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Civil Engineering
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Article history: The current study aims to investigate the influence of the addition of fine materials on the engineering
Received 26 July 2019 properties of silty sand soil. An intensive laboratory study of saturated and unsaturated silty sand soil
Revised 2 November 2019 treated with different percentages of fine materials of clayey soil (passing sieve #40 and ranging of 5,
Accepted 26 November 2019
10, 20, 40 and 80%) was investigated by conducting Oedometer and permeability tests. Unsaturated per-
Available online 24 December 2019
meability and soil–water characteristics curve (SWCC) were also examined. Test results show that soil
plasticity increases as the fine materials increase. The maximum dry unit weight (cdmax) increased up
Keywords:
to 10% of fine materials then decreased, while the optimum moisture content (OMC) increased along with
Silty sand
Fine materials
the increase of fine materials. One dimensional compression test results show that the fine materials
Permeability influence the compression characteristics and the compression index of the soil samples increased with
Compressibility the increase of fine materials. In contrast, the saturated permeability sharply decreased as fine materials
SWCC were increased. For higher percentages of fine content, the reduction in soil permeability becomes less
significant. In addition, the unsaturated permeability decreases with fine materials and suction pressure
increases. The effects of fine materials are more evident at lower suction pressures. Furthermore, the
water holding capacity and air entry value increased with the addition of fine materials.
Ó 2019 THE AUTHORS. Published by Elsevier BV on behalf of Faculty of Engineering, Ain Shams Uni-
versity. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/
by-nc-nd/4.0/).
https://doi.org/10.1016/j.asej.2019.11.005
2090-4479/Ó 2019 THE AUTHORS. Published by Elsevier BV on behalf of Faculty of Engineering, Ain Shams University.
This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).
718 A. Aldaood / Ain Shams Engineering Journal 11 (2020) 717–725
materials on the geotechnical properties of sand soils. Monkul and respectively. The specific gravity of the solid (Gs) was 2.67. Based
Ozden [9] studied the effect of kaolinite clay on the compressional on the ASTM D-422, the grain size analysis results showed a soil
characteristics of coarse-grained sand soil. They found that the per- composition of 59% sand, 37% silt and 4% clay. According to the
centages of fines along with the stress conditions affect the com- Unified Soil Classification System, USCS (ASTM D-2487), the soil
pressional behavior of sand soil. Bandini and Sathiskumar [12] was classified as a non-plastic silty sand (SM).
illustrated that the hydraulic conductivity and the coefficient of The fine-grained clayey soil used as an additive fine material
consolidation of sand soil were larger than those of sand soil mixed was collected from Al-Sedeeq district in Mosul city–Iraq with coor-
with 25% fine material. Konime [15] investigated the hydraulic dinates of 36° 230 2300 N; 43° 090 1700 E. The characteristics of these
conductivity of the sand–bentonite mixtures. It was concluded that soil samples are tabulated in Table 1. The soil samples have a med-
the hydraulic conductivity of sandy soil decreased as the bentonite ium consistency which allows ease grinding of the soil particles
percentage increased. This mixture could be used in the backfill for and use as fine materials. The grain size distribution curve of
the underground disposal of radioactive wastes. clayey soil (Fig. 2) showed that 98% of the soil particles passed
A few studies have been documented in the literature to deter- sieve # 200. Thus, only fine materials of clayey soil passing sieve
mine the effect of fine materials on compressibility, saturated and #40 were used in the preparation of the samples. Finally, a wide
un-saturated permeability, and soil–water characteristic curve range of fine materials were added to the silty sand soil and varied
(SWCC) of the silty sand soil. Thus, the main objective of this between 5% and 80%.
research study was to investigate the effect of the fine materials
on the aforementioned properties of silty sand soils. Index proper- 3.2. Samples preparation
ties, compaction characteristics and micro–structural changes
were also evaluated. Furthermore, the unsaturated permeability An oven dry silty sand soil that passed sieve #4 was mixed with
was investigated using the Van Genuchten [16] model. a predetermined amount of dried fine materials. In this study dif-
ferent percentages of fine materials were chosen as 5, 10, 20, 40
2. Soil-water characteristic curve (SWCC) and 80% of the dry weight of the soil. A predetermined water con-
tent related to the OMC of silty sand soil was added to the mix-
Numerous geotechnical and geo-environmental applications tures. Subsequently, the mixture was put into sealed
depend on unsaturated soil such as liners, and engineered barriers. polyethylene bags and left for 24 h as mellowing time. The mix-
The properties of unsaturated soils are important in the design and tures were statically compacted in a specific mold of each type of
evaluation of the geotechnical structures. The SWCC; the water the required testing at a strain rate of 1 mm/min using modified
holding capacity of the unsaturated soil; is the relation between compaction effort (ASTM D-1557). It is important to note that all
the volumetric water content (or degree of saturation) and the soil soil samples were compacted at the OMC and the cdmax of silty
suction [17]. The SWCC can be used to estimate some important sand soil.
engineering properties such as shear strength, permeability, and
volume change (swelling and collapsing) [18–20]. Many empirical 3.3. One-dimensional compression test
models have been proposed to fit the SWCC through experimental
results [16,17]. Chiu et al. [21] mentioned that, the Van Genuchten A one-dimensional compression (consolidation) test using an
model [16] is simple and accurate to fit the SWCC. Also, Aldaood Oedometer device was used to study the influence of fine materials
et al. [22] and Abhisekh et al. [23] reported that in both empirical on the compressibility of silty sand soil. The prepared samples with
models, Van Genuchten [16] and Fredlund and Xing [17] gave 5, 10, 20, 40 and 80% fine materials were statically compacted in
approximately similar results for fitting of the experimental SWCC consolidation rings that were 63.5 in diameter and 19 mm in
and found the accuracy of these models is practically good; for height. The soil samples were compacted at the OMC and the cdmax
more details see Aldaood et al. [22]. Thus, in this study only the of silty sand soil. The consolidation test was performed based on
Fredlund and Xing [17] model was used to fit the experimental the ASTM D-2435 standard. During the consolidation test, any
results of SWCC as shown below: increase in the height of the sample (especially the samples con-
taining a high percent of fine materials) was prevented by adding
30 loads. The soil samples were loaded incrementally, starting at
2 1m
ln 1 þ WWr 1
6.9 kPa and going up to 800 kPa. The incremental load was applied
h ¼ hs 41 5@ h n iA ð1Þ to the soil samples after the dial gauge reading was constant for at
ln 1 þ 1000000
Wr ln e þ Wa least three successive values.
W and Wr = the soil suction and residual soil suction, respec- A permeability test was carried out on the natural soil (i.e. silty
tively in (kPa). sand soil) and on soil mixed with 5, 10, 20, 40 and 80% of fine mate-
a, n and m = positive parameters of fitting curve. rials. This test was performed in a permeameter device using a
e = 2.71818. . ... constant head test according to ASTM D-2434. The soil samples
(which were 97 mm in diameter and 38.5 mm in height) were stat-
3. Experimental program ically compacted inside a stainless steel mold and used as part of
the permeability apparatus. This procedure was followed to reduce
3.1. Soils the disturbance of the soil sample during extrusion from the mold.
Two types of soils were used in this research study: silty sand 3.5. Suction measurements
and clayey soils, as illustrated in Fig. 1. The silty sand soil was col-
lected from the Al-Gabat region in Mosul city–Iraq with coordi- Three complementary techniques were used in this study to
nates of 36° 220 3800 N; 43° 060 5500 E, at a depth of 1.0–1.5 m determine the SWCCs of the all soil samples for suction pressures
from the ground surface. The in situ water content was 7.8%. The which varied between 10 and 1,000,000 kPa. These techniques
Atterberg limits were 27% and 22% for liquid limit and plastic limit, were the vapour equilibrium technique, the osmotic membrane
A. Aldaood / Ain Shams Engineering Journal 11 (2020) 717–725 719
Table 1 for soil samples with high total suction pressure (i.e. more than
Index properties of clayey soil. 37000 kPa).
Property Value
Liquid limit (%) 82 3.6. Micro-structural tests
Plastic limit (%) 35
Plasticity index (%) 47
The primary purpose of the micro–structural tests was to deter-
Specific gravity Gs 2.76
mine the variations in the structure of the soil samples due to fine
Grain size distribution Sand (%) 2
materials. In this research study two types of micro–structural
Silt (%) 50
Clay (%) 48
tests were adopted: scanning electron microscope (SEM) and mer-
cury intrusion porosimetry (MIP) tests. The SEM test was employed
Unified Soil Classification System CH
using a Table Top Microscope–TM 3000 device and followed the
test procedure reported by Aldaood et al. [25]. Several pieces of soil
sample (approximately 1 cm3 in volume) were initially injected by
100
epoxy fix resin, polished, coated with gold-palladium alloy, and
then scanned. The MIP test was performed on soil samples using
80 a Pore Seizer Porosimeter (9320). In this test, the mercury pressure
was raised continuously from 0.004 MPa to more than 210 MPa
0% F.M
and the apparent pore sizes that were measured ranged from
Finer (%)
60
3.6 nm to 350 lm. The soil samples were first trimmed to approx-
5% F.M
imately cubic shape and lyophilized to minimize the shrinkage,
10% F.M
40 especially for the samples high with percentages of fine materials.
20% F.M
40% F.M
20 4. Results and discussion
80% F.M
100% F.M
4.1. Evolution of index properties
0
1 0.1 0.01 0.001
The consistency properties of soil samples with different per-
Diameter (mm)
centages of fine materials is summarized in Fig. 3. The variation
Fig. 2. Variation of consistency limits of soil samples with fine materials.
of these properties was observed to correlate with the percentages
of the fine materials. As expected, the consistency limits increased
with additional amounts of fine materials. Furthermore, the soil
samples became more plastic upon the addition of fine materials
technique, and tensiometric plates. The first technique measures and transform from SM to MH when 80% fine materials were added
the total suction while the other techniques measure the matric (the 100% fine materials was clayey soil; i.e. CH). Similar observa-
suction [24]. The vapour equilibrium technique was used to obtain tions were documented by Al-Shayea [7]. The increase in consis-
the SWCC up to suction pressure 1500 kPa, while the osmotic tency limits is attributed to the clay content added to the soil
membrane technique was used to determine the SWCC in suction samples, resulting in an increase of the intake of water molecules.
pressures which ranged between 100 and 1500 kPa. The determi-
nation of the SWCC was continued in low suction pressure ranging 4.2. Pore size distribution (PSD) analysis
between 10 and 20 kPa using tensiometric plates. For more details
about these techniques see the reference Aldaood et al. [22]. The Fig. 4 shows the variations in PSD of soil samples with different
time required to reach equilibrium during testing for the determi- percentages of fine materials. It is worth noting that the PSD of the
nation of the SWCCs varied between 28 and 45 days, depending on silty sand soil and soil samples treated with 5% fine materials were
the specified technique. It worth noting that, there was no any des- not possible to determine because they failed under mercury intru-
iccation cracks in soil samples during the equilibrium time, even sion pressure. It is observed that all soil samples exhibited a bi-
720 A. Aldaood / Ain Shams Engineering Journal 11 (2020) 717–725
100 20
0% F.M
L.L P.L P.I L.S 5% F.M
80 18 20% F.M
40% F.M
80% F.M
100% F.M
60 ZAVC-0% F.M
16
ZAVC-100% F.M
40
14
20
12
0 0 5 10 15 20 25 30 35 40 45
0 5 10 20 40 80 100 Water Content (% )
Fine Materials (% ) Fig. 5. Compaction characteristics of soil samples with fine materials.
0 17.3 13
40% F.M
5 17.8 16.1
0.015 80% F.M 10 18.2 16.5
20 18 17
40 17.6 18
80 16.4 21.5
0.01 100 15.65 24.5
0.8
0% F.M
5% F.M
10% F.M
20% F.M
0.7 40% F.M
80% F.M
Void Ratio
0.6
0.5
0.4
10 100 1000
2
Pressure (kN/m )
Table 3
Consolidation parameters of soil samples with fine materials.
cles become more dispersed and float within the finer particles
(see Fig. 9). However, the compressibility of the soil samples is
expected to be mainly governed by the finer particles matrix and
there is no obvious contact between coarser particles [5].
The coefficient of volume compressibility (mv) was estimated to
understand the compressible nature of the silty sand soil samples
with the addition of fine materials, and these values are presented
in Table 3. It is important to note that only the maximum values of
Fig. 9. Fabric change mechanism of the soil samples with fine materials.
(mv) are mentioned in Table 3. The table shows that the fine mate-
rials cause a slight increase in the coefficient of volume compress-
ibility, and can be considered as medium compressible according
to Tomlinson [27] classification. ous lines) of the soil samples with various percentages of fine
To identify the yield points and measure strains following yield, materials. By viewing this figure, the most interesting observation
the consolidation curves of the soil samples with different fine is that the influence of fine materials is significant for the portion of
materials percentages were presented in terms of axial strain (e) SWCC with suction pressure less than 1500 kPa, for the soil sam-
(Fig. 10). In general, there is an initial stage where no effective ples with fine materials up to 40%. The action of 80% fine materials
deformation occurred for samples treated with 20, 40 and 80% of was obvious along the range of suction pressure (i.e. from 10 to
fine materials. This stage ranges from 6.9 kN/m2 to 100 kN/m2 1,000,000 kPa). This behavior is attributed to the SWCC being
which represents the swelling action. Thereafter, an initial yield mainly affected by soil structure at suction pressure ranges
was noticed and continued to reach about 1.21 to 1.31% of axial between 0 and 100 kPa, while at higher suction pressure (i.e., more
strain for the samples subjected to 800 kN/m2. While the axial than 100 kPa), it was affected by the composition of the soil matrix
strain values of the natural soil samples (i.e. silty sand samples) and the specific surface area of soil particles [28].
and samples treated with 5 and 10% of fine materials were ranged Generally, the volumetric water content for a particular suction
from 1.16 to 1.19%. Finally, the largely elastic nature of strains was pressure elevated with an increase in fine materials. This behavior
confirmed by the curves in Fig. 10, which present that about 17.5– is attributed to the high capillary and absorptive forces resulting
53% of axial strains were recovered during the unloading stage from the high surface area of the finer soil particles. Furthermore,
(rebound stage). The higher value of recovered strain (i.e.: 53%) the pore space of soil samples with fine materials (especially
occurred due to the swelling action and this value was recorded higher percent of fine materials) is smaller and contains much
for the soil samples with 80% fine materials. more pore space may exist in soil samples (see Figs. 4 and 7). How-
ever, increasing the percentage of fine materials resulted in higher
4.6. Evolution of SWCC air-entry value (AEV or Wa) and increased the water holding capac-
ity of the soil samples. This was expected, since the incorporation
The measured SWCC was fitted using Fredlund and Xing [16] of fine materials increased the plasticity of the soil samples (as
model defined by Eq. (1). Fig. 11 shows the fitted curves (continu- mentioned previously) and therefore more water was retained at
A. Aldaood / Ain Shams Engineering Journal 11 (2020) 717–725 723
0 0
0.3 0.3
Strain (%)
Strain (%)
0.6 0.6
0.9 0.9
1.2 1.2
0% F.M 5% F.M
1.5 1.5
10 100 1000 10 100 1000
Pressure (kN/m )
2 Pressure (kN/m2)
0 0
0.3 0.3
Strain (%)
Strain (%)
0.6 0.6
0.9 0.9
1.2 1.2
10% F.M 20% F.M
1.5 1.5
10 100 1000 10 100 1000
2 2
Pressure (kN/m ) Pressure (kN/m )
0 0
0.3 0.3
Strain (%)
Strain (%)
0.6 0.6
0.9 0.9
1.2 1.2
40% F.M 80% F.M
1.5 1.5
10 100 1000 10 100 1000
Pressure (kN/m2) Pressure (kN/m2)
0
10 100 1000 10000 100000 1000000
Table 4
Suction Pressure (KPa)
Variation of volumetric water content due to change in suction. pressure.
Fig. 11. SWCCs of soil samples with fine materials (continuous lines represent the Fine materials (%) h at 10 kPa (%) h at 1500 kPa (%)
best fitting while the points represent the experimental data).
0 24.9 10.1
5 25.2 10.2
10 25.7 10.7
any given suction pressure. Similar observations were documented 20 26.7 15.2
by [20]. Sequentially, there was a decrease in volumetric water 40 31.2 16.6
content as suction pressure increased from 10 to 1500 kPa. This 80 42.3 30.0
724 A. Aldaood / Ain Shams Engineering Journal 11 (2020) 717–725
Table 5
Saturation and de-saturation states values of soil samples with fine materials.
Table 6
SWCC parameters and statistical indices of soil samples with fine materials.
(n) values of soil samples with the addition of fine materials, while 0.01
(m) values decreased with increasing fine materials, referred to the 0% F.M
Coefficient of Permeability
80% F.M
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Declaration of Competing Interest treated gypseous soil. Appl Clay Sci 2014;88–89:39–48.
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