close at hand.
5) Ensure the operative breaking the flange is wearing suitable PPE as defined in the MSDS for
the activity.
6) Loosen the bolts around the flange just enough to allow any trapped liquids to weep into the
drip-tray in a slow and controlled manner
7) W hen there is no evidence of liquids draining, loosen the bolts further and break the connection.
8) Drain any further liquids into the drip-tray or container and ensure that the lines are completely
empty.
Page 7 of 14
Rev: 0
5.3 Spills within the Chem ical Storage Area
IBC’s of concentrate chemical (40% hydrofluoric acid, 30 -35% hydrogen peroxide, 25% Ammonia, etc.)
shall be kept on dedicated IBC bunds at all times. These chemicals are primarily used for dosing/spiking
the circulating solution and as such, transportation of these products should be kept to a minimum.
Transfer of chemicals from these containers shall ALW AYS be done using a dip-pipe and pump (<2 bar
pressure). Under no circumstances shall they be decanted from the drain valve. The drain valve shall
be locked closed and a blind/cap fitted to the outlet.
Transfer of concentrate chemicals shall be tightly controlled and supervised. A stand-by man, dressed
in full, appropriate PPE shall overlook the operation from a safe distance (typically 5 metres) and be
ready to administer assistance as and when necessary. This includes first-aid as well as spill response.
Spill materials shall be close at hand and ready for deployment.
5.4 Spills within the System Area

All temporary connections are subject to multiple inspections and leak tests prior the addition of
chemicals to the system. At key locations around the temporary circulation loop, 50 litre spill kits and
drip-trays shall be positioned. The circulation loop and temporary connections are constantly monitored
by Vecom staff during the process. In the instance of a leak or failed connection, the operative who
discovered it shall notify the pump operator immediately by radio to stop the pump.
Depending on the severity of the leak, the operative shall take one of two courses of action:
1. Small Leak (drip or weeping flange, etc.)

a) Inform the pump operator of the small leak and proposed plan of action
b) Allow the system to drain back to the circulation tank. Open vents if necessary to ensure
there is no chemical trapped in the line.
c) Once the pump operator confirms that the chemical has been recovered, isolate the valves
either side of the leak and follow the procedure defined in section 6.2 for breaking flanged
connections.
d) If any surrounding surfaces / materials / equipment has been in contact with the chemical,
notify Klimaoprema/Sisk site immediately.
2. Significant Leak (completely failed connection or ruptured hose, etc.)

a) Inform the pump operator of the significant leak.
b) Pump operator shall notify all workers in the area of the leak. All non-Vecom staff evacuate
the area.
c) Pump operator notifies Klimaoprema/Sisk site of the incident.
d) Isolate the system up-stream of the failed connection. Allow the down-stream system to
drain back to the circulation tank and/or waste storage tank
e) Vecom staff attend the scene with additional spill materials, contain and clean up the
spillage.
Page 8 of 14
Rev: 0
f) Assess the location of the incident and determine how much chemical has been lost and
any possible routes that the spillage could have escaped containment (through floor/wall
penetrations, down adjoining pipework or steelwork, into any electrical equipment, etc.)
5.5 Spills onto the Road (during transport of chem icals)

Transportation of chemicals around site (unloading delivery vehicles or relocating to a different location
shall be carried out using a forklift truck. The forklift truck driver shall be trained, competent and
authorised to operate the vehicle. The forklift truck driver shall have read and signed on to the task
specific risk assessment and attended the Dangerous Goods TBT carried out at the start of the activity.
The vehicle shall travel no faster than a walking-pace from its start-point until it reaches the final
destination.
The forklift truck driver shall be familiar with the peculiarities associated with transporting liquid loads
(shifting centre-of-gravity) and take any necessary precautions to minimise the effects.
A banksman provided by Vecom shall accompany the forklift truck, dressed in appropriate PPE as
defined in the MSDS. The banksman shall ensure that there are no obstructions en-route and guide the
driver away from / around potholes, etc.
A 1,100 litre spill kit shall be close at hand at all times.
There are three possible scenarios that could result in leak from an IBC.
1. Defective drain connection:
This is the most common issue with IBC’s and results from an ineffective seal on the butterfly
valve. This type of leak is usually nothing more than a drip and is easily contained using a
suitable screw-cap on the outlet pipe. If this is ineffective, the recessed area around the drain
connection should be packed full of spill-kit material and the IBC taken directly to the nearest
available IBC bund.
2. Defective lid or vent connection:

Although more unusual, if the liquids inside the IBC are disturbed sufficiently (by driving over a
large bump for example), the resulting “wave” in the IBC can escape through the lid or vent
connection(s) on top of the IBC.
Before transporting an IBC, ensure that all the top connections have a lid/cap and are securely
fastened.
If the lid / vent does leak, stop the forklift truck and put down the IBC. The forklift truck should
reverse away from the load, allowing full access to the IBC for the Vecom operative.
Most liquids spilled in this manner will gather in the depression around the lid. Apply spill-kit
material to this area and contain/absorb the chemical. Remove the lid and wipe the internal
surfaces before reattaching to prevent any further chemical from dripping out during the
remainder of the journey. Thoroughly wipe all surfaces of the IBC with spill-kit material to ensure
that no chemical has run down the IBC walls and is left on.
Page 9 of 14
Rev: 0
3. Puncture to the IBC wall or dropped load (IBC on its side):

By far the most serious of the three scenarios is when the integrity of the IBC is compromised
and cannot be remedied in-situ.
This type of incident will result in a large proportion, if not all, of the IBC contents being spilled.
Upon occurrence, the forklift driver should back his vehicle away from the load and allow full
access to the Vecom employee(s).
The Vecom employee should radio his Supervisor and request immediate assistance, specifying
his location and the nature of the chemical that has been spilled.
The spill should be immediately contained using spill-kit material and the affected area cordoned
off. Priority should be given to sealing any drains – or gulley/routes that lead directly into the
sea.
Once contained, the spill should be completely cleaned up as quickly and as safely as possible.
Klimaoprema/Sisk site should be notified immediately.
Page 10 of 14
Rev: 0
6. Im plem entation of Spill Response Plan
6.1 Location of Spill Kits

Spill kits and absorbent materials shall be kept in suitable storage containers, always accessible by on-
duty staff. The containers shall be located in all areas in which chemicals are being stored. Smaller
containers shall be placed in temporary locations during chemical circulation and returned to the Vecom
storage container when not required.
6.2 Staff Training

All Vecom staff have been briefed and formally trained on spill prevention and emergency procedures.
The HSE Manager, or other competent persons, shall conduct task specific toolbox talks to the site
workers on a daily basis.
Vecom Supervisors shall be responsible for regularly checking, amongst other things, their spill-kit
materials and chemical storage facilities. This will be documented on a daily work-place inspection
sheet.
W orkplace Inspection Sheets and toolbox talks shall be submitted to the Vecom Project Manager and
Klimaoprema site safety department on a regular basis.
Page 11 of 14
Rev: 0
7. Project Contacts
Vecom
Nam e Role Contact Num ber
Gert Germs Site Supervisor +31(0) 6 10 90 93 64
Lucas Vroon Project Manager /Chemical +31(0) 6 22 43 74 55

Engineer
Klim aoprem a
Nam e Role Contact Num ber
Karl Heinz Kwakman H&S Manager Klimaoprema +31(0) 6 13 00 34 02

Package Manager Sisk TBD
Emergency number Emergency +31(0) 6 57 54 96 63
Page 12 of 14
Rev: 0
Appendix I: W orkplace Inspections/toolbox
Subject: W orkplace Inspection Sheet Revision: 1 Number: VN-2-13.1
Date: Sheet 13 of 14
No. Inspection location: Date: Findings:
1 Is the workplace clean and tidy?
2 Are there any obstacles which could result in slips, trips, falls?
If yes, why have they not been removed?
3 Are all hoses, leads, equipment securely fastened out of

pedestrian routes and where necessary, made visible?
4 Are appropriate signage and barriers in place and in good

condition?
5 Is the workplace free of all non-Vecom equipment / materials?
6 Are escape routes free from obstacles?
If no, why have they not been removed?
7 Can fire-extinguishing resources be quickly deployed?

• Can they be reached quickly and appropriately?
Have they been certified recently?
8 Is work set-up in accordance with the work permit?
9 Is the required protection equipment available?

• PPE (Personal Protection Equipment)
• Absorbent Spill Materials
• Drip trays / Bunds
• First aid material
Safety Shower (available and working?)

10 Are chemicals being stored in the correct manner?
• Are acids and alkaline solutions being kept separate?
• Are oxidisers being kept separate –and in a suitable
location?
Are all chemicals suitably bunded?

11 Establish adequate communication channels between Vecom
and Klimaoprema/Sisk
Page 13 of 14
Rev: 0
Page 14 of 14
Pre commissioning passivation of pipework
W aste water treatment and storage
Project : BMS Leiden
Subject
05: W aste water treatm ent, storage and disposal
Validation
BMS-Klim aoprem a
Project: Purified water system
Project: Pre commissioning passivation of pipework
G.Germs
Job Number P/O Date

2300210

Mozartlaan 3
3144NA Maassluis
Nederland
Revision history

List - ENG 0 NL. 1/2
1
Introduction:
During a system passivation, different types of waste water will be released during the
different stages of the Passivation.
To be able to collect this waste water, one (1) 1m3 waste water tank (IBC) will be placed
close to the system to be passivated.
During the passivation of the system, 3 different types of waste water will be released into
the waste water tank.
Overview waste water types:
2.1 First pre-flush water
This flushing water (which does not contain any chemicals) will be released during the pre-
flush of the system and contains mainly loose dirt like sand and possible iron oxides.
This water will be released into the waste water IBC and will be drained into the sewage
system
2.2 Passivation phase waste water
After the passivation phase of the cleaning is finished, the passivation waste water will be
drained into the waste water IBC as much as possible.
2.3 Second phase flush water
After the passivation phase waste water has been drained, the system will be flushed to
remove any remaining passivation fluid untill the water is within set limits.
Approx. 2-3 volumes of water will be needed to perform this flush. This second phase flush
water will be added to the passivation waste water which is already in the waste water tanks.
2
Please find below an overview of the non-neutralised waste water as it will be drained from
the system.
Tabel 1: Pre-flush water

Parameter Content
pH value 6,0 –8,0

COD Value < 20 mg/l O2
Temperature Ambient
Suspended solids Present
Tabel 2: Passivation waste water

Parameter Content
pH value 0-2
Chlorine < 10 mg/l
Temperature Ambient
Suspended solids Non present
Tabel 3: Second phase flush water

Parameter Content
pH value 6,0 –8,0

Chlorine < 5 mg/l
Temperature Ambient
Suspended solids Non present
3.1 Neutralisation of the waste water
Not applicable, as waste is transported from site to an accredited waste treatment company
3
4. W aste water tank inform ation
Vecom will supply one (1) 1m3 IBC to collect all the passivating waste water which will be
released during the chemical cleaning.
The exact dimensions of the effluent tank supplied are:
- W aste water tank 1m 3 : length 1 m eter / width 1 m eter/ Height 1 m eter Footprint
1000 kg/m 2
4
PRS International and Vecom Klimaoprema Chemical Cleaning TP 820
Limit status checklist Purified water
Limit/Valve
P&ID No. Valve TAG/NUM Position Checked? (Encircle)
No.
1 Inlet from Vecom pump OPEN YES / NO

LEI-310-820-41-001
2 Outlet. Return to Vecom pump OPEN YES / NO
LEI-310-820-41-003 4 MV-001 CLOSED YES / NO
Check performed by (date & sign):
Witnessed by (date & sign):
D. TP 820 Limit check list Page 1 of 1

Note: Item 8. will only be used for the DN150 system
8.
Detail A: 3. PG
4.
Hydrostatic
Test pump
System in DN150 for heating & chilled
System in DN50 for all other systems 2.
Chemical injection line
1.
7.
5.
Water 1,5 m³/hr

Chemical cleaning Steam injection line
To waste water tank 6.
Position Equipment 380V / 32Amp
Mixing tank
1. Dieseloil
2. Return manifold
3.
4.
Silencer
PRS Hydro test set-up
VECOM B.V.
5. Circulation pump 0.0 1.0 Detail A
6. Aux. boiler 11-07-23 31-07-23
M.Hans M.Hans
Circulation Skid set-up
7. Chemical injection pump M.Hans M.Hans
G. Germs G. Germs
8. Filters for final flush (only for DN150) G. Germs G. Germs
032-P23 032-P23_Circulation_set-up 1/1
Outlet,
50
see
detail A
50
2. 003
A
1. 003
DV-xxx
905
Inlet, see
detail A
NOTES:
1. PIPE WORKTO BE CUTAT63+/-3 DEGREE ANGLE.
2. GREEN LIGHTATCONSUMPTION PANEL INDICATES PUW IS

AVAILABLE. RED LIGHTATCONSUMPTION PANEL INDICATES PUW IS
NOTAVAILABLE.
NOTICE
3. CONSUMPTION/SAMPLING PANEL SHALL INCLUDE THE CAPABILITY THE DRAWINGS AND OTHER INFORMATION INCLUDED ON THIS
TO TESTTHE LAMPS USING A "LAMP TEST" PUSH BUTTON. SHEET ARE THE PROPERTY OF BRISTOL MYERS SQUIBB,
TECHNICAL OPERATIONS DIVISIONS, FACILITIES ENGINEERING
4. HIGH POINTVENTTO BE A MINIMUM DISTANCE FROM THE PUW AND IS LOANED TO YOU SUBJECT TO RETURN UPON DEMAND
STORAGE TANK RETURN ATTHE HIGHESTPOINT. AND UPON THE EXPRESS CONDITION THAT ALL CONFIDENTIAL
SUBJECT MATTER BE KEPT STRICTLYCONFIDENTIAL AND SHALL
NOT BE USED IN ANY WAYDETRIMENTAL TO THE INTEREST OF
BRISTOL MYERS SQUIBB, TECHNICAL OPERATIONS DIVISION,
FACILITIES ENGINEERING AND FOR NO OTHER PURPOSE OTHER
THAN THIS LOAN.
GENERAL NOTES
Vent valve
A. FOR GENERAL NOTES, SYMBOLOGYAND NUMBERING CONVENTION,
SEE LEAD SHEETS.
B. ALL AUTOMATED VALVES ARE FAIL CLOSED UNLESS OTHERWISE
NOTED.
C. SINGLE USE COMPONENTS SETUP MAYCHANGE BASED UPON
PRODUCTAND PROCESS STEP.
3.
D. THE SYSTEM NUMBER FOR ALL INSTRUMENTS AND VALVES IS THE
P&ID NUMBER UNLESS SHOWN OTHERWISE.
E. ALL EQUIPMENTAND INSTRUMENTTAGS ON DRAWING ARE
ABRIDGED. FULL TAG IS PREFIXED WITH SITE, BUILDING AND
A B F.
SYSTEM NUMBERS. EG. DRAWING TAG: TI-001, FULL TAG:
LEI-310-101-TI-001.
REFER TO LEAD SHEETS LEI-310-01-001/002/003/004/005, FOR
MV-003
INSTRUMENT, CONTROL SYSTEM SIGNAL AND CONTROL VALVE
25-SS5-LEI-310-820-015-PUW-PP SLOPE SLOPE HPV NOTE 4 DETAILS.
SLOPE
G. REFER TO LEAD SHEETS LEI-310-01-001/002/003/004/005, FOR
DETAILS OF SIGNALS ASSOCIATED WITH MOTOR VARIABLE SPEED
DRIVES.
APPROVED BY
DRAFTER MM/DD/YYYY
PROJECT MANAGER MM/DD/YYYY
ENGINEERING MANAGER MM/DD/YYYY
QUALITY ASSURANCE MM/DD/YYYY
KEYPLAN
NOORDEN
P P P P P
P P P P P
GREEN RED
GREEN RED MV-001 MV-002
4. 5.
E
XL XL
D
P
P
XL XL
A
F
P
020 021
010 011
PUW PUW NOT
B
C
PUW PUW NOT AVAILABLE AVAILABLE
AVAILABLE AVAILABLE FO FO
P
3 mm 3 mm
001
P
P
002
P
20-SS5-LEI-310-820-016-PUW-NI
20-SS5-LEI-310-820-017-PUW-NI
ETHERNET
P
ETHERNET
P
P
HS
P
HS
XA
XA
021
011 LAMP TEST
P
LAMP TEST NOTE 1 NOTE 1 XA
P
P
XA
P
020
010 JANITOR CLOSETSINK FITROOM SINK
CONSUMPTION/SAMPLE PANEL
CONSUMPTION/SAMPLE PANEL 310-10-514 310-10-513
NOTE 2,3
NOTE 2,3 1 14.FEB.23 RE-ISSUE FOR CONSTRUCTION JS
P P P P P
P P P P P 0 16.FEB.22 ISSUE FOR CONSTRUCTION TS
820 981 50-LEI-SS1-310-981-007-PD-NI 820 981 50-LEI-SS1-310-981-008-PD-NI
C 13.DEC.21 ISSUE FOR TENDER TS
B 28.SEP.21 ISSUE FOR DESIGN TS
A 16.JUN.21 ISSUE FOR COMMENT JH
REV DATE DESCRIPTION BY
TITLE: PIPING AND INSTRUMENTATION DIAGRAM

FOR PURIFIED WATER DISTRIBUTION
PROJECT: EU CELL THERAPY FACILITY

PHASE: CONSTRUCTION
LOCATION: LEIDEN BIO SCIENCE PARK
NETHERLANDS
CAR#: - SHEET #:
DATE: - 1 0F 1
SCALE: NTS DRAWING #:
PRJ MGR: EB
DESIGNER: JH
LEI-310-820-41-003
VENDOR NAME: DPS ENGINEERING
AUTHOR: SJ
DISCIPLINE: PR
SYSTEM: PROCESS
SYSTEM #: -
EQUIPMENT: N/A
CSI CATEGORY: -
OBJECT NAME: -
DOCUMENT TYPE: -
DEPARTMENT: -

820-Puri Voda

Uploaded by

Document Information

Original Description:

Original Title

Copyright

Available Formats

Share this document

Share or Embed Document

Sharing Options

Did you find this document useful?

Is this content inappropriate?

Copyright:

Available Formats

820-Puri Voda

Uploaded by

Copyright:

Available Formats

Contractor: Client:

KLIMAOPREMA d.d. Bristol Myers Squibb, Bio Science

PLAN FOR HYDROTEST AND FLUSHING OF THE SYSTEM

1. VECOM hydrotest plan:

Author Nick Berens

Checked by: Signature:

PRS International | Industrieweg 10 | 7761 PV Schoonebeek | The Netherlands a VolkerWessels company

a VolkerWessels company 1|P a g e

2. Responsibilities and authorities

• The commitment of qualified personnel

• Obtaining the necessary permits

• Working in accordance to the project / job specific work instruction

a VolkerWessels company 2|P a g e

a VolkerWessels company 3|P a g e

The following safety rules shall be adhered to at all times:

a VolkerWessels company 4|P a g e

Slips, trips and falls

Hazard Suggested Action

Clean spills up immediately. If a liquid is greasy ensure a

Position equipment to avoid cables crossing pedestrian

Choose suitable footwear, particularly with the correct type

Slopes Improve visibility, provide hand rails, use floor markings.

Ensure mats are securely fixed and do not have curling

Poor lighting Improve lighting levels and placement of light fittings.

a VolkerWessels company 5|P a g e

Manual handling and lifting

Many injuries are caused by poor lifting practices.

Back injuries can be eliminated by following these simple rules:

To make a manual lift from floor level, you should:

a VolkerWessels company 6|P a g e

Personnel protect equipment

The minimum standard of protective clothing provided and worn includes:

• Footwear: safety boots/shoes to the newest standard.

a VolkerWessels company 7|P a g e

Hoses (hydraulic oil and high-pressure gas) shall be routed so as to:

a VolkerWessels company 8|P a g e

Actions in the event of an emergency

a VolkerWessels company 9|P a g e

Site induction and permit to work

Pre-job safety meeting

• A review of the job procedure / work scope and timings.

• Risks and hazards mentioned in the Task Risk Analysis

Points that need to be discussed in meeting:

• Status of the work during the previous shift

All above points need to be recorded on a PRS shift handover form

Post-job safety meeting

• Work scope summary.

Establishment of job pressure

Rig-up / Rig-down (General)

System over pressurization protection

Hose over pessurization protection

6. Work method statement

Pre-notification provided by customer

Pressure measurement requirement

Filling of system (performed by Vecom)

TEST PRESSURE IN BAR(G)

Start 50% 60% 70% 80% 90% 100%

Item Deviation % Exactitude Range

1. Chart recorder information showing temperature sequence

8. Disassembly / Demobilization of equipment

Hydrostatic pressure testing Job Number: 032-P23

ACTIVITY: Hydrostatic testing ■ NEW TRA VALIDATED BY: S. Valkem a