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Z. ASTM C1876-19, Bulk Resist
Z. ASTM C1876-19, Bulk Resist
Z. ASTM C1876-19, Bulk Resist
for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: C1876 − 19
1
3.2.2.1 Discussion—Bulk electrical conductivity is the re-
This test method is under the jurisdiction of ASTM Committee C09 on
Concrete and Concrete Aggregates and is the direct responsibility of Subcommittee ciprocal of bulk electrical resistivity.
C09.66 on Concrete’s Resistance to Fluid Penetration.
Current edition approved June 15, 2019. Published Aug. 2019. DOI: 10.1520/
C1876-19
2 4
Annex A in Form and Style for ASTM Standards, www.astm.org/COMMIT/ For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Blue_Book.pdf. contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
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Section on Safety Precautions, Manual of Aggregate and Concrete Testing, Standards volume information, refer to the standard’s Document Summary page on
Annual Book of ASTM Standards, Vol. 04.02. the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
5.1 The electrical resistivity of a concrete is the opposition NOTE 1—Similarly, other admixtures containing water-soluble ionic
to the movement of ions under an applied electric field. The compounds might affect the results of this test method. Long-term
chloride ion diffusion tests are recommended if an admixture effect is
electrical conductivity of a concrete is a measure of how suspected. Alternately, this interference can be minimized by expressing
readily the ions in the pore solution can be transported through results as a formation factor (see Appendix X1).
the concrete under an applied electric field (the higher the
conductivity, the greater the rate of transport). The electrical 6.2 Because the test results are a function of the electrical
resistivity or conductivity is a material property that depends resistance or conductance of the specimen, the presence of
upon the pore volume, the pore structure (size and reinforcing steel, metal fibers, or other embedded electrically
connectivity), the pore solution composition, the degree of conductive materials, including some types of aggregates, may
saturation of the concrete specimen, and the specimen’s tem- yield unrepresentative results, as these will result in higher
perature. Concrete mixture characteristics that are known to conductivity than a concrete of similar quality but with no
affect concrete electrical resistivity, as well as resistance to embedded conductive material. The test is not applicable to
chloride ion penetration, include water-cementitious materials specimens containing reinforcing steel positioned longitudi-
ratio, pozzolans, slag cement, the presence of polymeric nally that provide a continuous electrical path between the two
admixtures, air-entrainment, aggregate type, aggregate volume ends of the specimen, and it is not applicable to specimens
fraction, degree of consolidation, curing method, and age. containing discrete metallic fibers.
5.2 The bulk electrical resistivity of concrete is the inverse 6.3 Leaching of ions from the pore solution of concrete is
of its bulk electrical conductivity. Bulk electrical conductivity known to affect measured resistivity or conductivity values.
can also be measured by Test Method C1760, which uses the Even standard curing in water saturated with calcium hydrox-
apparatus described in Test Method C1202. This test method, ide can influence the resistivity of the solution inside the pores
however, uses apparatus specifically designed to measure bulk of the concrete as potassium and sodium hydroxides are
conductivity or bulk resistivity. leached out. As such, concrete cylinders and cores are im-
5.3 The purpose of conditioning in a simulated pore solution mersed in simulated pore solution for at least 6 days prior to
is to bring the specimen to a level of near complete saturation testing.
of the capillary and gel pores. When comparing two different 6.4 The level of saturation of the concrete has a major
concrete specimens, it is important to condition both specimens impact on resistivity or conductivity because the electric
as close as possible to a comparable saturation state, using the current is mainly conducted through the liquid in the pores.
same solution for conditioning, so that values can be compared Achieving full saturation is difficult, so while not perfect, the
in a meaningful way. This is particularly true for using the conditioning procedures used in this test method provide a
measured resistivity or conductivity, along with other methodology for achieving a high and reproducible level of
information, to estimate the diffusivity. saturation without allowing excessive leaching of alkalis.
5.4 The bulk electrical resistivity or conductivity of con- 6.5 Because concrete has a capacitive component, its elec-
crete can provide a rapid indication of its resistance to chloride trical response is characterized by a magnitude and a phase
ion penetration and resistance to penetration of other fluids. difference that is a function of the AC frequency. This may
Resistivity or conductivity measurements have shown good have an effect on the measured test result. The desired quantity
correlations with other electrical indication tests including Test is the magnitude of the impedance that is measured at the
Method C1202 (1, 2, 3).5 Bulk electrical resistivity results have frequency that yields the minimum phase difference between
the applied voltage and the measured current; that is, the
5
The boldface numbers in parentheses refer to the list of references at the end of system is behaving most like a resistor. A number of commer-
this standard. cial devices operate at a single fixed frequency, typically
FIG. 1 Schematic of electric circuit inside verification cylinder. Precision resistors are labeled R1 to R5. The switch is labeled S1. The
circuit is connected to plate electrodes at each end.
6
11. Verification
Reagent Chemicals, American Chemical Society Specifications, American
Chemical Society, Washington, DC. For suggestions on the testing of reagents not 11.1 Prior to testing concrete specimens on a given day,
listed by the American Chemical Society, see Analar Standards for Laboratory
verify the accuracy of measurements made by the test device
Chemicals, BDH Ltd., Poole, Dorset, U.K., and the United States Pharmacopeia
and National Formulary, U.S. Pharmacopeial Convention,Inc. (USPC), Rockville, over the range of expected values of resistivity or conductivity
MD. using the verification cylinder described in 7.4.
12.1 Remove the test specimen from the container of pore where:
solution, blot off excess liquid, and transfer to the specimen L = average specimen length, m to the nearest 0.001 m,
holder (see 7.6) or place into a test device designed to hold A = specimen cross-sectional area, m2, to three significant
specimens vertically. To minimize drying of the concrete digits,
surface, do not leave the specimen exposed to air for longer V = voltage, V, and
than 5 min before performing tests. I = current, A.
12.2 Saturate the sponges with conductive fluid and place 13.1.2 For devices that display the electrical resistance of
between the plate electrodes and end surfaces of the specimen. the specimen, calculate the bulk electrical resistivity using Eq
Center the electrodes and sponges on the ends of the specimen 2:
and press the sponges against the end faces of the specimen in ρ 5 RA⁄L (2)
accordance with manufacturer’s instructions.
where:
NOTE 11—To obtain repeatable measurements, sufficient pressure R = electrical resistance of specimen, ohms, and
should be applied to provide firm contact between the electrodes and the A and L = as defined for Eq 1.
specimen. This can be provided using a clamping device, bolts, or use of
a weight of at least 3 kg on top of the top electrode of a vertically oriented 13.1.3 For devices that calculate bulk electrical resistivity
test setup. The mass of a concrete cylinder of 100 × 200 mm nominal using Eq 1, no additional calculation is needed.
dimensions is typically sufficient for use as a weight.
13.2 Calculate the average resistivity for the set of replicate
12.3 Make measurements on the test specimen in accor-
specimens tested in ohm-m and report to the nearest 0.1
dance with the manufacturer’s instructions.
ohm-m.
12.3.1 For test devices with capabilities to measure ac
current at variable frequency, perform tests at 1 kHz, unless 13.3 If required by the specifier of the tests, calculate the
otherwise specified. bulk electrical conductivity by taking the inverse of Eq 1 or Eq
12.3.2 If the test device is designed to display resistivity or 2 and multiplying by 1000 to obtain values in units of mS/m.
conductivity, enter the average specimen dimensions into the
device in accordance with the manufacturer’s instructions. 14. Report
12.4 Record the values after allowing the readings stabilize 14.1 Report the following information:
for 2 to 5 s. For devices that perform the calculations internally, 14.1.1 Source of the core; if removed from a structure,
record the displayed resistivity or conductivity. For devices report the location from within the structure,
that display electrical resistance, record the value of resistance 14.1.2 Identification number of the core or cylinder
in ohms. For other devices, record the voltage in volts, V, and specimen,
current, I, in amperes. Remove the electrodes from the 14.1.3 Type of concrete, including binder type, water-
specimen, reapply the electrodes, and repeat the measurement. cementitious materials ratio, and other relevant data supplied
Make at least two repeat measurements. with specimens, if known,
APPENDIX
(Nonmandatory Information)
X1.1 FORMATION FACTOR degree of hydration, (4) by pore solution extraction and
X1.1.1 Electrical tests of concrete, including Test Method conductivity measurement, or (5) by direct measurement of
C1202 and Test Method C1760, are also influenced by the conductivity with an embedded sensor (8).
conductivity of the pore fluid in addition to the porosity and X1.1.3 The resistivity of the pore solution (ρo) (ohm-m) is
pore connectivity. Only the latter factors, however, are indica- the inverse of pore solution conductivity (S/m). Based on the
tive of the resistance of concrete to fluid penetration. This work reported by Snyder (9), pore solution conductivity can be
interference can be removed by use of the formation factor.
estimated using the on-line calculator by following the link:
X1.1.2 The formation factor is a material property that https://www.nist.gov/el/materials-and-structural-systems-
relates to the pore geometry and connectivity. The formation division-73100/inorganic-materials-group-73103/estimation-
factor can be calculated as the ratio of the resistivity of a bulk pore
body (ρ) to the resistivity of the pore solution in the body (ρo):
F5ρ⁄ρo . The resistivity of the pore fluid can be determined by X1.1.4 If resistivity is measured at a temperature other than
calculation using models based on (1) thermodynamics, (2) a 23.0 6 2.0°C, the measured resistivity must be divided by the
mathematical model (see X1.1.3) based on mixture resistivity of the pore solution at the same temperature in order
proportions, (3) the alkali content of the binder and assumed to obtain the formation factor.
REFERENCES
(1) Hooton, R.D., Charmchi, G., “Adoption of Resistivity Tests for (4) Shahroodi A., Hooton R.D., “Development of Test Methods for
Concrete Acceptance,” ACI Special Publication SP-303, Proceedings, Assessment of Concrete Durability for Use in Performance-Based
Recent Advances in Concrete Technology and Sustainability Issues, Specifications,” Final Report Submitted to Ministry of Transportation
Ottawa, July 2015, pp. 269-279. of Ontario and Department of Civil Engineering, University of
(2) Hooton, R.D., Charmchi, G. and Karkar, E., “Development and Toronto, 2010.
Standardization of Rapid Methods for Assessing the Fluid Penetration (5) Spragg, R., Villani, C. and Weiss, J., “Electrical Properties of
Resistance of Concrete,” Proceedings, XIII International Conference Cementitious Systems: Formation Factor Determination and the
on the Durability of Building Materials, Sao Paolo, Brazil, Sept. 2014, Influence of Conditioning Procedures,” Advances in Civil Engineer-
pp.1111-1117. ing Materials, Vol. 5, No. 1, pp. 24-48, 2016.
(3) Gudimettla, J., and Crawford, G., “Resistivity tests for concrete – (6) Spragg, R., Villani, C., Snyder, K., Bentz, D., Bullard, J.W., and
recent field experience,” ACI Materials Journal, Vol. 113, No. 4, Weiss, J., “Factors That Influence Electrical Resistivity Measurements
2016. in Cementitious Systems,” Transportation Research Record: Journal
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