MTR 4130 75K

AISI 4130 API 6A 75K MINIMUM -50°F

N.A.C.E. (H2S) SERVICE, API 6A
PSL 1, 2, 3

1. Scope: Casing bowls / spools, tubing heads / spools, adapter & loose flanges,
O.E.C’s, tubing and casing hangers, secondary and primary seals, from forgings, bar –
stock, mill – shapes, and rings

2. Responsibility:
• Purchasing personnel – To ensure conformity to this specification while
purchasing.
• Receiving – Shall be done by QA/QC or delegate to ensure that purchased
materials conform to the requirements of this specification.
• GNWF/Material Suppliers – Ensure referenced standards and specifications are
met.

3. References:
3.1 API 6A
3.2 N.A.C.E. MR01-75 / I.S.O. 15156
3.3 A.S.M. VOLUME 4
3.4 Great North Wellhead & Frac General Material Specification (GNWF MS-01)

4. Chemical Requirements
4.1 Material chemical composition shall be determined on a heat basis (or a re–melt
ingot basis for re – melt grade materials) in accordance with nationally/internationally
recognized standards specified by the manufacturer.
4.2 Element limits are expressed in percentage mass fraction, and shall conform to the
limits below for API 6A, PSL 1 - 3:

ELEMENT MIN.% MAX.%

CARBON (C) 0.28 0.33
SILICON (Si) 0.15 0.35
MANGANESE (Mn) 0.4 0.6
PHOSPHORUS (P) PSL 1-2 0 0.04
PHOPHORUS (P) PSL 3 0 0.025
SULFUR (S) PSL 1-2 0 0.04
SULFUR (S) PSL 3 0 0.025
NICKEL (Ni) 0 0.50
CHROMIUM (Cr) 0.8 1.1
COPPER (Cu) 0 0.35
MOLYBDENUM (Mo) 0.15 0.25
ALUMINUM (Al) 0 0.050
VANADIUM (V) 0 0.035
*The total sum of residual elements (Ni, Cu, V) shall not exceed 1.00%.

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MTR 413075K-14
 MTR 4130 75K
AISI 4130 API 6A 75K MINIMUM -50°F
N.A.C.E. (H2S) SERVICE, API 6A
PSL 1, 2, 3

5. See GNWF MS-01 for the following:

• General Material Qualification Testing
• Processing
• General Heat Treatment Requirements
• Qualification Test Coupons(QTC’s)
• Heat Treatment Equipment Qualification

6. Grade Specific Material Qualification Testing

MINIMUM TENSILE TEST REQUIREMENTS

0.2” MIN. YIELD MIN. TENSILE

ELONGATION IN 50MM (2") REDUCTION IN AREA
STRENGTH (MPA / STRENGTH (MPA /
MIN. % MIN. %
PSI) PSI)
517 (75 000) 655 (95 000) 17 35

TRANSVERSE TEST DIRECTION VALUES “L” TEMPERATURE RATED

API TEST MIN. AVERAGE

TEMPERATURE TEMPERATURE VALUE JOULES
CLASSIFICATION °C (°F) (FT./LBS.) PSL 1-4

L -46 (-50) 20 (15)

K -60 (-75) 20 15)

LONGITUDINAL TEST DIRECTION VALUES

API TEST MIN. AVERAGE

TEMPERATURE TEMPERATURE VALUE JOULES
CLASSIFICATION °C (°F) (FT./LBS.) PSL 1-4

L -46 (-50) 27 (20)

K -60 (-75) 27 (20)

HARDNESS REQUIREMENTS

STANDARD BRINELL SCALE "B"

HARDNESS RANGE 197-237 HBW

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MTR 413075K-14
 MTR 4130 75K
AISI 4130 API 6A 75K MINIMUM -50°F
N.A.C.E. (H2S) SERVICE, API 6A
PSL 1, 2, 3

7. Grade Specific Heat Treatment Procedure

PROCESS TEMPERATURE RANGE TIME @ TEMPERATURE COOLING / MEDIUM

INERT GAS OR AIR COOL IN

NORMALIZING 1675°F +/-50°F (913°C +/- 1/2 HOUR PER INCH OF STILL AIR, MINIMUM 1 HOUR
(OPTIONAL) 30°C) THICKNESS COOL TO BELOW 400°F
(204°C)

1/2 HOUR PER INCH OF

1550°F - 1625°F (843°C -
AUSTENIZE THICKNESS, MINIMUM 1 WATER OR POLYMER,
885°C)
HOUR

Water Quenching – The temperature of the water or *other quenching media used to
approximate the cooling rate of water, shall not exceed 38°C (100°F) at the start of the
QUENCH*
quench. For bath - type quenching, the temperature of the water of quench media shall
not exceed 49°C (120°F) at the completion of the quench.

1 HOUR PER INCH OF

THICKNESS. BEYOND INERT GAS OR AIR COOL IN
1175°F - 1300°F (635°C -
TEMPERING 8” *T, ½ HOUR PER STILL AIR TO BELOW 400°F
704°C)
INCH MAY BE (204°C)
ACCEPTABLE.

8. Certification
8.1 Off – shore vendors shall submit a Material Test Report (MTR) in the format
provided, to the customer representative or its agent prior to, and with the material
shipment.
8.2 Domestic vendors shall submit a Material Test Report (MTR) as directed by the
purchaser; otherwise, it shall be shipped with the material.

Revision Date Description Of Changes Reviewed & Approved By

October 28, • REMOVED GENERAL MATERIAL SPECIFICATIONS AS THESE ARE

13 HOLLY MCOUAT
2019 ADDRESSED IN GNWF MS-01

December 1, • Clerical Change - PAR 038 – update quenching media temperature to

14 Holly McOuat
2021 correct conversions

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MTR 413075K-14