Date

Expt. No.
Pageblo,

ExPER1MENT- 10
Salk Analysis-1 (NH], S04
Aim
Toidemfy tha acidi and basie radicals in a aivem
5all

Appavatus
Test abes lest tebe helelen , dnebper bumsen bunne
EzperMem Ghservation
Pnalininar lac
Colou ihe sal-| h l e MC FeN
F3, C** arne
SouililsSoluble in absem
uwalen
Odlouh of tha Saul faim ammcuiacal N may be pheoen
Smel

Ca2,Ba*, S.*
Flame Teat No charactioioie
abseu.
Prepasasd a loanlo celour ebsexuse | ma
Hue Scul wik conc. He
aud Homma. ul-io dona

*lests For Aeioic Radicalss-

2 DRY
TEST=
Dl.Sulbhusie aid kest
No ga is eveluaoco S 50, Na
Sallk + di HaSO4 L_ a n a absemt
aumao
Teacher's Signature
 Dote-
Expt. No.
Page No. 24

Expenemem
Conc Hs04 Tes bsewaHen Jnexame

pineh o sa+ one, No gas r heachcm e, B L

Ha s04+ haalaa ia obsesued Cits Coo NOCO
0ne absen
cCoue S04+ u-ksmi malTer
A pmeh cd sal + C No boon omen NO is absenl
tuounim3 t Come, bso absenuss
hearey

3 Cenirmatoy ats fon So PO

Peparaien Ar Extsuek Walir askrac- (wE) is
aaaa.clbdisspluina a small amaugk ot sal in 5
iealecd al0
so BaCl, (an) BaS04 ( +2e14)
shilE p B.e Test
E feo derobs E p- ineousle So4 is
dil Helt Baelh soluin cme. Hel ia Comiemnas
Lsadl-acezli Testesil soalublaS s conn
So+Pb(ecoo)g ()>Phso,1+2oo OE +ed ocops in eacess o Qmmoni- mad,
Leac-acenla sal u acakai soluion

Ammoni am Molyladali lest for PO

WE+ Cne, Hroa tboi No eamauup elad| PO s abseu
exeess wiouihaal t han amd
Moiybelai soa +

Teacher's ignature.
 Expt. No,
Dato-
Page No 28
xbeimew-
B Test Fo Basic Radiealsbsevaiom
s
RuP ANALYSLs BF BAGse KADICALS Praparaiom o Oriainal souion imeh ot Sall-+ disilao walan
aSeium Hycbuozide Ten
0:5 Sau- +tone.Na0Hslatu0a Saell of
ü Bring aqlom hoe didaaa in ammoniaCroup
CoLouR OF THE PPT Hd nean he mouh o
con Nh is pheseanl
GRoUp tha Demse tohili fuman
eo tube.
G1Rup CATION REAGE NTS NE toromad NH tNaoH
NaOH + Nesslats Reddish -Porocon pE-
NH Reageul Nta Ha OHaI
Pbe- n l a
NHa+He NM
I P dil. He Cominna tonyTes N icm
PbS-Black, Cus-Black,
Nessler's Reagent test
PLa, Cu2 Hu+ HS OSNa0Hseu
C d , As t |d
Cds-yello AsSs-Yellou
Nesslers Reageml- Anedelish-bcoo NH4 ion
Fe Fe2 A| Solld NH+ FeloH) -RrroOk pbe isoee iscenameel
L ALlOH)- disls
tohilk
|Pass thegan obtainec
-

Cum NH4OH
Za, Ni2
NHC)+NHOH
ZunS CohilG),M,s(Pie) in a Ssugh Nasslers PKaHa4+4 NH
M , C+
+HS) NS CBlack) Cos (elack) Leage +Hao (0)
N(+ NHaDH BoCOs
SCO 4 T +3 NH4I
+(RA)CO3 Co Coa
N aC+ NtaOH MaNH4 PO4 hila
+Na2H PO4
Result
Aeiolic Raclicalz SO,
Baie Raolieal- N
Sal Giveu N t 4SO4

Toachor's Signaluro.
 Dato

Expt. No.
Page No.

ExPERlMENT-L
SALT ANALISIS- 2 PbeH,coom
Aim
To idemu he acidhe amc basie Tadieals
ina ginam Sample
wmknotdn_ Sall- No-2

Appara kus:
Test tubes, lest tube holclea, olaolae buwaen Hame, haaaemis
Expetemem-
bservaiom
EPerelininar leds i
Colou op Hia Sall Mn,C cot FeF
Solubilil Fe3 N ana
Saluble n alo ubsenl-

Odou ai vimeqcs Smel CH3 COO ma

heneul

Flame led- 1

Sall- t cone.teiPanliBlueh whal PL2 may be hanen

is pul- imlo the tHame lekerimg ame

A.ests For eid Radicsls

2D lesk =
Di Acid Tesat|
Sal+ dil. HSOa + No gan 13 evolues cos so
ama.d No ate absent
6Conc. H,504 Test
CHCOO+ s04ene)> Hs+ CHcooH (vap) Sall+one. a 504 + Vimeqcs k e smel taCoO may be
Vinegan ânol
ameo Phesenl-

Teacher's Signature,
 Date.
Expt. No,
Page No. 30

Experdmem aiom outran

Conc H,S04+akonsng64
CalCu-buaenianaa tGmu Ne braun eman
4sO4kaaedskemg haued abseuk-

aContemaronueska o acide nadicals

Bebaseahion uZalkn Extaact
LAtpproimatel O.5 salt o clissodhuad i 1o-15m d lstlee!
wah Jhis is usec am wali extrae(WE)
COOH CHCoOH +
Coo
eoo
coOH
+ CHacoo Oxali aeia Test
Vhego Apionch o sal- soliel | Vnegc like Ctta Coo
Smel Oxaic uid + fes orobsamels benceiveccn med
of wale to make a pan
betoeem too gens ame
Be.

Foela les
A postor of E , + Dea o colous Clt c00 is
o-(a4) + Fedsl) > Fe(taoo), ) + 3 e eus dbuops nesral eh dhamaen o canamed

Reol eolous
Feea soekien thaa |redolin roron ht|
Fernic Acatale
co lowiain ds-
Re
abheaTS l e d i . He
CHCoof oH, Fe v +deCoot
FelHa coo)g+2H02 BAsfe Ferrie kratal
eEste Tesi- s
A pinelh ot-Sal+ teuo dorobsoil Smel 4,Co
Reol Broon bht ot comc tHaSO4 + eaHs-t +*| estes con mac

haalea
CHaCoo- +aHs OH + OH Teacher's Signature.
F zsmel
 Date

NpIehLS Page No. 32

BE BrsIc Expt.No.
RouP ANALY61s
PPT A CoLOUR

GROup CATIONS REA 6ENTS Bestajon Basis Radicala .

NH NaOH+Ka4 NHts aDHa aparaticn Oioinal salubiocn
P h - kiG D2 Sall- iadimaluaed an 2 ml disklled roal
T Pba+ dfl. He O.S
shade pellhe enullank seluio
Pt* dil. He +Ha PbsBlack GhhExpesu mend- Cbser 12aiom Lnerem ca
ed, A3+ Garou Anausia o Basio Radieal i
cas 1 yel lo
AsS O|Salkare 0. +NaoH +No brauninp4-cuael
Fe(oH) Brou
Nessleas heagpm- No snell s is absea.
U Fat/Fe3t, Souo NH+
Ae)aelatimaus Ph (Gr-1)
At3+ NH4OH le O.S. t dL H 1il Phe
i tormed. maybe bheseu
NH4C()+NHaOH ZnS-hiG

u2 N2 Mns Ligh Prnk Pb3T+2He Pbe2(s) + 24T

+HaS
Mn Co2 N'S 1-Black
CoS
Contimaote Test Pat
hila pple GrIis 4lesecl amd beiled eih dieile
S, B, | NHe() Sr CO waler to dissolue i la cloas Seluion is diisloc
Nhot+ Baco W Anto too paes
Cacos
Passium Lodide Tom-
Saluuin KI so _ elle e
Ma (tHP Ph2 on
Ma Nt (5)+
NitGt ila
PbT
Consmed
NaHP04 Potassiun clichzomat lene Bniak yallo
L KI Tent>Pb2+ +kI » PLT +2k Soluon kc04 sal PheO4 Pa s conin
veu o PFt
Result
Basie Racdical-P2
kCO Tun P k,COa Pb0a+2 redolie Raolieal i-CHoo Teacher's Signoture
Sall - PbleH Coo