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Internship Report (Dyeing) On Zaheen Knitwear's Ltd.
Internship Report (Dyeing) On Zaheen Knitwear's Ltd.
Internship Report (Dyeing) On Zaheen Knitwear's Ltd.
Batching or
Batch
4.1 Definition
“A "batch" is defined as a discrete and quantifiable amount of textile materials, which might
include fibers, yarns, fabrics, or even whole textile products, in the context of textile engineering.
This grouping is distinguished by being handled as a single, integrated entity that is processed
through a single action or cycle. A batch is a specified and controllable collection of components
moving through different processes during production or treatment.”
To give an example, consider dyeing. To ensure consistent color results throughout the dying
batch, identical textiles or yarns are carefully organized into batches. Similarly, during finishing
procedures like painting or laminating, materials are carefully batched to guarantee the even and
consistent application of finishing chemicals.
Rope Length
Loading / Nozzle= m.
Nozzle Number
Chapter 5
Lab Section
Receipe Prediction
Pipe-ting
Add soda
Unload
Cold wash
Cold wash
Squeezing
Drying
Fabric is always recommended by buyer & dyes selection depends upon the technician decision.
1. Swatch receives: Swatch is received from the buyer & it comes to the lab section through
the merchandiser.
2. Fabric & dye selection: According to the buyer swatch, the type of fabric is selected &
the dye selection depends on the following factor:
The dyestuff contains “Metamerism” or not.
The dye stuff is suitable for producing particular color.
Sometimes buyers recommend the dye to produce a particular color.
The cost of dyestuff.
3. Recipe prediction: Recipe is determined by matching with reference book or
Spectrophotometer.
By the spectrometer the std. of the swatch is saved in computer.
Then by data color software after selecting the dye some recipes are found with the best
suitable recipe comes first & then others.
If the recipe shows “Metamerism” then changes the selected dye.
4. Sampling & pipetting: According to the recipe, the required fabric, dyes & chemicals are
weighted & stock solutions are made. Then pipe ting is done according to the recipe.
Stock solutions are made according to the recipe%. Such as-
For Dye
If recipe % (0.0001- <0.001) then stock solution % (0.01%)
If recipe% (0.001- <0.1) then stock solution % (0.1%)
If recipe % (0.1-0.8) then stock solution% (0.5%)
If recipe% (0.9-4.9) the stock solution% (2.5%)
If recipe % (≥5) then stock solution % (5%)
For Auxiliaries:
Salt– 20% stock solution;
Soda: 10% stock solution.
Acetic Acid: 0.5 g/l;
Detergent: 200ml/l;
Leveling agent: 3.5 g/l;
Pipette use in lab section: 0.1 ml – 1 ml & 5 ml to 10 ml.
5. Dyeing: After completing pipe ting according to the recipe, the weighted fabric is taken in
a sample dyeing Machine beaker & dyeing is completed. Here sample wt. 10gm & liquor
ratio 1:8.
6. Dispatch: After completing dyeing, the samples are checked by a spectrophotometer or
by eye vision in the verified matching cabinet. If it shows “Metamerism” then recipe
correction is done & again samples are prepared until no “Metamerism” & shade match
occurs. Then in a lab dip card, 3 samples are attached. One card is sent to the
merchandiser & another to the buyer through the merchandiser.
If the buyer chooses the sample, then the recipe is sent to the dyeing section for bulk production
through lab dip program card.
5.1.3 Spectrophotometer
The main function of spectrophotometer is to provide the best suitable recipe to dye sample
comparing with corresponding standard. If the first recipe fails to fulfil the expectation, then
it corrects the recipe.
Necessity:
a. Color matching is hard task so it makes the task easier.
b. It saves our times which provide assistance on production process.
c. It works upon some proved theory so the answer is approximately correct.
5.1.3.1 Theory
Spectrophotometer is based upon “Kubelka-mank” theory which builds up a relation
between reflectance & concentration. The “Kubelka-mank” values (k/S) is calculated from
the reflectance value of standard by the following equation—
Components
1. Computer
2. Spectroflash
3. CIE lab software.
5.1.3.2 Working Procedure
1. Calibration: The Machine is calibrated for different aperture view with three different
calibration standard, they are—
a. Black b. Green. c. White.
Two types of view are mostly used. They are—
Small aperture view (aperture is 9 mm in dia.)
Large aperture view (aperture is 30mm in dia.)
Valid time– The valid time for work can be varied according to the users. It can be set for 2, 6,
and 8 hours or more.
2. Data input: Self shades of particular company are prepared with various percentage in
the lab & the reflectance value of each sample is scanned in spectrophotometer.
3. Reflectance value measurement of swatch: Buyer provides either color or certain
pantone number. This is set on to the spectroflash & the Machine will automatically calculate
the reflectance value & saved it in memory.
4. Recipe giving: Considering all parameters we have to select suitable dyes & the
Machine will show some possible recipes. The factor affects dye selection much is
“Metamerism”.
5. Compare: After preparing the sample, the reflectance value of the samples is compared
with std. one, depending upon L* a* b* values the computer will show the dE value which
represents the total color difference between the sample & the STD.
If dE> 1 the color does not match.
If dE ≤ 1 then color match.
6.Recipe correction: Depending upon the reflectance value & dE value the computer corrects
the recipe until acceptable dE value & color matching are not obtained.
Working Procedure
Put the sample for dyeing and washing.
Dry the sample by dryer.
Measure the dot distance.
Finally, we got the shrinkage or stretch test.
5.2.4 PH Test
Fig: PH Test.
At first, a dyed sample (15× 5) cm is placed on the base of the crock meter.
Then an un-dyed crocking cloth (5× 5) cm is attached to the finger (Which is
used for rubbing action) of the crocking cloth which is white, plain weave,
scoured, de-sized, and bleached but without finishing.
Rubbing is done to & fro motion for both warp and weft way, 10 cycles at 10
second that mean 20 rubs in 20 s & finger pressure on the sample is 9 N.
At first perspiration solution that can be acidic or basic is taken into per-
spirometer which is 50 times the sample weight.
Put the sample into solution for 30 minutes at room temperature.
Then the liquor is drained and places the sample between two glass plate and
applied 4.5 Kg pressure on the plate and gives the screw.
After that per spirometer is kept into an incubator for 4 hrs. At (37±2) ℃
temperature.
Finally, take out the sample and dry.
Then assess the sample by gray scale.
Dyeing Manger
Dyes origin
Sumifix: Japan. Ciba: Switzerland.
Drimaren: Germany. SK: Korea
Remazol: Germany. Terasil: Switzerland
Levafix: Germany. Benzactive: Switzerland.
Terasil & Disperse dyes are mainly used for dyeing polyester. Acid dyes are used in Nylon.
Sumifix, Drimaren, Remazol, Levafix, Ciba, Sk all these dyes are used to dye the Cellulose
or Cellulose-based fabric.
6.4.3 CHEMICAL & AUXILIARIES:
Chemicals & Auxiliaries Function
1. Sunmoral CK-2/ Pitch run L-2/ NDA. Wetting agent & Detergent.
2. Neocrystal DMBF. Sequestering agent.
3. Invatex CS/ / Neocrystal 150F. Sequestering agent & wetting agent.
4. Albatex FFC. Antifoaming agent.
5. Pitch run L-100f. All remover it is mainly used for lycra mixed
fabric.
6. Neorate PH 150F/ Neorate pH 55F. Stabilizer used during peroxide bleaching.
7. Caustic Soda/ Soda Ash. Give alkali media during reactive dyeing &
fixation. It also used as saponification agent.
8. Hydrogen peroxide. Bleaching agent.
9. Croaks NF/ Sodium Bisulphate. Peroxide killer, It is enzyme based peroxide
killer.
10. Acetic acid. Give Acetic media & mainly used as
neutralizer.
11.Bio touch C-35/ Bio touch C-30/ Enzyme.
Invazyme CEL.
12. Hydrose. Reducing agent.
13. Neocrystal-200 BF/ Cibacel DBC/ GSS/ Leveling agent.
Drimagen E3R.
14. NicepoleD-1044/Lyocol-o-Powder/ Anti-creasing agent.
Serabid MIP.
15.Serabid IPD/ Ladiquest/ Eganol PS Sequestering agent.
16.Glabuer salt/ Serabid IPF/ San Salt LD4F Electrolyte.
17. NaHCO3. Used where slightly alkali media is required.
FABRIC LOADING
PRETREATMENT
DYEING
POST TREATMENT
UNLOAD