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  • Production of Dipersbyk 142

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    Method 1 describes the production of Dipersbyk 142 using a reaction of propylene oxide, methyl alcohol, methyl acetate, and sodium methoxide catalyst. It yielded 87.1% with a 92% conversion rate over 4 hours at 100°C. Method 2 uses propylene glycol monomethyl ether, acetic acid, vitriol oil, and n-butyl acetate and yielded 75.7% with an 87.7% conversion rate over 5 hours at 120-140°C. Method 1 produces Dipersbyk 142 through an etherification reaction while Method 2 uses an esterification reaction.

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    PRODUCTION OF DIPERSBYK 142

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    Method 1 describes the production of Dipersbyk 142 using a reaction of propylene oxide, methyl alcohol, methyl acetate, and sodium methoxide catalyst. It yielded 87.1% with a 92% conversion rate over 4 hours at 100°C. Method 2 uses propylene glycol monomethyl ether, acetic acid, vitriol oil, and n-butyl acetate and yielded 75.7% with an 87.7% conversion rate over 5 hours at 120-140°C. Method 1 produces Dipersbyk 142 through an etherification reaction while Method 2 uses an esterification reaction.

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    19 views2 pages

    Production of Dipersbyk 142

    Uploaded by

    Paraben
    Method 1 describes the production of Dipersbyk 142 using a reaction of propylene oxide, methyl alcohol, methyl acetate, and sodium methoxide catalyst. It yielded 87.1% with a 92% conversion rate over 4 hours at 100°C. Method 2 uses propylene glycol monomethyl ether, acetic acid, vitriol oil, and n-butyl acetate and yielded 75.7% with an 87.7% conversion rate over 5 hours at 120-140°C. Method 1 produces Dipersbyk 142 through an etherification reaction while Method 2 uses an esterification reaction.

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    of 2

    PRODUCTION OF DIPERSBYK 142

    PROPYLENE GLYCOL METHYL ETHER ACETATE


    METHOD 1

    RAW MATERIAL QUANTITY


    A PROPYLENE OXIDE 174g
    B METHYL ALCOHOL 192g
    C RITALIN (METHYL ACETATE) 666g
    D SODIUM METHYLATE (Catalyst) 3g

    PROCEDURE
    1. Mix A – D in the reactor ( reactor with a Nitrogen Purging Reactor)
    2. Turn on reactor agitator (300 – 800rpm)
    Yield: 87.1%
    3. Heat to 100oC and timing begins (Reaction time : 4hrs)
    Conversion Rate: 92%
    4. Maintain Pressure at 0.15 MPa
    5. After reaction is completed, cool reactor to room temperature
    6. Reclaim Methyl alcohol by rectifying separation

    METHOD 2

    RAW MATERIAL QUANTITY


    A Propylene Glycol monomethyl ether 360g
    B Acetic acid 277g
    C Vitriol oil 1.3g
    D N – Butyl Acetate 51g

    PROCEDURE
    1. Add A – D in the reactor (1000ml boiling flask with a condenser and a 20 * 800 packing
    tower)
    2. Heat and maintain temperature to 120 – 140oC Yield: 75.7%
    3. Reaction time: 5hrs Conversion Rate: 87.7%
    4. Cool reactor and remove product
    PRODUCTION OF DIPERSBYK 2013
    STYRENE MALEIC ANHYDRIDE COPOLYMER

    RAW MATERIAL QUANTITY


    A Maleic Anhydride 0.57g
    B Styrene 0.61g
    B Benzoyl peroxide BPO (Initiator) 0.024g
    C Butylacetate (Medium) 5ml
    Maleic Anhydride and styrene mole proportioning 5:5

    PROCEDURE

    1. Employ oil bath heating was reacted 1.5hrs under 100oC temperature under nitrogen
    protection
    2. Dry the liquor to obtain a white powder
    Yield: 88%

    METHOD 2

    RAW MATERIAL QUANTITY


    A Maleic Anhydride 4.904g
    B Styrene 5.2g
    B Diisopropyl azodicarboxylate (AIBN) 0.03g
    (Initiator)
    C Isoamyl acetate FCC (Medium) 45ml
    Maleic Anhydride and styrene mole proportioning 1:1

    PROCEDURE
    1. Adopt heating in a water bath under nitrogen protection
    Heating time: 6hrs
    Heating temperature should be under 70oC
    Results

    Median size Dn 1081microns


    Dispersion coefficient U 1.006
    Molecular weight 111987g
    Polymerisation yield 88%

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