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of Wire-Electric Discharge
Machined Ultrathin Silicon
Downloaded from http://asmedigitalcollection.asme.org/micronanomanufacturing/article-pdf/8/4/041006/6627576/jmnm_008_04_041006.pdf by Indian Institute of Technology Bombay, Deepak Marla on 07 October 2023
Divyanshu Bhartiya
Department of Mechanical Engineering,
Wafers Using Response
Indian Institute of Bombay,
Mumbai 400076, India Surface Methodology for
Pinal Rana
Department of Mechanical Engineering, Solar Cell Applications
Indian Institute of Bombay,
Mumbai 400076, India Recent investigations on the fabrication of ultrathin silicon (Si) wafers using wire-
electric discharge machining (wire-EDM) were observed to possess some inherent limita-
Meinam Annebushan Singh tions. These include thermal damage (TD), kerf-loss (KL), and low slicing rate (SR),
Department of Mechanical Engineering, which constraints its industrial use. The extent of TD, KL, and SR largely depends on the
Indian Institute of Bombay, process parameters such as open voltage (OV), servovoltage (SV), and pulse on-time
Mumbai 400076, India (Ton). Therefore, optimizing the parameters that pertain to minimum TD and KL while
maintaining a higher SR is the key to improvement in the fabrication of Si wafers using
Deepak Marla1 wire-EDM. Thus, this study is an effort to analyze and identify the optimal parameters
Department of Mechanical Engineering, that relate to the most effective Si slicing in wire-EDM. A central composite design
Indian Institute of Bombay, (CCD)-based response surface methodology (RSM) was used for optimizing the process
Mumbai 400076, India parameters. The capability to slice Si wafers in wire-EDM was observed to be influenced
e-mail: dmarla@iitb.ac.in by the discharge energy, which significantly impacted the overall responses. The severi-
ties of TDs were observed to be mainly dominated by the variation in OV and Ton due to
the diffusion of thermal energy into the workpiece, leading to melting and subsequent
resolidification. For high productivity, the optimized parameters resulted in a SR of
0.72 mm/min, TD of 17.44 lm, and a kerf-loss of about 280 lm.
[DOI: 10.1115/1.4049362]
Downloaded from http://asmedigitalcollection.asme.org/micronanomanufacturing/article-pdf/8/4/041006/6627576/jmnm_008_04_041006.pdf by Indian Institute of Technology Bombay, Deepak Marla on 07 October 2023
anode, respectively. The dielectric was maintained at around
parameters on the overall machining characteristics. The incorpo- 25 C temperature using a water chilling plant. The kerf-loss was
ration of the multi-objective optimization will help identify the measured using an optical Rapid Eye microscope. Further, the
process parameters for the slicing of Si wafers corresponding to severity of thermal damages was measured using a field emission
the most optimal machining scenario (high slicing rate, low kerf- scanning electron microscope (SEM) (Ultra 55, Carl Zeiss).
loss, and thermal damage), which can enhance productivity. Preliminary experiments were conducted to identify the operat-
ing range of the process parameters, viz., OV, SV, and Ton. The
2 Experiments working range of the process parameters was chosen with wire
breakage as the limiting factor. The final working range was cho-
Experiments were carried out to slice Si wafers at a different sen as 65–95 V for OV, 34–50 V for SV, and 0.3–1.2 ls for Ton,
set of process parameters using wire-EDM. In this section, the with corresponding levels shown in Table 1. The reason behind
details of the experimental setup and design of experiments are choosing this range is that at 65 V of OV and 0.3 ls of Ton, spark
presented. produces minimal energy, below which there was no material
removal. At 95 V of OV and 1.2 ls of Ton spark produces maxi-
2.1 Design of Experiments. This work employs RSM to mum energy, above which there was frequent wire breakage. A
design and analyze the experiments with slicing rate, thermal constant pulse off-time of 15 ls, wire tension 6.86 N, wire feed of
damage, and kerf-loss as the response parameters. A central com- 92 mm/s, and water pressure of 10 bar/kg were considered in this
posite design (CCD)-based RSM was chosen because of its supe- study.
rior prediction quality over other designs. The axial points in the
CCD demarcate the values chosen for the considered factors. A 3 Optimization Methodology
basic factorial design is created within these axial points, consist-
ing of a central point representing the mean value of all the fac- The objective of this study is to optimize the overall process
tors. The axial points help estimate the curvature used for parameters during Si-wafer slicing with regard to a high slicing
circumscribing the cube formed by the factorial points with a cen- rate, low thermal damage, and kerf-loss. The design and optimiza-
tral point at the center. The RSM estimates the value of responses tion were performed using open source R programing software.
at each point within the volume circumscribed by the CCD curva- The optimization methodology, along with the objective func-
ture (see Fig. 1). The design consists of three controlled variables tions, is summarized as:
(OV, SV, and Ton) and three responses, viz., SR, KL, and TD. For (i) Find process parameters: X ¼ [OV, SV, Ton]
the application of CCD, the chosen range of values of the con- (ii) F ¼ f [maximize (SL), minimize (KL, TD)]
trolled variables was demarcated into five levels. With k factors in (iii) Given objective functions:
an experiment, CCD proposes 2k factorial points, 2k axial points, slicing rate (SR) ¼ f1 (OV, SV, Ton);
and a central point (Cp), culminating into 2k þ 2k þ Cp number of kerf-loss (KL) ¼ f2 (OV, SV, Ton);
experiments. Hence with k ¼ 3, the number of experimental points thermal damage (TD) ¼ f3 (OV, V, Ton)
is 23 þ 2 3 þ 1 4 ¼ 18; here central point was repeated four (iv) Subject to constraints:
times. Therefore, 18 different sets of parametric combinations 65 V OV 95 V;
with two repetitions were chosen to carry out the experiments. 34 V SV 50 V;
Following the experiments, the RSM was used to develop a 0.3 ls Ton 1.2 ls;
second-order equation based on the retrieved data and assist in (v) Find individual desirability (d)
evaluating response surfaces and contour plots to understand the
effects of controlled variables on the responses. The accuracy of SRn minðSRÞ
the model was accessed by the repeated experimentation of the dðSRn Þ ¼
maxðSRÞ minðSRÞ
central points, which measure the process variability to gain a bet-
ter error estimate. These central points also help identify the cur-
maxðKLÞ KLn
vature of the model and estimate the significance of each factor. dðKLn Þ ¼
After modeling of the experimental data, the desirability function maxðKLÞ minðKLÞ
was used for multi-objective optimization.
Levels
Process parameters 2 1 0 1 2
Downloaded from http://asmedigitalcollection.asme.org/micronanomanufacturing/article-pdf/8/4/041006/6627576/jmnm_008_04_041006.pdf by Indian Institute of Technology Bombay, Deepak Marla on 07 October 2023
Pulse on-time (ls) 0.3 0.5 0.75 1 1.2
maxðTDÞ TDn
dðTDn Þ ¼
maxðTDÞ minðTDÞ
(vi) Find overall desirability (D) using Fig. 4 Variation of slicing rate with Ton and OV (SV 5 42 V)
Fig. 3 Variation of slicing rate with SV and OV (Ton 5 0.75 ls) Fig. 5 Variation in slicing rate with Ton and SV (OV 5 80 V)
Downloaded from http://asmedigitalcollection.asme.org/micronanomanufacturing/article-pdf/8/4/041006/6627576/jmnm_008_04_041006.pdf by Indian Institute of Technology Bombay, Deepak Marla on 07 October 2023
different locations. The average value of kerf-loss for OV ¼ 95 V,
Ton ¼ 1.2 ls, SV ¼ 34 V (first set of parameters) is 0.2710 mm as
shown in Fig. 6(a) and for OV ¼ 65 V, Ton ¼ 0.3 ls, SV ¼ 50 V
(second set of parameters) is 0.2903 mm as shown in Fig. 6(b). As
the wire diameter is 250 lm, the calculated interelectrode gap
from Fig. 6 is approximately 10 lm and 20 lm, respectively, for
the first and second sets of parameters. Fig. 7 Variation of kerf-loss with SV and OV (Ton 5 0.75 ls)
Figure 7 shows the variation of KL with varying OV and SV. A
gradual increase in KL was observed with an increase in OV for
lower SVs. This variation is mainly due to the increase in dis-
charge energy with OV, which leads to higher removal of material
from both the machining as well as transverse direction. However,
at higher SVs, the variation in KL was observed to be almost con-
stant throughout. At a lower value of OV, KL increases with an
increase in SV. This is mainly attributed to the higher probabilistic
discharge concentration in the transverse direction, leading to a
larger KL. However, for the case with higher OV, the KL initially
decreases and then increases with an increase in SV. Initially,
when the SV was maintained at a lower value and OV at a higher
value, profound interaction of the wire electrode and the work-
piece material occurs. This directly corresponds to larger material
removal and hence, larger KL as well.
For the machining scenario with larger OV (90–95 V), when Fig. 8 Variation of kerf-loss with Ton and OV (SV 5 42 V)
the SV increases, the intensity of discharges decreases due to the
increasing interelectrode gap, which correlates with the reduction
in KL, as observed in Fig. 7. Further increase in the SV increases ultimately leading to a comparatively larger KL, as reported in
the interelectrode gap to a sufficiently large value that the dis- Fig. 8.
charge concentration gets highly focused toward the transverse
direction. As a result, the KL concomitantly increases. In this
work, the SV in the range of 40–45 V was observed as the thresh- 4.3 Thermal Damage. The minimization of the severity of
old boundary over which the KL varies. thermal damage is an essential criterion for solar cell applications,
Figure 8 shows the variation in kerf-loss with OV and Ton. For with regard to the power conversion efficiency. Higher thermal
a given value of OV, an increase in Ton decreases the KL initially damage leads to higher recombination, which reduces the effi-
and then gradually increases beyond a certain threshold Ton value ciency of solar cells [12]. Figure 9 shows the variation in the ther-
(Fig. 8). This is because when Ton increases, the discharge energy mal damage obtained during the slicing of Si wafers using wire-
increases, which cause significant melting, vaporization, and ther- EDM. By measuring the difference in surface texture from the
mal spalling. As a result, the wire electrode has a higher probabil- base material, thermal damages were measured. The severity of
ity of moving in the machining direction. This leads to a reduced the net thermal damages was observed as a consequence of both
spark initiation and propagation in the transverse direction. There- the recast layer and the heat-affected zone, which extends beneath
fore, KL decreases. However, with a further increase in Ton, the the resolidified layer.
increased discharge energy generates high debris, which increases The variation in the thermal damage with OV is shown in
the chances of clogging in the machining gap. This leads to a Figs. 10 and 11. The severity of thermal damages was observed to
higher probability of spark generation in the transverse direction, increase with an increase in OV. When OV increases, the
Fig. 6 Optical images for measuring the kerf-loss (a) OV 5 95 V, Ton 5 1.2 ls, SV 5 34 V and (b) OV 5 65 V,
Ton 5 0.3 ls, SV 5 50 V
associated discharge energy increases as well. Consequently, dif- the eroded material. A combined effect of high material erosion
fusion of heat into the workpiece material increases, resulting in and poor flushing leads to a high amount of material getting rede-
higher melting, resolidification, and thermal affected zones. This posited on the machined surface, thereby leading to poor surface
ultimately increases the thermal damages, as observed in Figs. 10 characteristics, as seen in Fig. 12(a). In comparison, the crater
and 11. When OV increases from 65 to 95 V, there is a 21% density is lower in Fig. 12(b) with a low amount of redeposited
increase in thermal damage. For a given OV, the thermal damage material. Besides, the size of the craters is higher in Fig. 12(b)
increases with an increase in SV (see Fig. 10) as well. The SV because of wider interelectrode gap, which could be due to the
being an interelectrode gap function, an increase in SV increases generation of a thicker (discharge) plasma.
the interelectrode gap maintained between the tool and the work-
piece. This leads to higher severity of spark concentration in the 4.5 Optimization. In order to find the optimal process param-
transverse direction, which subsequently leads to higher thermal eters, the RSM package in the R language was used. The model-
damage. In the present analysis, an increase in SV from 35 to ing approach described in Sec. 3 was used to find the response
50 V caused a 13% increase in the thermal damage. variables (KL, SR, and TD) as a function of OV, SV, and Ton. Fur-
A similar influence was observed with varying Ton (Fig. 11), ther, desirability (d) values for each of the response variables
where an increase in Ton leads to higher discharge duration, were calculated. Table 2 depicts the value of individual desirabil-
which increases the overall heat diffusion, ultimately leading to ity corresponding to each of the response variables at different
enhanced thermal damages. The thermal damages were observed experiment conditions. From these individual desirability values
to increase by about 133% when the Ton increases from 0.3 to (d(KL), d(SR), d(TD)), overall desirability (D) for each experi-
1.2 ls. ment is calculated. The parametric optimization resulted in
OV ¼ 84.32 V, SV ¼ 42.98 V, and Ton ¼ 0.62 ls. The values of
thermal damage, kerf-loss, and slicing rate corresponding to the
4.4 Machined surface. Figures 12(a) and 12(b) show the above set of parameters are 20.69 lm, 279.27 lm, and 0.6134 mm/
SEM images of the machined surfaces at two different parameters min, respectively. However, the obtained optimized parameter
pertaining to the extreme conditions. The surface consists of cra- cannot be directly used due to the associated limitations of the
ters, pores, and redeposited debris. A qualitative comparison of present experimental setup in selecting the parameter values.
the two surfaces suggests that the density of craters and the rede- Thus, the nearest settings were considered to perform the final val-
posited material is higher in Fig. 12(a) than Fig. 12(b). This is idation (OV ¼ 83 V, SV ¼ 43 V, and Ton ¼ 0.6 ls). A moderately
because the spark energy increases with an increase in OV, and higher slicing rate of 0.6560.04 mm/min, kerf-loss of 28063 lm,
the number of sparks increases with an increase in Ton. Therefore, and thermal damage of 1862 lm was observed during experimen-
at higher values of OV and Ton, the material erosion is more tal characterization. This is the global optimum value for the pres-
severe, as is evident in Fig. 12(a) with a higher density of craters. ent experimental study and is observed to be well within the limit
Also, the discharge gap is smaller at lower values of SV. Due to of value obtained from optimization, thus validating the accuracy
the narrow discharge gap at SV ¼ 34 V (Fig. 12(a)), the flushing of the optimization model.
capability is poor, which subsequently leads to the redeposition of
Fig. 10 Variation of thermal damage with SV and OV Fig. 11 Variation of thermal damage with Ton and OV
(Ton 5 0.75 ls) (SV 5 42 V)
Table 2 Desirability function of machining parameters with their levels and responses
OV (V) SV (V) Ton (ls) SR (mm/min) KL (mm) TD (lm) d(SR) d(KL) d(TD) D
However, the observed global optimal value of thermal dam- discharge time higher is the heat penetration into the work-
age, kerf-loss, and slicing rate is not suitable for high productivity piece. Thermal damage increased by 133% when Ton was
owing to the low slicing rate (0.65 mm/min) and high thermal varied from 0.3 ls to 1.2 ls.
damage (18 lm). Furthermore, the overall variation in kerf-loss (4) The optimal parameters from the model were obtained as
for all the experiments is around 20 lm, which is insignificant. OV ¼ 83 V, SV ¼ 43 V, and Ton ¼ 0.6 ls with the corre-
Therefore, another case was taken into account that considered sponding value of slicing rate, kerf-loss, and thermal dam-
slicing rate and thermal damages as the major desirability func- ages are 0.6134 mm/min, 279.27 lm, and 20.69 lm,
tions. Following the optimization steps mentioned in Sec. 3, the respectively.
optimized parameters for high productivity are OV ¼ 87.84 V, (5) The thermal damage and slicing rate are the two essential
SV ¼ 35 V, and Ton ¼ 0.4 ls. The corresponding theoretical value factors for improving productivity. The optimized parame-
of thermal damage and slicing rate is 17.44 lm and 0.72 mm/min, ters for high productivity (high slicing rate and low thermal
respectively. Therefore, performing the wire-EDM process at damage) were OV ¼ 87.84 V, SV ¼ 35 V, and Ton ¼ 0.4 ls,
these parameters can significantly enhance productivity. with corresponding thermal damage and slicing rate of
17.44 lm and 0.72 mm/min, respectively.
5 Conclusions
This work is an effort to optimize ultrathin Si wafer slicing Acknowledgment
using wire-EDM with slicing rate, kerf-loss, and thermal damage
as the output characteristics. The following are the main conclu- The authors are greatly thankful to National Centre for Photo-
sions of the work. voltaic Research and Education (NCPRE), IIT Bombay, for allow-
ing the use of their facilities to carry out the experimental work.
(1) The slicing rate was mainly dominated by OV. This is
mainly due to the increased discharge energy with higher
OV, leading to higher melting and vaporization.
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