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Barnstead Labline Maxq4000 5 Manual
Barnstead Labline Maxq4000 5 Manual
LAB-LINE@
MAX Q 4000
INCUBATED & REFRIGERATED
SHAKERS
MODEL NO. SHKA4000 I
SHKA4OOO-1CE
&
* BarnsteadInternational1lab-line
.A*snts Y o u Lab Starts Here
1999 North 15th Ave.. Melrose Park. IL 60160-1491 USA
PHONE: (563) 556-2241 or (800) 522-5463: FAX: (563) 589-0516
TABLE OF CONTENTS -
TABLE OF CONTENTS: (Con't)
- - -
SAFETY INFORMATION
NOTE
Notes alert you to pertinent facts and conditions.
A HOT SURFACE
Hot surfaces alert you to a possibility of personal injury if you come in contact with a
surface during use or for a period of time after use.
INTRODUCTION
THANK YOU
for selecting Lab-Line Instruments for your equipment needs. For maximum value and ease of
start-up,
Read this operation manual thoroughly before deciding upon an appropriate location for
the unit.
Insist that every operator of this unit becomes familiar with the Operation Section of this
manual.
0 Be sure to fill out the Warranty Registration Card and mail it in to Lab-Line Instruments
within seven (7) days after receiving the unit.
after reading this manual you should have any difficulties with the installation or operation
instructions, please call:
A L L RIGHTS RESERVED
The infomiation contained in this manual is the exclusive property of 1,ab-Line Instruments. Inc.. and has been provided solel\
to enable the users of the equipment described herein to operate and maintain such equipment.. Any other use of this
infomiation, or the reproduction or transniission of all or any portion of this manual without prior written consent of the
manufacturer is expressly prohibited. 02004, L,ab-Line Instruments. Inc.
SECTION 2
SAFE OPERATION
~!!l NG:
DO NOT MODIFY CONSTRUCTION AND/OR ASSEMBLY OF EQUIPMENT.
0 DO NOT REMOVE TAGS, LABELS, DECALS OR OTHER INFORMATION
FROM THE UNIT.
STAND CLEAR OF EQUIPMENT WHEN IT IS OPERATING.
IF SHAKING ACTION WILL RESULT IN THE EVOLUTION OF GASES OR
FUMES, CARRY OUT THE OPERATION IN A WELL-VENTILATED
LABORATORYHOOD.
DO NOT USE EQUIPMENT FOR OTHER THAN ITS INTENDED PURPOSE.
USE ONLY THE ACCESSORIES AND ATTACHMENTS THAT ARE SHIPPED
WITH THE EQUIPMENT OR ARE SPECIFIED FOR IT. SUBSTITUTING
OTHER ATTACHMENTS OR ACCESSORIES CAN PRODUCE HAZARDS OR
MAKE THE UNIT INOPERATIVE.
PERFORM REGULAR MAINTENANCE SERVICE AS SPECIFIED IN THIS
MANUAL AND KEEP UNIT IN GOOD REPAIR. DO NOT OPERATE WITH
KNOWN DEFECTS.
0 DO NOT USE THE SHAKER TO MIX FLAMMABLE MATERIALS OR WHERE
THE TRANSFER OF MECHANICAL ENERGY TO GLASS COULD CAUSE
GLASS BREAKAGE.
SECTION 3
PRODUCT PROFILE
3.1 OVERVIEW:
The Lab-Line MAX Q 4000 series of bench top, incubated and refrigerated shakers are
available in either analog or digital control configurations:
A-Class shakers: SHKA4000, SHKA4000-I CE, SHKA4000-5, SHKA4000-6CE,
SHKA4000-7, SHKA4000-8CE: control temperature by a Proportional/Integral/Derivative
microprocessor-based controller. Solid-state control maintains time and speed and is
adjustable with rotary dials. Analog tachometer displays speed in RPM, verifying accuracy
of speed setting. Refrigerated units feature environmentally safe CFC free insulation and
coolant.
0 E-Class shakers: SHKE4000, SHKE4000-1 CE, SHKE4000-5, SHKE4000-6CE, SHKE4000-7,
SHKE4000-8CE: control temperature, time and speed by a Proportional/Integral/Derivative
(PID) microprocessor-based controller that is adjustable with membrane switches on a keypad
in 1 rpm increments. Refrigerated units feature environmentally safe CFC free insulation and
coolant. Flashing display indicates power interruption. Pressing any key will clear display.
Non-volatile memory maintains speed and time set points in the event of a power interruption.
Speed and time set points are automatically reactivated after power is restored.
Temperature range and accuracy follow. All units have a uniformity of kO.S°C at 37OC
in flask:
Standard Temperature: SHKA4000, SHKA4000-1 C E , SHKE4000, SHKE4000-ICE,
5OC above ambient to 60°C, k 0 . I 0 C at 37OC in flask.
High Temperature: SHKA4000-5, SHKA4000-6CE, SHKE4000-5, SHKE4000-6CE,
5OC above ambient to 80°C, +0.I0C at 37OC in flask.
Refrigerated: SHKA4000-7, S H KA4000-8CE, S H KE4000-7, SHKE4000-8CE, 15OC
BELOW ambient to 60°C, kO.l OC at 37OC in flask. Refrigeration system needs to be
turned off whenever the set point is at or above 32°C.
In addition, all versions offer:
Space efficient tubular heaters.
0 Drive interrupt halts shaking action when lid is opened.
All set points are retained by non-volatile memory that automatically reactivates after power
is restored.
Visual, user adjustable over-temperature safety signal with independent thermostat controls
the heat if main controller fails.
% inch (1.9 cm) triple eccentric orbital drive.
0 6 permanently lubricated ball bearings.
50 Ib (22.7 kg) platform load capacity at safe speeds less than 400 rpm for A-Class shakers and
less than 500 rpm for E-Class shakers.
UL, cUL and CE certification.
PRODUCT PROFILE (Con?): 3.2 SPECIFICATIONS:
INSTALLATION
4.1 SHIPPING CARTON:
This should be inspected upon delivery. When received, carefully examine for any
shipping damage before unpacking. If damage is discovered, the delivering carrier
should specify and sign for the damage on your copy of the delivery receipt.
Open the carton carefully making certain that all parts are accounted for before
packaging materials are discarded. After unpacking, if damage is found, promptly
report it to the carrier and request a damage inspection promptly.
e IMI'OKTANT: I-ailurc to rcquest an inspution of damayc mithin a few days aftcr
rcceipt of sl~ipmentabsolbcs the carrier fi-onl an! liabilit~'for damage. You must call
for a damage impection promptlj.
4.2 LOCATION:
Put the shaker on a level table or bench capable of supporting the weight of the
shaker with any accessories while in operation.
Place shaker near an electrical outlet that matches the unit's nameplate requirements.
0 Allow approximately 2" (5 cm) of clearance around the unit for free air convection,
accessory attachments and user convenience.
Shakers with refrigeration should be placed near an accessible drain.
INSTALLATION: (Con't)
To eliminate hazard of electrical shock, make sure floor around shaker is dry. In the
event of accidental spilling or splashing of liquids, clean up andlor neutralize the
spilled liquids before continuing.
2. Carefully position the platform horizontally over the shaker's mounting plate aligning
the 4 mounting holes.
3. Positions one of the thumbscrews provided through each of the 4-platform mounting
holes and tighten securely.
4.5 FLASK CLAMP INSTALLATION:
Each flask clamp contains a support spring located at the narrow top of the
clamp.
Depending on the size of the clamp, the clamp base may contain one or
several screws necessary to secure the clamp to the platform. All screws
provided with the clamp must be properly attached to the platform.
1 . Carefully place the desired vessel in the clamp by first pulling the clamp spring far
enough apart to enable the flask base to be positioned inside the clamp. Secondly,
gently slide the flask into its proper position securing it to the wider bottom of the
clamp. The spring will hold the body of the flask securely in place and provide
security during shaking.
2. Make sure all vessels are securely clamped before turning on unit.
Wherever possible, vessels should contain a stopper to prevent hazardous substances being
thrown out during the mixing action.
4.6 TEST TUBE RACK INSTALLATION:
1 . Position the test tube rack on the combination platform so that the cutouts on the
rack's outside bottom are aligned with corresponding mounting holes on the platform.
There are two cutouts on each side of the rack.
2. Secure the rack to the platform with mounting screws provided with the rack.
17
SECTION 5
OPERATION
5.1 A-CLASS:
Please refer to page 13 for control panel reference.
5.1D T E M P E R A T U R E C O N T R O L L E R - S E T T I N G T E M P E R A T U R E :
CONTROL BUTTONS
+ I T Im
1. CONTROLLER SELF-TEST: When the shaker is powered up, the controller will
display 8888 along with the three decimal points and the HEAT ON indicator lamp.
The display will then blank out for 2 seconds before showing the chamber temperature.
2. HEAT ON INDICATOR: The HEAT ON indicator lamp is lit when the chamber
heaters are receiving power. The lamp will normally flash when the chamber
temperature is at set point.
3. SET POINT ADJUSTMENTS: The temperature controller normally displays the
chamber temperature. To view or change the temperature set point proceed as follows:
PRESS CONTROLLER
* View set point
*v Decrease set point
*A Increase set point
A. Press and hold the " S T A R (*) key and use either the up or down arrow key
to adjust the set point to the desired temperature. Release the "STAR (*)
key.
B. Allow sufficient time for chamber temperature to stabilize.
OPERATION: (Con't)
5.1 A - C L A S S : (Con't)
Please refer to page 13 for control panel reference.
Install a thermocouple inside the flask with the thermocouple junction in direct
contact with the water.
Press and hold the "STAR" (*) key and using the up or down arrow key, adjust
the set point to the desired temperature.
The controller display should now be indicating the set point temperature. Make
note of the thermometer reading.
Press and hold both arrow keys until the controller display indicates tunE.
Release the arrow keys. Press and release the down arrow key, the display should
now indicate LEUL. Press and hold the "STAR" (*) key and using the up arrow
key adjust the display to read. Release the "STAR" (*) key. Press and release
the up arrow key until the display indicates Zero. The display should now
alternate between Zero and a numerical value.
Using the examples shown below and the thermometer value obtained in step 5
above, enter the correct Zero value into the controller by pressing the "STAR"
(*) key and using the up or down arrow key. If there is already a Zero value
present then add the new value to the one already present.
Thermometer = 60 "C Thermometer = 70 OC
Controller Reading = 65 "C Controller Reading = 65 OC
Subtract -
- -5 "C Subtract = +5 OC
When the correct Zero value has been entered, press and hold the two arrow keys
together until the display again indicates the chamber temperature. If the
procedure was done correctly, the controller display should now agree with the
thermometer reading to within 10S°C.
3. Once set, temperature control is initiated by pressing the heat on button; the
heater will react and start increasing the temperature to reach the set point.
4. During operation, both the up and down arrow keys can be used to adjust the
temperature to a new set point.
9. Press the HEAT OFF button. The beeper will sound indicating that the new
calibration value you have entered is now stored in the nonvolatile memory of
the temperature controller.
10. Press HEAT O N button twice to complete return to normal operating mode.
OPERATION: (Con't)
5.2 E-CLASS: (Con't)
Please refer to page 14 for control panel reference.
HYPERTERMINAL CONFIGURATION:
1. Power up the host computer and close any running applications.
12. Power up shaker. Shaker will screen print speed, time and temperature at
one-minute intervals.
OPERATION: (Con't)
8 High-Limit Control
5. Allow sufficient time for chamber temperature to stabilize before setting the
high-limit control.
6B. For E-Class shakers, when set point is reached, high-limit status lamp will
flash and the audible alarm will beep once. Rotate the high-limit control
slowly clockwise approximately 118 of a turn beyond this point.
0 High-Limit Control
I , Turn ON refrigeration switch located to the left of the defrost timer on the
right rear of the shaker cabinet.
2. Rotate low-limit control fully counterclockwise.
3. Set chamber temperature.
4. Allow sufficient time for chamber temperature to stabilize before setting the
low-limit control.
5. Rotate low-limit control slowly clockwise. When the set point is reached,
low-limit status lamp will illuminate. Rotate the low-limit control slowly
counterclockwise until the low-limit status lamp goes out.
6. Continue rotating the low-limit control about 5 degrees of rotation to set it
about 1°C to 3OC below the set point, the low-limit status lamp will extinguish
and the temperature control status lamp stays lit.
7. When desired temperature is achieved, load the shaker.
OPERATION: (Con't)
5.5 OPTIONAL KEFRIGERATION SYSTEM:
NOTE: This section applie, onl> to unit> wppliecl u ith t h i s crplicm. 'l'he refrigeration
sqstcrn on the A and C s e r ~ e sshakers are identical in operation. Plcasc rof'er tn thc
refrigeration schematic on page 5 1 Ibr refiigeraticw rqldccment pdrts.
When the unit power is on, refrigeration can be initiated by turning ON the refrigeration switch
which is located to the left of the defrost timer on the lower right side panel of the shaker cabinet. This
should be initiated (turned on) only when a temperature set point of approximately 32°C or less is
required (based on your ambient temperatures). Both the main power switch and the refrigeration switch
need to be ON for the refrigeration system to work. When the refrigeration switch is activated, the
compressor system will run continuously and the system will go through the following routine:
Upon every activation of the refrigeration switch to the ON position, there is an approximate 2-
minute delay until the compressor becomes activated. This is a safety feature, to prevent damage to the
compressor in the case of quickly switching the refrigeration switch off and on again. Because the
compressor does not turn on immediately after switching the refrigeration switch to on, please note, THIS
IS NORMAL. The defrost timer will begin initiation. This may turn the fans off for several minutes until
it completes a normal defrost cycle.
During operation, the defrost timer will automatically "engage" every 4 hours, switching cold gas
through the evaporator (inside) coils to hot gas in order to defrost the coils. There is a dedicated sensor
inside the coils which will terminate the defrost when the temperature reaches a point where it is assured
that there is no ice or frost on the coil. At low set point temperatures (i.e. S°C), this defrost time will be
longer than higher set point temperatures (i.e. 25"C), which may initiate and terminate immediately
because the coils will be much warmer at higher set point temperatures.
The defrost timer, part #270-108-00, is located on the lower right side panel of the shaker cabinet
to the right of refrigeration power switch and is engaged whenever the refrigeration system is turned on.
I 2 3 4
1 . REFRIGERATION POWER SWITCH: Activates refrigeration system, 1 is ON, 0 is
OFF.
2. DEFROST TIME POWER STATUS LAMP (POWER): Timer is powered along with
refrigeration system whenever green power status lamp is lit.
3. DEFROST STATUS LAMP (DEFROST): Cooling coil is being defrosted whenever
yellow defrost status lamp is ON. Hot gas is being bypassed through the iced coil.
When ice on the coil has melted, defrost cycle ends automatically.
4. FAN DELAY STATUS LAMP (FANS): During defrost timer power-up and after
defrost cycle, the circulating fan is locked off for a I-% minute delay. Green fan
status lamp flashes during this fan-delay period.
28
SECTION 6
TROUBLE SHOOTTNG
The following is intended as a reference guide to help in servicing this unit if
problems should occur.
SYMPTOMS THINGS TO LOOK FOR RESOLUTION
Shaker doesn't operate Check if power cord is Plug in
MAINTENANCE
a
SUGGESTED WITH EVERY 3 MONTHS OF CONSTANT USE:
SECTION 8
REPLACEMENT PARTS
S H K A 4 0 0 0 , S H K A 4 0 0 0 - I C E , SHKA4000-5, SHKA4000-6CE, SHKA4000-7, S H K E 4 0 0 0 -
8CE
SHKE4000, SHKE4000- I CE, SHKE4000-5, SHKE4000-6CE, SHKE4000-7, SHKE4000-8CE
Lab-Line's warranty provided hereunder shall be null and void and without further force or
effect if there is any (i) repair made to the product by a party other than Lab-Line or its duly
authorized service representative, (ii) misuse (including use inconsistent with written operating
instructions for the product), mishandling, contamination, overheating, modification or alteration
of the product by any customer or third party or (iii) use of replacement parts that are obtained
from a party who is not an authorized dealer of
Lab-Line.
IN NO EVENT SHALL LAB-LINE BE LIABLE TO ANY PARTY FOR ANY DIRECT,
INDIRECT, SPECIAL, INCIDENTAL, OR CONSEQUENTIAL DAMAGES, OR FOR ANY
DAMAGES RESULTING FROM LOSS OF USE OR PROFITS, ANTICIPATED OR
OTHER WISE, ARISING OUT OF OR IN CONNECTION WITH THE SALE, USE OR
PERFORMANCE OF ANY PRODUCTS, WHETHER SUCH CLAIM IS BASED ON
CONTRACT, TORT (INCLUDING NEGLIGENCE), ANY THEORY OF STRICT
LIABILITY OR REGULATORY ACTION.
The name of your nearest authorized Lab-Line dealer may be obtained by calling
1-800-522-5463.
& Barnsteadlnternationalllab-Atne
Your Lab Starts Here