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Facile and Low Cost Temperature Compensated Humidity Sensor and Signal Conditioning System
Facile and Low Cost Temperature Compensated Humidity Sensor and Signal Conditioning System
Facile and Low Cost Temperature Compensated Humidity Sensor and Signal Conditioning System
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JAVED et al.: FACILE AND LOW COST TEMPERATURE COMPENSATED HUMIDITY SENSOR 14907
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14908 IEEE SENSORS JOURNAL, VOL. 21, NO. 13, JULY 1, 2021
Fig. 1. Detailed schematic design of controlled environmental setup for electrical characterizations.
Fig. 2. Physical and chemical characteristics of sensing material with (a) showing surface SEM and (b) showing the FTIR of PEO thin film.
To investigate the effect of temperature, the chamber was created in the gel like thin film of the amorphous PEO due to
heated using an in-built convection heating filament. Transient trapped air.
response of the sensor was recorded by quickly switching The micro-pores result in substantially improving overall
between one stream of air saturated with water vapor and one porosity of the active layer, thus increasing the surface area
stream of dry Nitrogen. Further details on the characterization to volume ratio that is ideal for humidity and gas sensors
setup can be found in our previous works [2], [18]. as it allows maximum sites for the adsorption of water and
gas molecules [30]. The amorphous behavior of PEO is also
clearly visible from the FTIR results presented in III-B(b). The
III. R ESULTS AND D ISCUSSION three characteristic triplet absorption bands of C-O-C at 1060,
A. Morphological and Chemical Characterizations 1105, and 1144 cm−1 representing crystallinity of the material
SEM results presented in III-B(a) show micro-level cracks are missing from the results [32]. The remaining bands,
formed in the surface due to melting of the material during however, confirm the material to be PEO with the absorption
curing at high temperature (PEO melting point 74◦C) and then bands in the region with wavenumber lower than 1000 cm−1
re-solidification when the temperature was returned to normal. representing CH2 rocking, the band at 1290 cm−1 represent-
The phase of PEO was also changed from semi-crystalline to ing CH2 twisting mode, and the sharp peak at 2871 cm−1
amorphous during curing as the glass transition temperature of corresponding to C-H stretching mode. The wide absorption
PEO is 69◦ C [32]. This effect is visible from the micro-pores in the band around 3400 cm−1 represents the presence of
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JAVED et al.: FACILE AND LOW COST TEMPERATURE COMPENSATED HUMIDITY SENSOR 14909
Fig. 3. Impedance response of the devices at various temperatures showing (a) output curve of open sensor and (b) output curve of encapsulated
sensor.
OH (hydroxyl) group due to physical adsorption while the humidity if the temperature changes by even 1◦ C (1◦ C change
band near 1643 cm−1 represents hydrogen bonded hydroxyl in temperature will result in an error of 2% RH). In terms
ions with the polymer [32]. The attachment of hydroxyl ions of real life scenario, the environmental temperature of most
with the polymer through hydrogen bonding results in higher areas around the globe roughly change on average by around
sensitivity of the material towards lower humidity levels. 10◦C in a 24 hours duration. This means an error of 20% in
It facilitates the flow of electronic and ionic current through the relative humidity readings over the course of a day which is
random paths in amorphous polymer matrix, thus decreasing unacceptable. The magnitude of change in sensor resistance
the resistance when the humidity levels increase [32]. due to change in temperature will be different for different
materials but some effect is there nevertheless for the majority
of devices.
B. Electrical Response and Behavior Specificity of a sensor is its ability to respond to only
Two identical devices were fabricated and one of them was the targeted parameter and reject the effect of anything else
encapsulated to isolate it from the effect of humidity while the (noise). This means that a humidity sensor responding to
other one was left open. Impedance response of both devices temperature variations is a non-specific sensor that is highly
was investigated towards increasing relative humidity and the undesirable. To address the issue of temperature dependence
results are presented in Fig. 3(a). Initially, the temperature was and improve the specificity of humidity sensors, an extremely
kept constant at room temperature and the relative humidity affective and simple approach has been developed in this work.
was changed from 0% RH to 80% RH. Results show that the The sensors were connected in a bridge configuration with the
impedance of non-encapsulated device (black) decreases with open sensor connected in one potential divider branch of the
increasing temperature with a slope of ∼15 k/%RH while bridge, while the identical but encapsulated sensor connected
the impedance of encapsulated device (green) is not affected in the opposing potential divider branch of the same bridge.
by the changing relative humidity and remains constant for a The bridge was excited with an AC waveform of 1 kHz having
fixed temperature. This confirms that the encapsulated sensor an RMS value of 1 V. AC excitation source was used instead of
was successfully isolated from the humid environment. The DC to prevent possible polarization of hydroxyl ions and water
dependence of device impedance (Z) on temperature (T) molecules under a fixed applied electric field. Also, a low volt-
was investigated by taking the Z vs RH curves at various age excitation source was used to avoid damage to the active
temperatures for the open sensor, while Z vs T curves for layer and keep the power consumption low at the same time.
the encapsulated sensor. The results presented in Fig. 3(a) As per the results presented in Fig. 3, it is expected that the
show that the impedance of open sensor is highly dependent output voltage of the branch with open sensor would change
on the surrounding temperature. The impedance decreases for both changing temperature and relative humidity but the
with increasing temperature shifting the whole curves (red output voltage of the encapsulated branch will respond only
& blue) of Z vs RH to a different level. This is due to to changes in temperature. Results of the bridge configuration
the change in conductivity of amorphous PEO with chang- with outputs of individual divider branches are presented in
ing temperature [32]. Similarly, the Z vs T plot (black) of Fig. 4. As theorized, Fig. 4(a) shows that voltage of open
encapsulated sensor presented in Fig. 3(b) shows that the sensor branch (red) is dependent on both the temperature and
impedance decreases with increasing temperature with a slope relative humidity while the voltage of encapsulated sensor
of about 29.5 k/◦ C and is independent of the change in branch (blue) is only dependent on changes in temperature.
relative humidity. This dependence of device impedance on Results at constant temperature presented in Fig. 4(b) show
temperature will result in a huge error in the reading of relative that the voltage of encapsulated sensor branch (blue) remains
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14910 IEEE SENSORS JOURNAL, VOL. 21, NO. 13, JULY 1, 2021
Fig. 4. Output response of open and encapsulated devices connected in a bridge configuration showing (a) temperature dependence of open
and encapsulated sensors, (b) output of both branches and the overall bridge versus humidity, (c) temperature compensation using bridge, and
(d) comparison of normalized compensated and uncompensated outputs with the standard.
constant for changing humidity while the voltage of open of bridge; thus automatically cancelling each other out and
sensor branch (red) decreases almost linearly with increasing resulting in temperature compensation.
humidity. Relatively lower sensitivity of the sensor towards The compensation effect can be better visualized from
lower humidity levels was resulting in a non-linear Z vs RH Fig. 4(d) where the three curves are normalized and plot-
curve as presented in Fig. 3. But, as potential divider itself has ted together. The uncompensated curve (blue) shows huge
non-linear response for linear changes in resistance, the non- deviation from the standard (black) due to slight change in
linearity in resistance was cancelled out by the opposing temperature while the compensated curve (red) remains fairly
non-linearity of divider; thus, resulting in a fairly linear voltage close to the standard curve. Relative percentage error of the
output. Though, it would not be a universal case and is uncompensated curve (blue) with the standard curve (black)
only true for this particular device. Differential output of the was calculated to be 20.8% (absolute error of 5.61) for ∼6.3◦ C
bridge (green) in Fig. 4(b) will be considered as the standard variation in temperature. The percentage error was reduced
output of humidity sensor system at a constant temperature to just 5.4% (absolute error of 1.97) for the compensated
from this point onwards. Compensation performance of the curve (red) that shows a huge improvement. It is worth noting
developed signal conditioning system was then evaluated for here that the reference sensor used in this work (HTU-21D)
varying temperatures while recording its response towards also had a rated maximum error of up to 3% [33] while
change in humidity. Fig. 4(c) presents multiple curves includ- linear approximation of the standard curve (green) of Fig. 4(c)
ing open sensor branch output (red), encapsulated sensor also resulted in a standard error of 1.1%. This means that if
branch output (blue), differential compensated output (green), the linear approximations are not made and the actual curves
and change in temperature (black) for better visualization. are considered, the error will be further reduced. Also, this
It can be observed from the results that the open sensor branch configuration of bridge based compensation will work for
output (red) no longer remains linear when the surrounding sensors with any form of output, whether linear or non-linear,
temperature changes. But, the encapsulated sensor branch out- resistive or capacitive, and increasing or decreasing. This
put (blue) no longer remains constant as well. The differential makes out proposed solution to be close to a universal solution
compensated output (green) however remains fairly linear even for temperature compensation in humidity sensor chips.
with continuously varying surrounding temperature. This is To improve the sensitivity of the system, the differential
due to an equal effect of temperature on the opposing branches output of bridge was amplified using an instrumentation
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JAVED et al.: FACILE AND LOW COST TEMPERATURE COMPENSATED HUMIDITY SENSOR 14911
Fig. 5. Detailed signal conditioning circuit design for the temperature compensated humidity measurement system.
Fig. 6. Real-life parameters of the developed humidity sensing system showing (a) response and recovery time curve, (b) long term stability and
reproducibility, and (c) real-time measurement of relative humidity in open environment.
amplifier based signal conditioning circuit that has an added was selected to be in the same order of magnitude that is
advantage of automatically rejecting any common mode noise 3 M. Slightly higher value of fixed resistors was selected to
from the output signal. The detailed signal conditioning circuit compensate for the non-linear effects of a bridge circuit and
diagram/schematic is presented in Fig. 5. The circuit was keep the voltage output approximately linear in a short defined
designed based on actual parameters of sensor resistance, range. This will no doubt affect the maximum sensitivity of
signal amplitude, and desired output. Maximum value for differential bridge output but will let us operate the system in a
the intrinsic impedance of both sensors was recorded to be linear range that is of higher importance in this kind of signal
∼1.25 M at 0% RH. As the sensors were used in potential conditioning circuits. Sensitivity of the overall system was
divider based bridge configuration, the value of fixed resistors later improved by signal amplification as described above. The
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14912 IEEE SENSORS JOURNAL, VOL. 21, NO. 13, JULY 1, 2021
TABLE I
D ETAILED C OMPARISON OF THE P ERFORMANCE PARAMETERS OF VARIOUS H UMIDITY S ENSING D EVICES
gains and reference voltage were selected to directly obtain a (recover to 10% of maximum output starting from 90%) was
voltage reading roughly corresponding to the actual % relative recorded to be ∼2.88 s. Long term stability and reproducibility
humidity with 0.1 V representing 1% RH (0.0 V for 00% RH of the sensors was investigated by recording the full range
and 8.0 V for 80% RH). AD620 instrumentation amplifier output response curve with an interval of 100 days between
was used for signal amplification while LM741 was used for two readings. During that time, to ensure real-life applicability,
offset correction at 0% RH. Both are readily available and cost the devices were stored in nominal open environment without
a fraction of a dollar. Furthermore, the effect of mismatch in any special precautions other than avoiding physical damage
resistance of both sensors was investigated to verify the system or contamination of the active layer. The results presented
robustness in various conditions. The effect was investigated in Fig. 6(b) indicate the maximum absolute error of around
through simulations by changing the value of encapsulated 5.8% between the two curves showing outstanding stability of
sensor. It was observed that the overall system equation the devices making the developed system an ideal candidate
changes but the compensation effect remains intact because for weather monitoring. The real-life weather monitoring
as presented in Fig. 4(a), the voltage output of encapsulated capabilities of the developed system were tested by deploying
sensor changes linearly with temperature. it for real-time monitoring of relative humidity in an open
This means that the change in voltage (V) for a change environment with varying temperature and humidity. The data
in temperature (T) will remain same regardless of the initial was recorded for both the bridge output and the overall
value of encapsulated sensor resistance. So, a mismatch in system output. Temperature of the environment (red) was
the sensor pair resistances is not a cause of concern here. varied intentionally between 31.7◦C and 43.7◦C using a room
The only affect will be observed on the intercept of the linear heater installed near the setup for a measurement time of
relationship that can be easily tuned by changing the offset 1 hour. Temperature was changed forcefully to maximize the
voltage at the last stage. Further details and simulation results induced error in the system and check its robustness and
are presented in supplementary information section-II. effectiveness in compensation for more challenging condi-
As the final evaluation measurement, transient response, tions. The results presented in Fig. 6(c) show that relative
long term stability & repeatability, and real-life output results humidity (green) of the environment changed from 47.5%
were recorded for the developed sensor solution. Results of RH to 33.8% RH during the same time. The dependence of
the transient response presented in Fig. 6(a) show that the various sensor parameters towards the changing environmen-
response time (to achieve 90% of maximum output starting tal conditions show that the voltage output of encapsulated
from 10%) of the sensors was ∼1.88 s while the recovery time sensor branch (light green) is only dependent on the changing
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JAVED et al.: FACILE AND LOW COST TEMPERATURE COMPENSATED HUMIDITY SENSOR 14913
temperature as expected; the voltage output of the open sensor mode noise. Cost of the overall system was estimated to
branch (grey) is dependent on both temperature and humidity; be less than a dollar for mass production. The developed
while the differential output of bridge (pink) is dependent only sensor system was capable to measure relative humidity with
on humidity. Continuous output of the overall system after a bridge sensitivity of 2.9 mV/%RH while the final output
temperature compensation, that is voltage represented as a sensitivity of 100 mV/%RH in a wide range of 0% to 75% RH.
function of relative humidity (orange) is almost overlapping Temperature compensation results show that the error due to
the reference relative humidity (dark green). The absolute temperature changes was successfully reduced from 22.4% to
error or difference between the two curves is just 1.24%. 1.24%. The system had a transient response time of ∼2.4 s and
For comparison, the uncompensated output of the open sen- a long term accuracy of ∼95%. The output response was linear
sor branch (grey) and the calculated uncompensated relative and can be directly read as relative humidity being represented
humidity as a result (blue) are also plotted on the same graph. in terms of voltage output. The system would be valid for
The uncompensated humidity value exhibits an enormous error non-linear devices as well. Only the voltage output will not
of 22.4% when compared to the reference humidity curve directly represent humidity that is not an issue and can be
(dark green). This means that a change in temperature of just tackled by solving the non-linear equation of response curve.
12◦ C results in huge errors in calculation of relative humidity The same system can be further used to measure temperature
that have been successfully eliminated using the proposed if required with an additional circuit connected only to the
approach making the developed sensor system an ideal and compensation branch of the bridge.
complete solution for real-life humidity sensing applications.
Various performance parameters of the fabricated sensor C ONFLICT OF I NTEREST
solution in this work were compared with the state-of-the-
The authors declare no conflict of interest.
art commercially available relative humidity sensors and those
reported in literature. A detailed comparison is presented in
TABLE I. Sensor with the best performance in each category R EFERENCES
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14914 IEEE SENSORS JOURNAL, VOL. 21, NO. 13, JULY 1, 2021
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with integrated temperature compensation mechanism,” Sens. Actuators the supervision of Dr. Khasan Karimov and Dr. Memoon Sajid. His
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metal carbide and polymer thin films,” Sens. Actuators B, Chem., USA, in 2007. His research interests include communication systems,
vol. 252, pp. 725–734, Nov. 2017. Ad hoc networks, channel coding, and computer architecture.
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