Reg. No.

BANNARI AMMAN INSTITUTE OF TECHNOLOGT

Afliated to Anna University, Chennai)
(An Autonomous Institution
SATHYAMANGALAM -638 401

Slay Ahead PERIODICAL TEST I| - SEPTEMBER 2023

VII Semester

18EI702 & ANALYTICAL INSTRUMENTS

Degree &Branch: B.E. & EI
Time: 1:30 Hrs. Maximum: 50 Marks

Instructions:
1. Students shoukd not markwrite anything on tho Question Papar other than the register number.,
2. SectionA of the Question Paper contains questions for 15 Marks. Section Band Ccontains questlions for 30 Marks each.
3. 20
Student can attempt answering any two out of three subsecions in each sedtion. Maxdmum mark is limited to 10 in section Aand
in sedionsB&c.
Q.No. Questions
SECTION A MAXIMUM: 10 MARKS
COURSE OUTCOME 3
The single beam analyzer in figure A1.1 is used to analyze the beverages in food processing industries
jquantitatively and qualitatively.
Sompo Sample

Waveb Sampio

D
Retorenr
Figure A1.1. Single Beam Analyzer

Indicate the suitable component A, B. Cand Dto be placed in figure A1.1 for proper analysis of
the ambient air.
(2 Marks- [UIC,2])
Reconstruct the figure A1.1 to analyze the ambient air using two beans of lR rays in industries
(3 Marks- [An/C,2])
A2 The chemiluninescent analyzer in figure A2.1 is used for estimating the nitrogen dioxide in the flue gas
emitted from the industries. There are also various analyzers like NDIR and coulometric analyzers
available for estimating the sulphur and carbon monoxide respectively.

Page 1 of 9
 Fowmeter

Opticalfitter

JRead ou
igh voitan
PowersuppN
OFlovw meter

Air sample
A2.1. Chemiluminescent Analyzer
Fgure
Restructure the above fiqure A2.1 as suitable forrestimating the carbon monoxide in the samole
Nitrogen Dioxide
gas instead of 5 Marks- [IC 2
of components for detecting smoke emitting t
schematic arrangement
A3 Figure A3 1 shows theindustries
chimneys in the paper
through
POSITIVE()

sOURCE TO TRIGGER CIRcUIT

Capacitor

cOLLECTORA

CHAMBER coVER

NEGATVE (4
Fiqure A3.1 Smoke Detector
smoke using an ionization smoke detector by
(0 Draw a process flow structure for detecting the
referring the cornponents in figure A3.1 3Marks- [Ap/C 21)
is replaced by inductor.
Indicate the change that happens in figure A3.1 if the capacitor (2 Marks-[UIC 2)
MAXIMUM: 20 MARKS
SECTION A COURSE OUTCOME 4
solution. The chan
is used to measure the oH of chemical
h nydrogen electrode shown in figure B1.1 on its nature
in figure B1.2 shows the pH scale for the categorization of items based

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 Coppe Pure anxd dy ll;
wite
Glass jacket
Vessel
-Mercury
Platinum
win
-Platinised
Seluion af -L Po olatinum foil
l'ions (M) P

Figure B1.1.Electrode

Figure B1.2 pH Scale

replaced by sllver- silver chioride in figure
Draw the structure of electrode, If standard hydrogen ls
B1.1 for measuring pH of sample ions.
(4 Marks-[Ap/C. 2) |
the reaction can be obtained as,
If the electrode in figure B1.1 acts as anode,
H(g)2H* +2e
B1.1 If the electrode acts as cathode.
Predict the chemical reaction (Equation) happens in figure -[UIC,2)
its nature by relerring figur
Real the items with the respective pH range based on 3Marks- An/C,2])
aturo pH Range
Item 8-9

CAUSTIG

A2 A3
A1

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 Acid

DISTILLO

B3
B2
a1
Base

C3

given sample. Glass electrode is

technique for mneasuring pHH value in a detector type mneter.
pH meter is a Figure
The nu Itype this B2.1 shows the
matic of null
B2 technique.
troduced
Evacualed
glass tube

Grid

-IB
Baltery
D

TesLEN
SolutionRR

meter given sample

B2.1. Null Detector Type pH
for proper analysis of pH5inMarks-
AB.C. Dand E
in figure B2.1 (UIC,2))
ldentity the missing parts type techniques
above figure B2.1 to analyze p of solution using direct reading
Reconstructt the reliminating Ihe suitable
instrurnents as given below.
by n n oter
2. Anmeter
Voltmeter [UIC, 2))
4. Potentiometer (3 Marks-

Page 4 of 9
 instruments.
(u)A$sereason:lion Potentio
inrimeler is aspeclal device to
To
detector
bo introduced in null type tions for assertion.
Assertion and rindication during balanced bridge condtiexplanations for assertion
ASertion and roason both areot Reason is correct exp t
d) Aen is correct but the reason is wrong staterment correct
Ion and reason both are nol
The silica correct. (2 Marks- (An/C,21)
content
performance nftheof the liauid in the process creasing the
process The procedural prndustrieIs is necessary to be analyzed for
Dcess is shown in figure B3,1
Constant Head Tank
B
Amplifer
H Indicator

Drain
Figure B3.1. Silica Analyzer
Indicate the proper element to be
introduced for A, B, Cand D in fiqure B3,1.
Reconstruct the above figure B3.1, by rearranging the (4 Marks- [UIC,2)
amount of oxygen in the solution components as suitable for analyzing the
(i Assertion The eficiency of the sodium analyzer in fiqure B3.1 is improved by (4 Marks-[UIC.2)
Cleaning. standardization and
Reason: To get the correct value,
Accuracy, and long life for the electrodes
e) Assertion reason both are correct Reason is
) Assertion rect hutnare correct Reason is not
correct explanations for assertion
g) Assertion is correc correct explanations for assertion.
s wrong statement.
n) Assertion and reason both not correct
(2 Marks- (UIC 21)
SECTION C COURSE OUTCOME 5
The below figure C1.1 shows the
MAXIMUM: 20 MARKS
process low of gamma camera for capturing image using radio waves
for medical applications

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 Defector Cystal
PMT Amy
oroan wilh)
radio active
Collimator
emission

Posibon Logic
Circuit

Computer and
ad ou

Figure C1.1Gamma Camera

fthe gamma camera in figure C1.1 is replaced bythe x-ray spectrometer then represent the flow
process for capturing medical imaging for gnosis.

HH
Read out
device

(5 Marks- Iu/C.21)
(W) Reconstructthe block obBained in Question () as suitable for detecting radiation by non-dispersive
x ray absorption meter.
(5 Marks- (UIC,21)
c2 NMR spectroscopy is the use of NMR Phenomena to study the physical, chemical and biological
properties of matter as shown in figure C2.1.

Page 6 of 9
 9of
Page7
atof
mass relativedetermining or molecules. nd
alyzing
ie
sonal
treaueny
to E
Continuously
Field(HO
Constant 4.
isWith NMR in
rum
usingpatients diagnosithe ng for C2.1 figurintroduced
e in
Speciroscopy NMR C2.1 Figure
 Sorting
Ioniztion
Detection
Mass
Ton Analysed
signal
processe Traasdutkr

Vacum Pump Gaseous

Ion Sourti

Mass $pectrum

C3.1 Mass Spectrorneter the

in proper seguence based on the mode of operation for analyzing
Rearrange the fiqure C3.1 sequence.
mass spectrum. Justify the (5 Marks- [Ap/C.2)
involved.
with respect to mode of spectrum
(u) Relate the types of mass spectrometer Structure
Spectrum
Involved
Electrostatic and
Magnetic Magnetic Field
Sector
Analyser et

A2
41
Double
Electrostatic Field
Focusing
Analyser Dg

B3
B1

Page 8 of 9
 Time of Flight Magnelc Fleld Maonete
Analyser Electr ontabe
anatyzer

(ESA)

Plane of enery
Pon ol
doute l

Source colector
eot s plane of drenna
ocving

lon
sOuroe
C1 C2
C3
(3 Marks- (An/C,2)
Assertion: Mass Spectrometer separate lons produced in ion source based on different mass and
charge ratio
Reason: Allows sufficient number of ions to produce measurable ion currents.
a) Assertion and
b) Assertion and reason
reason both are correct.
both are correct. Reason
Reason isis correct explanations
not correct for assertion.
explanations for assertion.
c) Assertion is correct but the reason is wrong statement.
d) Assertion and reason both are not correct
(2 Marks- [U/C, 2)
***End of Question Paper**

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